#------------------------------------------------------------------------------ #$Date: 2018-01-26 10:36:15 +0200 (Fri, 26 Jan 2018) $ #$Revision: 205718 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/23/2242336.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242336 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.9560 _cell_length_b 10.6970 _cell_length_c 20.3310 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.8406 _cod_data_source_file lh58571sup2.hkl _cod_data_source_block 1 _shelx_title ' 1 in P2(1)/c New: Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 267.60 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 631.69 658.34 18.82 o 4 0 0 71608.93 69985.18 2259.12 o 6 0 0 5567.11 5649.90 193.16 o 8 0 0 4023.83 3969.56 145.57 o 10 0 0 40.09 41.29 21.70 o 2 1 0 8227.58 7940.50 141.81 o 4 1 0 501.90 614.37 16.06 o 6 1 0 950.83 949.35 24.68 o 8 1 0 305.59 287.06 36.39 o 10 1 0 438.04 447.53 28.95 o 0 2 0 6995.68 6803.26 218.35 o 2 2 0 2128.10 2143.02 39.29 o 4 2 0 22979.69 23278.59 412.37 o 6 2 0 102.36 126.60 9.35 o 8 2 0 755.82 727.68 24.88 o 10 2 0 957.23 915.02 51.79 o 2 3 0 15173.22 13965.29 388.98 o 4 3 0 1978.24 1965.62 39.77 o 6 3 0 8781.64 8823.74 161.85 o 8 3 0 783.72 824.59 22.11 o 10 3 0 1167.51 1146.38 69.99 o 0 4 0 5859.74 6325.12 148.87 o 2 4 0 1371.90 1405.66 29.03 o 4 4 0 126.07 118.84 7.78 o 6 4 0 146.63 126.48 9.99 o 8 4 0 546.90 499.32 17.84 o 10 4 0 3.36 1.22 14.59 o 2 5 0 29299.12 28792.69 447.89 o 4 5 0 616.49 637.79 18.14 o 6 5 0 12356.93 12481.91 230.82 o 8 5 0 499.79 517.38 18.78 o 0 6 0 1742.90 1587.96 43.69 o 2 6 0 1004.85 1119.85 21.13 o 4 6 0 3878.57 3732.73 93.40 o 6 6 0 11.19 17.42 7.33 o 8 6 0 95.72 127.51 12.18 o 2 7 0 15417.16 15792.63 225.96 o 4 7 0 2.38 2.62 5.91 o 6 7 0 1824.68 1813.94 46.97 o 8 7 0 310.68 318.42 18.28 o 0 8 0 16766.63 17601.27 590.67 o 2 8 0 68.48 75.57 7.21 o 4 8 0 2153.23 2172.00 51.72 o 6 8 0 1924.83 1886.55 45.80 o 8 8 0 1815.07 1779.95 40.59 o 2 9 0 3120.43 3285.38 81.07 o 4 9 0 55.64 76.95 9.80 o 6 9 0 78.24 67.07 13.30 o 0 10 0 4046.34 4633.02 173.56 o 2 10 0 42.56 39.21 10.56 o 4 10 0 7373.26 7457.07 876.91 o 6 10 0 50.42 37.64 14.94 o 2 11 0 3272.33 3239.37 218.00 o 4 11 0 499.52 465.97 27.19 o 0 12 0 3013.38 2989.77 125.27 o 2 12 0 0.27 2.46 14.29 o 1 1 1 32451.35 29284.09 440.60 o 2 1 1 4837.72 4807.44 57.20 o 3 1 1 20018.53 20249.49 237.38 o 4 1 1 3.98 7.53 2.41 o 5 1 1 8349.94 8159.10 97.91 o 6 1 1 2646.49 2572.78 35.21 o 7 1 1 839.44 804.22 20.92 o 8 1 1 78.45 75.63 9.30 o 9 1 1 1187.31 1165.33 29.82 o 10 1 1 320.87 364.99 18.78 o 0 2 1 16100.68 1692.34 7033.56 o 1 2 1 1206.12 1228.64 15.70 o 2 2 1 471.63 454.01 7.14 o 3 2 1 1267.42 1101.35 15.07 o 4 2 1 2725.88 2730.65 37.45 o 5 2 1 98.23 80.07 5.02 o 6 2 1 998.10 1013.28 18.22 o 7 2 1 2681.14 2612.47 36.19 o 8 2 1 360.37 367.16 14.67 o 9 2 1 260.02 256.68 15.19 o 10 2 1 184.50 195.09 14.82 o 1 3 1 7764.41 7840.98 114.54 o 2 3 1 2715.77 2722.04 31.77 o 3 3 1 13515.31 13927.83 163.37 o 4 3 1 567.45 569.25 9.75 o 5 3 1 647.96 591.55 11.55 o 6 3 1 1201.94 1175.18 19.05 o 7 3 1 1319.71 1333.62 21.66 o 8 3 1 359.77 351.16 12.83 o 9 3 1 774.74 744.48 22.52 o 10 3 1 252.61 259.98 17.27 o 0 4 1 15754.36 15723.51 293.62 o 1 4 1 12706.43 9657.29 1519.37 o 2 4 1 4219.16 4761.12 51.64 o 3 4 1 14606.54 14230.39 158.17 o 4 4 1 2956.12 2693.28 32.76 o 5 4 1 2462.69 2406.00 32.62 o 6 4 1 1511.59 1544.71 26.96 o 7 4 1 3304.45 3342.93 45.08 o 8 4 1 8.46 12.50 5.88 o 9 4 1 129.76 129.90 8.50 o 10 4 1 96.42 115.50 11.27 o 1 5 1 568.26 585.56 10.76 o 2 5 1 198.17 233.06 6.10 o 3 5 1 1253.68 1377.28 17.38 o 4 5 1 187.02 214.05 9.08 o 5 5 1 199.95 179.58 7.12 o 6 5 1 297.61 311.28 9.92 o 7 5 1 68.62 72.34 7.40 o 8 5 1 0.05 -8.54 5.75 o 9 5 1 244.08 231.24 10.39 o 0 6 1 4404.97 4325.94 74.55 o 1 6 1 20972.09 21541.78 264.72 o 2 6 1 678.64 800.22 12.06 o 3 6 1 13128.75 12887.36 167.71 o 4 6 1 3955.34 3984.72 51.11 o 5 6 1 4732.58 4785.02 85.03 o 6 6 1 54.96 58.17 5.99 o 7 6 1 3665.65 3812.84 48.68 o 8 6 1 1976.59 1945.50 36.93 o 9 6 1 153.13 165.39 9.62 o 1 7 1 4728.81 4952.72 60.89 o 2 7 1 2399.19 2339.86 32.50 o 3 7 1 3795.01 3722.59 42.87 o 4 7 1 331.98 323.70 9.90 o 5 7 1 1766.75 1805.87 34.39 o 6 7 1 973.69 976.60 17.67 o 7 7 1 291.86 338.50 13.67 o 8 7 1 125.03 121.87 8.79 o 0 8 1 30.31 36.71 6.89 o 1 8 1 1839.06 1888.92 26.88 o 2 8 1 84.78 94.65 5.17 o 3 8 1 1351.60 1328.31 18.18 o 4 8 1 226.25 249.03 9.37 o 5 8 1 490.04 486.53 12.54 o 6 8 1 26.46 20.36 4.67 o 7 8 1 172.36 180.59 9.81 o 8 8 1 166.95 178.73 10.22 o 1 9 1 3472.40 3736.10 52.13 o 2 9 1 735.69 804.94 14.62 o 3 9 1 1309.78 1332.41 26.09 o 4 9 1 116.35 128.96 8.47 o 5 9 1 2659.99 2124.45 489.91 o 6 9 1 641.54 655.85 19.29 o 7 9 1 149.24 156.36 10.45 o 0 10 1 141.40 152.71 14.71 o 1 10 1 256.00 254.01 12.84 o 2 10 1 70.85 77.87 7.50 o 3 10 1 1533.90 1498.26 55.30 o 4 10 1 140.16 142.15 11.78 o 5 10 1 15.70 9.84 9.65 o 6 10 1 83.23 81.88 12.05 o 1 11 1 1800.98 1933.92 43.83 o 2 11 1 1974.82 1878.52 68.69 o 3 11 1 754.82 778.27 35.96 o 4 11 1 43.54 23.53 10.17 o 5 11 1 1376.01 1316.99 58.69 o 0 12 1 815.76 824.15 39.34 o 1 12 1 231.55 240.82 13.10 o 2 12 1 1.05 -2.34 10.14 o 3 12 1 1460.40 1491.68 39.90 o 0 0 2 41592.56 36426.58 1165.25 o 1 0 2 48608.32 31830.59 8186.48 o 2 0 2 13704.54 14141.18 423.46 o 3 0 2 7821.60 7496.12 118.77 o 4 0 2 9236.34 8938.48 146.99 o 5 0 2 1073.67 1048.03 25.73 o 6 0 2 406.42 448.78 16.04 o 7 0 2 9549.98 9346.83 181.00 o 8 0 2 1385.08 1386.76 45.76 o 9 0 2 2490.77 2396.65 70.02 o 10 0 2 444.19 469.20 28.69 o 1 1 2 2639.15 2625.55 66.02 o 2 1 2 771.34 773.94 17.75 o 3 1 2 85.02 71.68 4.26 o 4 1 2 390.14 450.39 7.91 o 5 1 2 386.44 282.75 7.64 o 6 1 2 192.56 202.68 7.49 o 7 1 2 0.58 -6.15 5.40 o 8 1 2 2.94 -4.41 7.16 o 9 1 2 1347.02 1306.20 32.45 o 10 1 2 162.38 187.23 14.69 o 0 2 2 26793.42 25251.63 1491.03 o 1 2 2 443.48 380.70 5.61 o 2 2 2 22.47 24.41 2.39 o 3 2 2 16464.20 16422.74 181.34 o 4 2 2 10967.69 11265.74 125.70 o 5 2 2 3929.34 4077.06 51.26 o 6 2 2 61.15 64.07 5.47 o 7 2 2 1854.89 1841.33 27.35 o 8 2 2 434.89 443.33 13.67 o 9 2 2 3.33 0.25 8.55 o 10 2 2 82.92 72.04 11.97 o 1 3 2 14347.70 14194.00 183.21 o 2 3 2 9057.05 9090.11 101.06 o 3 3 2 5418.25 4997.29 69.37 o 4 3 2 10.04 8.68 2.42 o 5 3 2 10562.36 10538.84 126.25 o 6 3 2 3509.48 3513.09 45.91 o 7 3 2 321.87 328.22 10.22 o 8 3 2 17.23 14.64 5.26 o 9 3 2 2275.79 2262.42 41.14 o 10 3 2 473.40 474.96 20.88 o 0 4 2 105.67 189.21 47.24 o 1 4 2 211.34 185.70 5.56 o 2 4 2 405.33 463.74 9.12 o 3 4 2 1640.93 1634.64 19.60 o 4 4 2 163.50 190.64 7.01 o 5 4 2 687.24 756.97 13.71 o 6 4 2 61.51 72.90 5.61 o 7 4 2 559.32 594.75 13.57 o 8 4 2 40.50 40.52 6.56 o 9 4 2 309.94 286.02 11.95 o 10 4 2 13.95 3.66 8.96 o 1 5 2 12000.09 8502.70 1734.81 o 2 5 2 5470.12 5284.21 57.65 o 3 5 2 6237.94 6040.27 72.77 o 4 5 2 1959.46 2061.22 33.26 o 5 5 2 5713.74 5535.57 69.05 o 6 5 2 1436.34 1432.87 22.73 o 7 5 2 712.56 719.31 15.40 o 8 5 2 414.52 435.05 12.98 o 9 5 2 1141.73 1204.60 22.05 o 0 6 2 19.19 16.80 6.56 o 1 6 2 15.82 3.69 2.84 o 2 6 2 173.94 194.59 6.00 o 3 6 2 3310.74 3325.37 39.30 o 4 6 2 572.48 538.72 10.99 o 5 6 2 468.49 420.70 31.65 o 6 6 2 131.69 143.45 7.67 o 7 6 2 96.02 120.64 7.91 o 8 6 2 50.58 65.89 7.66 o 9 6 2 40.35 35.99 7.73 o 1 7 2 1682.10 1679.31 25.22 o 2 7 2 7592.53 7924.93 141.22 o 3 7 2 2102.05 2076.35 42.11 o 4 7 2 35.94 48.67 4.77 o 5 7 2 754.01 813.35 16.07 o 6 7 2 957.11 969.96 18.46 o 7 7 2 433.92 430.37 19.71 o 8 7 2 38.42 42.88 7.44 o 0 8 2 2640.86 2793.63 52.38 o 1 8 2 8503.14 8955.82 106.88 o 2 8 2 104.51 118.07 5.70 o 3 8 2 4778.49 4793.34 93.41 o 4 8 2 669.43 679.10 14.76 o 5 8 2 37.67 30.04 5.98 o 6 8 2 95.86 96.26 7.38 o 7 8 2 4535.71 4660.91 91.14 o 8 8 2 398.96 405.61 14.38 o 1 9 2 715.20 753.00 17.76 o 2 9 2 479.27 503.01 12.63 o 3 9 2 109.27 112.54 7.53 o 4 9 2 782.72 783.42 23.78 o 5 9 2 843.71 781.63 19.05 o 6 9 2 38.26 35.15 8.60 o 7 9 2 8.51 3.29 8.17 o 0 10 2 4780.18 5065.94 143.47 o 1 10 2 464.10 497.06 17.44 o 2 10 2 87.55 80.57 7.56 o 3 10 2 3976.74 4099.32 88.03 o 4 10 2 2341.90 2273.88 58.08 o 5 10 2 1413.73 1341.28 67.64 o 6 10 2 14.22 26.63 9.67 o 1 11 2 1255.87 1292.97 29.01 o 2 11 2 426.11 423.22 16.82 o 3 11 2 902.19 883.56 51.52 o 4 11 2 235.84 229.01 15.24 o 5 11 2 551.22 502.87 24.95 o 0 12 2 1133.10 1135.94 46.22 o 1 12 2 1018.97 1000.25 25.41 o 2 12 2 42.89 32.01 11.33 o 3 12 2 416.82 389.11 19.37 o 1 1 3 1458.85 1504.77 16.76 o 2 1 3 16980.17 16058.19 212.27 o 3 1 3 692.17 676.47 9.49 o 4 1 3 454.91 391.99 7.51 o 5 1 3 33.53 30.26 3.59 o 6 1 3 8991.81 8972.51 110.88 o 7 1 3 0.44 2.23 5.71 o 8 1 3 445.14 435.77 17.75 o 9 1 3 27.19 27.69 9.49 o 10 1 3 1371.13 1364.10 43.44 o 0 2 3 14834.86 14049.58 352.03 o 1 2 3 3584.84 3591.12 40.60 o 2 2 3 11.81 13.57 2.71 o 3 2 3 155.15 181.87 6.30 o 4 2 3 7044.91 6676.74 75.78 o 5 2 3 16.49 13.44 3.49 o 6 2 3 1620.47 1628.82 25.86 o 7 2 3 9.09 7.28 5.31 o 8 2 3 881.15 863.56 18.98 o 9 2 3 1.99 -6.95 8.49 o 10 2 3 973.35 911.48 27.60 o 1 3 3 5947.39 6372.31 124.21 o 2 3 3 11428.82 11290.85 139.46 o 3 3 3 1643.85 1662.53 27.29 o 4 3 3 2399.62 2428.50 29.75 o 5 3 3 97.07 132.89 7.14 o 6 3 3 4282.14 4188.72 53.78 o 7 3 3 53.50 47.91 5.71 o 8 3 3 1230.93 1196.58 22.63 o 9 3 3 339.93 354.30 15.03 o 10 3 3 868.09 868.78 27.17 o 0 4 3 30024.50 28408.05 529.50 o 1 4 3 2383.93 2793.39 55.61 o 2 4 3 412.75 468.70 10.33 o 3 4 3 0.32 -1.18 1.90 o 4 4 3 17697.57 16856.94 215.41 o 5 4 3 623.51 644.08 11.13 o 6 4 3 1133.97 1149.42 20.11 o 7 4 3 210.92 195.62 8.59 o 8 4 3 3311.39 3293.54 45.48 o 9 4 3 70.98 64.47 7.84 o 10 4 3 833.84 819.20 22.83 o 1 5 3 378.79 461.60 9.83 o 2 5 3 202.08 225.72 9.29 o 3 5 3 2635.94 2987.42 34.07 o 4 5 3 790.53 829.46 13.33 o 5 5 3 1.39 4.37 3.35 o 6 5 3 509.77 485.79 11.79 o 7 5 3 1449.77 1470.54 23.88 o 8 5 3 101.69 86.16 7.67 o 9 5 3 134.11 121.83 9.20 o 0 6 3 16939.08 17158.02 322.08 o 1 6 3 270.76 284.75 9.56 o 2 6 3 9.86 13.98 3.47 o 3 6 3 217.83 202.74 6.07 o 4 6 3 9875.81 9843.66 153.61 o 5 6 3 112.95 114.50 6.45 o 6 6 3 312.21 326.13 10.45 o 7 6 3 127.75 114.06 7.82 o 8 6 3 2922.01 2918.81 50.38 o 9 6 3 5.17 2.17 7.01 o 1 7 3 716.75 619.84 62.35 o 2 7 3 7703.59 7682.77 116.17 o 3 7 3 775.23 818.09 18.23 o 4 7 3 2177.63 2223.91 30.32 o 5 7 3 0.12 -2.95 4.67 o 6 7 3 3552.71 3759.40 93.24 o 7 7 3 32.46 23.01 6.71 o 8 7 3 795.43 810.41 24.73 o 0 8 3 2612.37 2533.03 54.81 o 1 8 3 0.00 2.65 4.82 o 2 8 3 146.87 188.99 10.45 o 3 8 3 124.57 132.17 6.49 o 4 8 3 1221.36 1230.87 37.30 o 5 8 3 0.07 -1.95 5.72 o 6 8 3 80.04 77.44 8.56 o 7 8 3 33.12 37.29 11.74 o 8 8 3 140.80 130.13 10.20 o 1 9 3 20.25 20.50 6.36 o 2 9 3 10561.35 10620.80 175.75 o 3 9 3 161.45 175.94 9.82 o 4 9 3 1619.16 1663.21 46.15 o 5 9 3 4.08 -5.61 7.06 o 6 9 3 3246.43 3333.75 140.70 o 7 9 3 93.70 85.98 9.80 o 0 10 3 1967.45 1932.77 60.37 o 1 10 3 912.50 961.13 21.75 o 2 10 3 57.86 55.71 6.51 o 3 10 3 95.94 97.59 11.03 o 4 10 3 1041.57 1006.05 36.36 o 5 10 3 81.53 94.19 9.69 o 6 10 3 93.87 104.95 11.97 o 1 11 3 18.73 16.42 8.65 o 2 11 3 2875.28 2947.56 63.45 o 3 11 3 32.57 46.13 10.63 o 4 11 3 9.87 11.01 9.82 o 5 11 3 1.42 2.02 10.47 o 0 12 3 3781.72 4026.34 111.81 o 1 12 3 104.80 94.17 12.63 o 2 12 3 8.36 11.37 10.34 o 3 12 3 4.26 16.26 11.09 o 0 0 4 16423.80 15556.88 994.84 o 1 0 4 15648.67 14905.88 211.75 o 2 0 4 163.87 130.40 7.31 o 3 0 4 10485.43 9817.57 157.33 o 4 0 4 1255.98 1270.11 33.54 o 5 0 4 1616.97 1633.19 36.74 o 6 0 4 5202.01 5330.38 105.98 o 7 0 4 11876.45 11966.88 338.38 o 8 0 4 2732.06 2628.03 73.48 o 9 0 4 1292.05 1219.63 44.29 o 10 0 4 2.94 -10.93 13.55 o 1 1 4 40331.86 35585.80 1266.20 o 2 1 4 11709.46 12375.24 123.38 o 3 1 4 1587.62 1525.47 18.98 o 4 1 4 22.54 44.04 3.07 o 5 1 4 6918.52 7206.49 89.34 o 6 1 4 29.94 28.81 4.55 o 7 1 4 106.24 110.07 7.45 o 8 1 4 297.37 269.21 14.24 o 9 1 4 444.19 447.80 19.31 o 10 1 4 94.83 113.18 12.89 o 0 2 4 782.91 950.92 20.99 o 1 2 4 468.01 433.01 9.11 o 2 2 4 1969.27 2094.28 27.43 o 3 2 4 10878.74 11006.47 115.87 o 4 2 4 3999.16 4108.72 47.96 o 5 2 4 1817.80 1839.99 25.29 o 6 2 4 19.16 8.33 3.74 o 7 2 4 3159.61 3133.20 46.82 o 8 2 4 484.58 486.54 14.41 o 9 2 4 9.45 9.45 9.22 o 10 2 4 338.02 353.89 18.78 o 1 3 4 25329.59 24269.89 600.72 o 2 3 4 614.77 520.43 8.23 o 3 3 4 3211.32 3011.80 39.64 o 4 3 4 288.39 313.80 7.50 o 5 3 4 10495.84 10126.80 114.39 o 6 3 4 1162.21 1175.11 19.12 o 7 3 4 3.32 -1.81 4.77 o 8 3 4 236.46 247.90 17.09 o 9 3 4 1492.26 1484.88 30.85 o 10 3 4 337.35 375.72 19.23 o 0 4 4 826.46 1005.56 29.94 o 1 4 4 845.36 854.85 13.24 o 2 4 4 216.82 244.37 6.58 o 3 4 4 520.70 492.01 8.74 o 4 4 4 277.89 329.42 10.40 o 5 4 4 4.43 -1.92 3.00 o 6 4 4 301.47 323.19 9.59 o 7 4 4 129.99 137.39 8.20 o 8 4 4 1.07 9.51 6.25 o 9 4 4 42.23 20.25 8.08 o 1 5 4 7182.36 6982.03 115.93 o 2 5 4 7484.08 7475.37 84.86 o 3 5 4 6409.68 6287.66 88.73 o 4 5 4 278.21 251.07 6.97 o 5 5 4 3540.29 3486.91 45.50 o 6 5 4 1803.09 1808.83 27.85 o 7 5 4 773.49 747.14 19.41 o 8 5 4 154.43 172.25 9.21 o 9 5 4 1171.62 1132.61 21.85 o 0 6 4 82.29 64.48 10.58 o 1 6 4 493.38 427.17 13.59 o 2 6 4 142.24 154.10 6.45 o 3 6 4 1805.67 1841.11 22.93 o 4 6 4 1525.15 1541.67 23.66 o 5 6 4 1839.39 1873.09 27.61 o 6 6 4 182.96 154.64 12.21 o 7 6 4 599.69 615.74 14.86 o 8 6 4 8.53 9.06 6.84 o 9 6 4 53.11 64.24 8.99 o 1 7 4 2373.08 2472.72 43.89 o 2 7 4 1484.75 1432.37 22.32 o 3 7 4 1253.48 1233.41 21.87 o 4 7 4 230.70 260.43 9.59 o 5 7 4 1994.73 1975.96 34.25 o 6 7 4 522.82 554.71 13.82 o 7 7 4 194.14 189.30 15.78 o 8 7 4 236.37 213.10 10.66 o 0 8 4 6327.75 6750.56 164.84 o 1 8 4 3867.13 4025.89 75.86 o 2 8 4 20.67 26.66 5.07 o 3 8 4 2971.74 2971.54 48.99 o 4 8 4 558.95 572.58 14.68 o 5 8 4 54.84 60.64 7.28 o 6 8 4 1018.02 981.17 23.89 o 7 8 4 3384.63 3441.27 102.20 o 8 8 4 889.07 938.63 26.83 o 1 9 4 218.55 213.40 12.73 o 2 9 4 269.65 258.38 10.13 o 3 9 4 37.33 26.58 6.33 o 4 9 4 841.32 791.00 22.34 o 5 9 4 284.78 277.83 13.25 o 6 9 4 4.56 9.38 8.39 o 7 9 4 126.06 97.81 10.88 o 0 10 4 82.07 71.81 15.40 o 1 10 4 1974.19 2070.40 32.94 o 2 10 4 462.85 452.07 15.96 o 3 10 4 6717.08 6589.32 193.68 o 4 10 4 701.02 723.24 22.17 o 5 10 4 625.18 629.49 20.64 o 6 10 4 30.67 31.42 8.98 o 1 11 4 794.11 852.29 20.95 o 2 11 4 1757.59 1613.88 30.11 o 3 11 4 786.48 764.52 38.59 o 4 11 4 19.05 25.43 9.52 o 5 11 4 421.16 413.95 26.47 o 0 12 4 717.12 745.73 37.57 o 1 12 4 776.04 762.55 25.22 o 2 12 4 1.51 0.42 10.29 o 3 12 4 402.04 349.70 26.00 o 1 1 5 32143.53 29892.01 337.98 o 2 1 5 3860.52 3671.69 39.99 o 3 1 5 4370.36 4425.78 85.21 o 4 1 5 2317.67 2315.13 66.48 o 5 1 5 14593.17 14700.61 237.11 o 6 1 5 2133.25 2136.83 37.72 o 7 1 5 276.19 290.97 10.81 o 8 1 5 576.16 609.91 20.97 o 9 1 5 1854.10 1851.50 41.53 o 10 1 5 391.43 399.96 26.57 o 0 2 5 14894.04 14775.16 240.20 o 1 2 5 1027.65 939.11 10.91 o 2 2 5 330.82 335.12 5.84 o 3 2 5 268.17 175.32 5.57 o 4 2 5 2942.34 2782.82 33.68 o 5 2 5 1020.78 977.54 14.75 o 6 2 5 143.20 147.08 8.39 o 7 2 5 1736.06 1717.09 29.02 o 8 2 5 183.05 168.94 9.45 o 9 2 5 99.10 95.99 11.88 o 10 2 5 212.53 213.42 15.48 o 1 3 5 138.02 103.34 3.82 o 2 3 5 1069.07 1058.45 16.26 o 3 3 5 377.10 459.22 8.41 o 4 3 5 1662.59 1667.99 28.32 o 5 3 5 2338.31 2230.04 28.43 o 6 3 5 594.16 570.19 11.23 o 7 3 5 9.45 11.25 5.05 o 8 3 5 277.30 255.94 32.40 o 9 3 5 1022.00 1019.21 24.65 o 10 3 5 206.38 206.44 15.41 o 0 4 5 10698.36 10933.83 255.34 o 1 4 5 2387.06 2115.52 33.43 o 2 4 5 665.69 835.98 12.05 o 3 4 5 9633.88 9293.76 122.41 o 4 4 5 5311.47 5230.23 60.80 o 5 4 5 579.02 539.20 10.33 o 6 4 5 196.34 198.90 8.95 o 7 4 5 4081.78 4135.22 54.43 o 8 4 5 2800.24 2672.53 38.50 o 9 4 5 7.75 9.42 7.80 o 1 5 5 5940.34 6501.90 95.27 o 2 5 5 114.66 146.22 4.80 o 3 5 5 529.21 517.88 9.52 o 4 5 5 625.01 669.85 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10.80 6.66 4.20 o 6 6 7 19.18 11.78 5.20 o 7 6 7 2986.60 3047.84 51.73 o 8 6 7 221.88 243.99 16.27 o 1 7 7 2216.76 2354.87 49.40 o 2 7 7 1232.85 1193.26 21.67 o 3 7 7 1944.11 1935.95 30.76 o 4 7 7 10.10 9.04 5.38 o 5 7 7 2078.64 2105.90 36.91 o 6 7 7 17.51 26.24 7.51 o 7 7 7 443.91 435.47 17.93 o 8 7 7 39.13 18.65 8.86 o 0 8 7 2344.62 2456.91 69.28 o 1 8 7 469.25 507.16 16.34 o 2 8 7 68.63 72.40 6.99 o 3 8 7 871.32 901.41 18.64 o 4 8 7 824.49 804.53 25.61 o 5 8 7 42.14 39.06 7.87 o 6 8 7 0.14 -2.81 7.81 o 7 8 7 484.49 482.15 19.45 o 1 9 7 5115.82 5042.03 79.22 o 2 9 7 1643.91 1664.16 29.16 o 3 9 7 2267.97 2255.19 52.25 o 4 9 7 297.02 286.98 21.21 o 5 9 7 2988.61 2815.49 67.68 o 6 9 7 449.45 429.70 41.85 o 0 10 7 30.40 18.90 15.40 o 1 10 7 403.27 376.67 15.22 o 2 10 7 6.94 8.34 6.96 o 3 10 7 1063.79 1067.66 22.55 o 4 10 7 3.00 16.62 8.44 o 5 10 7 28.67 31.75 9.29 o 1 11 7 1303.45 1397.76 27.92 o 2 11 7 540.04 582.30 17.26 o 3 11 7 148.38 160.64 12.04 o 4 11 7 0.77 11.04 8.90 o 0 12 7 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2511.46 28.85 o 3 3 8 2750.12 2628.24 35.47 o 4 3 8 78.79 65.84 3.77 o 5 3 8 5366.54 5357.91 65.19 o 6 3 8 2966.91 2963.56 41.21 o 7 3 8 612.86 587.88 15.61 o 8 3 8 314.20 331.25 17.26 o 9 3 8 1139.72 1118.49 36.61 o 0 4 8 767.64 984.53 40.94 o 1 4 8 451.27 363.04 10.66 o 2 4 8 173.40 202.37 5.33 o 3 4 8 2194.56 2214.66 26.32 o 4 4 8 31.82 40.46 4.10 o 5 4 8 99.09 95.37 5.34 o 6 4 8 196.12 195.11 7.45 o 7 4 8 693.37 710.88 20.95 o 8 4 8 125.08 119.21 9.39 o 9 4 8 4.78 3.97 8.68 o 1 5 8 5218.88 5150.66 77.12 o 2 5 8 1414.13 1323.72 18.00 o 3 5 8 2131.09 2028.49 34.15 o 4 5 8 603.64 637.97 11.61 o 5 5 8 5353.16 5400.29 78.42 o 6 5 8 1711.11 1755.57 29.78 o 7 5 8 865.79 844.67 17.08 o 8 5 8 588.04 539.93 14.54 o 9 5 8 1261.13 1372.43 31.08 o 0 6 8 3444.23 3500.78 91.04 o 1 6 8 175.59 164.13 8.08 o 2 6 8 7.67 15.80 4.75 o 3 6 8 1982.00 1973.44 28.12 o 4 6 8 634.86 640.90 17.07 o 5 6 8 924.78 907.51 16.75 o 6 6 8 28.06 22.01 6.26 o 7 6 8 269.24 283.78 13.56 o 8 6 8 70.91 62.29 8.48 o 1 7 8 5836.78 5977.74 90.32 o 2 7 8 1496.63 1572.26 30.15 o 3 7 8 3575.59 3551.83 51.20 o 4 7 8 1683.41 1575.40 26.89 o 5 7 8 1272.11 1229.93 31.25 o 6 7 8 230.74 243.71 12.96 o 7 7 8 285.21 287.82 13.63 o 8 7 8 431.44 363.84 16.23 o 0 8 8 2771.51 2792.52 77.45 o 1 8 8 5020.99 5085.29 87.11 o 2 8 8 75.04 75.12 6.96 o 3 8 8 1463.82 1554.00 29.63 o 4 8 8 2067.11 1994.95 42.31 o 5 8 8 85.38 92.44 8.96 o 6 8 8 2.15 2.32 7.58 o 7 8 8 2561.79 2516.83 84.29 o 1 9 8 46.15 41.39 9.44 o 2 9 8 5.35 9.84 6.66 o 3 9 8 95.97 92.36 8.27 o 4 9 8 1.50 0.63 7.29 o 5 9 8 199.90 179.15 12.39 o 6 9 8 2.14 13.12 8.87 o 0 10 8 2468.73 2429.99 71.97 o 1 10 8 1624.12 1659.27 33.20 o 2 10 8 0.66 -4.39 6.92 o 3 10 8 4254.64 4159.19 79.13 o 4 10 8 1185.63 1141.07 55.56 o 5 10 8 527.57 550.99 20.51 o 1 11 8 214.22 232.72 13.51 o 2 11 8 427.10 410.83 15.27 o 3 11 8 111.76 110.46 11.09 o 4 11 8 108.22 106.65 11.22 o 0 12 8 4.27 11.17 11.11 o 1 1 9 27.18 56.44 3.20 o 2 1 9 18594.13 18301.58 207.16 o 3 1 9 600.75 635.76 10.41 o 4 1 9 157.13 166.76 5.78 o 5 1 9 119.09 119.74 7.01 o 6 1 9 8795.09 8890.25 153.23 o 7 1 9 313.04 312.01 13.25 o 8 1 9 235.11 242.01 15.05 o 9 1 9 27.16 22.37 10.40 o 0 2 9 14570.05 14650.49 240.02 o 1 2 9 37.78 41.42 3.29 o 2 2 9 3646.92 3427.38 220.23 o 3 2 9 2296.48 2351.12 30.18 o 4 2 9 9107.59 9154.21 106.06 o 5 2 9 12.00 14.15 4.12 o 6 2 9 1605.18 1599.00 27.39 o 7 2 9 12.25 17.72 6.53 o 8 2 9 981.43 1046.82 24.68 o 9 2 9 0.77 0.34 10.12 o 1 3 9 53.17 82.15 5.67 o 2 3 9 11394.18 11278.48 114.20 o 3 3 9 219.29 258.80 6.26 o 4 3 9 256.43 245.29 7.66 o 5 3 9 6.88 14.74 4.65 o 6 3 9 141.17 154.55 8.12 o 7 3 9 230.25 223.84 9.69 o 8 3 9 273.06 287.52 14.20 o 9 3 9 149.43 155.46 12.22 o 0 4 9 34299.30 34089.20 646.30 o 1 4 9 38.48 53.37 9.52 o 2 4 9 27.94 22.70 2.75 o 3 4 9 66.26 66.39 3.82 o 4 4 9 11594.80 11395.89 121.75 o 5 4 9 1004.91 940.19 15.33 o 6 4 9 1345.03 1328.26 21.50 o 7 4 9 260.57 273.03 15.09 o 8 4 9 2741.56 2751.98 44.46 o 9 4 9 8.49 1.52 9.01 o 1 5 9 79.80 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6 10 1455.86 1407.18 24.53 o 5 6 10 3.78 4.85 5.73 o 6 6 10 11.93 8.80 7.04 o 7 6 10 670.54 700.06 18.88 o 8 6 10 83.88 82.65 10.20 o 1 7 10 997.64 993.60 21.04 o 2 7 10 4022.29 3971.99 56.81 o 3 7 10 1158.53 1217.29 22.33 o 4 7 10 38.44 38.27 6.51 o 5 7 10 504.91 487.50 15.93 o 6 7 10 323.19 312.47 19.42 o 7 7 10 220.95 213.65 12.44 o 0 8 10 212.32 202.82 18.51 o 1 8 10 3282.36 3219.33 63.54 o 2 8 10 241.55 224.46 13.15 o 3 8 10 3658.74 3582.13 52.95 o 4 8 10 13.99 16.94 6.58 o 5 8 10 857.19 853.49 25.65 o 6 8 10 331.49 332.72 20.90 o 7 8 10 1503.56 1511.73 38.78 o 1 9 10 524.88 510.41 16.35 o 2 9 10 333.46 325.20 12.58 o 3 9 10 251.84 230.56 10.97 o 4 9 10 0.27 -0.47 7.37 o 5 9 10 0.12 0.44 10.04 o 6 9 10 3.72 7.33 11.53 o 0 10 10 125.73 127.85 18.51 o 1 10 10 2611.32 2542.23 54.55 o 2 10 10 224.17 208.15 13.17 o 3 10 10 1562.17 1467.95 32.53 o 4 10 10 744.64 688.35 30.92 o 1 11 10 60.23 65.35 11.12 o 2 11 10 129.63 120.51 12.02 o 3 11 10 67.94 76.75 16.36 o 1 1 11 11304.19 11385.40 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6.73 12.14 o 1 4 20 361.48 340.42 17.26 o 2 4 20 5.72 -9.03 8.43 o 3 4 20 45.14 28.23 9.44 o 4 4 20 57.18 52.11 12.80 o 1 5 20 740.69 692.58 37.45 o 2 5 20 914.49 911.24 65.55 o 3 5 20 655.88 662.50 25.34 o 4 5 20 38.50 19.76 12.53 o 0 6 20 477.80 500.30 33.15 o 1 6 20 29.52 23.09 11.89 o 2 6 20 53.89 36.03 12.85 o 3 6 20 258.02 238.01 18.21 o 1 7 20 54.34 67.53 13.88 o 1 1 21 94.94 98.62 8.77 o 2 1 21 1199.11 1265.77 24.92 o 3 1 21 57.82 62.40 8.80 o 4 1 21 6.68 2.50 7.83 o 5 1 21 164.49 191.76 17.79 o 0 2 21 1718.96 1814.78 62.17 o 1 2 21 12.84 24.92 8.66 o 2 2 21 122.18 110.83 10.89 o 3 2 21 25.71 16.87 9.26 o 4 2 21 915.24 907.33 30.06 o 5 2 21 5.52 -5.15 10.86 o 1 3 21 65.75 82.63 10.38 o 2 3 21 1394.44 1377.49 35.00 o 3 3 21 8.84 5.22 9.35 o 4 3 21 97.26 94.90 13.14 o 0 4 21 5162.87 4801.23 105.92 o 1 4 21 113.67 134.75 17.01 o 2 4 21 66.82 46.74 10.22 o 3 4 21 251.21 232.31 14.14 o 4 4 21 1264.48 1273.51 68.51 o 1 5 21 19.90 -3.98 9.98 o 2 5 21 64.51 48.73 11.57 o 3 5 21 13.38 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