#------------------------------------------------------------------------------ #$Date: 2018-03-10 10:11:27 +0200 (Sat, 10 Mar 2018) $ #$Revision: 206888 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242416.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242416 _cell_angle_alpha 90.000 _cell_angle_beta 118.175 _cell_angle_gamma 90.000 _cell_length_a 19.7898 _cell_length_b 19.9497 _cell_length_c 20.2246 _exptl_crystal_F_000 2992.00 _reflns_d_resolution_high 0.7741 _cod_data_source_file su5428Isup2.hkl _cod_data_source_block I _shelx_title ' I in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 451.58 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 3486.74 3080.39 231.26 o 4 0 0 47205.50 46671.10 3959.94 o 5 0 0 9.71 20.88 12.96 o 6 0 0 2588.66 2514.46 541.33 o 7 0 0 110.72 85.73 78.50 o 8 0 0 18825.95 17710.72 1402.08 o 9 0 0 1272.47 1265.56 287.10 o 10 0 0 90819.41 91003.54 2504.46 o 11 0 0 4701.58 4231.62 907.61 o 12 0 0 25947.30 25396.52 5386.38 o 13 0 0 925.06 940.21 247.53 o 14 0 0 1583.77 1311.35 293.79 o 15 0 0 12485.12 14211.67 4244.11 o 16 0 0 6616.57 7540.45 2267.21 o 17 0 0 653.88 1110.11 363.19 o 18 0 0 4084.22 5576.76 799.73 o 19 0 0 3095.19 4693.80 1426.90 o 20 0 0 299.90 350.77 190.66 o 21 0 0 5443.45 6645.55 2006.58 o 22 0 0 5324.24 6584.12 1999.16 o 2 1 0 2509.96 2466.16 112.37 o 3 1 0 48100.80 49009.45 1641.18 o 4 1 0 86834.85 89874.46 3179.32 o 5 1 0 238.10 191.81 24.48 o 6 1 0 10734.38 10230.19 493.08 o 7 1 0 11949.20 11629.41 560.12 o 8 1 0 125.42 147.90 31.38 o 9 1 0 57.59 88.00 45.41 o 10 1 0 13010.10 13578.44 898.69 o 11 1 0 33342.36 32783.46 1178.02 o 12 1 0 12626.62 11696.62 1136.88 o 13 1 0 7251.39 7204.98 1092.38 o 14 1 0 33.24 49.07 48.91 o 15 1 0 3747.50 4892.59 655.93 o 16 1 0 36.69 41.20 89.97 o 17 1 0 111.28 176.26 118.82 o 18 1 0 26.95 54.15 87.46 o 19 1 0 84.14 164.44 111.97 o 20 1 0 1044.25 1249.28 289.04 o 21 1 0 2017.68 2523.73 391.34 o 22 1 0 3055.35 3492.67 467.46 o 2 2 0 5846.31 5029.06 187.97 o 3 2 0 70664.80 77982.00 1803.93 o 4 2 0 45494.82 44449.82 1515.06 o 5 2 0 27031.92 26203.34 728.37 o 6 2 0 1319.67 1300.83 71.51 o 7 2 0 9386.87 8710.93 386.57 o 8 2 0 16035.59 13946.04 554.35 o 9 2 0 74627.20 80765.12 2098.08 o 10 2 0 5913.64 6428.39 498.58 o 11 2 0 1393.89 1902.44 255.18 o 12 2 0 7343.10 7283.79 799.46 o 13 2 0 4509.75 4537.92 570.53 o 14 2 0 216.28 215.34 71.77 o 15 2 0 6205.53 7049.74 1497.52 o 16 2 0 744.76 1103.47 262.16 o 17 2 0 752.05 1163.34 278.54 o 18 2 0 150.03 205.32 120.21 o 19 2 0 1644.63 2671.64 585.99 o 20 2 0 4023.65 5394.67 1156.52 o 21 2 0 2127.39 2468.44 445.90 o 22 2 0 1132.78 1119.30 288.60 o 1 3 0 34167.91 32759.88 880.76 o 2 3 0 1475.48 965.64 48.93 o 3 3 0 16417.19 14674.17 451.52 o 4 3 0 5622.30 5127.33 185.00 o 5 3 0 3501.64 3095.93 125.34 o 6 3 0 9785.82 8703.65 327.84 o 7 3 0 10679.96 9647.03 359.50 o 8 3 0 860.54 1164.12 66.91 o 9 3 0 1220.64 1368.55 98.08 o 10 3 0 1304.13 1347.82 138.53 o 11 3 0 11.02 108.94 28.24 o 12 3 0 120.47 183.60 69.69 o 13 3 0 306.66 262.20 72.94 o 14 3 0 11786.75 11358.47 1095.78 o 15 3 0 15595.19 18879.64 1439.52 o 16 3 0 512.93 757.25 204.74 o 17 3 0 6242.92 7807.81 1660.38 o 18 3 0 2923.31 3637.41 461.99 o 19 3 0 38.21 60.38 98.77 o 20 3 0 126.59 155.88 118.82 o 21 3 0 1274.90 1474.29 319.48 o 22 3 0 96.05 105.12 158.38 o 0 4 0 71974.40 69005.41 2166.52 o 1 4 0 7977.48 6856.40 231.08 o 2 4 0 957.77 1033.53 48.58 o 3 4 0 11866.12 10769.92 355.33 o 4 4 0 21790.98 20851.35 672.98 o 5 4 0 76689.98 81995.91 1594.71 o 6 4 0 54724.53 57247.67 1397.93 o 7 4 0 6644.61 6286.29 246.90 o 8 4 0 11123.88 11222.39 374.89 o 9 4 0 8010.24 7077.83 285.78 o 10 4 0 806.64 1211.53 109.45 o 11 4 0 4052.33 4254.45 274.61 o 12 4 0 461.34 601.43 131.05 o 13 4 0 4100.25 4448.35 563.61 o 14 4 0 4876.20 4337.76 578.72 o 15 4 0 10131.59 12348.49 1144.32 o 16 4 0 1749.05 2236.30 420.75 o 17 4 0 228.69 279.79 129.36 o 18 4 0 1321.70 1517.09 350.19 o 19 4 0 269.07 317.05 132.80 o 20 4 0 1296.36 1790.58 364.94 o 21 4 0 645.44 834.81 237.28 o 22 4 0 374.41 134.36 160.65 o 1 5 0 189.61 205.73 12.64 o 2 5 0 10826.57 9018.54 299.78 o 3 5 0 456.49 349.59 21.85 o 4 5 0 46806.98 46093.76 1365.15 o 5 5 0 3433.29 2999.00 123.45 o 6 5 0 177213.45 200333.55 7067.80 o 7 5 0 1737.74 1636.61 85.15 o 8 5 0 24478.02 22704.18 702.63 o 9 5 0 12877.25 12068.68 413.46 o 10 5 0 14160.78 13312.51 507.56 o 11 5 0 1041.87 974.35 94.77 o 12 5 0 5095.07 4805.84 307.53 o 13 5 0 5099.63 4781.83 322.43 o 14 5 0 12516.14 13427.95 1234.55 o 15 5 0 3166.98 4191.00 900.35 o 16 5 0 38473.93 47940.82 10082.34 o 17 5 0 4600.56 5607.37 753.73 o 18 5 0 119.95 80.54 106.04 o 19 5 0 4064.49 4839.72 659.25 o 20 5 0 360.05 550.58 172.46 o 21 5 0 781.56 1031.55 265.21 o 22 5 0 337.51 406.52 261.43 o 0 6 0 23353.81 17536.75 821.37 o 1 6 0 319.38 468.10 25.06 o 2 6 0 1781.56 1770.52 69.57 o 3 6 0 17483.04 15794.01 525.87 o 4 6 0 86214.69 94661.59 2500.63 o 5 6 0 20768.94 18096.12 586.38 o 6 6 0 64950.68 70001.04 1865.87 o 7 6 0 519.27 500.22 29.95 o 8 6 0 2778.26 3549.81 149.37 o 9 6 0 12538.52 12798.06 462.37 o 10 6 0 1578.44 1849.10 100.27 o 11 6 0 524.47 523.37 48.75 o 12 6 0 336.34 306.63 49.66 o 13 6 0 3282.85 3311.36 263.98 o 14 6 0 4911.91 4216.44 352.23 o 15 6 0 4543.43 5310.10 739.16 o 16 6 0 1511.57 2031.58 381.22 o 17 6 0 391.55 539.06 160.47 o 18 6 0 1786.73 2069.11 395.42 o 19 6 0 3161.49 4116.31 882.77 o 20 6 0 20.94 -29.54 71.08 o 21 6 0 1.00 1.16 124.07 o 1 7 0 468.21 285.57 17.70 o 2 7 0 735.50 955.48 45.46 o 3 7 0 33268.04 29803.66 923.16 o 4 7 0 831.67 678.64 39.39 o 5 7 0 28249.77 26941.23 770.61 o 6 7 0 12413.02 12231.34 444.54 o 7 7 0 95225.18 99869.43 2518.94 o 8 7 0 869.70 1067.25 57.42 o 9 7 0 5657.58 6013.75 259.76 o 10 7 0 3531.14 3468.17 163.56 o 11 7 0 2420.85 2437.93 124.75 o 12 7 0 1674.99 1827.30 111.37 o 13 7 0 1422.50 1567.78 132.50 o 14 7 0 1779.93 1715.73 155.54 o 15 7 0 20386.34 13804.48 2996.76 o 16 7 0 514.49 593.15 175.86 o 17 7 0 625.75 767.68 204.24 o 18 7 0 2236.14 2306.77 369.13 o 19 7 0 2620.34 2941.64 486.97 o 20 7 0 1.50 13.93 95.46 o 21 7 0 976.01 971.77 270.04 o 0 8 0 8508.16 7361.65 331.20 o 1 8 0 2707.31 2793.34 101.66 o 2 8 0 1464.61 1512.14 60.71 o 3 8 0 1636.98 1900.78 76.24 o 4 8 0 3258.06 2662.82 106.13 o 5 8 0 887.24 998.39 51.66 o 6 8 0 25.03 63.98 14.35 o 7 8 0 2000.90 1995.14 83.47 o 8 8 0 3777.10 3524.43 151.77 o 9 8 0 15532.39 17160.54 555.32 o 10 8 0 733.54 757.71 51.30 o 11 8 0 204.70 373.93 38.85 o 12 8 0 2651.26 2769.98 150.54 o 13 8 0 2744.00 2519.03 161.68 o 14 8 0 751.94 655.92 88.40 o 15 8 0 199.65 248.12 64.10 o 16 8 0 426.47 415.43 144.20 o 17 8 0 1.97 -12.40 76.05 o 18 8 0 192.60 215.89 115.92 o 19 8 0 3484.29 4388.45 947.98 o 20 8 0 2040.93 2055.82 405.31 o 21 8 0 26.06 102.79 141.44 o 1 9 0 15258.86 14439.34 445.96 o 2 9 0 5605.90 6137.14 225.65 o 3 9 0 16755.97 17182.57 550.69 o 4 9 0 570.34 706.58 37.91 o 5 9 0 1521.17 1519.35 65.73 o 6 9 0 11219.34 10530.78 363.20 o 7 9 0 16857.17 16366.48 485.70 o 8 9 0 5947.91 6857.98 257.77 o 9 9 0 1133.64 1234.04 75.55 o 10 9 0 5183.69 5385.28 232.39 o 11 9 0 8423.18 9138.28 360.68 o 12 9 0 4518.70 4901.54 279.63 o 13 9 0 1165.40 1356.59 113.52 o 14 9 0 10435.76 10241.74 1139.95 o 15 9 0 3582.32 3493.69 501.00 o 16 9 0 1076.88 1014.63 345.65 o 17 9 0 1771.74 2007.60 400.91 o 18 9 0 4665.98 4937.63 1059.13 o 19 9 0 62.67 24.30 92.85 o 20 9 0 340.42 363.81 162.01 o 0 10 0 94080.55 96321.81 4297.17 o 1 10 0 315.36 420.21 22.06 o 2 10 0 2148.78 2461.50 102.79 o 3 10 0 18.31 20.55 10.84 o 4 10 0 9953.67 8259.08 301.27 o 5 10 0 3.64 22.35 11.76 o 6 10 0 18704.31 18862.30 567.05 o 7 10 0 823.15 785.66 47.23 o 8 10 0 1414.10 1404.47 66.14 o 9 10 0 72.72 56.12 19.62 o 10 10 0 23180.82 25192.79 913.12 o 11 10 0 5439.82 5704.89 225.87 o 12 10 0 3275.17 2952.27 144.38 o 13 10 0 1180.76 1073.40 87.60 o 14 10 0 8747.42 6608.55 916.33 o 15 10 0 3113.68 4027.71 859.53 o 16 10 0 3.23 75.88 74.11 o 17 10 0 965.86 643.28 291.97 o 18 10 0 5341.31 6018.82 785.63 o 19 10 0 2195.40 2195.28 491.27 o 20 10 0 747.42 885.90 264.41 o 1 11 0 3922.24 3900.11 152.35 o 2 11 0 15535.45 14980.54 531.40 o 3 11 0 10171.64 9946.80 342.31 o 4 11 0 773.69 782.96 41.55 o 5 11 0 182.29 166.68 19.06 o 6 11 0 580.04 558.45 37.85 o 7 11 0 959.01 1053.59 53.35 o 8 11 0 3736.98 3685.24 155.35 o 9 11 0 1473.95 1600.28 90.61 o 10 11 0 1274.05 1411.40 77.41 o 11 11 0 5406.25 5679.67 239.14 o 12 11 0 3541.72 3034.86 155.34 o 13 11 0 10972.83 10370.37 1032.28 o 14 11 0 679.52 526.83 108.55 o 15 11 0 90.14 101.33 75.06 o 16 11 0 409.13 380.32 170.70 o 17 11 0 991.41 1379.79 297.82 o 18 11 0 591.83 922.04 246.77 o 19 11 0 70.80 39.38 124.76 o 20 11 0 533.78 35.38 234.65 o 0 12 0 1871.48 1612.97 108.20 o 1 12 0 15875.65 15552.12 585.98 o 2 12 0 60.58 74.11 15.33 o 3 12 0 3399.70 3154.97 126.31 o 4 12 0 330.38 332.28 25.30 o 5 12 0 322.92 332.81 26.15 o 6 12 0 295.03 278.36 25.04 o 7 12 0 32.21 43.31 17.14 o 8 12 0 1796.73 1588.48 79.61 o 9 12 0 17900.12 18179.11 686.73 o 10 12 0 1.10 15.66 23.62 o 11 12 0 0.83 33.02 29.98 o 12 12 0 1661.44 1547.18 113.06 o 13 12 0 11477.56 11136.92 1162.02 o 14 12 0 28.39 87.97 60.99 o 15 12 0 56.83 2.94 67.51 o 16 12 0 135.91 95.65 94.61 o 17 12 0 477.01 558.20 201.15 o 18 12 0 82.92 26.04 133.41 o 19 12 0 458.51 114.46 147.97 o 1 13 0 484.16 594.49 37.13 o 2 13 0 1012.05 1004.19 51.54 o 3 13 0 1108.61 1216.69 58.25 o 4 13 0 1007.92 970.29 57.64 o 5 13 0 2.58 40.03 16.01 o 6 13 0 1853.60 2000.60 94.31 o 7 13 0 1235.87 1297.47 69.38 o 8 13 0 3034.11 2629.66 118.36 o 9 13 0 47.46 124.23 27.48 o 10 13 0 3565.63 3201.10 153.25 o 11 13 0 689.34 700.13 67.65 o 12 13 0 552.13 503.05 67.28 o 13 13 0 2573.30 2476.20 202.45 o 14 13 0 1137.38 1057.41 131.95 o 15 13 0 1047.53 676.60 168.88 o 16 13 0 52.56 91.97 93.22 o 17 13 0 703.29 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941.19 112.15 o 14 15 0 935.80 446.10 162.00 o 15 15 0 6.25 52.97 89.49 o 17 15 0 3134.91 1041.95 795.54 o 0 16 0 15426.95 15027.34 823.88 o 1 16 0 66.60 127.75 23.87 o 2 16 0 2073.39 1837.76 87.53 o 3 16 0 1086.21 1077.03 60.55 o 4 16 0 2027.07 2067.36 92.96 o 5 16 0 6130.77 6038.67 283.29 o 6 16 0 26.24 48.70 23.93 o 7 16 0 3673.51 3855.50 204.30 o 8 16 0 3225.98 3436.13 206.03 o 9 16 0 5.00 54.62 38.90 o 10 16 0 1811.53 1774.78 125.73 o 11 16 0 86.11 54.90 43.93 o 12 16 0 71.23 54.50 62.11 o 13 16 0 743.75 216.97 142.04 o 14 16 0 613.65 355.98 173.02 o 15 16 0 1257.27 453.33 226.24 o 16 16 0 287.66 5.51 129.57 o 1 17 0 52.74 60.40 25.80 o 2 17 0 1592.54 1956.58 113.14 o 3 17 0 6653.81 7335.12 328.60 o 4 17 0 12.52 27.26 26.20 o 5 17 0 494.72 523.95 48.22 o 6 17 0 2525.93 2906.92 155.95 o 7 17 0 7999.94 8523.57 398.87 o 8 17 0 97.74 118.39 44.96 o 9 17 0 6.96 31.76 44.76 o 10 17 0 1283.32 1310.62 107.29 o 11 17 0 18.05 56.20 59.62 o 12 17 0 81.51 73.77 98.53 o 13 17 0 550.17 261.58 150.72 o 14 17 0 574.52 191.35 106.90 o 15 17 0 1737.97 375.35 375.02 o 0 18 0 59.80 112.44 47.16 o 1 18 0 164.52 309.22 42.64 o 2 18 0 2832.80 3124.65 144.40 o 3 18 0 808.52 1072.63 64.31 o 4 18 0 356.20 420.32 52.64 o 5 18 0 3521.87 3921.25 200.92 o 6 18 0 319.56 365.82 51.22 o 7 18 0 5.42 31.56 40.17 o 8 18 0 227.51 274.70 54.78 o 9 18 0 2327.88 2515.52 160.22 o 10 18 0 170.08 119.92 69.45 o 11 18 0 117.07 83.36 76.71 o 12 18 0 280.49 72.79 87.03 o 13 18 0 1085.58 410.11 229.92 o 14 18 0 6.98 28.85 95.86 o 1 19 0 1124.36 1478.10 88.59 o 2 19 0 3541.16 4309.39 229.08 o 3 19 0 4447.69 5132.26 257.21 o 4 19 0 533.61 682.39 59.48 o 5 19 0 596.91 648.99 61.97 o 6 19 0 424.16 544.80 62.36 o 7 19 0 5326.45 5877.03 330.13 o 8 19 0 418.57 441.07 74.97 o 9 19 0 65.44 56.19 55.04 o 10 19 0 495.03 169.14 132.00 o 11 19 0 909.05 386.98 209.44 o 12 19 0 1205.34 747.11 280.54 o 13 19 0 848.91 446.56 149.27 o 0 20 0 17334.78 20557.44 1351.63 o 1 20 0 599.68 762.49 71.98 o 2 20 0 72.89 18.78 38.88 o 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0 1450.79 1596.88 139.37 o 4 23 0 18.37 92.73 54.50 o 5 23 0 622.60 625.45 100.01 o 6 23 0 199.65 189.83 112.21 o 7 23 0 747.13 284.24 284.54 o 8 23 0 974.63 477.16 430.89 o 9 23 0 827.97 764.47 210.73 o 0 24 0 740.74 636.11 146.92 o 1 24 0 2537.28 2513.85 214.21 o 2 24 0 23.92 29.12 60.62 o 3 24 0 1318.52 1110.57 115.92 o 4 24 0 1357.83 1323.95 200.61 o 5 24 0 440.59 397.88 309.15 o 6 24 0 106.94 68.43 140.08 o 7 24 0 46.41 -41.09 168.12 o 1 25 0 1186.62 1313.84 153.52 o 2 25 0 6556.38 6664.67 494.69 o 3 25 0 1.06 -26.55 97.44 o 4 25 0 898.37 758.10 428.28 o 5 25 0 61.17 -30.37 162.94 o -22 1 1 865.20 910.57 265.19 o -21 1 1 2171.77 2619.96 578.30 o -20 1 1 583.74 770.64 213.22 o -19 1 1 4523.61 5694.88 576.38 o -18 1 1 2644.21 3012.95 418.38 o -17 1 1 25.29 17.26 73.58 o -16 1 1 1778.74 2118.33 402.34 o -15 1 1 4649.80 4500.01 651.66 o -14 1 1 125.93 113.92 64.95 o -13 1 1 1209.91 1227.75 202.73 o -12 1 1 567.74 759.88 131.24 o -11 1 1 40979.88 34311.23 3069.63 o -10 1 1 20977.53 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