#------------------------------------------------------------------------------
#$Date: 2018-04-30 19:24:07 +0300 (Mon, 30 Apr 2018) $
#$Revision: 207545 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242445.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2242445
_cell_angle_alpha                90.000
_cell_angle_beta                 100.557
_cell_angle_gamma                90.000
_cell_length_a                   3.9431
_cell_length_b                   10.7566
_cell_length_c                   9.9643
_exptl_crystal_F_000             356.00
_reflns_d_resolution_high        0.7544
_cod_data_source_file            su5433Mo-CAsphere_fsup7.hkl
_cod_data_source_block           Mo-CAsphere_f
_shelx_title                     ' '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            159.80
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 849.24 792.96 63.27 o
4 0 0 946.23 860.81 149.61 o
1 1 0 5602.38 5884.31 91.05 o
2 1 0 1381.64 1345.90 49.34 o
3 1 0 1254.63 1316.48 84.81 o
4 1 0 699.36 646.56 85.29 o
5 1 0 0.73 -185.69 185.69 o
1 2 0 7500.88 6778.49 469.27 o
2 2 0 1310.90 1249.29 56.07 o
3 2 0 579.10 576.70 53.65 o
4 2 0 4.81 -27.18 49.99 o
5 2 0 79.96 236.26 136.12 o
1 3 0 4872.55 5034.69 207.28 o
2 3 0 10177.58 9274.39 171.53 o
3 3 0 67.42 10.43 25.76 o
4 3 0 29.22 249.50 136.65 o
5 3 0 40.65 265.07 202.32 o
1 4 0 839.61 1297.78 312.89 o
2 4 0 224.37 220.69 35.57 o
3 4 0 551.09 530.50 85.38 o
4 4 0 3.77 -9.14 107.91 o
3 5 0 582.23 481.06 68.35 o
4 5 0 87.51 277.54 195.16 o
2 6 0 246.98 49.95 82.33 o
3 6 0 1950.60 2352.96 293.70 o
4 6 0 286.75 446.40 359.87 o
4 7 0 17.26 1464.17 665.20 o
-5 0 1 21.44 4.46 347.34 o
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1 0 1 25537.44 24318.82 347.25 o
3 0 1 116.46 71.63 52.25 o
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0 1 1 355.28 402.54 18.99 o
1 1 1 19628.73 20669.17 211.68 o
2 1 1 7239.24 7258.85 204.06 o
3 1 1 432.54 431.41 54.63 o
4 1 1 0.12 16.77 69.68 o
5 1 1 0.16 493.86 183.92 o
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0 2 1 3668.21 3784.90 61.01 o
1 2 1 286.08 274.16 17.32 o
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3 2 1 1501.67 1372.26 114.93 o
4 2 1 216.82 211.39 86.26 o
5 2 1 0.72 568.10 337.58 o
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1 3 1 517.58 491.95 30.87 o
2 3 1 75.35 68.84 23.05 o
3 3 1 2078.56 2624.19 248.01 o
4 3 1 151.18 153.85 81.98 o
-4 4 1 827.84 694.63 327.04 o
-3 4 1 30.35 117.73 50.00 o
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2 4 1 3140.52 3035.09 95.79 o
3 4 1 392.22 323.11 75.47 o
4 4 1 93.32 61.91 115.34 o
-4 5 1 193.61 376.33 127.27 o
-3 5 1 1165.14 1463.09 153.54 o
1 5 1 4566.74 5219.48 185.01 o
2 5 1 1693.10 1621.61 98.96 o
3 5 1 281.14 202.34 77.92 o
4 5 1 375.61 631.15 168.78 o
-4 6 1 388.85 143.58 159.58 o
1 6 1 1979.92 1799.59 156.72 o
2 6 1 3446.28 4037.76 171.41 o
3 6 1 252.32 215.11 70.88 o
4 6 1 287.72 141.81 144.49 o
3 7 1 7.00 216.97 90.04 o
4 7 1 42.52 -103.92 133.31 o
3 8 1 22.04 -17.85 222.85 o
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-2 0 2 18688.51 18908.26 302.04 o
2 0 2 1722.62 1631.81 130.06 o
4 0 2 47.25 61.88 154.25 o
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-3 1 2 631.32 681.01 54.07 o
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-1 1 2 322.17 316.67 20.35 o
1 1 2 3329.33 3187.92 191.07 o
2 1 2 6736.50 6805.74 321.27 o
3 1 2 1397.70 1397.53 156.53 o
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0 2 2 7834.73 7931.33 90.37 o
1 2 2 250.86 231.03 21.18 o
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3 2 2 721.48 923.47 118.23 o
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-5 3 2 15.05 -61.12 278.13 o
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1 3 2 713.84 682.49 40.86 o
2 3 2 1152.48 1334.17 97.99 o
3 3 2 291.49 145.62 106.75 o
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-4 4 2 1.47 -6.02 57.00 o
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0 4 2 713.81 712.43 37.33 o
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2 4 2 408.92 446.92 49.39 o
3 4 2 1635.89 1693.75 318.14 o
4 4 2 148.93 54.83 201.00 o
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-2 5 2 453.13 402.65 55.35 o
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1 5 2 2309.20 1866.07 77.41 o
2 5 2 2089.96 2109.75 116.40 o
3 5 2 143.30 204.53 92.82 o
4 5 2 12.43 -91.37 142.08 o
-2 6 2 1951.49 2439.84 243.96 o
-1 6 2 3862.05 4572.45 700.64 o
0 6 2 2817.21 3346.58 270.11 o
1 6 2 3715.55 3007.68 216.45 o
2 6 2 147.55 108.34 35.38 o
3 6 2 38.51 -29.99 108.92 o
4 6 2 197.14 113.06 244.33 o
0 7 2 879.64 701.21 148.59 o
1 7 2 2005.79 2365.14 181.22 o
2 7 2 12.49 29.24 53.10 o
3 7 2 1645.42 1914.86 243.19 o
4 7 2 16.34 79.87 163.67 o
2 8 2 435.84 449.73 121.92 o
3 8 2 44.09 293.69 285.21 o
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-5 0 3 0.79 100.89 94.22 o
-3 0 3 51.83 79.33 50.65 o
-5 1 3 172.00 204.57 134.82 o
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-2 1 3 42.81 59.45 12.78 o
-1 1 3 11574.21 11811.13 245.06 o
1 1 3 572.43 605.42 143.77 o
2 1 3 458.10 515.77 82.18 o
3 1 3 5.82 -41.22 48.61 o
-5 2 3 95.72 181.23 188.70 o
-4 2 3 9.08 63.65 54.84 o
-3 2 3 3911.37 3717.88 130.19 o
-2 2 3 1335.37 1414.82 89.68 o
-1 2 3 184.55 135.57 16.04 o
0 2 3 9494.42 9687.28 194.46 o
1 2 3 2373.21 2299.78 184.14 o
2 2 3 865.21 890.05 103.85 o
3 2 3 96.07 39.57 79.65 o
4 2 3 581.63 309.71 209.51 o
-5 3 3 28.64 -56.53 308.41 o
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-3 3 3 997.22 904.62 75.13 o
-2 3 3 719.14 709.28 68.82 o
-1 3 3 1003.72 993.43 53.27 o
0 3 3 129.59 116.71 15.74 o
1 3 3 13531.92 13415.07 234.82 o
2 3 3 2033.56 2188.55 148.52 o
3 3 3 503.21 750.49 173.89 o
4 3 3 49.65 21.37 85.37 o
-4 4 3 71.24 121.92 66.77 o
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-1 4 3 444.77 497.05 55.84 o
1 4 3 1354.01 1360.89 76.01 o
2 4 3 152.17 160.51 49.29 o
3 4 3 55.35 271.14 109.16 o
4 4 3 82.09 18.77 131.17 o
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1 8 3 297.87 437.37 76.96 o
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1 2 4 128.13 147.12 52.69 o
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