#------------------------------------------------------------------------------
#$Date: 2018-04-30 19:24:07 +0300 (Mon, 30 Apr 2018) $
#$Revision: 207545 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242448.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2242448
_cell_angle_alpha                90.000
_cell_angle_beta                 100.557
_cell_angle_gamma                90.000
_cell_length_a                   3.9431
_cell_length_b                   10.7566
_cell_length_c                   9.9643
_exptl_crystal_F_000             356.00
_reflns_d_resolution_high        0.7544
_cod_data_source_file            su5433Mo-CAsphere-Ciso_isup10.hkl
_cod_data_source_block           Mo-CAsphere-Ciso_i
_shelx_title                     ' '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            160.24
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 853.30 792.98 63.27 o
4 0 0 976.70 860.83 149.61 o
1 1 0 5591.31 5884.47 91.05 o
2 1 0 1384.66 1345.93 49.34 o
3 1 0 1251.23 1316.52 84.82 o
4 1 0 691.34 646.58 85.30 o
5 1 0 0.21 -185.69 185.69 o
1 2 0 7525.25 6778.67 469.28 o
2 2 0 1296.09 1249.32 56.07 o
3 2 0 584.71 576.71 53.65 o
4 2 0 4.38 -27.18 49.99 o
5 2 0 72.00 236.26 136.12 o
1 3 0 4826.29 5034.81 207.29 o
2 3 0 10229.97 9274.63 171.53 o
3 3 0 60.36 10.43 25.76 o
4 3 0 25.63 249.50 136.65 o
5 3 0 36.37 265.07 202.32 o
1 4 0 851.74 1297.81 312.90 o
2 4 0 237.63 220.70 35.57 o
3 4 0 539.38 530.52 85.38 o
4 4 0 1.23 -9.14 107.91 o
3 5 0 615.64 481.07 68.36 o
4 5 0 87.23 277.55 195.17 o
2 6 0 255.02 49.96 82.33 o
3 6 0 1885.14 2353.02 293.71 o
4 6 0 292.72 446.41 359.88 o
4 7 0 10.50 1464.20 665.22 o
-5 0 1 14.34 4.46 347.35 o
-3 0 1 569.65 684.72 81.45 o
-1 0 1 1146.20 1234.25 32.48 o
1 0 1 25676.74 24319.45 347.26 o
3 0 1 129.74 71.63 52.25 o
-5 1 1 43.68 107.43 98.70 o
-4 1 1 245.44 247.17 53.46 o
-3 1 1 3676.65 3652.36 119.40 o
-2 1 1 4663.92 4723.06 80.43 o
-1 1 1 217.93 274.95 16.81 o
0 1 1 362.85 402.55 18.99 o
1 1 1 19680.86 20669.71 211.68 o
2 1 1 7365.15 7259.03 204.07 o
3 1 1 430.00 431.42 54.63 o
4 1 1 0.21 16.77 69.68 o
5 1 1 0.17 493.87 183.93 o
-5 2 1 57.52 142.05 116.26 o
-4 2 1 5.94 -60.80 69.63 o
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-2 2 1 769.76 741.85 34.09 o
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0 2 1 3655.59 3785.00 61.01 o
1 2 1 284.72 274.17 17.32 o
2 2 1 492.78 454.35 59.37 o
3 2 1 1553.61 1372.29 114.93 o
4 2 1 222.99 211.40 86.26 o
5 2 1 1.24 568.11 337.59 o
-5 3 1 94.24 244.98 328.73 o
-4 3 1 0.67 -19.52 105.18 o
-3 3 1 465.05 474.39 44.04 o
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-1 3 1 414.90 461.38 60.53 o
0 3 1 3219.67 4104.32 435.03 o
1 3 1 506.99 491.97 30.87 o
2 3 1 78.17 68.84 23.06 o
3 3 1 2104.32 2624.26 248.01 o
4 3 1 136.54 153.86 81.99 o
-4 4 1 809.02 694.65 327.05 o
-3 4 1 40.77 117.73 50.00 o
-2 4 1 4348.85 5321.49 379.73 o
-1 4 1 3886.62 5143.21 619.20 o
2 4 1 3107.38 3035.17 95.79 o
3 4 1 375.83 323.12 75.47 o
4 4 1 99.96 61.91 115.34 o
-4 5 1 174.46 376.34 127.28 o
-3 5 1 1165.91 1463.13 153.54 o
1 5 1 4521.59 5219.61 185.01 o
2 5 1 1680.21 1621.65 98.96 o
3 5 1 279.84 202.34 77.92 o
4 5 1 386.68 631.17 168.79 o
-4 6 1 373.57 143.58 159.59 o
1 6 1 1950.83 1799.63 156.72 o
2 6 1 3397.95 4037.87 171.41 o
3 6 1 263.95 215.11 70.88 o
4 6 1 271.31 141.81 144.50 o
3 7 1 13.08 216.98 90.04 o
4 7 1 44.94 -103.92 133.32 o
3 8 1 20.10 -17.85 222.85 o
-4 0 2 264.87 241.85 133.40 o
-2 0 2 18670.69 18908.75 302.05 o
2 0 2 1665.42 1631.85 130.06 o
4 0 2 62.81 61.89 154.25 o
-5 1 2 98.23 136.07 95.24 o
-4 1 2 41.36 9.85 67.67 o
-3 1 2 618.12 681.02 54.07 o
-2 1 2 181.73 207.14 19.63 o
-1 1 2 316.61 316.68 20.35 o
1 1 2 3292.65 3188.00 191.07 o
2 1 2 6750.24 6805.92 321.28 o
3 1 2 1480.85 1397.57 156.53 o
4 1 2 1.82 180.93 111.55 o
-5 2 2 163.29 106.92 101.06 o
-4 2 2 153.33 189.27 67.84 o
-3 2 2 452.77 418.63 33.27 o
-2 2 2 1092.85 1120.54 63.34 o
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0 2 2 7822.75 7931.53 90.37 o
1 2 2 252.81 231.04 21.18 o
2 2 2 965.93 1115.19 95.41 o
3 2 2 730.19 923.49 118.24 o
4 2 2 855.25 720.14 170.75 o
-5 3 2 15.49 -61.12 278.14 o
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-2 3 2 2224.07 2028.42 182.78 o
-1 3 2 2085.91 1922.93 62.38 o
0 3 2 17906.33 17352.43 152.15 o
1 3 2 714.61 682.51 40.86 o
2 3 2 1153.41 1334.20 97.99 o
3 3 2 273.41 145.62 106.76 o
4 3 2 72.26 -3.47 88.69 o
-4 4 2 0.83 -6.02 57.01 o
-2 4 2 92.93 55.41 19.27 o
-1 4 2 1524.01 1255.93 77.41 o
0 4 2 750.46 712.45 37.33 o
1 4 2 9733.75 8507.64 155.43 o
2 4 2 399.67 446.93 49.39 o
3 4 2 1646.98 1693.79 318.15 o
4 4 2 142.21 54.83 201.00 o
-4 5 2 143.42 -19.02 80.10 o
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-2 5 2 464.41 402.66 55.35 o
-1 5 2 5242.37 5826.13 267.72 o
1 5 2 2357.08 1866.12 77.41 o
2 5 2 2138.67 2109.80 116.41 o
3 5 2 138.80 204.53 92.82 o
4 5 2 9.03 -91.37 142.08 o
-2 6 2 1902.11 2439.90 243.97 o
-1 6 2 3991.14 4572.57 700.66 o
0 6 2 2865.97 3346.66 270.12 o
1 6 2 3689.23 3007.76 216.46 o
2 6 2 135.40 108.34 35.39 o
3 6 2 27.55 -29.99 108.92 o
4 6 2 211.91 113.07 244.34 o
0 7 2 831.75 701.23 148.59 o
1 7 2 1972.84 2365.20 181.22 o
2 7 2 19.94 29.24 53.10 o
3 7 2 1695.28 1914.91 243.19 o
4 7 2 11.62 79.87 163.67 o
2 8 2 428.90 449.75 121.92 o
3 8 2 34.76 293.69 285.22 o
3 9 2 103.81 -167.62 196.19 o
-5 0 3 0.72 100.90 94.22 o
-3 0 3 50.34 79.33 50.65 o
-5 1 3 165.08 204.57 134.82 o
-4 1 3 1036.06 920.12 113.44 o
-3 1 3 655.79 805.52 66.15 o
-2 1 3 41.47 59.45 12.78 o
-1 1 3 11611.21 11811.44 245.07 o
1 1 3 571.92 605.44 143.78 o
2 1 3 451.23 515.78 82.18 o
3 1 3 5.58 -41.22 48.61 o
-5 2 3 96.54 181.23 188.71 o
-4 2 3 11.40 63.65 54.85 o
-3 2 3 3910.08 3717.97 130.19 o
-2 2 3 1339.96 1414.86 89.68 o
-1 2 3 189.27 135.57 16.04 o
0 2 3 9486.99 9687.53 194.47 o
1 2 3 2358.37 2299.84 184.15 o
2 2 3 861.84 890.08 103.86 o
3 2 3 107.04 39.57 79.65 o
4 2 3 595.16 309.72 209.52 o
-5 3 3 23.45 -56.54 308.41 o
-4 3 3 36.68 29.15 60.38 o
-3 3 3 1001.80 904.65 75.13 o
-2 3 3 725.61 709.30 68.82 o
-1 3 3 1012.43 993.46 53.27 o
0 3 3 126.29 116.71 15.74 o
1 3 3 13532.23 13415.41 234.83 o
2 3 3 2050.16 2188.61 148.52 o
3 3 3 518.85 750.51 173.90 o
4 3 3 43.96 21.37 85.37 o
-4 4 3 65.86 121.92 66.77 o
-3 4 3 498.21 510.61 68.45 o
-2 4 3 8876.40 8436.21 278.86 o
-1 4 3 423.89 497.06 55.84 o
1 4 3 1346.50 1360.93 76.01 o
2 4 3 141.81 160.51 49.29 o
3 4 3 59.47 271.14 109.16 o
4 4 3 97.34 18.77 131.17 o
-4 5 3 10.87 169.87 98.53 o
-3 5 3 419.58 510.92 84.01 o
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0 5 3 1417.07 1505.02 67.61 o
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2 5 3 4010.17 4172.47 235.73 o
3 5 3 15.07 -53.50 123.38 o
4 5 3 126.75 510.85 184.03 o
-4 6 3 7.60 159.11 227.81 o
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0 6 3 7215.12 6771.47 545.75 o
1 6 3 8.84 1.46 40.74 o
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3 6 3 380.85 533.91 165.09 o
4 6 3 133.91 248.18 240.18 o
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-1 7 3 262.75 302.27 60.26 o
0 7 3 4072.41 4477.25 181.95 o
1 7 3 581.29 599.30 79.41 o
2 7 3 91.76 62.38 51.76 o
3 7 3 0.06 2.28 105.61 o
-1 8 3 1970.00 2196.66 252.84 o
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1 8 3 267.21 437.38 76.96 o
2 8 3 579.54 630.11 108.13 o
3 8 3 675.14 967.42 220.32 o
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3 9 3 0.38 120.53 164.25 o
2 10 3 399.70 693.75 451.30 o
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-1 2 4 368.60 303.30 57.92 o
0 2 4 3255.01 2834.04 125.88 o
1 2 4 124.78 147.12 52.69 o
2 2 4 3646.79 3897.23 216.82 o
3 2 4 93.31 618.14 304.90 o
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3 9 4 60.35 -71.96 232.83 o
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