#------------------------------------------------------------------------------
#$Date: 2018-04-30 19:24:07 +0300 (Mon, 30 Apr 2018) $
#$Revision: 207545 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242442.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2242442
_cell_angle_alpha                90.000
_cell_angle_beta                 100.486
_cell_angle_gamma                90.000
_cell_length_a                   3.9390
_cell_length_b                   10.7805
_cell_length_c                   9.9444
_exptl_crystal_F_000             356.00
_reflns_d_resolution_high        0.6241
_cod_data_source_file            su5433Ag-CAsphere_csup4.hkl
_cod_data_source_block           Ag-CAsphere_c
_shelx_title                     ' '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            163.52
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 837.98 842.15 40.87 o
4 0 0 885.41 910.10 34.41 o
1 1 0 5465.57 5732.04 101.11 o
2 1 0 1335.30 1294.46 27.44 o
3 1 0 1352.03 1310.14 36.20 o
4 1 0 718.43 741.63 32.60 o
5 1 0 1.69 39.00 39.23 o
1 2 0 7536.28 7607.07 218.41 o
2 2 0 1501.29 1657.42 68.89 o
3 2 0 586.08 573.38 34.39 o
4 2 0 6.45 -2.36 18.76 o
5 2 0 61.70 39.11 40.34 o
1 3 0 4822.72 4582.39 231.36 o
2 3 0 10169.75 10401.99 233.81 o
3 3 0 49.32 43.19 16.76 o
4 3 0 19.82 30.00 14.43 o
5 3 0 34.21 36.48 36.88 o
6 3 0 4.12 -85.59 113.16 o
1 4 0 902.01 984.79 62.74 o
2 4 0 271.32 279.87 32.97 o
3 4 0 540.49 563.41 45.96 o
4 4 0 2.00 34.54 28.16 o
5 4 0 136.09 172.58 61.08 o
2 5 0 783.59 870.53 55.58 o
3 5 0 540.66 489.56 23.14 o
4 5 0 89.26 105.12 78.11 o
5 5 0 35.76 186.98 89.61 o
2 6 0 276.20 367.38 60.17 o
3 6 0 1711.33 1764.12 93.60 o
4 6 0 259.96 263.38 82.12 o
5 6 0 19.99 148.26 92.97 o
2 7 0 44.88 -4.12 81.73 o
4 7 0 7.53 -4.58 96.18 o
5 7 0 23.27 35.26 105.44 o
4 8 0 164.23 198.94 138.36 o
-5 0 1 24.17 -6.44 84.90 o
-3 0 1 715.07 708.83 30.52 o
-1 0 1 1080.19 1152.19 29.65 o
1 0 1 26737.24 27098.29 593.10 o
3 0 1 126.93 126.26 21.23 o
5 0 1 333.27 392.85 119.43 o
-5 1 1 40.32 20.59 30.09 o
-4 1 1 267.02 263.23 21.38 o
-3 1 1 3539.33 3469.62 63.89 o
-2 1 1 4715.10 4791.43 84.55 o
-1 1 1 247.32 276.87 8.88 o
0 1 1 386.45 395.50 15.18 o
1 1 1 20185.45 21458.25 170.15 o
2 1 1 7371.69 7556.92 168.72 o
3 1 1 444.76 403.32 18.86 o
4 1 1 0.37 14.58 20.02 o
5 1 1 0.04 25.28 81.73 o
-6 2 1 21.35 84.64 103.29 o
-5 2 1 54.09 106.59 38.71 o
-4 2 1 1.82 17.73 20.30 o
-3 2 1 479.15 471.43 15.65 o
-2 2 1 853.02 872.11 19.95 o
-1 2 1 22047.22 22793.16 558.16 o
0 2 1 3686.45 3893.79 86.74 o
1 2 1 248.63 255.14 7.72 o
2 2 1 549.56 519.69 27.91 o
3 2 1 1460.70 1491.22 40.28 o
4 2 1 270.44 242.58 38.63 o
5 2 1 1.47 36.73 51.58 o
-6 3 1 11.27 36.42 98.46 o
-5 3 1 112.64 153.60 47.09 o
-4 3 1 1.71 11.28 18.59 o
-3 3 1 444.75 450.42 24.31 o
-2 3 1 939.95 926.69 26.31 o
-1 3 1 328.50 356.71 20.68 o
0 3 1 3169.92 3044.47 89.20 o
1 3 1 500.02 551.09 16.11 o
2 3 1 99.77 127.87 21.56 o
3 3 1 2329.16 2322.99 110.16 o
4 3 1 140.56 191.56 73.64 o
5 3 1 0.03 52.25 57.78 o
-6 4 1 12.50 54.60 92.40 o
-5 4 1 55.90 6.45 40.99 o
-4 4 1 693.94 663.43 56.47 o
-3 4 1 37.62 38.09 8.20 o
-2 4 1 4163.67 4390.09 165.14 o
0 4 1 20744.89 21101.64 733.20 o
1 4 1 63.41 61.00 14.87 o
2 4 1 2997.44 3074.69 93.67 o
3 4 1 357.14 435.79 68.59 o
4 4 1 96.65 111.92 75.88 o
5 4 1 0.14 -41.75 52.51 o
-5 5 1 14.67 145.16 63.05 o
-4 5 1 213.40 229.08 33.36 o
-3 5 1 1092.51 1023.22 47.14 o
-2 5 1 536.90 381.39 244.20 o
1 5 1 4410.73 4339.03 158.85 o
2 5 1 1719.58 1547.81 98.44 o
3 5 1 270.16 206.75 58.63 o
4 5 1 369.84 341.50 53.42 o
5 5 1 20.75 63.46 87.39 o
-5 6 1 43.55 134.24 86.15 o
-4 6 1 343.54 294.63 104.79 o
-3 6 1 0.88 -45.27 57.18 o
1 6 1 1846.33 1641.97 102.25 o
2 6 1 3238.93 3310.36 175.03 o
3 6 1 210.11 216.25 48.64 o
4 6 1 269.11 257.99 83.89 o
5 6 1 70.37 -40.10 88.27 o
1 7 1 29.20 19.85 26.26 o
2 7 1 2203.03 2446.09 382.08 o
3 7 1 13.59 10.73 25.49 o
4 7 1 29.01 123.78 85.60 o
2 8 1 1149.41 1024.39 201.85 o
3 8 1 13.66 0.50 9.93 o
4 8 1 57.14 4.52 94.80 o
3 9 1 0.36 -7.04 50.47 o
-6 0 2 43.25 -29.60 96.22 o
-4 0 2 268.93 236.96 38.42 o
-2 0 2 19115.31 18716.76 530.49 o
2 0 2 1737.08 1771.79 53.10 o
4 0 2 56.83 35.72 25.93 o
-5 1 2 100.99 118.94 33.76 o
-4 1 2 27.10 47.30 22.44 o
-3 1 2 600.50 605.22 18.18 o
-2 1 2 116.45 116.97 8.81 o
-1 1 2 284.03 266.99 16.19 o
0 1 2 5783.80 5566.53 159.02 o
1 1 2 3556.99 3455.81 88.34 o
2 1 2 7357.17 7186.31 148.63 o
3 1 2 1531.05 1543.09 61.78 o
4 1 2 1.37 -10.81 16.97 o
5 1 2 51.79 162.05 120.77 o
-6 2 2 6.95 3.96 91.71 o
-5 2 2 154.30 171.63 36.46 o
-4 2 2 176.23 189.08 22.71 o
-2 2 2 1084.08 1131.72 26.09 o
-1 2 2 14797.66 15073.59 303.18 o
0 2 2 8085.84 8054.14 150.75 o
1 2 2 253.64 243.83 10.56 o
2 2 2 950.32 964.54 34.37 o
3 2 2 691.88 661.77 57.26 o
4 2 2 898.11 938.00 67.97 o
5 2 2 0.77 -12.48 55.45 o
-6 3 2 2.29 75.72 86.86 o
-5 3 2 11.39 83.31 49.86 o
-4 3 2 1434.96 1468.10 62.80 o
-3 3 2 704.08 694.87 17.76 o
-2 3 2 2145.90 2339.55 351.45 o
-1 3 2 1986.68 1938.75 45.98 o
0 3 2 18643.66 18576.06 345.08 o
1 3 2 701.74 702.85 21.87 o
2 3 2 1148.84 1148.77 38.02 o
3 3 2 272.99 288.35 71.15 o
4 3 2 44.57 122.32 54.28 o
5 3 2 3.13 5.25 55.39 o
-6 4 2 1.15 22.18 85.16 o
-5 4 2 2.36 -13.69 40.89 o
-4 4 2 0.18 -6.27 21.12 o
-3 4 2 22.67 38.42 9.03 o
-2 4 2 83.97 48.91 21.24 o
-1 4 2 1478.29 1473.68 41.43 o
0 4 2 743.91 718.08 20.79 o
1 4 2 9782.39 10148.84 205.95 o
2 4 2 388.45 406.14 29.39 o
3 4 2 1716.55 1743.90 193.65 o
4 4 2 155.38 186.97 56.01 o
5 4 2 81.47 -51.88 91.95 o
-6 5 2 0.98 7.52 81.93 o
-5 5 2 4.37 -13.01 53.56 o
-4 5 2 150.60 113.82 18.69 o
-3 5 2 3650.53 3478.58 84.44 o
-2 5 2 393.03 436.00 48.24 o
-1 5 2 5057.86 5030.68 127.63 o
0 5 2 117.04 113.18 14.29 o
1 5 2 2275.62 2227.72 54.82 o
2 5 2 2177.56 2208.01 72.60 o
3 5 2 133.38 72.25 60.82 o
4 5 2 11.87 37.00 53.74 o
5 5 2 10.49 31.28 94.40 o
-5 6 2 95.14 92.55 65.92 o
-4 6 2 5.21 19.95 19.32 o
-3 6 2 427.76 515.12 66.38 o
-2 6 2 1852.62 2027.44 102.71 o
0 6 2 2682.35 2644.30 83.71 o
1 6 2 3585.69 3697.69 101.99 o
2 6 2 149.28 124.21 14.73 o
3 6 2 39.05 104.17 67.16 o
4 6 2 192.02 305.46 83.02 o
-3 7 2 14.30 -11.35 78.56 o
-1 7 2 2639.65 3801.02 859.58 o
0 7 2 736.71 743.96 69.07 o
1 7 2 1948.75 1826.77 72.04 o
2 7 2 14.22 17.27 17.25 o
3 7 2 1538.65 1589.08 73.80 o
4 7 2 6.91 -20.86 63.84 o
1 8 2 2005.72 1890.54 177.14 o
2 8 2 380.59 435.71 39.92 o
3 8 2 23.12 68.48 42.87 o
4 8 2 12.97 30.31 60.72 o
2 9 2 1748.50 1787.59 161.22 o
3 9 2 104.17 95.49 43.68 o
3 10 2 155.52 130.65 101.04 o
-5 0 3 2.40 11.90 47.46 o
-1 0 3 14110.67 13614.43 670.98 o
-6 1 3 14.87 -12.67 66.51 o
-5 1 3 151.94 175.82 33.65 o
-4 1 3 1032.89 1113.45 101.09 o
-3 1 3 729.38 715.19 21.55 o
-2 1 3 62.61 67.57 12.11 o
-1 1 3 12346.07 12565.67 357.82 o
1 1 3 648.09 681.57 62.26 o
2 1 3 544.33 470.65 58.89 o
3 1 3 12.07 4.91 20.95 o
4 1 3 3.24 -2.18 17.46 o
5 1 3 0.39 -1.61 52.01 o
-5 2 3 92.45 84.22 30.68 o
-4 2 3 4.68 -1.33 30.30 o
-3 2 3 3958.38 3950.35 84.08 o
-2 2 3 1393.14 1380.76 62.03 o
-1 2 3 208.25 191.29 9.05 o
0 2 3 9892.07 9897.08 218.30 o
1 2 3 2482.70 2446.51 65.08 o
2 2 3 962.55 958.76 29.59 o
3 2 3 113.67 86.78 13.63 o
4 2 3 610.03 549.00 49.20 o
-6 3 3 0.23 47.88 80.83 o
-5 3 3 27.95 73.43 52.40 o
-4 3 3 38.51 21.28 29.89 o
-3 3 3 929.90 956.91 26.51 o
-2 3 3 652.27 648.07 30.38 o
-1 3 3 958.63 1002.80 24.06 o
0 3 3 139.10 141.15 7.85 o
1 3 3 14555.50 14568.65 294.25 o
2 3 3 2167.66 2139.65 54.34 o
3 3 3 534.09 464.31 46.66 o
4 3 3 54.32 68.75 33.53 o
5 3 3 183.88 220.08 105.29 o
-5 4 3 6.02 -48.23 59.17 o
-4 4 3 52.26 34.05 11.91 o
-3 4 3 511.03 494.54 31.00 o
-2 4 3 9215.91 9109.48 323.48 o
-1 4 3 434.81 393.20 16.61 o
0 4 3 707.24 704.48 18.62 o
1 4 3 1422.15 1460.30 34.26 o
2 4 3 127.14 138.76 25.30 o
3 4 3 60.90 54.11 42.66 o
4 4 3 104.63 4.96 55.15 o
5 4 3 0.14 -49.63 72.52 o
-5 5 3 95.74 97.36 60.21 o
-4 5 3 10.71 1.71 21.04 o
-3 5 3 426.98 497.49 64.52 o
-1 5 3 1470.73 1328.64 45.31 o
0 5 3 1461.71 1507.68 32.08 o
1 5 3 1258.08 1221.47 30.74 o
2 5 3 4167.39 4375.03 165.28 o
3 5 3 16.90 26.14 54.64 o
4 5 3 153.08 219.36 60.27 o
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1 6 3 6.15 -1.35 16.16 o
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0 7 3 3860.89 3813.90 102.11 o
1 7 3 526.57 490.79 33.76 o
2 7 3 69.97 50.17 25.90 o
3 7 3 0.05 18.63 66.21 o
4 7 3 29.79 41.67 62.04 o
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-2 8 3 10.45 2.77 61.08 o
0 8 3 5799.42 6061.44 378.18 o
1 8 3 234.63 275.16 24.13 o
2 8 3 560.29 584.82 32.27 o
3 8 3 662.36 569.57 81.24 o
4 8 3 159.78 316.26 94.39 o
-1 9 3 1452.26 1102.10 160.53 o
0 9 3 27.45 31.34 37.22 o
1 9 3 360.36 362.68 34.43 o
2 9 3 1272.11 1280.03 52.59 o
3 9 3 0.73 10.63 69.51 o
0 10 3 31.63 19.28 87.15 o
1 10 3 338.28 325.56 68.44 o
2 10 3 318.31 297.57 33.82 o
3 10 3 140.00 144.90 99.54 o
2 11 3 152.66 33.82 64.99 o
3 11 3 7.96 44.51 143.46 o
-6 0 4 119.76 38.29 89.38 o
-4 0 4 1379.97 1539.88 53.94 o
-2 0 4 4206.32 4256.01 219.44 o
-6 1 4 0.68 -3.87 61.00 o
-5 1 4 189.02 193.95 35.17 o
-4 1 4 20.90 37.03 17.61 o
-3 1 4 920.88 935.75 28.73 o
-2 1 4 4140.93 4048.88 120.21 o
-1 1 4 4007.25 4214.33 215.15 o
2 1 4 672.58 778.05 104.97 o
3 1 4 36.07 80.52 85.06 o
4 1 4 199.41 133.36 54.45 o
-5 2 4 0.09 -39.48 58.76 o
-4 2 4 110.29 108.73 16.36 o
-3 2 4 2015.43 2161.11 60.93 o
-2 2 4 4214.84 4317.26 125.11 o
-1 2 4 367.87 379.87 25.08 o
0 2 4 3544.48 3526.98 90.40 o
1 2 4 140.55 178.01 17.47 o
2 2 4 4229.76 4446.79 232.01 o
3 2 4 118.78 121.68 20.85 o
4 2 4 20.60 42.69 70.67 o
5 2 4 62.70 84.69 149.87 o
-5 3 4 67.31 73.96 39.95 o
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-3 3 4 154.45 171.05 49.50 o
-2 3 4 2254.73 2301.13 72.56 o
-1 3 4 1301.86 1323.02 39.61 o
0 3 4 1559.79 1538.05 32.71 o
1 3 4 2025.80 2006.62 45.02 o
2 3 4 256.62 243.30 24.70 o
3 3 4 247.85 245.79 23.33 o
4 3 4 25.53 136.36 54.16 o
5 3 4 0.53 -41.93 128.22 o
-5 4 4 13.37 -133.65 140.87 o
-4 4 4 29.25 22.56 43.03 o
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1 4 4 1167.69 1173.80 37.62 o
2 4 4 1512.89 1449.96 47.60 o
3 4 4 1607.81 1549.67 87.57 o
4 4 4 4.75 1.17 39.63 o
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-3 5 4 84.70 57.21 30.15 o
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0 5 4 3257.19 3284.15 65.45 o
1 5 4 150.40 144.29 17.12 o
2 5 4 618.90 589.06 31.10 o
3 5 4 184.43 163.07 33.51 o
4 5 4 65.90 39.37 50.56 o
-5 6 4 0.17 -58.84 70.04 o
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-3 6 4 1543.92 1529.08 91.02 o
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0 6 4 172.36 162.70 14.64 o
1 6 4 100.34 102.63 27.49 o
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3 6 4 64.01 51.12 29.68 o
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-5 7 4 3.32 25.59 71.50 o
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-3 8 4 525.18 542.19 48.76 o
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0 8 4 118.83 84.32 27.13 o
1 8 4 32.99 12.98 22.56 o
2 8 4 20.86 35.15 33.86 o
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-4 9 4 15.12 -29.97 83.72 o
-3 9 4 44.38 1.25 43.01 o
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-2 10 4 26.46 -25.27 81.21 o
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3 12 4 21.46 43.40 317.25 o
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1 5 5 228.43 212.97 23.69 o
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