#------------------------------------------------------------------------------
#$Date: 2018-04-30 19:24:07 +0300 (Mon, 30 Apr 2018) $
#$Revision: 207545 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242441.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2242441
_cell_angle_alpha                90.000
_cell_angle_beta                 100.486
_cell_angle_gamma                90.000
_cell_length_a                   3.9390
_cell_length_b                   10.7805
_cell_length_c                   9.9444
_exptl_crystal_F_000             356.00
_reflns_d_resolution_high        0.6241
_cod_data_source_file            su5433Ag-Absorb7_bsup3.hkl
_cod_data_source_block           Ag-Absorb7_b
_shelx_title                     ' '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            163.60
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 841.06 842.86 44.18 o
4 0 0 897.75 926.86 34.90 o
1 1 0 5479.97 5728.72 103.27 o
2 1 0 1339.28 1267.75 27.27 o
3 1 0 1367.15 1326.44 27.91 o
4 1 0 730.69 756.17 34.28 o
5 1 0 1.86 39.00 38.67 o
1 2 0 7542.41 7561.54 221.43 o
2 2 0 1511.68 1680.33 82.06 o
3 2 0 592.39 580.16 28.63 o
4 2 0 6.34 -2.40 18.62 o
5 2 0 63.34 38.88 39.44 o
1 3 0 4845.49 4740.94 244.09 o
2 3 0 10252.54 10349.10 210.00 o
3 3 0 48.46 44.93 17.15 o
4 3 0 19.99 29.92 14.06 o
5 3 0 34.43 35.53 34.95 o
6 3 0 4.36 -83.90 108.68 o
1 4 0 909.61 1056.34 67.64 o
2 4 0 277.63 280.20 37.50 o
3 4 0 548.59 575.15 46.36 o
4 4 0 1.88 35.08 27.72 o
5 4 0 141.62 173.43 60.14 o
2 5 0 787.79 885.34 78.41 o
3 5 0 549.55 507.67 25.79 o
4 5 0 93.17 109.68 79.87 o
5 5 0 36.62 190.19 89.34 o
2 6 0 276.60 397.86 64.10 o
3 6 0 1750.35 1863.81 120.53 o
4 6 0 266.86 278.82 85.27 o
5 6 0 20.78 154.17 94.75 o
2 7 0 43.96 -4.74 92.00 o
4 7 0 8.01 -4.93 101.31 o
5 7 0 25.12 37.52 109.93 o
4 8 0 169.58 220.54 150.31 o
-5 0 1 25.28 -6.41 84.63 o
-3 0 1 725.79 713.37 30.67 o
-1 0 1 1079.16 1158.67 30.36 o
1 0 1 26765.71 26990.81 604.20 o
3 0 1 127.98 128.64 21.24 o
5 0 1 341.77 380.42 113.44 o
-5 1 1 41.49 20.68 29.72 o
-4 1 1 273.57 269.46 21.54 o
-3 1 1 3568.89 3510.42 65.80 o
-2 1 1 4728.06 4785.51 86.20 o
-1 1 1 248.25 279.23 9.57 o
0 1 1 382.82 397.63 15.97 o
1 1 1 20206.29 21798.18 190.49 o
2 1 1 7403.68 7465.17 170.82 o
3 1 1 448.22 412.56 18.95 o
4 1 1 0.40 14.71 19.90 o
5 1 1 0.04 24.51 78.02 o
-6 2 1 22.06 84.42 100.95 o
-5 2 1 55.95 107.57 38.53 o
-4 2 1 1.92 17.96 20.23 o
-3 2 1 481.99 481.23 15.86 o
-2 2 1 862.47 862.50 19.90 o
-1 2 1 22078.33 22738.90 569.52 o
0 2 1 3688.84 3923.87 89.20 o
1 2 1 250.51 254.02 7.67 o
2 2 1 552.05 517.01 26.51 o
3 2 1 1477.40 1517.08 41.01 o
4 2 1 278.33 241.08 39.06 o
5 2 1 1.61 36.28 49.94 o
-6 3 1 11.60 36.48 96.64 o
-5 3 1 115.83 151.97 45.68 o
-4 3 1 1.98 11.60 18.78 o
-3 3 1 450.67 457.20 24.45 o
-2 3 1 951.97 944.68 26.94 o
-1 3 1 325.87 358.08 20.67 o
0 3 1 3180.02 3078.60 91.96 o
1 3 1 498.79 543.86 16.60 o
2 3 1 102.20 127.40 21.45 o
3 3 1 2369.84 2357.05 89.19 o
4 3 1 141.86 187.65 70.73 o
5 3 1 0.03 51.95 56.29 o
-6 4 1 12.78 55.27 91.64 o
-5 4 1 57.70 6.33 41.15 o
-4 4 1 708.55 678.09 64.07 o
-3 4 1 39.74 39.51 8.35 o
-2 4 1 4199.16 4500.18 173.54 o
0 4 1 20848.46 21712.83 771.29 o
1 4 1 62.77 60.49 14.44 o
2 4 1 3023.62 3069.91 94.97 o
3 4 1 361.76 435.91 67.51 o
4 4 1 99.03 110.80 73.62 o
5 4 1 0.14 -41.92 51.69 o
-5 5 1 15.01 151.71 64.48 o
-4 5 1 221.45 236.81 33.86 o
-3 5 1 1115.22 1087.76 49.56 o
-2 5 1 544.82 403.26 255.25 o
1 5 1 4473.75 4341.53 161.73 o
2 5 1 1749.48 1575.17 100.69 o
3 5 1 273.46 207.34 57.69 o
4 5 1 379.52 351.33 54.00 o
5 5 1 21.06 64.46 86.98 o
-5 6 1 46.51 148.42 93.35 o
-4 6 1 355.49 315.32 109.97 o
-3 6 1 0.67 -47.42 58.74 o
1 6 1 1893.65 1682.94 131.75 o
2 6 1 3306.08 3356.49 139.00 o
3 6 1 215.03 228.78 55.63 o
4 6 1 277.56 279.68 100.99 o
5 6 1 73.06 -41.59 89.71 o
1 7 1 27.55 20.87 26.99 o
2 7 1 2254.34 2545.82 428.23 o
3 7 1 13.20 11.22 26.14 o
4 7 1 30.36 129.53 87.79 o
2 8 1 1183.87 1090.58 242.98 o
3 8 1 14.10 0.51 9.78 o
4 8 1 59.83 4.84 99.63 o
3 9 1 0.38 -7.80 54.82 o
-6 0 2 45.85 -28.78 91.67 o
-4 0 2 273.77 245.56 39.11 o
-2 0 2 19164.07 18700.33 541.52 o
2 0 2 1745.78 1756.11 45.60 o
4 0 2 57.75 36.15 24.66 o
-5 1 2 104.48 119.22 33.18 o
-4 1 2 27.27 47.89 22.26 o
-3 1 2 608.22 619.17 19.22 o
-2 1 2 115.72 117.08 8.67 o
-1 1 2 281.81 269.09 16.35 o
0 1 2 5774.16 5566.81 162.43 o
1 1 2 3563.06 3487.69 90.51 o
2 1 2 7388.34 7169.09 198.64 o
3 1 2 1544.46 1640.69 91.26 o
4 1 2 1.30 -10.49 16.75 o
5 1 2 53.51 155.23 113.37 o
-6 2 2 7.38 4.15 94.38 o
-5 2 2 156.98 174.03 36.33 o
-4 2 2 179.58 195.42 23.00 o
-2 2 2 1083.64 1153.48 31.36 o
-1 2 2 14831.89 14900.54 306.29 o
0 2 2 8072.56 8025.90 153.44 o
1 2 2 252.72 241.96 11.19 o
2 2 2 956.95 969.30 28.09 o
3 2 2 697.35 665.64 49.64 o
4 2 2 917.38 937.52 67.26 o
5 2 2 0.94 -12.20 53.09 o
-6 3 2 2.22 78.24 87.94 o
-5 3 2 11.57 83.01 47.31 o
-4 3 2 1460.41 1505.14 52.84 o
-3 3 2 712.27 703.55 17.94 o
-2 3 2 2165.40 2239.54 256.43 o
-1 3 2 1994.58 1920.28 46.23 o
0 3 2 18725.74 18493.89 351.04 o
1 3 2 700.55 694.71 21.80 o
2 3 2 1154.60 1167.66 38.77 o
3 3 2 273.65 285.11 68.51 o
4 3 2 44.40 122.34 53.18 o
5 3 2 3.13 5.15 53.28 o
-6 4 2 1.13 22.91 86.16 o
-5 4 2 2.34 -13.98 40.67 o
-4 4 2 0.19 -6.49 21.43 o
-3 4 2 24.08 39.96 9.21 o
-2 4 2 86.83 48.65 20.70 o
-1 4 2 1486.14 1473.85 41.95 o
0 4 2 751.42 719.14 23.25 o
1 4 2 9840.61 10089.63 208.89 o
2 4 2 392.50 406.13 29.00 o
3 4 2 1744.64 1749.95 164.72 o
4 4 2 158.91 184.66 54.28 o
5 4 2 84.44 -51.72 89.82 o
-6 5 2 1.12 7.62 81.40 o
-5 5 2 4.30 -12.75 50.78 o
-4 5 2 154.43 118.27 19.08 o
-3 5 2 3725.42 3563.38 106.87 o
-2 5 2 392.76 439.79 48.09 o
-1 5 2 5101.20 5094.94 131.65 o
0 5 2 114.47 113.31 14.85 o
1 5 2 2289.45 2212.92 59.02 o
2 5 2 2218.56 2223.33 73.93 o
3 5 2 135.43 71.45 58.94 o
4 5 2 12.12 36.76 52.29 o
5 5 2 10.85 32.17 95.12 o
-5 6 2 98.70 85.59 59.74 o
-4 6 2 6.08 19.60 18.31 o
-3 6 2 438.66 543.13 67.02 o
-2 6 2 1902.39 2148.90 84.97 o
0 6 2 2693.84 2654.16 77.37 o
1 6 2 3642.23 3688.43 110.35 o
2 6 2 151.19 124.73 14.55 o
3 6 2 40.52 103.51 65.40 o
4 6 2 197.81 313.18 91.41 o
-3 7 2 14.31 -12.25 83.10 o
0 7 2 741.03 755.04 80.66 o
1 7 2 1975.55 1830.95 73.28 o
2 7 2 13.38 17.52 17.17 o
3 7 2 1588.05 1641.89 76.63 o
4 7 2 7.26 -21.82 67.50 o
1 8 2 2065.47 1921.22 194.00 o
2 8 2 388.59 448.04 40.47 o
3 8 2 24.13 71.91 44.29 o
4 8 2 13.77 32.55 63.72 o
2 9 2 1807.60 1887.48 176.60 o
3 9 2 110.81 100.28 46.33 o
3 10 2 163.83 140.86 106.75 o
-5 0 3 2.21 11.82 47.50 o
-1 0 3 14052.91 13196.67 664.47 o
3 0 3 3740.34 4110.80 234.85 o
-6 1 3 14.78 -12.39 63.72 o
-5 1 3 156.39 177.50 33.24 o
-4 1 3 1049.84 1112.95 88.86 o
-3 1 3 737.16 715.64 19.18 o
-2 1 3 62.47 67.32 11.81 o
-1 1 3 12325.39 12787.54 371.99 o
1 1 3 643.82 662.31 56.96 o
2 1 3 551.60 457.56 63.77 o
3 1 3 12.09 4.86 20.36 o
4 1 3 3.18 -2.20 17.39 o
5 1 3 0.45 -1.46 45.90 o
-5 2 3 95.18 85.54 30.60 o
-4 2 3 4.30 -1.35 30.10 o
-3 2 3 3989.93 3975.61 86.07 o
-2 2 3 1398.90 1370.15 51.79 o
-1 2 3 210.39 194.51 9.08 o
0 2 3 9886.42 10098.20 227.62 o
1 2 3 2487.37 2420.06 65.42 o
2 2 3 968.67 966.35 29.85 o
3 2 3 114.65 88.92 13.80 o
4 2 3 618.03 549.52 46.38 o
-6 3 3 0.28 51.48 85.15 o
-5 3 3 29.89 73.61 49.60 o
-4 3 3 39.08 21.63 29.87 o
-3 3 3 935.77 966.99 26.70 o
-2 3 3 648.63 640.31 29.92 o
-1 3 3 964.69 1003.21 24.34 o
0 3 3 138.70 141.23 7.75 o
1 3 3 14616.76 14348.88 295.96 o
2 3 3 2174.61 2141.85 55.07 o
3 3 3 540.13 469.75 46.87 o
4 3 3 54.93 69.52 33.33 o
5 3 3 188.16 214.22 100.46 o
-5 4 3 6.50 -49.58 59.60 o
-4 4 3 53.42 35.18 12.12 o
-3 4 3 516.68 505.20 31.37 o
-2 4 3 9301.31 9083.92 329.06 o
-1 4 3 438.52 388.51 18.92 o
0 4 3 706.28 702.92 18.58 o
1 4 3 1432.70 1442.87 34.22 o
2 4 3 127.64 138.94 24.83 o
3 4 3 61.90 53.54 41.35 o
4 4 3 107.74 4.96 54.09 o
5 4 3 0.15 -48.72 69.76 o
-5 5 3 99.67 94.37 58.03 o
-4 5 3 11.19 1.70 20.74 o
-3 5 3 435.94 509.08 62.86 o
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1 5 3 1259.27 1224.47 33.39 o
2 5 3 4215.83 4380.70 168.03 o
3 5 3 17.70 25.96 54.45 o
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2 7 3 73.32 51.10 25.86 o
3 7 3 0.06 18.48 64.36 o
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1 8 3 237.05 280.01 24.10 o
2 8 3 576.31 598.61 32.77 o
3 8 3 680.47 568.00 79.79 o
4 8 3 167.64 333.38 97.60 o
-1 9 3 1482.47 1158.89 166.21 o
0 9 3 27.54 31.89 37.06 o
1 9 3 376.73 370.07 34.57 o
2 9 3 1325.22 1319.85 54.24 o
3 9 3 0.84 11.24 72.04 o
0 10 3 32.13 19.58 86.72 o
1 10 3 347.29 331.83 68.52 o
2 10 3 331.14 311.98 34.80 o
3 10 3 144.44 153.35 103.24 o
2 11 3 159.71 35.22 69.14 o
3 11 3 8.01 45.86 149.13 o
-6 0 4 121.28 37.16 84.98 o
-4 0 4 1389.64 1562.00 55.11 o
-2 0 4 4230.02 4231.42 222.12 o
-6 1 4 0.72 -3.78 58.52 o
-5 1 4 191.53 196.70 34.80 o
-4 1 4 21.62 37.32 17.41 o
-3 1 4 924.59 946.34 29.08 o
-2 1 4 4136.59 4046.90 122.51 o
-1 1 4 4008.39 4096.97 213.10 o
2 1 4 677.00 757.05 81.02 o
3 1 4 35.32 71.99 74.51 o
4 1 4 203.90 126.41 51.72 o
-5 2 4 0.17 -40.11 59.07 o
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-3 2 4 2035.48 2183.86 62.18 o
-2 2 4 4212.69 4305.25 127.72 o
-1 2 4 372.96 382.25 24.01 o
0 2 4 3535.07 3485.50 90.93 o
1 2 4 140.05 175.33 16.95 o
2 2 4 4242.73 4353.36 242.20 o
3 2 4 121.94 123.65 20.86 o
4 2 4 21.22 43.51 70.57 o
5 2 4 63.39 258.79 132.29 o
-5 3 4 69.50 76.00 40.29 o
-4 3 4 665.46 599.63 37.38 o
-3 3 4 154.62 172.93 51.76 o
-2 3 4 2262.98 2284.35 73.07 o
-1 3 4 1309.25 1339.90 40.42 o
0 3 4 1562.15 1541.59 33.16 o
1 3 4 2022.00 2007.06 45.67 o
2 3 4 259.54 243.95 25.06 o
3 3 4 250.02 253.26 23.63 o
4 3 4 25.69 138.46 53.96 o
5 3 4 0.53 -39.17 117.35 o
-5 4 4 13.84 -125.02 125.02 o
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-3 4 4 148.58 149.01 30.67 o
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3 4 4 1627.94 1567.83 92.94 o
4 4 4 4.88 1.18 39.19 o
-5 5 4 311.59 235.05 71.73 o
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1 5 4 149.13 145.95 17.06 o
2 5 4 624.72 596.72 31.17 o
3 5 4 187.76 163.58 32.95 o
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-5 6 4 0.16 -59.54 69.45 o
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-1 6 4 3025.25 2830.46 91.92 o
0 6 4 173.44 163.50 14.43 o
1 6 4 100.50 102.44 26.92 o
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3 6 4 65.61 51.00 28.91 o
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-5 7 4 3.60 25.58 70.02 o
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3 8 4 0.06 4.87 54.95 o
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-3 9 4 47.06 1.34 44.92 o
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1 9 4 265.07 187.66 36.75 o
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-2 10 4 26.15 -25.97 81.84 o
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2 5 5 183.69 195.32 28.33 o
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