#------------------------------------------------------------------------------ #$Date: 2018-03-03 09:07:20 +0200 (Sat, 03 Mar 2018) $ #$Revision: 206761 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242404.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242404 loop_ _publ_author_name 'C\'ardenas-Valenzuela, A. Jaquelin' 'Gonz\'alez-Garc\'ia, Gerardo' 'Z\'arraga- Nu\~nez, Ram\'on' 'H\"opfl, Herbert' 'Campos-Gaxiola, Jos\'e J.' 'Cruz-Enr\'iquez, Adriana' _publ_contact_author_address ; Facultad de Ingenier\'ia Mochis, Universidad Aut\'onoma de Sinaloa, Fuente de Poseid\'on y Prol. A. Flores S/N, C.P. 81223, C.U. Los Mochis, Sinaloa, M\'exico. ; _publ_contact_author_email cruzadriana@uas.edu.mx _publ_contact_author_fax ? _publ_contact_author_id_orcid ? _publ_contact_author_name 'Adriana Cruz-Enr\'iquez' _publ_contact_author_phone 6684801459 _publ_section_related_literature ? _publ_section_title ; 3-Cyanophenylboronic acid: crystal structure and Hirshfeld surface analysis ; _publ_section_title_footnote . _publ_section_keywords ; Boronic acid, Molecular and supramolecular structure, Hirshfeld surface analysis. ; _chemical_formula_moiety 'C7 H6 B N O2' _chemical_formula_sum 'C7 H6 B N O2' _chemical_formula_weight 146.94 _chemical_melting_point ? _chemical_name_common ? _chemical_name_systematic ? _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _atom_sites_solution_secondary ? _audit_creation_date 2017-12-16 _audit_creation_method ; Olex2 1.2 (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _audit_update_record ; 2018-02-09 # Formatted by publCIF ; _cell_angle_alpha 90 _cell_angle_beta 93.472(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 3.8064(2) _cell_length_b 16.1560(10) _cell_length_c 11.4585(4) _cell_measurement_reflns_used 4312 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 29.0530 _cell_measurement_theta_min 4.3500 _cell_volume 703.36(6) _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution ; Superflip (Palatinus & Chapuis, 2007;Palatinus & van der Lee, 2008; Palatinus et al., 2012) ; _diffrn_ambient_temperature 293(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 8.0945 _diffrn_detector_type EosS2 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -1.00 83.00 0.30 5.04 -- 15.81 57.00 30.00 280 2 \w -1.00 83.00 0.30 5.04 -- 15.81 57.00 150.00 280 3 \w -35.00 49.00 0.30 5.04 -- -17.84 57.00 -90.00 280 4 \w -1.00 83.00 0.30 5.04 -- 15.81 57.00 -90.00 280 5 \w 6.00 72.00 0.30 5.04 -- 15.81-130.00-156.00 220 6 \w -52.00 1.10 0.30 5.04 -- 15.81 -77.00 0.00 177 7 \w -90.00 -34.80 0.30 5.04 -- -17.84 178.00 -30.00 184 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Single source at offset, EosS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0367450000 _diffrn_orient_matrix_UB_12 0.0217991000 _diffrn_orient_matrix_UB_13 -0.0530451000 _diffrn_orient_matrix_UB_21 0.0139583000 _diffrn_orient_matrix_UB_22 0.0380914000 _diffrn_orient_matrix_UB_23 0.0307674000 _diffrn_orient_matrix_UB_31 0.1824372000 _diffrn_orient_matrix_UB_32 0.0014819000 _diffrn_orient_matrix_UB_33 -0.0092709000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0231 _diffrn_reflns_av_unetI/netI 0.0145 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 4 _diffrn_reflns_limit_h_min -4 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 7332 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.367 _diffrn_reflns_theta_min 3.563 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.100 _exptl_absorpt_correction_T_max 0.996 _exptl_absorpt_correction_T_min 0.992 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.388 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 304 _exptl_crystal_size_max 0.476 _exptl_crystal_size_mid 0.25 _exptl_crystal_size_min 0.199 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _refine_diff_density_max 0.202 _refine_diff_density_min -0.240 _refine_diff_density_rms 0.073 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.088 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 102 _refine_ls_number_reflns 1434 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.088 _refine_ls_R_factor_all 0.0441 _refine_ls_R_factor_gt 0.0422 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0566P)^2^+0.1839P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1089 _refine_ls_wR_factor_ref 0.1103 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1347 _reflns_number_total 1434 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL CF solution in P21/c exp_585.res created by SHELXL-2016/4 at 15:07:53 on 16-Dec-2017 CELL 0.71073 3.8064 16.156 11.4585 90 93.4719 90 ZERR 4 0.0002 0.001 0.0004 0 0.004 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H B N O UNIT 28 24 4 4 8 L.S. 10 PLAN 25 SIZE 0.199 0.25 0.476 BOND MORE -1 CONF fmap 2 acta REM REM REM WGHT 0.056600 0.183900 FVAR 11.23736 O2 5 0.890589 0.493510 0.349346 11.00000 0.06793 0.03706 = 0.02425 -0.00045 -0.00917 0.01026 AFIX 147 H2 2 0.881271 0.482459 0.279381 11.00000 -1.50000 AFIX 0 O1 5 0.814345 0.607010 0.471871 11.00000 0.08097 0.04137 = 0.02777 -0.00288 -0.01205 0.01652 AFIX 147 H1 2 0.900315 0.572989 0.518407 11.00000 -1.50000 AFIX 0 N1 4 0.076206 0.585877 -0.122427 11.00000 0.06254 0.04743 = 0.03390 -0.00439 -0.01146 0.00768 C3 1 0.342356 0.650061 0.069421 11.00000 0.03031 0.03605 = 0.02538 0.00006 -0.00011 0.00254 C7 1 0.190867 0.614623 -0.037432 11.00000 0.03984 0.03652 = 0.02946 0.00282 -0.00313 0.00774 C1 1 0.624561 0.629609 0.262142 11.00000 0.03038 0.03318 = 0.02669 0.00168 -0.00021 0.00144 C2 1 0.476532 0.597440 0.157751 11.00000 0.03428 0.02913 = 0.02898 0.00049 -0.00115 0.00191 AFIX 43 H2A 2 0.467006 0.540428 0.146805 11.00000 -1.20000 AFIX 0 C4 1 0.356123 0.735416 0.082861 11.00000 0.04262 0.03527 = 0.03195 0.00674 0.00040 0.00626 AFIX 43 H4 2 0.267843 0.770116 0.023320 11.00000 -1.20000 AFIX 0 C6 1 0.632467 0.715748 0.274230 11.00000 0.03975 0.03576 = 0.02961 -0.00314 -0.00162 -0.00195 AFIX 43 H6 2 0.727616 0.738593 0.343630 11.00000 -1.20000 AFIX 0 C5 1 0.503139 0.768020 0.186152 11.00000 0.05201 0.02867 = 0.03901 0.00012 0.00088 0.00073 AFIX 43 H5 2 0.515094 0.825073 0.196425 11.00000 -1.20000 AFIX 0 B1 3 0.782695 0.573236 0.364416 11.00000 0.03847 0.03474 = 0.02677 0.00095 -0.00380 0.00058 HKLF 4 REM CF solution in P21/c REM R1 = 0.0422 for 1347 Fo > 4sig(Fo) and 0.0441 for all 1434 data REM 102 parameters refined using 0 restraints END WGHT 0.0566 0.1839 REM Highest difference peak 0.202, deepest hole -0.240, 1-sigma level 0.073 Q1 1 0.7349 0.6013 0.3001 11.00000 0.05 0.20 Q2 1 0.9924 0.6569 0.2014 11.00000 0.05 0.19 Q3 1 -0.0688 0.6767 0.1243 11.00000 0.05 0.19 Q4 1 1.1008 0.6391 0.2650 11.00000 0.05 0.18 Q5 1 0.8288 0.6280 0.0982 11.00000 0.05 0.18 Q6 1 1.1306 0.6563 0.3424 11.00000 0.05 0.17 Q7 1 -0.2294 0.5800 0.0219 11.00000 0.05 0.15 Q8 1 0.8288 0.5646 0.0951 11.00000 0.05 0.15 Q9 1 1.1950 0.6021 0.3346 11.00000 0.05 0.14 Q10 1 0.6379 0.6250 -0.0217 11.00000 0.05 0.14 Q11 1 0.8945 0.5911 0.1665 11.00000 0.05 0.14 Q12 1 0.4753 0.9133 0.1206 11.00000 0.05 0.13 Q13 1 0.4755 0.5262 0.4632 11.00000 0.05 0.13 Q14 1 0.4940 0.4367 0.3624 11.00000 0.05 0.13 Q15 1 1.0447 0.5668 0.2280 11.00000 0.05 0.12 Q16 1 0.1795 0.7144 0.3028 11.00000 0.05 0.12 Q17 1 0.5448 0.5297 0.5574 11.00000 0.05 0.12 Q18 1 0.6226 0.8363 0.4187 11.00000 0.05 0.12 Q19 1 0.3577 0.8349 0.2494 11.00000 0.05 0.12 Q20 1 0.6835 0.4684 0.5556 11.00000 0.05 0.12 Q21 1 0.5236 0.9013 0.1965 11.00000 0.05 0.12 Q22 1 0.3819 0.8585 0.0218 11.00000 0.05 0.11 Q23 1 0.5804 0.8163 0.3713 11.00000 0.05 0.11 Q24 1 0.4552 0.5801 0.5356 11.00000 0.05 0.11 Q25 1 0.3736 0.8116 0.3209 11.00000 0.05 0.11 REM The information below was added by Olex2. REM REM R1 = 0.0422 for 1347 Fo > 4sig(Fo) and 0.0441 for all 7499 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.20, deepest hole -0.24 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0441 REM R1_gt = 0.0422 REM wR_ref = 0.1103 REM GOOF = 1.088 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 7499 REM Reflections_gt = 1347 REM Parameters = n/a REM Hole = -0.24 REM Peak = 0.20 REM Flack = n/a ; _cod_data_source_file su5425Isup2.hkl _cod_data_source_block I _iucr_geom_hbonds_special_details ; ; _publcif_datablock.id {1eabab0e-05e6-49dd-b377-a6df6b5e513e} _shelx_shelxl_version_number 2016/4 _chemical_oxdiff_formula 'B1 C7 N1 O2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.980 _shelx_estimated_absorpt_t_min 0.954 _exptl_absorpt_special_details ? _reflns_odcompleteness_completeness 99.67 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: C2(H2A), C4(H4), C6(H6), C5(H5) 2.b Idealised tetrahedral OH refined as rotating group: O2(H2), O1(H1) ; _olex2_date_sample_data_collection 2017-12-15 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.429 _oxdiff_exptl_absorpt_empirical_full_min 0.737 _publcif_info_exptl_table_max_cols 4 _publcif_info_exptl_table_use_headnotes n _publcif_funding_html ; ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O2 O 0.8906(3) 0.49351(6) 0.34935(8) 0.0436(3) Uani 1 1 d . . . . . H2 H 0.881271 0.482459 0.279381 0.065 Uiso 1 1 calc GR . . . . O1 O 0.8143(3) 0.60701(6) 0.47187(8) 0.0507(3) Uani 1 1 d . . . . . H1 H 0.900315 0.572989 0.518407 0.076 Uiso 1 1 calc GR . . . . N1 N 0.0762(4) 0.58588(8) -0.12243(11) 0.0485(4) Uani 1 1 d . . . . . C3 C 0.3424(3) 0.65006(8) 0.06942(10) 0.0307(3) Uani 1 1 d . . . . . C7 C 0.1909(4) 0.61462(8) -0.03743(11) 0.0355(3) Uani 1 1 d . . . . . C1 C 0.6246(3) 0.62961(8) 0.26214(10) 0.0302(3) Uani 1 1 d . . . . . C2 C 0.4765(3) 0.59744(8) 0.15775(11) 0.0309(3) Uani 1 1 d . . . . . H2A H 0.467006 0.540428 0.146805 0.037 Uiso 1 1 calc R . . . . C4 C 0.3561(4) 0.73542(8) 0.08286(12) 0.0367(3) Uani 1 1 d . . . . . H4 H 0.267843 0.770116 0.023320 0.044 Uiso 1 1 calc R . . . . C6 C 0.6325(4) 0.71575(8) 0.27423(11) 0.0352(3) Uani 1 1 d . . . . . H6 H 0.727616 0.738593 0.343630 0.042 Uiso 1 1 calc R . . . . C5 C 0.5031(4) 0.76802(8) 0.18615(12) 0.0400(3) Uani 1 1 d . . . . . H5 H 0.515094 0.825073 0.196425 0.048 Uiso 1 1 calc R . . . . B1 B 0.7827(4) 0.57324(9) 0.36442(12) 0.0336(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O2 0.0679(7) 0.0371(5) 0.0242(5) -0.0004(4) -0.0092(5) 0.0103(5) O1 0.0810(8) 0.0414(6) 0.0278(5) -0.0029(4) -0.0120(5) 0.0165(5) N1 0.0625(9) 0.0474(7) 0.0339(7) -0.0044(5) -0.0115(6) 0.0077(6) C3 0.0303(6) 0.0361(7) 0.0254(6) 0.0001(5) -0.0001(5) 0.0025(5) C7 0.0398(7) 0.0365(7) 0.0295(7) 0.0028(5) -0.0031(5) 0.0077(5) C1 0.0304(6) 0.0332(7) 0.0267(6) 0.0017(5) -0.0002(5) 0.0014(5) C2 0.0343(7) 0.0291(6) 0.0290(6) 0.0005(5) -0.0011(5) 0.0019(5) C4 0.0426(8) 0.0353(7) 0.0320(7) 0.0067(5) 0.0004(5) 0.0063(5) C6 0.0397(7) 0.0358(7) 0.0296(6) -0.0031(5) -0.0016(5) -0.0019(5) C5 0.0520(8) 0.0287(7) 0.0390(8) 0.0001(5) 0.0009(6) 0.0007(6) B1 0.0385(8) 0.0347(8) 0.0268(7) 0.0010(5) -0.0038(6) 0.0006(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 -16 11 0.1521 -5 3 1 0.2929 0 16 -11 0.0462 5 1 -5 0.1089 0 1 16 0.1849 -5 -1 2 0.2968 0 -1 -16 0.0978 0 -19 -9 0.0649 0 19 9 0.1485 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C3 C7 119.00(12) . . ? C4 C3 C7 119.98(11) . . ? C4 C3 C2 121.02(12) . . ? N1 C7 C3 178.81(15) . . ? C2 C1 C6 117.51(11) . . ? C2 C1 B1 122.70(11) . . ? C6 C1 B1 119.79(11) . . ? C1 C2 C3 120.50(12) . . ? C5 C4 C3 118.95(12) . . ? C5 C6 C1 122.04(12) . . ? C4 C5 C6 119.98(12) . . ? O2 B1 C1 123.75(11) . . ? O1 B1 O2 119.15(12) . . ? O1 B1 C1 117.10(12) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O2 B1 1.3661(18) . ? O1 B1 1.3455(17) . ? N1 C7 1.1416(18) . ? C3 C7 1.4401(18) . ? C3 C2 1.3948(17) . ? C3 C4 1.3882(19) . ? C1 C2 1.3917(17) . ? C1 C6 1.3987(18) . ? C1 B1 1.5747(18) . ? C4 C5 1.3825(19) . ? C6 C5 1.3834(19) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O1 H1 O2 3_766 ? ? 0.82 1.98 2.791(1) 170 ? O2 H2 N1 3_665 . . 0.82 2.13 2.909(2) 160 . C2 H2A N1 3_665 . . 0.93 2.71 3.452(2) 138 . C4 H4 O1 4_475 . . 0.93 2.67 3.469(2) 144 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C3 C4 C5 C6 -0.2(2) . . . . ? C7 C3 C2 C1 -179.96(12) . . . . ? C7 C3 C4 C5 -179.92(12) . . . . ? C1 C6 C5 C4 0.9(2) . . . . ? C2 C3 C4 C5 -0.5(2) . . . . ? C2 C1 C6 C5 -0.8(2) . . . . ? C2 C1 B1 O2 21.3(2) . . . . ? C2 C1 B1 O1 -159.37(13) . . . . ? C4 C3 C2 C1 0.64(19) . . . . ? C6 C1 C2 C3 0.00(18) . . . . ? C6 C1 B1 O2 -158.17(13) . . . . ? C6 C1 B1 O1 21.14(19) . . . . ? B1 C1 C2 C3 -179.50(12) . . . . ? B1 C1 C6 C5 178.76(13) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 0 0 -2 3796.77 130.137 2 0 0 2 3767.35 131.45 2 0 0 3 -1.47074 11.2403 2 0 0 -3 5.78384 9.48992 2 0 0 -4 22942 541.25 2 0 0 4 24200.5 557.064 2 0 0 -4 23520.8 516.656 6 0 0 -5 23.9812 24.6827 6 0 0 5 -3.32679 14.6154 2 0 0 5 48.2385 27.3977 1 0 0 -5 -5.07895 18.5423 2 0 0 -6 15391.1 447.205 6 0 0 -6 16292.7 490.825 2 0 0 7 122.92 48.5528 1 0 0 -7 27.9466 30.5912 6 0 0 -7 56.0085 38.6407 2 0 0 -8 5842.88 314.212 2 0 0 8 6579.9 329.065 1 0 0 -8 5798.66 292.903 6 0 0 -9 47.019 39.1654 6 0 0 9 18.4021 28.8884 1 0 0 -9 74.2078 47.5716 2 0 0 -10 46870.1 1145.9 6 0 0 10 48482.7 1189.49 1 0 0 -10 43788.6 1161.89 2 0 0 11 37.0374 53.9673 1 0 0 -11 42.1191 47.8138 6 0 0 -12 69.2582 51.6424 6 0 0 12 95.2199 59.3733 1 0 0 13 134.906 69.1843 1 0 0 -13 116.306 68.7219 6 0 0 -14 1009.48 173.316 6 0 0 14 945.26 169.616 1 0 1 2 37474.9 656.437 2 0 -1 2 36774.8 666.757 2 0 -1 -2 36897.2 653.532 2 0 1 -2 36189.2 641.282 6 0 1 -2 37214.6 663.278 2 0 -1 2 34298.9 653.324 1 0 -1 -2 36243.7 639.681 4 0 -1 2 35980.3 640.311 6 0 1 -2 35663.1 659.807 1 0 -1 3 6383.98 214.392 2 0 -1 -3 6217.69 192.479 4 0 -1 -3 6402.18 208.638 2 0 1 -3 6373.2 213.514 2 0 1 -3 6369.11 198.385 6 0 1 3 6170.78 207.249 2 0 -1 3 6367.52 208.761 1 0 1 -4 38.9502 21.4024 2 0 -1 -4 37.9754 21.1073 4 0 -1 -4 63.0785 26.0802 2 0 1 -4 22.047 18.1042 6 0 -1 4 32.5463 22.8172 2 0 1 4 19.1281 15.2017 2 0 -1 4 12.3141 14.927 1 0 1 -5 83629.4 1499.45 2 0 1 -5 80678.3 1451.19 6 0 1 5 86509.8 1509.77 2 0 -1 5 77761.6 1475.12 1 0 -1 5 78591 1499.89 2 0 -1 -5 81150.2 1432.15 4 0 -1 -5 78191 1472.15 2 0 1 -6 4208.38 212.662 6 0 -1 -6 4344.54 210.45 6 0 -1 -6 4276.87 226.815 2 0 1 -6 4063.51 224.364 2 0 -1 6 4143.96 222.094 1 0 -1 -6 4268.57 204.245 4 0 1 -7 14409.6 488.821 2 0 -1 7 13994.1 475.645 1 0 -1 -7 14306.2 452.573 6 0 -1 -7 14126.4 480.296 2 0 1 -7 14487 463.742 6 0 -1 -8 3859.32 232.855 6 0 -1 8 4271.56 259.216 1 0 -1 -8 4131.3 258.56 2 0 1 -8 3844.25 236.582 6 0 1 8 3634.13 243.631 1 0 1 -8 3806.84 251.169 2 0 -1 9 1561.54 166.748 1 0 -1 -9 1290.41 143.543 6 0 1 -9 1090.89 135.779 6 0 1 9 1396.96 159.691 1 0 1 -9 1410.1 160.462 2 0 -1 -9 1670.94 173.21 2 0 -1 -10 104979 2167.32 2 0 1 -10 107816 2136.05 6 0 -1 -10 110631 2132.45 6 0 -1 10 109129 2170.66 1 0 1 10 108377 2184.78 1 0 -1 -11 5839.65 353.254 6 0 1 -11 5572.56 348.437 6 0 -1 -11 6292.05 384.789 2 0 -1 11 5537.85 350.51 1 0 1 11 5867.64 370.784 1 0 1 12 321.89 93.9319 1 0 -1 -12 385.124 102.182 6 0 -1 12 459.291 107.651 1 0 1 -12 367.251 100.299 6 0 -1 -13 3061.74 282.088 6 0 1 -13 2751.61 274.837 6 0 1 13 2539.76 265.92 1 0 -1 13 2607.49 263.074 1 0 1 14 75.7152 61.1346 1 0 -1 14 173.151 84.4047 1 0 1 -14 326.117 104.207 6 0 -1 -14 188.743 80.3536 6 0 -2 -2 16500.5 346.201 2 0 -2 2 17170.5 358.975 1 0 2 -2 16401.6 363.849 1 0 -2 2 15720.7 337.114 6 0 2 2 16612.3 345.024 2 0 2 -2 15591.7 336.294 6 0 2 -2 15304.6 332.363 3 0 -2 -2 15304.8 333.466 4 0 2 2 15568.5 336.975 4 0 2 -3 4696.58 169.369 6 0 -2 -3 4493.36 162.622 4 0 -2 3 4566.01 174.742 1 0 -2 -3 4717.26 175.538 2 0 2 3 5333.62 183.567 2 0 -2 3 4647.67 187.827 2 0 -2 3 4662.35 168.185 6 0 2 -4 136418 2268.69 6 0 -2 4 134273 2317.39 2 0 -2 -4 139928 2258.9 4 0 -2 4 139638 2288.71 1 0 -2 -4 138764 2290.08 2 0 2 4 136381 2295.41 2 0 -2 5 52616.1 1088.12 2 0 2 5 56064.4 1084.14 2 0 -2 -5 54814 1071.14 2 0 2 5 52431 865.892 7 0 -2 -5 54248.1 1026.45 4 0 -2 5 55396.9 1067.61 1 0 2 -5 54040 1046.43 6 0 -2 6 101154 1824.33 1 0 2 -6 100501 1803.09 6 0 2 -6 99505.3 1563.86 7 0 -2 -6 101108 1828.13 2 0 2 -7 783.803 100.313 6 0 -2 -7 810.692 104.721 2 0 -2 -7 873.42 100.403 6 0 -2 7 682.025 93.9578 1 0 -2 8 39961.9 968.564 1 0 -2 -8 39930.8 979.728 2 0 -2 -8 41428 945.224 6 0 2 -8 39533.4 953.846 6 0 -2 9 6719.29 348.047 1 0 -2 -9 6134.73 317.875 6 0 -2 -9 6163.83 343.752 2 0 2 -9 6744.4 340.358 6 0 2 -10 25198.1 775.599 6 0 2 10 26544.2 824.667 1 0 -2 -10 26771.9 779.819 6 0 -2 10 24724.2 778.49 1 0 -2 -10 25895.3 812.054 2 0 -2 11 15309.7 605.481 1 0 -2 -11 15050.9 619.861 2 0 -2 -11 15086.9 590.436 6 0 2 -11 15188.2 604.137 6 0 2 11 14758.4 618.627 1 0 -2 -12 2886.15 273.989 2 0 -2 12 3092.8 271.468 1 0 2 -12 2868.19 265.364 6 0 -2 -12 2903.6 258.966 6 0 2 12 2994.83 279.205 1 0 2 -13 498.065 116.425 6 0 -2 13 627.846 129.852 1 0 -2 -13 690.146 135.085 6 0 2 13 657.753 137.914 1 0 -2 -14 232.062 88.7002 6 0 -2 14 243.481 93.0868 1 0 2 14 244.869 98.5075 1 0 2 -14 252.604 97.2146 6 0 3 0 1.5019 7.27963 1 0 -3 0 5.93622 9.0398 1 0 3 0 1.65659 6.12937 3 0 3 0 12.069 8.83478 4 0 -3 0 4.64138 6.72453 4 0 -3 0 10.8837 8.65273 3 0 3 -1 130874 2023.95 3 0 -3 1 126835 2026.66 3 0 -3 -1 128570 2023.04 4 0 3 -1 129528 2051.57 1 0 3 -1 129793 2017.14 4 0 -3 -1 126824 2020.51 3 0 -3 1 130425 2015.7 6 0 -3 1 125161 2041.52 1 0 3 -1 130010 2019.53 6 0 3 1 123764 2021.91 4 0 3 2 234854 3690.42 2 0 -3 2 234398 3691.73 3 0 3 2 238898 3690.41 4 0 -3 2 235978 3706.29 1 0 3 -2 241905 3722.24 1 0 -3 -2 243892 3686.9 4 0 3 -2 229431 3687.37 3 0 -3 2 239478 3683.12 6 0 3 -2 241411 3685.46 6 0 -3 -2 233083 3690.52 2 0 3 3 21539.5 481.637 4 0 -3 3 22391.7 516.509 2 0 3 3 21561.2 483.132 2 0 -3 -3 22941.5 491.631 2 0 3 -3 23563.9 516.912 1 0 3 -3 21295.8 472.45 6 0 -3 -3 21948.2 473.004 4 0 -3 3 21607 494.081 1 0 3 -3 22366.5 478.182 3 0 -3 3 21641.1 475.022 6 0 3 4 114396 1940.82 2 0 -3 -4 112234 1934.16 2 0 -3 4 114183 1918.8 6 0 3 -4 113404 1925.57 6 0 -3 -4 112718 1911.93 4 0 3 -4 114590 1981.56 1 0 -3 4 114662 1985.05 2 0 -3 4 116447 1946.78 1 0 -3 5 67507.8 1272.3 1 0 -3 -5 66140.2 1233.88 4 0 3 5 70447.9 1285.63 2 0 3 -5 63752.9 1244.45 6 0 -3 5 68594 1321.77 2 0 -3 -5 65944.4 1266.66 2 0 3 6 8572.69 204.77 7 0 -3 6 8140.19 325.021 1 0 -3 -6 8481.45 333.339 2 0 3 -6 9153.56 333.024 6 0 -3 7 13730.4 463.032 1 0 3 -7 13960.9 457.755 6 0 3 -7 13654.1 290.186 7 0 3 7 13206.9 274.817 7 0 -3 -7 14240.3 476.196 2 0 3 -8 3859.82 241.624 6 0 -3 -8 4599.33 250.771 6 0 -3 8 4229.88 256.538 1 0 -3 -8 4484.69 264.851 2 0 -3 -9 31951.9 876.765 2 0 3 -9 30059.1 843.481 6 0 -3 -9 31473.4 826.111 6 0 -3 9 31587.8 856.513 1 0 3 -10 17579.9 632.183 6 0 3 10 16999 655.228 1 0 -3 -10 16911.5 636.16 2 0 -3 10 18181.1 636.328 1 0 -3 -10 17723.3 607.834 6 0 3 11 18.5086 40.217 1 0 -3 -11 0.20068 34.9528 2 0 3 -11 47.4091 47.0931 6 0 -3 11 -16.6077 37.2937 1 0 -3 -11 27.3393 37.9707 6 0 -3 -12 13026.2 598.421 2 0 3 -12 11905.3 561.77 6 0 -3 12 12178 561.593 1 0 3 12 13132 613.712 1 0 -3 -12 12413.1 555.574 6 0 3 -13 2775.75 277.485 6 0 -3 13 3067.99 282.652 1 0 -3 -13 2783.44 269.184 6 0 -3 -13 3221.67 302.223 2 0 3 13 2901.37 289.688 1 0 3 -14 2678.18 287.577 6 0 3 14 2560.92 284.894 1 0 -3 14 2035.71 244.604 1 0 -3 -14 2039.71 243.195 6 0 4 0 79919.2 1342.62 1 0 4 0 79937.1 1308.83 4 0 4 0 80214.2 1314.13 3 0 -4 0 79704.7 1318.85 4 0 -4 0 79755.3 1341.83 1 0 -4 0 80402.5 1321.72 3 0 4 -1 12639.8 307.163 1 0 -4 1 11656.6 271.214 6 0 -4 -1 11251.6 277.983 3 0 -4 1 12227.3 288.977 3 0 -4 1 11696 296.835 1 0 4 1 10987.6 273.082 4 0 -4 1 11931 283.876 4 0 4 -1 12229.4 278.595 3 0 -4 -1 11792.5 280.128 4 0 4 -1 11652.9 271.746 4 0 -4 2 208945 3191.13 6 0 -4 -2 199300 3206.64 2 0 -4 2 195549 3228.79 1 0 4 2 203133 3202.51 4 0 -4 -2 206471 3197.44 4 0 4 -2 204922 3199.51 6 0 -4 2 200573 3202.94 3 0 4 -2 205175 3196.6 3 0 4 -2 202638 3238.82 1 0 -4 3 6929.88 237.698 1 0 -4 3 6522.35 219.38 6 0 4 3 6409.59 222.674 4 0 4 -3 6267.12 216.764 6 0 4 -3 6327.08 216.08 3 0 4 3 6306.4 218.989 2 0 -4 -3 6828.05 228.886 2 0 4 -3 6629.16 243.146 1 0 -4 -3 6755.1 220.918 4 0 4 4 99122.5 1751.6 2 0 -4 -4 97374.1 1752.85 2 0 4 4 100860 1755.6 4 0 4 -4 100931 1747.57 6 0 -4 4 100369 1775 1 0 -4 4 101987 1810.8 2 0 -4 4 103881 1744.74 6 0 -4 -4 101780 1736.54 4 0 4 -4 105913 1813.56 1 0 4 -4 102364 1743.16 3 0 4 -5 43361.3 948.961 1 0 -4 5 42763.2 911.882 1 0 4 -5 42970.8 882.959 3 0 4 5 44319.3 909.877 2 0 4 -5 41138.6 881.318 6 0 -4 -5 42538 902.077 2 0 4 -6 6696.11 286.86 6 0 -4 6 6971.23 299.353 1 0 4 6 7127.72 196.321 7 0 -4 -6 6026.75 279.946 2 0 -4 7 34309.5 847.914 1 0 -4 -7 34659.9 854.007 2 0 4 7 35410 647.819 7 0 4 -7 35167.6 849.333 6 0 4 -8 6946.12 199.629 7 0 -4 -8 6649.31 333.133 2 0 -4 8 6249.47 321.961 1 0 4 8 6613.48 184.951 7 0 4 -8 6901.31 334.798 6 0 -4 9 3690.84 254.924 1 0 -4 -9 3622.51 238.446 6 0 4 -9 3820.53 258.69 6 0 -4 -9 3832.32 263.019 2 0 -4 10 8931.2 433.591 1 0 -4 -10 9166.8 447.915 2 0 4 -10 9134.94 437.254 6 0 -4 -10 9353.21 420.241 6 0 -4 11 75.9058 49.6221 1 0 -4 -11 78.8598 51.0595 2 0 -4 -11 204.835 69.5963 6 0 4 11 221.792 86.6647 1 0 4 -11 181.687 71.9773 6 0 -4 -12 5274.42 371.559 2 0 -4 12 5214.62 358.773 1 0 -4 -12 5023.08 342.362 6 0 4 -12 4845.87 352.541 6 0 -4 13 989.954 166.594 1 0 -4 -13 905.201 165.461 2 0 4 -13 949.018 163.628 6 0 4 13 940.71 175.734 1 0 -4 -13 974.819 159.798 6 0 -4 14 5070.17 386.026 1 0 4 14 4502.47 384.297 1 0 -4 -14 4944.13 379.421 6 0 -4 -14 4719.49 387.126 2 0 4 -14 4443.73 378.11 6 0 5 0 -0.28191 9.07142 1 0 5 0 -1.32963 7.36334 3 0 -5 0 9.93424 12.1342 3 0 -5 0 -1.82026 9.35936 4 0 5 0 -0.44894 7.87079 4 0 5 -1 47488.4 865.071 4 0 -5 -1 49096.5 883.291 4 0 5 1 48261.2 876.91 4 0 -5 1 49891.9 889.923 4 0 -5 1 50100.9 869.863 6 0 -5 -1 48606.6 885.168 3 0 5 -1 49878 876.659 3 0 5 -1 47653 910.277 1 0 -5 1 50531.1 918.918 1 0 -5 1 48428.1 892.57 3 0 -5 2 1427.68 89.8758 6 0 5 -2 1502.4 93.6668 3 0 5 -2 1578.07 97.5926 6 0 -5 2 1721.15 103.995 3 0 -5 -2 1522.79 99.0559 2 0 5 -2 1618.48 108.791 1 0 5 2 1440.23 95.2751 4 0 5 -2 1554.65 94.1657 4 0 -5 -2 1381 91.563 4 0 -5 -2 1502.14 95.5045 3 0 -5 2 1651.89 107.653 1 0 5 -3 339099 5310.67 3 0 -5 -3 345648 5330.28 2 0 -5 3 336807 5352.08 1 0 5 -3 330008 5367.1 1 0 -5 -3 344619 5314.21 4 0 -5 3 337686 5325 3 0 -5 3 342001 5309.18 6 0 5 -3 341681 5319.02 6 0 5 3 346951 5327.1 4 0 5 -4 3296.42 188.722 1 0 -5 -4 3392.61 168.259 4 0 -5 4 3379.35 179.443 1 0 -5 4 3323.69 169.02 6 0 5 4 3341.44 175.598 4 0 -5 -4 3008.84 166.478 2 0 5 -4 3198.65 167.255 6 0 5 4 3243.5 169.93 2 0 5 -4 3426.31 169.927 3 0 5 5 1737.77 133.682 2 0 5 -5 1837.8 132.033 3 0 5 -5 1975.2 141.802 6 0 -5 -5 1871.43 139.203 2 0 5 5 1933.74 140.01 4 0 -5 5 1777.2 139.22 1 0 5 -6 23354.5 598.373 3 0 -5 6 22315.1 615.392 1 0 -5 -6 21916.7 602.728 2 0 5 -6 21133.6 590.176 6 0 5 -7 14933.2 479.17 3 0 5 -7 14343.1 481.057 6 0 -5 7 13751.1 482.641 1 0 -5 -7 13499.9 475.874 2 0 5 7 14044.1 341.557 7 0 5 -8 1209.9 84.472 7 0 5 8 1407.39 88.8583 7 0 -5 8 1324.11 146.371 1 0 5 -8 1152.58 134.093 6 0 -5 -8 1263.8 143.407 2 0 -5 9 4551.68 289.797 1 0 5 -9 4049.92 273.031 6 0 -5 -9 4243.88 257.764 6 0 -5 -9 4951.96 301.885 2 0 5 -9 4215.36 166.313 7 0 -5 -10 324.655 85.6537 2 0 -5 10 381.869 91.1804 1 0 5 -10 448.126 97.5282 6 0 -5 -10 404.611 85.806 6 0 -5 11 3731.16 289.155 1 0 5 -11 3504.01 283.582 6 0 -5 -11 3342.56 260.109 6 0 -5 -11 3299.76 276.025 2 0 -5 -12 4141.72 307.136 6 0 -5 12 4177.76 322.23 1 0 5 12 3133.14 304.143 1 0 5 -12 4179.87 329.002 6 0 -5 -12 4447.57 341.179 2 0 5 13 1000.69 178.009 1 0 -5 -13 1014.44 174.54 2 0 -5 -13 779.867 144.546 6 0 5 -13 780.861 149.987 6 0 -5 13 1143.82 177.699 1 0 -6 0 284951 4618.14 3 0 6 0 297934 4601.02 4 0 -6 0 292947 4614.82 4 0 6 0 286973 4658.58 1 0 6 1 27354.7 575.089 4 0 6 1 29398.8 622.442 1 0 -6 -1 26874.5 582.568 3 0 6 -1 28002.6 572.498 3 0 -6 -1 27830.2 588.584 4 0 -6 1 28352.7 565.837 6 0 6 -1 29927.3 623.543 1 0 -6 1 28115.5 613.383 1 0 6 -1 27760.1 568.02 4 0 -6 1 27133.9 591.578 3 0 -6 1 28320.8 593.532 4 0 -6 -2 17449.8 431.795 3 0 6 2 17482.8 432.34 4 0 -6 -2 17491.3 439.25 2 0 -6 2 17624.6 447.098 3 0 6 -2 17924.5 431.206 6 0 -6 2 17457.8 417.683 6 0 6 -2 18122.9 420.842 4 0 -6 2 18822.2 465.588 1 0 6 -2 19028.6 432.01 3 0 -6 -2 17992.9 435.959 4 0 6 -2 19017.4 472.051 1 0 6 -3 3019.68 159.548 6 0 6 3 3100.72 162.984 4 0 6 -3 2876.51 145.962 4 0 6 -3 3024.52 153.617 3 0 -6 -3 2798.2 152.06 4 0 -6 -3 2756.74 150.836 3 0 -6 3 2633.15 142.957 6 0 6 -3 2988.97 176.193 1 0 -6 3 3027.41 168.794 1 0 -6 3 3032.38 161.286 3 0 -6 -3 2673.6 151.867 2 0 -6 4 2939.35 163.738 6 0 -6 -4 2946.18 168.736 2 0 -6 4 3093.51 180.486 1 0 6 -4 3048.23 169.928 6 0 6 -4 3210.91 169.25 3 0 6 4 2910.54 168.501 4 0 -6 -5 99.886 36.1609 2 0 6 5 81.1725 34.2517 2 0 6 5 75.05 33.2336 4 0 -6 5 51.0135 29.1493 1 0 6 -5 97.7575 35.5939 6 0 6 -5 92.8885 32.5256 3 0 -6 6 5646.05 278.828 1 0 6 -6 5800.71 264.489 3 0 -6 -6 5506.85 269.132 2 0 6 -6 5184.53 259.702 6 0 -6 7 9334.42 388.276 1 0 6 -7 9223.6 381.041 6 0 -6 -7 9632.99 390.847 2 0 -6 -8 4081.57 261.904 2 0 6 8 4147.25 175.019 7 0 -6 8 4220.21 269.283 1 0 6 -8 4109.46 260.18 6 0 -6 9 912.583 132.283 1 0 -6 -9 1035.34 138.615 2 0 6 -9 716.807 116.549 6 0 6 9 791.951 72.6126 7 0 6 -9 756.887 73.8311 7 0 -6 10 2449.27 223.242 1 0 6 -10 2186.39 212.947 6 0 -6 -10 2001.63 202.73 2 0 -6 -10 2242.86 199.256 6 0 -6 -11 1985 214.096 2 0 -6 -11 1745.54 185.585 6 0 -6 11 2399.67 234.261 1 0 6 -11 1628.93 197.111 6 0 6 -12 4189.78 331.158 6 0 -6 -12 4759.21 329.465 6 0 -6 12 4193.17 327.253 1 0 -6 -12 4251.35 338.915 2 0 -6 -13 4051.68 325.738 6 0 6 -13 3597.35 325.498 6 0 -6 13 3471.43 308.299 1 0 6 13 3437.97 335.538 1 0 -6 -13 3588.33 323.558 2 0 -7 0 37.2974 22.625 4 0 -7 0 33.9108 23.1044 3 0 7 0 19.0451 23.7797 1 0 7 0 20.5158 17.6414 3 0 7 0 61.3666 23.715 4 0 7 1 4.55012 13.3975 1 0 7 -1 6.10032 13.7968 3 0 -7 1 62.4928 27.7583 3 0 -7 1 5.70149 14.7129 4 0 7 1 5.66407 13.4759 4 0 7 -1 8.99088 15.6114 1 0 -7 1 127.178 30.5504 6 0 -7 -1 51.6011 25.732 4 0 -7 1 43.391 23.1251 1 0 7 -1 13.0063 17.1028 4 0 -7 -1 5.51813 16.5266 3 0 7 2 10164.4 317.09 4 0 7 -2 10762.2 304.918 4 0 7 -2 10593.3 348.014 1 0 -7 -2 10590.2 323.875 3 0 7 -2 10737.7 308.296 3 0 -7 2 10596 331.387 3 0 -7 2 10106.2 339.689 1 0 -7 2 10072.5 297.373 6 0 -7 -2 10952.3 327.735 4 0 -7 3 42237.5 867.655 1 0 7 -3 41102.8 809.394 3 0 -7 3 37878.3 822.869 3 0 -7 3 38097.4 793.168 6 0 7 -3 37936.3 787.918 4 0 -7 -3 38868.5 823.282 2 0 7 -3 39914 819.433 6 0 7 3 39037 825.307 4 0 -7 -3 38244.1 810.355 3 0 -7 4 43898.8 899.171 3 0 7 -4 40238.8 844.716 4 0 7 -4 41131.3 885.614 6 0 -7 4 40984.8 866.792 6 0 7 -4 42145.6 865.459 3 0 7 4 40343.1 884.809 4 0 -7 4 43957.1 922.49 1 0 -7 -4 40856 874.894 3 0 -7 -4 40216.7 880.253 2 0 7 -5 15829.8 487.95 6 0 7 5 16251.3 499.758 4 0 7 -5 17725.7 492.253 3 0 -7 5 17317.1 524.172 1 0 -7 -5 18487 516.409 2 0 -7 6 14905.2 492.69 1 0 7 -6 15000.5 458.732 3 0 7 -6 14493.3 478.459 6 0 7 6 14310.1 480.09 4 0 -7 -6 13843.1 469.28 2 0 -7 7 24666.4 698.359 1 0 7 -7 24108.6 689.91 6 0 -7 -7 23492.3 680.521 2 0 -7 8 13270.4 503.334 1 0 7 8 12928 369.835 7 0 -7 -8 12257.2 483.295 2 0 7 -8 12561.4 493.247 6 0 7 -9 178.155 70.0385 6 0 -7 -9 239.76 74.9514 2 0 -7 9 120.057 53.3563 1 0 7 9 108.714 33.28 7 0 7 -9 74.7169 30.4843 7 0 -7 -10 33504.4 970.846 2 0 -7 -10 35334.8 928.702 6 0 -7 10 35112.3 986.169 1 0 7 -10 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426.949 2 2 -4 7 -8.35737 17.5439 1 -2 4 -7 14.827 42.4205 2 -2 -4 -7 1.81865 36.3531 2 2 -4 7 3.59136 40.4557 5 2 4 7 70.3402 54.165 5 2 -4 8 14819.5 570.19 5 2 4 8 14907.4 577.36 5 -2 4 -8 15162.8 621.609 2 2 -4 8 15174.9 423.327 1 -2 -4 -8 14992.3 647.242 2 -2 4 -9 400.399 106.698 2 2 -4 9 517.925 73.3234 1 -2 -4 -9 597.657 129.584 2 2 -4 9 413.924 98.3962 5 2 4 9 487.655 106.349 5 -2 4 -10 43.6163 55.7179 2 -2 -4 -10 107.774 69.2729 2 -2 4 -10 39.7033 36.4047 6 2 -4 10 92.9329 60.3808 5 2 4 10 23.1631 44.8728 5 -2 4 -11 12489.9 566.346 6 2 -4 11 12454.8 592.643 5 2 4 11 12264 593.73 5 -2 4 -11 11194.3 606.429 2 -2 -4 -11 11402.4 640.5 2 -2 4 -12 1331.7 216.083 2 -2 -4 -12 1240.45 214.172 2 2 -4 12 1578.08 217.472 5 2 4 12 1530.85 215.341 5 -2 4 -12 1445.96 199.682 6 2 5 -12 55.7066 64.7892 6 2 -5 -12 68.7869 50.5692 6 2 -5 -12 81.9975 63.2271 3 -2 -5 12 146.519 80.3752 1 2 -5 -11 8037.33 411.438 3 2 5 -11 7747.77 482.503 6 2 -5 -11 7749.02 431.996 6 -2 -5 11 7186.65 474.354 1 2 5 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49673.7 1171.32 7 -2 5 3 51159.7 1028.04 4 -2 -5 3 45494.8 766.626 4 -2 5 2 1730.21 97.8023 6 2 -5 -2 1771.59 165.984 3 -2 -5 2 1715.59 100.194 3 -2 -5 2 1662.42 136.469 1 2 5 -2 1146.76 147.589 7 -2 5 2 1607.89 140.713 4 2 5 -1 20004.7 557.985 1 2 5 -1 20943.2 674.888 7 -2 -5 1 19474.9 514.951 1 2 -5 -1 21059.1 634.415 3 2 -5 -1 20012.9 553.749 5 2 5 -1 19620.4 550.545 5 -2 5 1 20113.9 391.156 2 -2 5 1 20191.2 594.869 4 -2 5 0 124.041 44.452 4 2 5 0 80.7953 47.3698 7 2 5 0 163.911 42.3583 1 -2 5 0 98.0064 25.7295 2 2 -5 0 129.69 42.552 5 2 5 0 86.3933 37.6307 5 2 -5 0 128.542 51.625 3 2 -5 0 101.64 26.4291 2 -2 -5 0 103.96 32.9736 1 2 -5 1 26583.7 607.877 2 2 5 1 26633.1 796.613 7 -2 -5 -1 27083.3 744.564 2 2 -5 1 28141 796.234 3 2 -5 1 26745.1 688.912 5 2 5 1 27547.4 701.224 5 -2 5 -1 26386.6 595.255 2 -2 -5 -1 27212.8 557.255 1 -2 5 -1 27646 759.807 4 2 5 1 26351.4 597.977 1 2 -5 2 13530.3 417.558 2 -2 -5 -2 13807.4 501.704 2 2 -5 2 13247.9 521.814 3 2 -5 2 13172.6 449.837 5 2 5 2 13954.8 465.222 5 2 5 2 13457.3 532.259 7 -2 5 -2 13537 408.303 2 2 5 2 13441.3 340.718 1 -2 5 -3 14535.1 394.575 1 -2 -5 -3 14872.2 541.533 2 2 5 3 14256.1 552.553 7 2 -5 3 14585.7 485.654 5 2 5 3 14595.8 489.919 5 -2 5 -3 13635.3 447.481 2 2 5 3 13725.8 316.933 1 -2 -5 -4 12747.1 510.466 2 2 5 4 12132.3 501.286 7 -2 5 -4 11909.8 348.982 1 2 -5 4 11793.8 437.968 5 2 5 4 11658.1 438.906 5 2 5 4 10256.1 234.775 1 -2 5 -4 12038.7 433.745 2 -2 -5 -5 11149.2 492.398 2 2 5 5 10600 468.881 7 -2 5 -5 10720.4 348.401 1 2 -5 5 10892.8 433.45 5 2 5 5 10420.1 428.189 5 -2 5 -5 10765.5 437.888 2 2 5 6 540.204 102.053 7 -2 5 -6 411.7 89.6574 2 -2 -5 -6 347.328 90.0848 2 2 -5 6 452.564 88.4789 5 2 5 6 440.433 88.4654 5 -2 5 -6 454.78 70.4494 1 -2 -5 -7 17031.8 687.289 2 2 -5 7 18007.2 615.431 5 2 5 7 18170.8 622.294 5 -2 5 -7 18153 659.547 2 -2 5 -8 1065.08 156.665 2 -2 -5 -8 1217.05 179.549 2 2 5 8 1088.74 148.052 5 2 -5 8 1056.57 144.066 5 2 -5 8 1094.75 107.086 1 -2 5 -9 1626.88 178.117 6 2 -5 9 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347.659 1 -2 6 8 5234.28 287.599 4 2 6 -7 983.158 141.814 7 2 -6 -7 1114.96 118.264 6 -2 -6 7 913.4 142.875 1 2 -6 -7 999.945 131.553 3 -2 6 7 946.647 116.06 4 2 6 -6 8458.21 424.971 7 2 -6 -6 9800.01 416.703 3 -2 -6 6 8831.02 424.322 1 -2 6 6 9108.86 362.322 4 2 6 -5 9925.32 457.205 7 2 -6 -5 10405.2 430.665 3 -2 -6 5 10016.4 433.546 1 -2 6 5 10131.2 379.281 4 -2 6 4 212.984 56.1027 4 2 6 -4 156.175 58.7924 7 -2 -6 4 110.997 45.1812 1 -2 6 4 191.181 33.7748 6 2 -6 -4 174.835 58.6453 3 2 6 -3 1665.43 177.855 7 2 -6 -3 1755.55 169.803 3 -2 6 3 1715.83 90.5498 6 -2 -6 3 1655.63 148.716 1 -2 6 3 1539.18 139.029 4 2 6 -2 63866.6 1440.09 7 -2 -6 2 67611.7 1297.72 1 -2 6 2 63756.1 1083.69 6 2 -6 -2 66532.5 1411.3 3 -2 -6 2 65086.1 1130.78 3 -2 -6 2 64009.4 1076.21 4 -2 6 2 64729.7 1315.21 4 -2 6 1 326.956 70.5998 4 2 6 -1 225.058 69.652 7 -2 6 1 393.738 41.0296 6 2 -6 -1 408.005 69.7439 5 2 6 -1 413.458 71.0904 5 2 -6 -1 447.839 86.5936 3 2 6 -1 273.857 59.946 1 -2 -6 1 341.573 59.1907 1 -2 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17574.8 562.112 5 -2 6 -4 16682.2 540.631 2 2 6 5 23.927 30.8767 7 -2 6 -5 2.46755 30.8211 2 -2 -6 -5 49.9053 47.34 2 2 -6 5 -5.82477 23.3773 5 2 6 5 67.187 40.6017 5 -2 -6 -6 8011.27 437.428 2 2 6 6 8439.93 424.444 7 2 -6 6 8771.6 397.363 5 2 6 6 8055.97 385.79 5 -2 6 -6 7536.68 387.212 2 -2 -6 -7 1506.56 193.39 2 2 6 7 1475.99 173.757 7 2 -6 7 1324.31 154.947 5 2 6 7 1341.35 158.321 5 -2 6 -7 1270.72 164.064 2 2 -6 8 491.932 77.3132 1 -2 6 -8 323.416 89.8686 2 -2 6 -8 330.963 78.685 6 -2 -6 -8 426.98 111.471 2 2 -6 8 432.732 96.6414 5 2 6 8 359.632 88.4879 5 -2 6 -9 103.57 62.8065 2 2 -6 9 36.9659 34.0319 1 -2 6 -9 36.9568 49.3543 6 -2 -6 -9 58.1452 46.697 2 2 -6 9 42.995 43.5532 5 2 6 9 60.9485 45.1048 5 -2 -6 -10 1202.18 198.111 2 -2 6 -10 877.664 141.086 6 2 -6 10 884.441 146.463 5 2 6 10 1006.57 159.675 5 -2 -6 -11 836.271 171.682 2 -2 6 -11 819.523 143.326 6 2 -6 11 1166.69 178.677 5 2 6 11 1350.06 192.784 5 -2 -7 12 1748.12 243.834 1 2 -7 -12 1486.44 192.562 6 2 -7 -12 1305.53 185.072 3 2 -7 -11 7339.04 417.022 3 2 -7 -11 7692.09 416.521 6 -2 -7 11 7205.99 479.873 1 -2 7 11 7206.5 410.523 4 -2 7 10 655.595 118.118 4 -2 -7 10 491.998 123.203 1 2 -7 -10 604.88 107.401 6 2 -7 -10 570.469 115.005 3 -2 7 9 118.149 51.3541 4 2 7 -9 118.872 63.3298 7 -2 -7 9 287.615 89.9118 1 2 -7 -9 230.193 65.9347 6 2 -7 -9 153.397 64.6389 3 2 7 -8 6014.81 365.078 7 2 -7 -8 6154.05 349.176 3 2 -7 -8 5668.36 291.626 6 -2 -7 8 5386.9 362.325 1 -2 7 8 5521.64 308.196 4 2 7 -7 23738.3 771.929 7 2 -7 -7 21599.3 594.838 6 -2 -7 7 21081.4 740.375 1 2 -7 -7 23292 718.964 3 -2 7 7 22381.6 658.891 4 2 7 -6 16818.8 624.261 7 2 -7 -6 16339.5 582.852 3 -2 -7 6 15673.7 598.979 1 -2 7 6 16754.6 532.796 4 2 7 -5 1343.83 164.088 7 2 -7 -5 1348.54 154.613 3 -2 -7 5 1320.8 151.412 1 -2 7 5 1540.45 144.577 4 2 7 -4 3875.09 281.412 7 2 -7 -4 3977.92 263.905 3 -2 -7 4 3743.81 246.916 1 -2 7 4 3502.24 219.043 4 2 7 -3 880.611 136.178 7 -2 -7 3 1022.32 118.744 1 2 -7 -3 827.305 122.898 3 -2 7 3 964.26 114.959 4 2 7 -2 29121.5 871.108 7 -2 -7 2 29465.8 727.828 1 2 -7 -2 29544.8 838.872 3 -2 -7 2 29442 549.375 4 -2 7 2 30402.5 778.011 4 -2 -7 1 25317.3 623.043 1 -2 7 1 22767 423.656 6 2 -7 -1 25734.2 753.624 3 2 7 -1 24953.2 780.265 7 2 -7 -1 24635 632.151 5 2 7 -1 25240.6 635.856 5 -2 -7 1 24388.8 509.053 4 -2 7 1 25673.4 704.803 4 -2 -7 0 421.087 56.7991 4 2 7 0 334.807 63.9715 1 -2 7 0 280.407 69.0128 4 2 -7 0 360.345 45.9383 2 2 7 0 295.747 78.852 7 -2 -7 0 305.422 55.149 1 2 -7 0 328.03 64.0456 5 2 7 0 306.164 62.6063 5 2 -7 0 364.298 86.6173 3 2 -7 1 7364.75 264.875 2 2 7 1 7495.98 397.846 7 2 -7 1 8027 403.871 3 2 -7 1 7258.92 313.532 5 2 7 1 7759.51 325.572 5 2 7 1 8071.61 297.023 1 -2 -7 -1 7723.79 267.864 1 -2 7 -1 8603.39 393.556 4 2 -7 2 2800.06 173.228 2 2 7 2 2662.76 232.354 7 -2 -7 -2 2679.42 221.306 2 2 -7 2 2903.56 243.648 3 2 -7 2 2394.65 177.512 5 2 7 2 2916.51 198.72 5 2 7 2 2493.59 146.927 1 -2 7 -2 2627 220.789 4 2 7 3 3009.2 244.485 7 -2 -7 -3 2909.52 234.647 2 2 7 3 2892.82 148.056 1 2 -7 3 2774.26 242.982 3 2 -7 3 3063.83 205.643 5 2 7 3 3008.58 206.872 5 2 7 4 174.391 35.7411 1 2 7 4 252.81 77.0463 7 -2 7 -4 132.611 47.1493 2 -2 -7 -4 273.123 79.3976 2 2 -7 4 193.83 60.4363 5 2 7 4 141.277 50.7116 5 -2 -7 -5 4578.25 319.977 2 2 7 5 4736.63 317.605 7 2 7 5 4405.7 167.988 1 2 -7 5 4752.11 278.251 5 2 7 5 4737.63 279.83 5 -2 7 -5 4318.53 271.496 2 -2 -7 -6 1748.52 204.076 2 2 7 6 1492.85 179.735 7 -2 7 -6 1711.45 148.598 6 2 -7 6 1919.35 181.256 5 2 7 6 1589.89 168.585 5 -2 7 -6 1749.63 181.431 2 2 7 7 69.7307 51.8202 7 -2 7 -7 127.02 52.9159 6 -2 -7 -7 66.2514 43.3198 2 2 -7 7 195.809 65.3655 5 -2 -7 -8 18633.1 759.449 2 2 7 8 17203.3 660.351 7 -2 7 -8 16951.6 589.896 6 2 -7 8 17550 636.654 5 2 7 8 18760.8 660.623 5 2 -7 9 102.536 49.1296 1 -2 7 -9 76.7857 52.6042 6 -2 -7 -9 71.7035 59.85 2 2 -7 9 40.4783 42.8219 5 2 7 9 7.76015 33.8252 5 -2 7 -10 207.524 73.7906 6 -2 -7 -10 152.812 79.4408 2 2 -7 10 207.362 77.7507 5 2 7 10 179.949 82.7317 5 -2 7 -11 1631.52 201.135 6 -2 -7 -11 1552.92 235.277 2 2 -7 11 1605.86 205.065 5 2 7 11 1840.35 228.157 5 -2 -8 12 916.353 179.809 1 -2 -8 11 1126.13 195.876 1 2 -8 -11 1113.67 167.597 3 -2 8 11 1227.83 172.964 4 -2 8 10 89.8181 62.3975 4 -2 -8 10 48.134 58.8815 1 2 -8 -10 18.4458 38.989 6 2 -8 -10 58.4464 46.4901 3 -2 8 9 1185.41 149.721 4 2 8 -9 810.017 143.953 7 -2 -8 9 908.904 158.86 1 2 -8 -9 1110.5 135.308 6 2 -8 -9 1019.98 150.627 3 2 8 -8 7636.75 425.193 7 2 -8 -8 7582.2 405.549 3 2 -8 -8 7444.05 329.098 6 -2 -8 8 7672.85 440.841 1 -2 8 8 7998.39 388.004 4 2 8 -7 1367.13 174.063 7 2 -8 -7 1943.68 195.807 3 2 -8 -7 1501.26 129.203 6 -2 -8 7 1596.37 189.909 1 -2 8 7 1431.03 153.273 4 -2 8 6 29.1962 33.1043 4 -2 -8 6 109.938 79.2636 1 2 8 -6 -0.76339 30.1052 7 2 -8 -6 86.5702 58.5938 3 2 8 -5 1863.25 202.943 7 2 -8 -5 2442.87 215.411 3 -2 -8 5 2144.76 198.155 1 -2 8 5 2216.37 180.328 4 2 8 -4 20113.9 712.941 7 -2 -8 4 19033.7 619.278 1 2 -8 -4 21611.4 692.101 3 -2 8 4 20466.3 609.394 4 2 8 -3 2132.64 212.385 7 -2 -8 3 1781.79 160.276 1 2 -8 -3 1823.9 185.483 3 -2 8 3 2030.78 172.087 4 2 8 -2 11803.5 518.472 7 -2 -8 2 11284.9 413.227 1 -2 -8 2 11506 273.25 3 2 -8 -2 12542.7 511.314 3 -2 8 2 11541.6 441.375 4 -2 -8 1 29722.6 717.835 1 2 8 -1 29770 893.092 7 2 -8 -1 31150.4 890.472 3 2 8 -1 29595 730.491 5 -2 -8 1 29194.3 596.686 4 -2 8 1 29421.7 796.722 4 -2 -8 0 61.8311 22.1821 4 -2 8 0 33.0528 33.6494 4 2 8 0 53.6938 42.1883 7 -2 -8 0 75.0885 30.2854 1 2 -8 0 50.3341 19.5426 2 2 -8 0 74.589 31.4005 5 2 8 0 39.9915 25.9694 5 2 -8 0 28.9364 31.2232 3 2 -8 1 7305.45 265.297 2 -2 8 -1 7130.52 192.258 6 2 -8 1 7740.37 407.065 3 2 -8 1 7432.19 312.259 5 2 8 1 7470.18 318.839 5 2 8 1 6730.23 287.976 1 2 8 1 8265.47 424.041 7 -2 -8 -1 7333.82 277.158 1 -2 8 -1 7640.99 381.093 4 2 -8 2 17113.6 500.223 2 2 8 2 19284.2 682.146 7 -2 -8 -2 17261.5 620.376 2 -2 8 -2 17582.3 402.399 6 2 -8 2 19460.4 688.531 3 2 8 2 16954.4 477.428 1 2 -8 2 17349.2 536.84 5 2 8 2 17697.1 545.991 5 -2 8 -2 18921.4 641.144 4 -2 8 -3 578.101 106.651 4 2 8 3 631.801 119.591 7 2 8 3 721.836 80.2356 1 -2 8 -3 751.433 74.8232 6 2 -8 3 833.786 108.377 5 2 8 3 909.193 113.604 5 -2 -8 -3 690.878 118.513 2 2 -8 3 621.755 119.423 3 2 8 4 32.933 22.4727 1 2 8 4 65.2639 51.3365 7 -2 8 -4 14.8728 17.9473 6 -2 -8 -4 40.1321 38.2562 2 2 -8 4 59.0304 35.071 5 2 8 4 96.4215 47.5431 5 2 8 5 966.393 83.7947 1 2 8 5 844.35 133.721 7 -2 8 -5 1073.3 109.097 6 2 -8 5 1135.53 136.698 5 2 8 5 948.532 126.23 5 -2 -8 -5 894.283 146.237 2 -2 -8 -6 7818.07 444.004 2 2 8 6 6962.29 402.689 7 -2 8 -6 7178.01 318.662 6 2 -8 6 7291.5 365.814 5 2 8 6 7291.72 370.183 5 -2 -8 -7 5212.81 373.322 2 2 8 7 5078.69 345.936 7 -2 8 -7 4889.39 278.051 6 2 -8 7 5013.74 312.838 5 2 8 7 4912.51 312.269 5 -2 -8 -8 5644.3 408.452 2 2 8 8 5056.72 346.091 7 -2 8 -8 5291.74 307.845 6 2 -8 8 5081.42 325.798 5 2 8 8 5586.62 346.53 5 2 8 9 1508.61 186.743 7 -2 8 -9 1609.13 180.159 6 -2 -8 -9 1366.82 204.781 2 2 -8 9 1310.44 170.319 5 2 8 9 1569.19 191.783 5 2 -8 9 1237.88 138.422 1 -2 8 -10 426.784 100.462 6 -2 -8 -10 334.139 115.195 2 2 -8 10 356.618 98.2949 5 2 8 10 331.174 92.4932 5 -2 8 -11 10408 529.732 6 2 -8 11 11573.1 569.122 5 2 8 11 11397.1 576.47 5 -2 -8 -11 11608.5 665.668 2 -2 -9 11 322.45 105.836 1 2 -9 -11 287.52 97.173 3 -2 9 11 376.03 103.18 4 2 -9 -10 3172.21 279.914 3 -2 -9 10 3102.01 303.392 1 -2 9 10 2818.16 253.716 4 -2 -9 9 1026.52 170.392 1 2 9 -9 1108.49 168.384 7 2 -9 -9 1043.1 159.263 3 -2 9 9 1421.59 171.411 4 2 9 -8 7339.87 427.572 7 2 -9 -8 8827.69 448.304 3 2 -9 -8 7617.78 324.507 6 -2 -9 8 8005.04 457.451 1 -2 9 8 7791.97 394.522 4 2 9 -7 6753.62 406.162 7 2 -9 -7 7223.56 397.982 3 2 -9 -7 6169.4 262.269 6 -2 -9 7 6507.38 390.364 1 -2 9 7 6709.92 349.975 4 2 9 -6 2648.91 252.164 7 -2 -9 6 2932.58 245.125 1 2 -9 -6 2962.96 247.909 3 -2 9 6 2598.78 208.665 4 2 9 -5 3554.3 288.381 7 -2 -9 5 3577.84 256.869 1 2 -9 -5 3742.4 279.736 3 -2 9 5 4029.86 253.701 4 2 9 -4 5962.75 370.642 7 -2 -9 4 5230.5 300.751 1 2 -9 -4 6297.55 360.742 3 -2 9 4 5547.89 298.744 4 -2 -9 3 11754.6 451.276 1 2 9 -3 12047 537.931 7 2 -9 -3 12513.2 526.993 3 -2 9 3 11480 450.972 4 -2 -9 2 2775.53 196.726 1 2 9 -2 2580.57 238.14 7 -2 -9 2 2504.48 113.881 3 2 -9 -2 2721.51 238.72 3 -2 9 2 2555.47 202.561 4 -2 -9 1 215.059 38.3438 4 -2 9 1 352.707 81.0415 4 2 9 -1 315.174 88.6386 7 -2 -9 1 306.846 64.5671 1 2 -9 -1 255.216 75.9467 3 -2 9 0 807.635 120.385 4 2 9 0 791.781 132.889 7 2 -9 0 708.806 91.6028 5 2 9 0 781.398 96.3557 5 2 -9 0 731.746 122.402 3 -2 -9 0 803.259 80.1545 4 -2 -9 0 844.731 99.9341 1 -2 9 -1 18.426 34.2468 4 2 9 1 1.14007 30.2379 7 -2 -9 -1 28.2596 26.3636 1 -2 9 -1 14.3806 9.10017 6 2 -9 1 -16.4914 19.0817 5 2 9 1 11.7632 28.869 5 2 -9 1 -0.28252 32.8652 3 2 9 2 18312.6 678.337 7 -2 -9 -2 17453.4 635.785 2 -2 9 -2 16857 386.771 6 2 9 2 16751.3 499.355 1 2 -9 2 17002.9 660.46 3 2 -9 2 17018.4 528.129 5 2 9 2 18304.7 550.22 5 -2 9 -2 18821.3 654.002 4 2 -9 2 16821.6 499.548 2 -2 -9 -3 38776.1 1051.8 2 2 9 3 35274.3 821.119 1 -2 9 -3 37889.8 766.126 6 2 -9 3 41062.8 1125.94 3 2 -9 3 37488.8 909.524 5 2 9 3 39161.3 929.98 5 2 9 3 38404.5 1073.65 7 -2 9 -3 40005.3 1061.52 4 -2 -9 -4 2851.9 253.961 2 2 9 4 2536.12 157.306 1 -2 9 -4 2618.39 159.259 6 2 -9 4 2803.69 206.535 5 2 9 4 2787.35 208.683 5 2 9 4 2702.41 247.515 7 -2 9 -4 2009.38 211.176 4 -2 -9 -5 2751.95 259.809 2 2 9 5 3395.47 279.93 7 -2 9 -5 3025.72 188.188 6 2 -9 5 2993.9 224.491 5 2 9 5 2678.72 214.001 5 -2 -9 -6 5766.84 388.911 2 -2 9 -6 5699.15 285.937 6 2 -9 6 6280.43 337.687 5 2 9 6 5929.95 332.799 5 2 9 6 6414.87 386.161 7 -2 -9 -7 12948.3 624.665 2 2 9 7 13823.3 602.712 7 -2 9 -7 13833.8 499.022 6 2 -9 7 13880 552.833 5 2 9 7 15464.3 582.686 5 2 9 8 58.9847 38.038 7 -2 9 -8 152.32 54.8313 6 -2 -9 -8 108.126 64.0641 2 2 -9 8 110.284 58.0918 5 2 9 8 174.104 66.7644 5 2 9 9 3484.93 290.201 7 -2 9 -9 3410.85 261.832 6 2 -9 9 3193.68 269.812 5 2 9 9 3380.84 280.215 5 2 -9 9 3172.58 234.97 1 -2 -9 -9 3011.82 310.98 2 -2 9 -10 2283.3 227.97 6 2 -9 10 2539.48 249.767 5 2 9 10 2415.95 247.468 5 -2 -9 -10 2537.33 296.659 2 -2 -10 11 349.478 115.857 1 2 -10 -11 268.151 91.8628 3 -2 10 11 113.577 66.1601 4 2 -10 -10 6347.07 415.149 3 -2 -10 10 6815.86 455.053 1 -2 10 10 7550.15 431.271 4 2 10 -9 16141.4 676.281 7 2 -10 -9 16245.6 673.881 3 -2 -10 9 16302.4 703.569 1 -2 10 9 17161.4 649.884 4 -2 10 8 306.115 90.7926 4 2 10 -8 181.114 77.5305 7 2 -10 -8 175.503 78.1481 3 -2 -10 8 167.37 71.818 1 2 10 -7 5504.37 377.445 7 -2 -10 7 5133.16 345.617 1 2 -10 -7 5548.82 360.912 3 -2 10 7 4797.89 304.12 4 -2 10 6 301.989 80.4956 4 2 10 -6 223.414 88.4562 7 2 -10 -6 376.114 99.5003 3 -2 -10 6 270.98 85.5568 1 -2 -10 5 1591.23 174.142 1 2 -10 -5 1531.31 185.063 3 2 10 -5 1710.08 203.595 7 -2 10 5 1557.59 163.167 4 -2 -10 4 1480.31 162.752 1 2 10 -4 1572.56 194.102 7 2 -10 -4 1731.48 195.753 3 -2 10 4 1738.87 170.849 4 -2 -10 3 4510.15 272.371 1 2 10 -3 4324.65 320.083 7 2 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36895.4 1082.35 3 2 -10 3 36677.6 886.36 5 2 10 3 36875.5 896.023 5 -2 10 -3 38283.8 1042.18 4 2 10 4 26536.5 885.673 7 -2 -10 -4 27796.1 893.438 2 -2 10 -4 27430.2 645.408 6 2 -10 4 28153.8 930.226 3 2 -10 4 28215.5 761.463 5 2 10 4 27759.7 762.087 5 -2 10 -4 28519.8 894.119 4 -2 10 -5 495.228 111.92 4 2 10 5 451.718 108.229 7 -2 10 -5 471.834 76.1044 6 -2 -10 -5 594.289 124.274 2 2 -10 5 506.51 94.5548 5 2 10 5 366.373 83.7667 5 2 10 6 140 73.0277 7 -2 10 -6 4.52647 20.5539 6 -2 -10 -6 6.38612 41.502 2 2 -10 6 58.4418 38.0531 5 2 10 6 106.738 52.4835 5 2 10 7 -1.06765 40.2154 7 -2 10 -7 47.4879 32.7003 6 -2 -10 -7 117.768 71.6956 2 2 -10 7 53.5695 38.5775 5 2 10 7 99.8301 55.8987 5 2 10 8 109.802 60.9977 7 -2 10 -8 157.091 59.9191 6 -2 -10 -8 282.028 102.512 2 2 -10 8 173.17 69.1652 5 2 10 8 243.934 78.517 5 2 10 9 96.19 63.3393 7 -2 10 -9 116.323 59.6433 6 -2 -10 -9 207.201 97.6772 2 2 -10 9 240.86 82.9089 5 2 10 9 57.4275 52.1062 5 -2 10 -10 357.346 93.7596 6 -2 -10 -10 207.791 94.4232 2 2 -10 10 371.235 100.247 5 2 10 10 383.859 108.843 5 -2 11 10 1203.59 176.698 4 2 -11 -10 1485.77 204.352 3 -2 -11 10 1306.52 199.263 1 2 11 -9 16766.4 712.647 7 -2 -11 9 17329.2 729.846 1 2 -11 -9 18197.8 729.952 3 -2 11 9 16864.9 667.871 4 -2 -11 8 1462.9 194.3 1 2 11 -8 1355 193.65 7 2 -11 -8 1203.6 180.416 3 -2 11 8 1585.95 185.807 4 2 11 -7 2085.85 239.602 7 -2 -11 7 1678.46 201.678 1 2 -11 -7 1622.29 203.71 3 -2 11 7 1963.65 198.41 4 2 11 -6 17586.5 717.44 7 2 -11 -6 17064.1 684.879 3 -2 -11 6 17219.9 657.84 1 -2 11 6 17416.9 623.001 4 -2 -11 5 4695.48 313.851 1 2 11 -5 4981.41 360.642 7 2 -11 -5 4830.16 346.989 3 -2 11 5 4621.54 295.119 4 -2 -11 4 4226.76 283.133 1 2 11 -4 4145.42 322.783 7 2 -11 -4 4476.01 323.308 3 -2 11 4 4035.73 272.648 4 -2 11 3 383.224 86.7485 4 2 11 -3 620.233 123.852 7 2 -11 -3 417.12 101.417 3 -2 -11 3 512.153 95.4774 1 2 11 -2 3154.94 277.239 7 2 -11 -2 3494.6 291.01 3 -2 -11 2 3632.01 162.361 3 -2 11 2 3429.88 253.62 4 -2 -11 2 3720.05 246.705 1 -2 11 1 944.639 131.436 4 -2 -11 1 715.702 77.576 3 2 11 -1 917.544 148.547 7 -2 -11 1 662.514 100.788 1 2 -11 -1 1093.48 162.07 3 -2 -11 0 20529.1 532.171 3 2 11 0 21460.9 772.115 7 2 -11 0 22038.3 772.08 3 2 11 0 20789.5 574.235 5 -2 -11 0 20459.3 612.71 1 -2 11 0 20961.8 692.966 4 2 11 1 58215.7 1430.08 7 2 -11 1 58823.8 1446.07 3 2 -11 1 56757.1 1163.86 5 2 11 1 55428.3 1164.8 5 -2 11 -1 58506.3 1348.17 4 -2 11 -2 233.518 79.093 4 2 11 2 287.452 89.5557 7 2 -11 2 313.901 65.4873 5 2 11 2 229.701 54.8493 5 2 -11 2 271.133 92.052 3 -2 -11 -2 171.325 67.5977 2 2 11 3 20079.3 753.728 7 -2 -11 -3 19042.8 718.259 2 -2 11 -3 19697.1 464.589 6 2 -11 3 21382.7 790.927 3 2 -11 3 18836.9 584.539 5 2 11 3 19793.7 602.898 5 -2 11 -3 21046 735.579 4 2 11 4 3990.88 320.425 7 -2 -11 -4 3504.61 296.314 2 -2 11 -4 4121.46 200.494 6 2 -11 4 4641.51 354.862 3 2 -11 4 4078.33 253.818 5 2 11 4 4067.94 256.008 5 -2 11 -4 3599.43 295.034 4 -2 11 -5 1246.7 176.467 4 -2 -11 -5 1561.88 204.027 2 2 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333.997 2 4 0 0 5167.64 374.371 5 -4 0 -1 64.8938 50.7375 2 4 0 1 23.2861 52.9943 5 -4 0 -2 695.894 136.096 2 4 0 2 575.361 129.684 5 -4 0 -3 41.7758 55.5288 2 4 0 3 118.025 77.478 5 4 0 4 11574.8 607.08 5 -4 0 -4 11198.5 574.425 2 -4 0 -5 38.9074 57.6344 2 4 0 5 18.1187 60.5992 5 4 0 6 1646.97 231.99 5 -4 0 -6 1914.41 249.865 2 -4 0 -7 52.6612 69.3573 2 -4 1 8 20.3473 49.8776 1 -4 -1 8 88.3575 68.6699 1 -4 1 7 672.299 166.261 1 -4 -1 7 694.487 157.594 1 -4 1 6 2487.81 281.915 1 -4 -1 6 3418.79 328.037 1 -4 1 5 7366.44 471.634 1 -4 -1 5 7167.37 453.683 1 -4 1 4 3855.92 318.856 1 -4 -1 4 4578.42 343.909 1 -4 1 4 3997.76 256.268 4 -4 1 3 21.5877 30.6446 4 -4 -1 3 8.23207 36.1962 1 -4 -1 3 -7.49604 31.9863 2 -4 1 3 11.2741 34.9762 1 -4 1 2 513.833 104.989 4 -4 -1 2 311.179 77.1895 4 -4 1 2 348.659 95.494 1 -4 -1 2 316.656 84.2256 2 -4 1 1 32.9008 45.857 4 -4 -1 1 160.274 67.2547 4 -4 1 1 122.506 56.6364 2 4 -1 -1 96.578 61.5118 5 4 1 -1 88.081 56.0127 5 -4 -1 1 88.7278 51.1276 2 -4 1 0 705.453 131.966 4 -4 1 0 867.068 131.496 2 -4 -1 0 1192.3 165.252 2 4 -1 0 1070.83 173.695 5 4 1 0 887.122 155.482 5 -4 1 -1 130.512 59.9377 2 -4 -1 -1 49.6363 40.7595 2 4 -1 1 98.0909 58.9629 5 4 1 1 33.4247 36.7636 5 -4 1 -2 661.937 128.056 2 -4 -1 -2 478.681 111.062 2 4 -1 2 376.032 108.772 5 4 1 2 418.324 112.131 5 -4 -1 -3 4132.41 334.212 2 4 -1 3 3846.01 332.808 5 4 1 3 3326.09 310.612 5 -4 1 -3 3677.43 305.225 2 -4 -1 -4 14991.2 681.069 2 4 -1 4 14471.2 682.615 5 4 1 4 13885.1 672.057 5 -4 1 -4 14208.2 645.376 2 -4 1 -5 706.201 149.964 2 -4 -1 -5 532.232 132.001 2 4 -1 5 462.736 126.863 5 4 1 5 609.921 145.721 5 -4 1 -6 10.2082 50.6087 2 -4 -1 -6 66.2476 65.1413 2 4 -1 6 -15.0596 52.0382 5 4 1 6 52.2645 67.1424 5 -4 -2 8 493.723 136.749 1 -4 2 8 428.154 136.497 1 -4 2 7 4192.06 387.006 1 -4 -2 7 4325.86 378.754 1 -4 2 6 2099.23 261.357 1 -4 -2 6 1886.46 241.666 1 -4 2 5 2965.36 300.273 1 -4 -2 5 3108.96 291.61 1 -4 -2 4 38.3251 51.2007 1 -4 2 4 6.35752 42.6932 1 -4 2 4 58.1846 46.187 4 -4 -2 4 -15.169 33.4979 2 -4 2 3 1384.85 189.333 1 -4 -2 3 1786.66 191.838 2 -4 -2 3 1663.03 189.777 1 -4 2 3 1789.73 184.812 4 -4 2 2 970.151 144.593 4 -4 -2 2 952.227 130.145 4 -4 2 2 634.275 125.374 1 -4 -2 2 1034.27 151.342 2 -4 2 1 85.2281 60.9603 4 -4 -2 1 13.4435 36.0402 4 4 -2 -1 1.32989 46.8312 5 4 2 -1 63.6312 57.4808 5 -4 -2 1 -24.9865 48.2462 2 -4 2 0 1383.91 161.486 2 4 -2 0 1573.77 205.27 5 -4 -2 0 1188.92 165.423 2 4 2 0 1076.99 170.579 5 -4 2 0 1586.04 197.979 4 -4 -2 -1 2757.84 261.406 2 4 -2 1 2419.9 259.405 5 4 2 1 3247.24 300.392 5 -4 2 -1 2995.64 246.588 2 -4 -2 -2 1986.19 230.424 2 4 -2 2 2145.71 243.905 5 4 2 2 2516.74 264.094 5 -4 2 -2 2525.28 234.59 2 -4 2 -3 585.199 120.86 2 -4 -2 -3 527.656 126.497 2 4 -2 3 632.837 136.659 5 4 2 3 444.665 119.046 5 -4 2 -4 522.321 122.378 2 -4 -2 -4 515.512 134.349 2 4 -2 4 493.431 132.803 5 4 2 4 407.269 121.928 5 4 -2 5 20517 846.404 5 4 2 5 21240.9 862.163 5 -4 2 -5 21225.8 818.871 2 -4 -2 -5 20985.8 862.653 2 4 -2 6 4196.64 371.715 5 4 2 6 4243.24 374.24 5 -4 2 -6 4482.55 370.053 2 -4 -2 -6 4454.72 388.04 2 -4 3 8 450.745 136.509 1 -4 -3 8 575.438 148.884 1 -4 3 7 290.489 112.156 1 -4 -3 7 170.748 81.3311 1 -4 3 6 24.7763 53.4883 1 -4 -3 6 94.7736 68.8045 1 4 -3 -5 3670.33 300.687 3 -4 -3 5 3193.99 296.027 1 -4 3 5 4319.1 274.87 4 -4 -3 4 1336.96 173.55 2 4 -3 -4 1867.32 217.101 3 -4 -3 4 1525.38 191.476 1 -4 3 4 1666.42 175.511 4 -4 -3 3 1862.53 202.035 2 -4 -3 3 1913.05 199.549 1 -4 3 3 1683.51 184.978 4 -4 3 2 174.3 66.5326 4 -4 -3 2 264.71 85.4409 2 -4 3 1 293.848 93.0882 4 4 -3 -1 159.754 67.8124 5 4 3 -1 174.108 81.3049 5 -4 -3 1 86.9424 60.4665 2 -4 3 0 55.7477 48.7368 4 4 -3 0 53.279 55.7541 5 4 3 0 139 70.7459 5 -4 -3 0 116.389 63.6251 2 -4 -3 -1 1812.43 215.837 2 -4 3 -1 1431.94 196.378 4 4 -3 1 1770.18 224.308 5 4 3 1 1578.73 211.396 5 -4 3 -2 40.2343 49.5366 2 -4 -3 -2 17.9022 48.4465 2 4 -3 2 27.4935 39.2647 5 4 3 2 15.0214 40.1108 5 -4 -3 -3 1723.16 223.247 2 4 3 3 1532.01 210.424 5 4 -3 3 1529.14 209.705 5 -4 3 -3 1736.81 200.708 2 -4 3 -4 17.7976 36.075 2 -4 -3 -4 67.1246 73.7166 2 4 -3 4 30.8705 57.9439 5 4 3 4 56.6467 55.9025 5 -4 3 -5 0.59046 45.4074 2 -4 -3 -5 86.9996 75.2856 2 4 -3 5 13.9891 48.6263 5 4 3 5 51.303 63.7708 5 -4 3 -6 671.058 141.224 2 -4 -3 -6 659.32 152.081 2 4 -3 6 718.875 158.567 5 4 3 6 738.138 159.182 5 -4 -4 7 -13.0913 53.1903 1 4 -4 -6 3325.4 296.249 3 -4 -4 6 3511.83 321.795 1 -4 4 5 82.0233 56.1129 4 -4 -4 5 66.9381 59.4504 1 4 -4 -5 105.833 70.0247 3 -4 4 4 541.235 107.052 4 -4 -4 4 687.002 129.092 1 4 -4 -4 739.327 147.937 3 -4 4 3 72.6687 51.9357 4 -4 -4 3 44.6077 37.71 1 -4 -4 3 37.6054 39.8829 2 4 -4 -3 64.3093 53.8772 3 -4 4 2 74.8103 54.3445 4 -4 -4 2 38.9999 48.756 2 -4 -4 1 12867.9 589.414 2 4 -4 -1 12856.1 600.095 5 4 4 -1 13237 614.286 5 -4 4 1 14056.1 615.53 4 -4 4 0 42.7889 53.7661 4 4 -4 0 0.79073 38.3695 5 4 4 0 2.76595 40.641 5 -4 -4 0 67.2246 50.966 2 -4 -4 -1 1615.26 209.685 2 4 -4 1 1517.39 207.521 5 4 4 1 1504.79 207.412 5 -4 4 -1 1695.21 219.537 4 -4 -4 -2 1384.2 200.419 2 4 -4 2 1406.66 199.013 5 4 4 2 1339.89 197.626 5 -4 -4 -3 256.467 96.7142 2 4 -4 3 170.266 75.5859 5 4 4 3 354.755 105.854 5 -4 -4 -4 8139.64 511.843 2 4 -4 4 8455.27 512.319 5 4 4 4 8481.24 515.591 5 -4 4 -4 8372.57 458.293 2 -4 4 -5 158.33 78.2036 2 -4 -4 -5 129.506 87.8721 2 4 -4 5 297.46 111.111 5 4 4 5 119.706 80.8537 5 -4 4 -6 38.1188 55.7202 2 -4 -4 -6 90.725 67.491 2 4 -4 6 53.7943 58.4943 5 4 4 6 74.4877 63.1336 5 -4 -5 7 273.284 104.39 1 -4 5 6 220.679 69.702 4 -4 -5 6 278.047 103.904 1 -4 -5 5 1633.37 208.802 1 4 -5 -5 1500.08 207.77 3 -4 5 5 1639.77 181.593 4 -4 5 4 44.0557 44.4037 4 -4 -5 4 53.8752 48.0163 1 4 -5 -4 72.3521 60.5764 3 -4 5 3 35.4016 50.4007 4 4 -5 -3 108.317 68.3394 3 -4 -5 3 -2.47916 35.9676 2 -4 5 2 6.45902 49.1309 4 -4 -5 2 32.9581 43.821 2 -4 5 1 165.59 79.683 4 4 -5 -1 46.9834 57.7174 5 4 5 -1 153.605 77.2353 5 -4 -5 1 125.384 63.8468 2 -4 5 0 150.115 76.7632 4 4 -5 0 179.612 77.7757 5 -4 -5 0 127.127 61.7493 2 -4 5 -1 64.8938 61.8848 4 4 -5 1 -4.76853 39.3106 5 4 5 1 59.2632 62.4409 5 -4 -5 -1 -11.8983 37.1093 2 -4 5 -2 53.3846 61.0298 4 -4 -5 -2 136.726 73.1778 2 4 -5 2 118.744 75.057 5 4 5 2 65.9759 54.3827 5 -4 -5 -3 7.00019 46.002 2 4 -5 3 22.7802 48.8396 5 4 5 3 20.5238 46.6595 5 -4 -5 -4 478.795 129.481 2 4 -5 4 532.834 132.147 5 4 5 4 487.808 127.992 5 -4 -5 -5 669.516 153.997 2 4 -5 5 1249.91 199.264 5 4 5 5 889.912 172.535 5 -4 5 -6 1495.11 205.641 2 -4 -5 -6 1479.26 232.857 2 4 -5 6 1426.55 217.986 5 4 5 6 1342.04 214.387 5 -4 -6 7 595.029 142.879 1 4 -6 -7 584.208 138.762 3 4 -6 -6 4553.27 372.319 3 -4 -6 6 4771.78 373.809 1 -4 6 6 4926.36 321.221 4 -4 6 5 47.5635 54.3881 4 -4 -6 5 16.516 39.4698 1 4 -6 -5 44.0918 64.4973 3 -4 6 4 405.043 100.212 4 -4 -6 4 445.099 105.789 1 4 -6 -4 456.017 129.008 3 -4 6 3 385.498 104.311 4 4 -6 -3 359.44 111.376 3 -4 -6 3 334.358 101.083 2 -4 -6 2 5745.31 396.666 2 4 -6 -2 6266.66 440.652 3 -4 6 2 6893.89 418.005 4 -4 6 1 1018.82 165.448 4 4 -6 -1 933.491 162.254 5 4 6 -1 1082.51 171.974 5 -4 -6 1 1259.6 186.083 2 -4 -6 0 3396.34 305.772 2 4 -6 0 4332.38 334.519 5 4 6 0 3184.6 291.077 5 -4 6 0 4095.19 341.287 4 -4 6 -1 614.959 143.266 4 4 -6 1 471.074 118.431 5 4 6 1 691.763 143.786 5 -4 -6 -1 658.649 142.842 2 -4 6 -2 1620.73 226.152 4 -4 -6 -2 1555.19 219.251 2 4 -6 2 1448.77 208.036 5 4 6 2 1437.08 204.917 5 -4 6 -3 618.533 146.41 4 -4 -6 -3 716.414 154.563 2 4 -6 3 569.048 129.267 5 4 6 3 749.319 151.358 5 4 6 4 1911.26 241.615 5 -4 -6 -4 1487.85 221.323 2 4 -6 4 1388.7 207.868 5 -4 -6 -5 2736.8 309.556 2 4 -6 5 2348.39 274.189 5 4 6 5 2662.03 293.946 5 -4 7 6 213.494 73.795 4 -4 -7 6 166.939 81.2014 1 4 -7 -6 361.177 114.372 3 -4 7 5 835.287 137.293 4 -4 -7 5 921.864 159.816 1 4 -7 -5 765.666 161.759 3 -4 -7 4 1212.45 170.238 1 4 -7 -4 1279.32 203.639 3 -4 7 4 1501.27 187.992 4 -4 7 3 119.544 68.5652 4 4 -7 -3 118.185 81.6258 3 -4 7 2 1353.38 185.947 4 4 -7 -2 1247.03 208.637 3 -4 -7 2 1320.09 196.547 2 -4 7 1 834.077 157.277 4 -4 -7 1 922.737 161.248 2 4 -7 -1 691.418 155.604 3 -4 7 0 133.803 78.6752 4 4 -7 0 74.607 56.3613 5 4 7 0 192.995 82.7787 5 -4 -7 0 134.874 71.6407 2 -4 7 -1 95.8798 73.9101 4 4 -7 1 117.25 68.1212 5 4 7 1 17.2962 38.6414 5 -4 -7 -1 100.623 69.0849 2 -4 7 -2 1091.34 189.528 4 -4 -7 -2 670.369 149.885 2 4 -7 2 832.469 156.449 5 4 7 2 948.553 168.239 5 -4 -7 -3 1857.5 249.852 2 -4 7 -3 1463.53 223.325 4 4 -7 3 1590.5 215.589 5 4 7 3 1598.57 217.692 5 -4 -7 -4 2600.82 301.311 2 4 -7 4 2472.23 277.022 5 4 7 4 2386.27 272.631 5 -4 7 -4 2454.91 292.83 4 -4 -7 -5 797.116 172.954 2 4 -7 5 995.939 179.938 5 4 7 5 886.403 175.167 5 -4 8 6 727.123 132.227 4 -4 -8 6 681.405 146.764 1 4 -8 -6 741.074 162.665 3 -4 -8 5 70.1997 61.3014 1 -4 8 5 -88.0901 55.085 4 4 -8 -5 -43.5331 61.5208 3 -4 8 4 1140.78 170.766 4 4 -8 -4 1079.36 196.683 3 4 -8 -3 2046.57 265.133 3 -4 8 3 1982.69 226.962 4 -4 -8 2 2764.39 286.391 2 4 -8 -2 2641.63 301.288 3 -4 8 2 3133.98 290.345 4 -4 8 1 1110.41 180.313 4 -4 -8 1 901.734 168.013 2 4 -8 -1 1013.37 189.637 3 -4 -8 0 3847.6 342.343 2 4 -8 0 3830.04 320.705 5 4 8 0 3785.98 326.198 5 -4 8 0 4535.87 367.79 4 -4 8 -1 1688.79 235.121 4 4 -8 1 2283.41 252.029 5 4 8 1 1741.78 224.98 5 -4 -8 -1 1543.23 221.251 2 -4 8 -2 1267.49 206.124 4 4 -8 2 1379.65 203.38 5 4 8 2 1030.45 178.199 5 -4 -8 -2 1244.17 204.216 2 -4 8 -3 718.14 160.901 4 -4 -8 -3 514.655 140.106 2 4 -8 3 549.501 135.706 5 4 8 3 604.732 137.501 5 -4 8 -4 308.97 115.945 4 -4 -8 -4 136.345 80.2664 2 4 -8 4 359.971 114.718 5 4 8 4 224.443 93.4762 5 -4 -9 5 2262.49 243.862 1 4 -9 -5 2025.91 271.612 3 -4 9 5 2208.62 236.347 4 -4 9 4 1061.99 168.08 4 4 9 -4 1021.71 214.616 7 4 -9 -4 596.86 148.807 3 -4 9 3 145.884 71.566 4 4 9 -3 241.54 128.45 7 4 -9 -3 122.147 74.7048 3 -4 9 2 1278.74 189.343 4 4 9 -2 1466.29 257.901 7 4 -9 -2 957.886 190.473 3 -4 -9 2 878.983 169.794 2 -4 9 1 56.697 58.9016 4 4 9 -1 54.9166 81.5299 7 -4 -9 1 42.4363 64.0771 2 4 -9 -1 52.2725 84.7602 3 -4 9 0 43.0224 65.8903 4 4 9 0 72.031 81.6081 7 4 -9 0 26.7812 59.7675 5 4 9 0 -16.1496 40.936 5 -4 -9 0 81.308 59.3209 2 4 -9 0 45.1296 53.7794 3 4 9 1 1443.06 255.422 7 4 -9 1 1682.06 213.908 5 4 9 1 1628.24 216.833 5 -4 -9 -1 1494.07 221.098 2 -4 9 -1 1943.41 251.041 4 -4 9 -2 760.241 170.911 4 4 9 2 734.381 182.364 7 4 -9 2 703.431 145.359 5 4 9 2 900.301 166.589 5 -4 -9 -2 866.905 176.023 2 -4 9 -3 1865.42 259.778 4 4 -9 3 1677.78 228.04 5 -4 -9 -3 1637.45 242.519 2 4 9 3 1401.27 212.981 5 4 10 -3 2553.45 344.573 7 -4 10 3 2407.88 259.108 4 -4 10 2 62.7219 50.4291 4 4 10 -2 8.38648 52.2058 7 4 -10 -2 -12.1737 53.273 3 -4 -10 2 51.2105 63.3147 2 4 10 -1 3810.83 415.037 7 -4 -10 1 3212.88 329.167 2 4 -10 -1 4135.97 402.904 3 -4 10 1 4043.35 350.161 4 -4 10 0 663.677 150.967 4 4 10 0 503.576 154.038 7 -4 -10 0 404.836 127.137 2 4 -10 0 352.063 124.867 3 -4 -10 -1 6848.12 487.137 2 4 10 1 6649.77 550.962 7 4 -10 1 6106.11 411.995 5 4 10 1 6565.08 431.786 5 -4 10 -1 6955.6 483.359 4 -4 -10 -2 2539.51 300.079 2 4 10 2 2186.72 313.751 7 4 -10 2 2022.91 245.143 5 4 10 2 2113.22 250.248 5 -4 10 -2 2113.15 277.162 4 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -0.2335 -16.3553 11.2474 -0.9446 -0.2802 -0.1711 -5.3296 2.7135 1.0197 0.2009 0.0603 -0.9778 0.2444 16.3510 -11.2504 0.9442 0.2801 0.1731 5.2037 0.6916 -4.8568 0.0815 -0.0505 0.9954 -0.1332 0.5135 16.1385 -0.8400 0.5142 -0.1732 -5.3428 -0.7958 2.4032 0.0515 -0.0309 -0.9982 -0.0210 -0.5380 -16.1154 0.8439 -0.5166 0.1448 0.2110 -18.6272 -9.2823 0.0786 -0.9922 0.0969 -0.0836 18.6838 9.2204 -0.0787 0.9942 -0.0730 loop_ _publcif_info_datablock.id _publcif_info_datablock.publ_exptl _publcif_info_datablock.publ_geom _publcif_info_datablock.structure {1eabab0e-05e6-49dd-b377-a6df6b5e513e} y y y loop_ _publcif_info_exptl_table_extra_item sin_theta_over_lambda_max loop_ _publcif_info_exptl_table_header_item ? loop_ _publcif_info_tables.block_id _publcif_info_tables.reference_item {1eabab0e-05e6-49dd-b377-a6df6b5e513e} '_publcif_info_datablock.publ_exptl' loop_ _publcif_info_cif.paper_type EE