#------------------------------------------------------------------------------ #$Date: 2018-04-30 19:27:26 +0300 (Mon, 30 Apr 2018) $ #$Revision: 207553 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242460.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242460 _cell_angle_alpha 90.000 _cell_angle_beta 90.396 _cell_angle_gamma 90.000 _cell_length_a 13.8129 _cell_length_b 12.6034 _cell_length_c 8.3595 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7918 _cod_data_source_file xi2002Isup2.hkl _cod_data_source_block I _shelx_title ' TFAP in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 318.33 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3008.95 2718.77 14.84 o 4 0 0 101334.30 97839.48 492.15 o 6 0 0 998.08 989.38 6.73 o 8 0 0 10828.25 11232.85 54.61 o 10 0 0 176.64 173.98 3.30 o 12 0 0 982.49 990.47 9.10 o 14 0 0 141.56 141.10 5.18 o 16 0 0 171.83 179.45 5.82 o 1 1 0 2409.89 2341.29 9.17 o 3 1 0 2992.95 2732.33 9.75 o 5 1 0 5084.58 4935.84 17.90 o 7 1 0 2121.77 2111.64 7.92 o 9 1 0 1591.84 1583.23 7.83 o 11 1 0 184.17 172.42 2.72 o 13 1 0 2057.41 2046.41 11.47 o 15 1 0 0.24 -1.52 1.52 o 17 1 0 7.42 2.54 1.86 o 0 2 0 5417.52 5317.02 29.17 o 2 2 0 338.89 324.40 1.78 o 4 2 0 22995.36 23138.12 83.13 o 6 2 0 1921.48 1923.35 7.64 o 8 2 0 8319.54 8715.96 30.44 o 10 2 0 8.75 16.28 1.12 o 12 2 0 2081.21 2136.00 11.53 o 14 2 0 15.73 13.19 1.65 o 16 2 0 348.76 327.20 4.88 o 1 3 0 2430.17 2547.21 9.70 o 3 3 0 0.99 1.07 0.67 o 5 3 0 1091.61 1138.85 4.92 o 7 3 0 1188.69 1214.06 5.96 o 9 3 0 348.94 397.12 3.31 o 11 3 0 1.94 3.09 0.95 o 13 3 0 6.19 3.81 1.34 o 15 3 0 1.77 0.92 1.38 o 17 3 0 9.39 12.25 2.45 o 0 4 0 512.73 452.46 3.99 o 2 4 0 615.80 571.71 3.32 o 4 4 0 30.46 38.49 0.88 o 6 4 0 236.16 211.07 1.79 o 8 4 0 248.98 261.24 2.51 o 10 4 0 46.93 42.08 1.45 o 12 4 0 358.49 372.50 3.89 o 14 4 0 335.11 344.78 5.12 o 16 4 0 160.14 155.39 3.45 o 1 5 0 113.96 91.50 1.20 o 3 5 0 2761.29 2575.68 11.78 o 5 5 0 3741.24 3754.53 15.41 o 7 5 0 60.09 43.39 1.20 o 9 5 0 1601.45 1630.49 8.62 o 11 5 0 60.05 47.51 1.58 o 13 5 0 1041.14 1024.72 6.92 o 15 5 0 51.00 50.73 2.22 o 0 6 0 19542.06 19427.27 98.65 o 2 6 0 2381.90 2308.74 9.64 o 4 6 0 1013.39 1021.22 5.53 o 6 6 0 226.44 211.27 2.33 o 8 6 0 132.95 120.65 2.29 o 10 6 0 603.88 557.01 4.58 o 12 6 0 0.11 -1.26 1.26 o 14 6 0 168.21 143.07 3.02 o 16 6 0 0.69 -1.34 1.78 o 1 7 0 2715.84 2858.94 12.23 o 3 7 0 991.96 1003.16 5.37 o 5 7 0 8.63 19.35 1.01 o 7 7 0 1010.00 1003.70 6.65 o 9 7 0 226.22 235.39 3.19 o 11 7 0 34.23 29.42 1.67 o 13 7 0 68.92 62.18 2.24 o 15 7 0 35.33 39.35 2.13 o 0 8 0 1209.82 1091.55 8.64 o 2 8 0 88.25 85.65 1.60 o 4 8 0 1280.42 1314.68 7.25 o 6 8 0 1393.48 1372.16 8.34 o 8 8 0 410.10 398.43 4.14 o 10 8 0 6.79 7.39 1.26 o 12 8 0 98.05 82.73 3.52 o 14 8 0 43.47 40.18 2.44 o 1 9 0 294.63 290.10 2.83 o 3 9 0 119.30 120.80 4.06 o 5 9 0 49.01 44.19 1.62 o 7 9 0 1158.41 1139.69 7.74 o 9 9 0 190.26 184.68 3.14 o 11 9 0 162.72 196.63 3.90 o 13 9 0 32.19 33.72 2.15 o 0 10 0 18.65 23.42 2.14 o 2 10 0 257.35 249.09 3.04 o 4 10 0 643.62 662.71 5.42 o 6 10 0 1752.76 1769.72 10.63 o 8 10 0 156.55 159.76 3.60 o 10 10 0 116.85 118.88 3.42 o 12 10 0 0.89 3.46 1.59 o 1 11 0 22.45 15.85 1.24 o 3 11 0 573.71 593.75 5.00 o 5 11 0 242.34 239.35 3.51 o 7 11 0 884.53 928.63 7.28 o 9 11 0 48.34 44.43 2.35 o 11 11 0 85.45 80.65 3.01 o 0 12 0 5.54 1.43 1.47 o 2 12 0 120.86 123.07 2.57 o 4 12 0 65.16 54.79 2.09 o 6 12 0 3.93 2.11 1.44 o 8 12 0 1.71 1.85 1.47 o 10 12 0 46.89 46.10 2.67 o 1 13 0 98.84 90.67 2.68 o 3 13 0 1.94 0.22 1.32 o 5 13 0 202.56 206.91 3.94 o 7 13 0 17.96 17.94 1.83 o 9 13 0 3.39 4.40 1.88 o 0 14 0 11.83 6.21 1.92 o 2 14 0 58.79 52.88 2.39 o 4 14 0 120.97 126.39 3.48 o 6 14 0 42.40 56.57 2.88 o 8 14 0 21.86 29.53 2.83 o 1 15 0 4.74 9.21 1.79 o 3 15 0 90.46 113.40 3.55 o 5 15 0 0.16 0.26 1.74 o -17 1 1 32.88 29.94 2.40 o -15 1 1 42.63 36.45 2.63 o -13 1 1 399.64 411.36 4.24 o -11 1 1 93.01 92.81 2.13 o -9 1 1 38.21 40.10 1.33 o -7 1 1 1429.57 1386.50 5.69 o -5 1 1 41.30 38.10 0.72 o -3 1 1 31.67 27.54 0.84 o -1 1 1 1587.82 1526.46 8.84 o 1 1 1 9399.39 9199.75 87.08 o 3 1 1 16365.49 16118.35 57.84 o 5 1 1 2437.60 2508.33 9.60 o 7 1 1 8754.45 9154.85 30.61 o 9 1 1 1450.67 1528.94 7.55 o 11 1 1 7750.52 7997.37 34.55 o 13 1 1 116.82 113.78 2.86 o 15 1 1 2211.42 2135.01 13.60 o 17 1 1 133.61 119.25 3.85 o -16 2 1 0.00 2.15 1.60 o -14 2 1 13.17 12.56 1.52 o -12 2 1 103.91 88.92 2.22 o -10 2 1 93.31 86.70 1.85 o -8 2 1 2.42 2.56 0.54 o -6 2 1 1995.94 1856.97 7.42 o -4 2 1 2422.45 2332.74 9.22 o -2 2 1 18858.14 18084.66 64.98 o 0 2 1 3013.29 2930.33 14.34 o 2 2 1 11869.56 11379.90 40.68 o 4 2 1 194.94 231.66 1.64 o 6 2 1 1529.52 1562.41 6.40 o 8 2 1 187.04 185.45 1.85 o 10 2 1 404.65 397.54 3.64 o 12 2 1 31.82 32.52 1.62 o 14 2 1 795.20 824.65 7.13 o 16 2 1 307.26 317.73 4.88 o -17 3 1 107.13 91.33 5.26 o -15 3 1 282.84 264.31 4.26 o -13 3 1 45.77 50.15 2.00 o -11 3 1 543.84 543.53 4.34 o -9 3 1 1541.53 1505.75 7.87 o -7 3 1 8269.27 8227.57 31.80 o -5 3 1 408.50 384.46 2.32 o -3 3 1 1074.21 1073.80 5.15 o -1 3 1 1590.60 1571.62 6.29 o 1 3 1 8190.72 7966.00 28.65 o 3 3 1 3.36 0.91 0.29 o 5 3 1 364.86 420.59 2.47 o 7 3 1 1079.41 1180.38 5.56 o 9 3 1 0.15 0.00 0.75 o 11 3 1 720.69 661.80 4.92 o 13 3 1 519.80 564.75 5.11 o 15 3 1 44.84 43.49 2.38 o 17 3 1 0.39 -2.29 2.29 o -16 4 1 0.51 1.14 1.43 o -14 4 1 212.98 220.90 3.53 o -12 4 1 434.79 409.42 3.75 o -10 4 1 181.34 167.33 2.21 o -8 4 1 76.62 69.83 1.59 o -6 4 1 711.61 716.72 3.79 o -4 4 1 3359.33 3259.78 13.82 o -2 4 1 24140.84 23549.03 95.18 o 0 4 1 2675.88 2671.25 11.17 o 2 4 1 14530.38 14200.09 57.26 o 4 4 1 867.24 907.98 4.72 o 6 4 1 4241.36 4186.25 15.27 o 8 4 1 185.91 208.84 2.24 o 10 4 1 3.17 0.64 0.88 o 12 4 1 149.61 140.62 2.62 o 14 4 1 200.67 194.61 3.37 o 16 4 1 8.25 5.79 1.61 o -15 5 1 1.49 1.01 1.36 o -13 5 1 679.60 696.55 5.56 o -11 5 1 25.74 25.99 1.33 o -9 5 1 164.44 170.92 2.35 o -7 5 1 485.49 460.78 3.27 o -5 5 1 320.56 322.39 2.55 o -3 5 1 2438.14 2478.03 11.42 o -1 5 1 190.03 176.39 1.80 o 1 5 1 13798.63 13832.77 56.09 o 3 5 1 114.00 118.63 1.50 o 5 5 1 15.03 10.16 0.68 o 7 5 1 1882.47 1915.47 8.65 o 9 5 1 158.23 138.32 2.26 o 11 5 1 585.45 557.19 4.30 o 13 5 1 48.88 44.17 1.87 o 15 5 1 140.44 126.11 3.54 o -16 6 1 5.83 3.01 2.68 o -14 6 1 0.00 -0.14 1.34 o -12 6 1 44.60 40.97 1.62 o -10 6 1 485.29 487.29 4.24 o -8 6 1 391.82 408.50 3.85 o -6 6 1 6979.57 6997.32 28.77 o -4 6 1 905.11 922.76 5.30 o -2 6 1 2887.59 3067.65 12.29 o 0 6 1 3813.17 3849.79 15.56 o 2 6 1 4293.01 4506.77 17.33 o 4 6 1 719.78 632.41 4.03 o 6 6 1 1268.49 1338.70 7.06 o 8 6 1 586.22 553.79 4.57 o 10 6 1 565.01 548.26 4.52 o 12 6 1 172.90 167.81 2.70 o 14 6 1 322.79 302.10 3.96 o 16 6 1 126.92 107.64 4.02 o -15 7 1 0.16 0.22 1.48 o -13 7 1 124.19 130.36 2.98 o -11 7 1 6.93 3.87 1.26 o -9 7 1 22.50 20.35 1.33 o -7 7 1 137.67 128.65 2.31 o -5 7 1 692.86 654.63 4.59 o -3 7 1 27.92 29.93 0.99 o -1 7 1 295.05 242.24 2.29 o 1 7 1 636.26 666.44 3.97 o 3 7 1 921.28 960.00 5.27 o 5 7 1 3322.79 3320.84 14.82 o 7 7 1 3007.48 3016.19 15.28 o 9 7 1 911.20 905.16 6.62 o 11 7 1 503.95 493.58 5.01 o 13 7 1 59.60 42.43 2.03 o 15 7 1 55.85 42.00 2.19 o -14 8 1 0.08 2.24 1.73 o -12 8 1 9.55 5.39 1.59 o -10 8 1 24.25 23.94 1.67 o -8 8 1 213.03 218.06 4.84 o -6 8 1 0.96 2.88 0.94 o -4 8 1 2706.23 2708.18 12.65 o -2 8 1 172.02 148.25 1.93 o 0 8 1 579.12 554.42 3.86 o 2 8 1 103.94 121.29 1.76 o 4 8 1 262.06 234.27 3.19 o 6 8 1 352.24 361.44 3.76 o 8 8 1 783.50 758.44 5.92 o 10 8 1 471.16 465.88 4.77 o 12 8 1 52.44 44.59 2.31 o 14 8 1 197.66 198.50 4.50 o -13 9 1 19.32 21.98 2.08 o -11 9 1 97.58 93.98 3.06 o -9 9 1 0.39 -1.08 1.10 o -7 9 1 813.05 838.41 6.34 o -5 9 1 560.56 565.54 4.77 o -3 9 1 494.34 475.26 3.97 o -1 9 1 1330.89 1323.83 7.06 o 1 9 1 141.28 142.64 2.13 o 3 9 1 0.42 1.80 0.90 o 5 9 1 3.28 3.26 0.96 o 7 9 1 9.76 9.42 1.42 o 9 9 1 146.13 146.19 2.88 o 11 9 1 90.61 86.15 2.88 o 13 9 1 42.21 38.18 2.33 o -12 10 1 280.06 320.23 5.08 o -10 10 1 61.81 60.13 2.49 o -8 10 1 802.36 850.91 6.73 o -6 10 1 626.47 621.35 5.39 o -4 10 1 0.01 0.10 0.94 o -2 10 1 558.80 572.10 4.64 o 0 10 1 887.76 880.06 6.27 o 2 10 1 55.57 60.08 1.81 o 4 10 1 2.42 5.07 1.01 o 6 10 1 255.08 270.42 3.51 o 8 10 1 21.90 20.98 1.63 o 10 10 1 65.45 67.30 2.61 o 12 10 1 43.02 36.81 2.40 o -11 11 1 137.48 135.02 4.01 o -9 11 1 133.79 143.39 3.51 o -7 11 1 133.56 132.94 2.97 o -5 11 1 148.70 151.61 2.88 o -3 11 1 93.71 77.58 2.35 o -1 11 1 23.49 18.91 1.22 o 1 11 1 5.84 1.48 0.92 o 3 11 1 87.60 83.57 2.15 o 5 11 1 1194.39 1195.55 8.25 o 7 11 1 345.47 332.27 4.19 o 9 11 1 15.58 13.73 1.79 o 11 11 1 52.86 50.96 2.85 o -10 12 1 102.01 99.33 3.63 o -8 12 1 9.11 3.30 1.55 o -6 12 1 273.79 277.72 4.38 o -4 12 1 75.58 59.89 2.20 o -2 12 1 34.45 28.68 1.52 o 0 12 1 123.26 132.42 2.82 o 2 12 1 101.39 98.14 2.54 o 4 12 1 738.14 752.91 6.36 o 6 12 1 5.17 5.18 1.51 o 8 12 1 447.20 480.98 5.97 o 10 12 1 18.06 19.49 2.87 o -9 13 1 10.41 4.64 1.96 o -7 13 1 28.35 22.35 2.11 o -5 13 1 72.07 74.48 2.75 o -3 13 1 486.93 430.45 5.00 o -1 13 1 4.83 3.20 1.32 o 1 13 1 558.35 512.59 5.51 o 3 13 1 97.71 97.72 2.84 o 5 13 1 51.06 60.02 2.53 o 7 13 1 836.64 861.16 8.15 o 9 13 1 10.62 15.61 2.22 o -8 14 1 3.32 2.68 2.57 o -6 14 1 461.89 502.32 6.80 o -4 14 1 112.62 96.56 3.50 o -2 14 1 225.13 268.14 4.30 o 0 14 1 201.89 173.15 3.64 o 2 14 1 241.52 271.91 4.30 o 4 14 1 113.08 140.27 3.67 o 6 14 1 122.02 148.36 5.35 o 8 14 1 180.51 204.07 6.22 o -5 15 1 430.18 490.55 8.32 o -3 15 1 99.68 117.20 5.58 o -1 15 1 316.34 367.21 5.52 o 1 15 1 54.04 62.52 2.88 o 3 15 1 8.58 11.13 2.12 o 5 15 1 43.76 41.32 2.86 o -16 0 2 10.81 16.19 2.98 o -14 0 2 160.03 159.06 4.96 o -12 0 2 605.25 645.86 6.95 o -10 0 2 11.38 9.78 1.32 o -8 0 2 1326.11 1256.17 8.24 o -6 0 2 4923.60 4822.31 25.88 o -4 0 2 3260.67 3126.97 22.32 o 4 0 2 22854.14 23021.62 137.32 o 6 0 2 141.09 132.84 2.01 o 8 0 2 3450.56 3416.47 18.32 o 10 0 2 12.04 12.42 1.38 o 12 0 2 1143.95 1246.62 11.62 o 14 0 2 883.02 911.85 10.50 o 16 0 2 122.48 106.18 6.30 o -17 1 2 7.69 9.00 2.05 o -15 1 2 282.90 288.36 4.47 o -13 1 2 294.41 324.49 3.83 o -11 1 2 51.09 43.19 1.78 o -9 1 2 1196.59 1197.88 6.71 o -7 1 2 7.43 8.21 0.50 o -5 1 2 4852.94 4853.44 17.61 o -3 1 2 49.72 47.72 0.81 o 3 1 2 1851.73 1734.72 8.13 o 5 1 2 2444.33 2442.93 9.39 o 7 1 2 3509.15 3481.50 12.97 o 9 1 2 654.24 685.73 4.31 o 11 1 2 326.34 345.57 3.64 o 13 1 2 234.03 241.51 3.34 o 15 1 2 45.81 56.36 2.57 o 17 1 2 23.06 19.27 2.31 o -16 2 2 36.75 33.39 2.26 o -14 2 2 5.18 7.47 1.48 o -12 2 2 178.59 185.04 2.87 o -10 2 2 3.16 5.62 1.13 o -8 2 2 2035.55 2034.09 8.47 o -6 2 2 3581.29 3559.61 13.10 o -4 2 2 834.37 827.71 3.87 o -2 2 2 20.73 28.14 0.70 o 0 2 2 1293.45 1347.61 9.92 o 2 2 2 506.42 512.78 3.69 o 4 2 2 366.96 368.75 2.35 o 6 2 2 1358.35 1392.99 6.05 o 8 2 2 75.41 88.73 1.43 o 10 2 2 65.51 60.93 1.67 o 12 2 2 712.14 700.65 5.44 o 14 2 2 55.76 54.98 2.35 o 16 2 2 3.15 3.97 1.65 o -15 3 2 0.05 -0.24 1.41 o -13 3 2 65.88 65.73 2.16 o -11 3 2 3.02 7.13 1.05 o -9 3 2 876.24 929.28 5.60 o -7 3 2 89.42 111.05 1.57 o -5 3 2 1153.77 1206.95 5.36 o -3 3 2 1319.39 1298.42 6.62 o -1 3 2 236.97 243.01 1.94 o 1 3 2 2092.16 2130.27 10.94 o 3 3 2 128.39 120.99 1.35 o 5 3 2 764.03 805.72 3.91 o 7 3 2 312.53 298.52 2.27 o 9 3 2 153.83 184.47 2.86 o 11 3 2 9.53 6.25 1.11 o 13 3 2 1.81 0.58 1.24 o 15 3 2 0.59 -0.42 1.48 o -16 4 2 11.10 10.91 1.75 o -14 4 2 49.36 37.60 1.91 o -12 4 2 17.31 15.72 1.21 o -10 4 2 22.80 19.99 1.21 o -8 4 2 150.84 128.65 2.01 o -6 4 2 1149.63 1163.84 5.31 o -4 4 2 11.27 15.72 0.60 o -2 4 2 3604.14 3563.89 15.34 o 0 4 2 182.88 168.21 1.65 o 2 4 2 1761.55 1817.95 9.30 o 4 4 2 36.79 41.75 0.88 o 6 4 2 4.17 7.16 0.51 o 8 4 2 77.60 77.88 1.63 o 10 4 2 0.05 -0.80 0.80 o 12 4 2 66.16 76.64 1.91 o 14 4 2 87.25 87.60 2.49 o 16 4 2 0.81 0.14 1.60 o -15 5 2 8.81 13.01 1.64 o -13 5 2 56.90 47.18 1.91 o -11 5 2 24.45 24.38 1.27 o -9 5 2 489.84 532.48 4.12 o -7 5 2 2.93 0.70 0.64 o -5 5 2 987.27 1046.82 5.24 o -3 5 2 1209.61 1206.72 6.31 o -1 5 2 1163.74 1130.86 5.58 o 1 5 2 5.84 4.32 0.57 o 3 5 2 1862.87 1815.98 8.73 o 5 5 2 4.05 3.66 0.55 o 7 5 2 3166.01 3152.33 13.07 o 9 5 2 1521.75 1567.38 8.38 o 11 5 2 106.71 107.46 2.14 o 13 5 2 295.76 300.30 3.72 o 15 5 2 33.25 27.72 1.80 o -14 6 2 64.28 67.96 2.47 o -12 6 2 210.04 212.76 2.91 o -10 6 2 351.49 377.66 3.75 o -8 6 2 448.19 441.98 4.14 o -6 6 2 951.33 965.08 5.64 o -4 6 2 426.52 424.24 3.32 o -2 6 2 150.40 133.76 1.54 o 0 6 2 259.61 250.41 2.16 o 2 6 2 10.24 8.28 0.66 o 4 6 2 845.78 839.66 4.87 o 6 6 2 56.74 41.19 1.27 o 8 6 2 4.47 0.30 0.94 o 10 6 2 206.79 198.25 2.81 o 12 6 2 1270.94 1264.37 7.34 o 14 6 2 53.96 58.82 2.11 o -15 7 2 27.75 23.18 1.91 o -13 7 2 142.38 142.03 3.37 o -11 7 2 174.71 187.75 4.06 o -9 7 2 318.60 331.22 3.82 o -7 7 2 580.72 578.97 4.77 o -5 7 2 1308.81 1301.54 7.31 o -3 7 2 432.53 393.31 2.98 o -1 7 2 761.15 769.73 4.46 o 1 7 2 2169.32 2056.22 8.92 o 3 7 2 0.01 -0.08 0.55 o 5 7 2 935.05 972.92 5.75 o 7 7 2 639.66 610.43 4.83 o 9 7 2 81.46 71.63 2.12 o 11 7 2 270.55 263.96 3.62 o 13 7 2 0.16 2.86 1.44 o 15 7 2 64.37 57.78 2.52 o -14 8 2 1.75 2.30 1.79 o -12 8 2 476.91 508.22 5.97 o -10 8 2 1.26 -1.32 1.32 o -8 8 2 152.82 135.97 2.78 o -6 8 2 1014.48 994.63 6.68 o -4 8 2 357.76 340.32 3.15 o -2 8 2 984.37 978.23 5.50 o 0 8 2 191.50 172.03 2.09 o 2 8 2 56.08 65.12 1.41 o 4 8 2 2552.00 2500.14 11.86 o 6 8 2 248.35 252.21 3.17 o 8 8 2 1960.29 1997.61 11.48 o 10 8 2 3.03 -1.12 1.17 o 12 8 2 23.15 24.64 1.94 o 14 8 2 13.74 16.92 2.11 o -13 9 2 0.09 2.74 1.92 o -11 9 2 333.43 346.28 4.95 o -9 9 2 887.49 889.65 6.96 o -7 9 2 595.20 615.71 5.36 o -5 9 2 1680.83 1676.78 9.85 o -3 9 2 194.47 192.97 2.60 o -1 9 2 61.61 51.18 1.43 o 1 9 2 24.89 23.38 1.16 o 3 9 2 1132.75 1113.57 6.90 o 5 9 2 2811.91 2830.43 14.75 o 7 9 2 148.80 155.78 3.17 o 9 9 2 413.60 424.42 5.22 o 11 9 2 414.39 429.30 5.47 o 13 9 2 6.94 7.03 1.63 o -12 10 2 121.92 108.44 4.76 o -10 10 2 1.72 0.21 1.52 o -8 10 2 1461.94 1469.68 10.32 o -6 10 2 0.02 -1.07 1.07 o -4 10 2 2165.02 2205.18 12.30 o -2 10 2 1894.59 1904.02 10.36 o 0 10 2 3077.64 3086.12 15.81 o 2 10 2 434.20 441.35 4.10 o 4 10 2 494.77 492.27 4.64 o 6 10 2 306.51 316.97 3.82 o 8 10 2 0.00 -0.57 1.13 o 10 10 2 126.76 141.59 3.51 o 12 10 2 89.09 77.05 2.97 o -11 11 2 24.06 25.03 2.36 o -9 11 2 516.73 527.38 6.09 o -7 11 2 209.07 218.62 3.67 o -5 11 2 1220.56 1177.73 8.19 o -3 11 2 1579.85 1635.28 9.63 o -1 11 2 1909.07 1804.02 10.22 o 1 11 2 1216.14 1227.03 7.83 o 3 11 2 762.47 741.42 5.74 o 5 11 2 10.64 11.93 1.69 o 7 11 2 104.84 120.56 2.98 o 9 11 2 168.19 159.27 3.67 o 11 11 2 11.30 13.96 1.86 o -10 12 2 517.83 525.51 6.96 o -8 12 2 296.65 288.16 4.68 o -6 12 2 64.04 57.34 2.44 o -4 12 2 4.78 2.48 1.26 o -2 12 2 36.57 32.03 1.56 o 0 12 2 2.61 2.85 1.08 o 2 12 2 144.29 137.47 2.72 o 4 12 2 0.48 0.24 1.13 o 6 12 2 2.61 2.24 1.44 o 8 12 2 0.27 1.40 1.44 o 10 12 2 8.47 2.57 2.93 o -9 13 2 124.75 115.61 3.90 o -7 13 2 116.16 112.08 3.80 o -5 13 2 35.66 35.14 2.08 o -3 13 2 0.04 -0.22 1.32 o -1 13 2 97.75 92.08 3.19 o 1 13 2 133.85 137.58 3.08 o 3 13 2 14.24 13.27 1.56 o 5 13 2 20.35 23.38 1.86 o 7 13 2 163.91 177.49 3.90 o 9 13 2 297.32 319.54 5.57 o -6 14 2 30.36 19.06 2.25 o -4 14 2 135.89 137.79 4.27 o -2 14 2 74.83 78.88 2.65 o 0 14 2 1.49 0.00 1.26 o 2 14 2 0.31 -0.11 1.32 o 4 14 2 9.47 16.92 1.83 o 6 14 2 0.78 1.95 1.74 o -3 15 2 12.00 5.31 1.96 o -1 15 2 1.04 -1.38 1.55 o 1 15 2 6.91 9.33 1.83 o 3 15 2 277.03 314.72 5.97 o -15 1 3 497.72 492.48 6.09 o -13 1 3 460.93 488.64 4.73 o -11 1 3 869.18 901.89 6.09 o -9 1 3 1065.07 1100.99 6.49 o -7 1 3 266.61 300.11 2.24 o -5 1 3 3297.26 3421.91 15.69 o -3 1 3 1156.62 1195.28 8.43 o 5 1 3 2564.29 2507.82 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