#------------------------------------------------------------------------------ #$Date: 2018-04-30 19:30:46 +0300 (Mon, 30 Apr 2018) $ #$Revision: 207561 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/24/2242473.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242473 _cell_angle_alpha 90.000 _cell_angle_beta 104.289 _cell_angle_gamma 90.000 _cell_length_a 16.2280 _cell_length_b 6.4392 _cell_length_c 15.5937 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.7570 _cod_data_source_file xi2001Vsup6.hkl _cod_data_source_block V _shelx_title ' 14a_JBF3_a in C2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.71 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -8 0 277.59 292.13 13.58 o 2 -8 0 60.94 65.18 5.18 o 4 -8 0 122.09 143.89 11.71 o 6 -8 0 72.22 101.51 13.31 o 1 -7 0 97.51 101.14 6.92 o 3 -7 0 44.03 49.50 3.69 o 5 -7 0 60.61 65.41 9.07 o 7 -7 0 164.53 154.76 8.88 o 9 -7 0 64.93 69.92 22.25 o 11 -7 0 110.28 123.73 11.09 o 0 -6 0 561.60 578.87 10.91 o 2 -6 0 241.78 223.71 5.68 o 4 -6 0 318.77 304.13 6.67 o 6 -6 0 740.60 733.96 18.29 o 8 -6 0 195.18 200.97 10.81 o 10 -6 0 74.05 84.13 7.53 o 12 -6 0 215.42 215.13 14.67 o 14 -6 0 86.23 97.67 11.56 o 1 -5 0 39.57 32.80 2.36 o 3 -5 0 28.03 21.83 2.46 o 5 -5 0 215.20 191.63 11.08 o 7 -5 0 642.59 646.95 12.08 o 9 -5 0 49.02 38.44 9.06 o 11 -5 0 312.62 326.21 12.05 o 13 -5 0 68.06 51.95 7.62 o 15 -5 0 65.92 66.00 9.68 o 0 -4 0 1656.89 1557.94 19.06 o 2 -4 0 430.50 414.33 6.57 o 4 -4 0 172.14 166.82 2.83 o 6 -4 0 915.84 855.49 10.79 o 8 -4 0 86.65 96.67 11.29 o 10 -4 0 66.05 59.97 5.16 o 12 -4 0 570.29 557.49 19.21 o 14 -4 0 114.73 108.37 5.28 o 16 -4 0 127.62 120.46 7.49 o 18 -4 0 80.62 83.48 10.77 o 1 -3 0 1191.43 1165.60 11.97 o 3 -3 0 1584.28 1748.32 20.11 o 5 -3 0 1187.59 1204.16 14.95 o 7 -3 0 1352.94 1335.69 17.82 o 9 -3 0 801.42 811.71 17.12 o 11 -3 0 323.31 321.33 5.76 o 13 -3 0 119.02 105.09 7.25 o 15 -3 0 154.82 150.51 7.55 o 17 -3 0 455.63 498.70 11.16 o 19 -3 0 1.24 -1.62 16.03 o 0 -2 0 4540.68 4215.98 42.61 o 2 -2 0 7132.31 7313.35 19.09 o 4 -2 0 3167.55 3348.10 61.23 o 6 -2 0 830.73 810.84 17.57 o 8 -2 0 301.35 267.64 4.28 o 10 -2 0 88.36 75.79 3.58 o 12 -2 0 126.21 122.43 4.96 o 14 -2 0 324.00 318.89 10.39 o 16 -2 0 161.16 170.80 11.48 o 18 -2 0 117.22 107.97 6.95 o 20 -2 0 52.49 55.59 10.99 o 1 -1 0 3634.95 2479.42 714.25 o 3 -1 0 1152.10 1143.59 123.11 o 5 -1 0 5467.32 5328.99 74.60 o 7 -1 0 6240.41 6564.68 89.15 o 9 -1 0 1005.45 1041.63 18.21 o 11 -1 0 378.37 420.22 8.62 o 13 -1 0 943.93 951.39 29.69 o 15 -1 0 82.11 75.82 5.33 o 17 -1 0 103.02 101.12 5.87 o 19 -1 0 72.76 72.35 7.25 o 4 0 0 30877.89 30538.70 452.69 o 6 0 0 5960.50 6033.91 61.91 o 8 0 0 736.54 711.34 7.47 o 10 0 0 4261.05 4678.45 38.55 o 12 0 0 281.82 285.18 6.34 o 14 0 0 2.54 -1.03 2.86 o 16 0 0 7.10 2.72 4.98 o 18 0 0 435.73 438.64 17.31 o 20 0 0 27.80 33.79 8.66 o 1 1 0 3747.65 3068.60 547.15 o 3 1 0 1157.13 1115.54 19.69 o 5 1 0 5388.26 5275.01 51.72 o 7 1 0 6355.95 6753.41 42.46 o 9 1 0 1011.55 1031.38 8.45 o 11 1 0 410.55 462.34 6.85 o 13 1 0 936.58 945.55 16.75 o 15 1 0 82.45 69.59 5.29 o 17 1 0 104.60 91.56 5.70 o 19 1 0 72.88 82.18 13.18 o 0 2 0 4453.77 3031.40 969.63 o 2 2 0 7184.79 7516.44 121.00 o 4 2 0 3178.46 3392.57 65.11 o 6 2 0 851.51 854.64 8.21 o 8 2 0 308.95 277.34 6.65 o 10 2 0 88.63 68.17 8.10 o 12 2 0 132.06 123.51 6.02 o 14 2 0 321.67 326.46 7.55 o 16 2 0 153.00 178.40 9.83 o 18 2 0 116.08 98.92 7.16 o 20 2 0 52.85 80.31 11.08 o 1 3 0 1165.93 1147.29 13.15 o 3 3 0 1580.71 1730.68 34.87 o 5 3 0 1218.64 1189.48 24.95 o 7 3 0 1362.80 1310.53 15.72 o 9 3 0 806.09 826.73 6.22 o 11 3 0 314.11 316.62 5.33 o 13 3 0 123.33 118.05 8.06 o 15 3 0 150.92 143.93 11.09 o 17 3 0 468.14 395.34 93.81 o 19 3 0 0.84 8.40 9.54 o 0 4 0 1729.44 1640.37 10.95 o 2 4 0 422.31 415.31 4.07 o 4 4 0 164.45 150.20 5.30 o 6 4 0 935.21 870.35 13.69 o 8 4 0 90.77 74.97 24.05 o 10 4 0 60.15 41.58 6.81 o 12 4 0 570.45 528.01 26.62 o 14 4 0 117.70 95.57 12.10 o 16 4 0 122.86 138.40 9.58 o 18 4 0 87.05 104.70 18.30 o 1 5 0 32.52 33.98 2.26 o 3 5 0 28.53 22.69 1.82 o 5 5 0 231.26 218.19 10.45 o 7 5 0 615.73 621.87 19.96 o 9 5 0 47.81 27.83 8.47 o 11 5 0 300.84 308.32 15.58 o 13 5 0 71.87 56.25 10.29 o 15 5 0 67.33 70.03 12.70 o 0 6 0 559.33 465.95 85.37 o 2 6 0 239.35 217.31 9.85 o 4 6 0 318.12 305.85 18.30 o 6 6 0 723.83 706.21 13.04 o 8 6 0 200.18 182.32 10.61 o 10 6 0 77.23 79.89 9.40 o 12 6 0 208.78 233.74 16.42 o 14 6 0 85.96 112.52 21.17 o 1 7 0 88.35 79.81 4.76 o 3 7 0 43.37 42.38 4.28 o 5 7 0 59.24 57.66 6.67 o 7 7 0 163.02 160.40 9.51 o 9 7 0 63.80 75.11 8.85 o 11 7 0 110.94 139.23 13.86 o 0 8 0 276.84 219.61 84.90 o 2 8 0 58.42 37.64 18.29 o 4 8 0 119.18 135.82 38.57 o 6 8 0 72.99 51.81 22.23 o -6 -8 1 1.65 15.23 18.75 o -4 -8 1 61.08 92.51 13.46 o -2 -8 1 166.61 176.38 9.34 o 0 -8 1 50.03 53.52 5.58 o 2 -8 1 169.14 190.80 9.04 o 4 -8 1 10.79 24.96 9.62 o 6 -8 1 142.56 164.59 14.04 o -11 -7 1 33.26 43.92 10.09 o -9 -7 1 120.40 135.92 11.17 o -7 -7 1 63.63 74.58 12.93 o -5 -7 1 48.49 44.85 8.22 o -3 -7 1 33.74 37.34 6.20 o -1 -7 1 462.26 469.57 11.00 o 1 -7 1 67.55 61.30 4.35 o 3 -7 1 38.80 32.59 3.86 o 5 -7 1 566.63 575.75 17.11 o 7 -7 1 241.32 261.90 12.98 o 9 -7 1 204.18 199.03 12.09 o 11 -7 1 177.23 207.87 12.77 o -14 -6 1 121.57 122.86 13.05 o -12 -6 1 74.64 101.54 12.10 o -10 -6 1 55.51 60.05 12.15 o -8 -6 1 118.66 106.10 6.77 o -6 -6 1 451.48 430.57 25.41 o -4 -6 1 37.75 38.47 3.15 o -2 -6 1 89.17 81.82 4.17 o 0 -6 1 328.72 321.77 6.50 o 2 -6 1 462.84 449.29 13.72 o 4 -6 1 280.66 292.00 6.13 o 6 -6 1 498.69 506.81 11.57 o 8 -6 1 95.96 93.22 6.92 o 10 -6 1 345.39 361.93 13.60 o 12 -6 1 383.09 404.48 16.41 o 14 -6 1 86.82 106.27 11.50 o -17 -5 1 129.13 134.28 13.37 o -15 -5 1 76.80 89.05 10.98 o -13 -5 1 80.42 85.08 8.61 o -11 -5 1 505.53 522.08 14.47 o -9 -5 1 240.33 232.53 9.53 o -7 -5 1 688.84 679.79 17.15 o -5 -5 1 284.27 277.32 7.97 o -3 -5 1 1277.85 1310.25 17.05 o -1 -5 1 2108.01 2096.73 21.62 o 1 -5 1 877.38 838.78 7.79 o 3 -5 1 1444.96 1458.49 9.74 o 5 -5 1 202.98 223.97 3.92 o 7 -5 1 584.01 531.23 16.71 o 9 -5 1 478.80 478.63 20.86 o 11 -5 1 850.59 800.09 17.77 o 13 -5 1 35.76 38.29 7.31 o 15 -5 1 91.38 103.41 10.27 o -18 -4 1 63.69 69.29 6.68 o -16 -4 1 136.72 139.31 11.61 o -14 -4 1 472.79 460.51 21.35 o -12 -4 1 498.96 504.93 12.58 o -10 -4 1 1000.11 1052.84 25.15 o -8 -4 1 162.35 146.72 6.86 o -6 -4 1 85.11 84.34 5.33 o -4 -4 1 362.87 360.16 7.10 o -2 -4 1 1263.56 1339.16 7.38 o 0 -4 1 1840.15 1841.08 11.70 o 2 -4 1 13.13 11.66 1.47 o 4 -4 1 1255.04 1219.83 9.47 o 6 -4 1 873.99 889.30 5.67 o 8 -4 1 102.92 92.56 4.93 o 10 -4 1 110.10 113.27 4.70 o 12 -4 1 693.65 694.11 12.40 o 14 -4 1 206.71 221.18 9.52 o 16 -4 1 21.72 34.58 7.97 o 18 -4 1 7.56 3.31 17.09 o -19 -3 1 151.90 163.42 11.47 o -17 -3 1 250.45 270.35 11.17 o -15 -3 1 64.78 63.10 5.06 o -13 -3 1 442.20 441.44 10.35 o -11 -3 1 388.31 402.46 13.10 o -9 -3 1 555.00 573.38 13.16 o -7 -3 1 2517.04 2597.49 46.29 o -5 -3 1 39.59 33.47 4.37 o -3 -3 1 580.08 541.82 5.36 o -1 -3 1 6769.43 7241.64 32.66 o 1 -3 1 2576.15 2821.19 21.21 o 3 -3 1 3731.64 3931.95 37.25 o 5 -3 1 251.37 229.85 3.45 o 7 -3 1 464.43 489.53 6.02 o 9 -3 1 147.53 142.00 4.85 o 11 -3 1 329.65 315.69 15.92 o 13 -3 1 78.55 71.99 4.53 o 15 -3 1 89.04 84.41 5.00 o 17 -3 1 192.48 195.63 11.24 o 19 -3 1 53.32 53.40 10.54 o -20 -2 1 131.08 147.09 12.10 o -18 -2 1 223.65 225.18 10.19 o -16 -2 1 25.87 24.09 4.43 o -14 -2 1 215.18 219.97 8.78 o -12 -2 1 573.67 617.33 17.25 o -10 -2 1 1579.00 1589.81 25.06 o -8 -2 1 673.02 636.99 20.52 o -6 -2 1 3288.71 3372.03 57.23 o -4 -2 1 2004.82 2071.80 75.92 o -2 -2 1 1184.57 1220.04 20.25 o 0 -2 1 3594.70 3471.75 16.03 o 2 -2 1 837.52 801.90 11.14 o 4 -2 1 3567.40 3726.88 74.12 o 6 -2 1 814.04 813.67 11.93 o 8 -2 1 201.02 213.98 5.11 o 10 -2 1 1077.28 1070.73 16.85 o 12 -2 1 29.93 35.64 3.14 o 14 -2 1 66.03 54.94 4.41 o 16 -2 1 152.51 149.25 12.01 o 18 -2 1 25.36 24.31 5.85 o -19 -1 1 63.64 76.18 6.79 o -17 -1 1 48.52 44.65 5.00 o -15 -1 1 150.15 153.56 10.32 o -13 -1 1 102.93 99.36 5.95 o -11 -1 1 618.03 600.66 14.29 o -9 -1 1 1541.20 1542.50 15.93 o -7 -1 1 4543.92 4856.67 97.84 o -5 -1 1 14914.86 15146.23 189.39 o -3 -1 1 43977.70 44580.09 772.94 o -1 -1 1 3230.27 2374.59 318.50 o 1 -1 1 4193.34 3369.13 458.09 o 3 -1 1 4711.27 5015.75 82.63 o 5 -1 1 2834.91 2768.05 42.22 o 7 -1 1 1330.91 1470.20 8.99 o 9 -1 1 230.83 208.39 4.59 o 11 -1 1 412.23 381.93 9.34 o 13 -1 1 172.90 165.85 8.47 o 15 -1 1 420.22 443.82 19.41 o 17 -1 1 243.39 237.03 10.48 o 19 -1 1 83.59 91.58 11.61 o -20 0 1 103.23 107.25 8.31 o -18 0 1 127.12 128.25 9.56 o -16 0 1 54.66 56.12 4.72 o -14 0 1 57.28 62.30 3.96 o -12 0 1 279.51 266.01 6.01 o -10 0 1 1443.50 1502.97 19.34 o -8 0 1 51.57 23.26 1.73 o -6 0 1 3932.39 3674.29 56.67 o -4 0 1 5367.25 5600.18 67.54 o 2 0 1 2960.65 2468.31 762.21 o 4 0 1 37486.38 37771.35 404.05 o 6 0 1 6000.10 6091.06 69.07 o 8 0 1 1872.27 1995.49 28.42 o 10 0 1 255.01 242.59 5.25 o 12 0 1 97.24 94.35 6.15 o 14 0 1 202.42 236.38 10.00 o 16 0 1 75.73 66.87 5.01 o 18 0 1 242.33 289.84 11.17 o 20 0 1 69.57 74.13 9.65 o -19 1 1 64.58 59.65 8.91 o -17 1 1 45.38 44.62 6.46 o -15 1 1 148.03 148.93 7.03 o -13 1 1 106.88 96.47 5.08 o -11 1 1 598.21 579.12 7.77 o -9 1 1 1533.78 1539.61 9.89 o -7 1 1 4432.81 4216.55 420.68 o -5 1 1 14906.01 15591.00 268.26 o -3 1 1 43831.07 44982.89 1383.79 o -1 1 1 3258.52 2791.70 417.86 o 1 1 1 4234.24 3269.28 783.30 o 3 1 1 4649.00 4928.65 99.89 o 5 1 1 2835.52 2924.87 433.25 o 7 1 1 1349.94 1497.19 12.27 o 9 1 1 235.14 207.23 4.57 o 11 1 1 397.77 376.47 8.38 o 13 1 1 177.04 183.16 7.29 o 15 1 1 417.23 456.14 11.10 o 17 1 1 250.46 241.52 10.17 o 19 1 1 83.29 72.20 7.18 o -20 2 1 135.54 128.46 18.37 o -18 2 1 219.82 218.07 19.34 o -16 2 1 26.05 13.26 4.96 o -14 2 1 216.62 221.40 9.20 o -12 2 1 610.13 558.14 78.78 o -10 2 1 1568.58 1621.05 12.69 o -8 2 1 678.47 640.51 6.17 o -6 2 1 3223.12 3359.69 36.73 o -4 2 1 2017.87 2011.56 14.54 o -2 2 1 1201.14 1221.61 23.69 o 0 2 1 3553.62 2901.47 333.15 o 2 2 1 839.29 803.43 20.41 o 4 2 1 3591.72 3655.44 119.66 o 6 2 1 765.74 763.94 30.55 o 8 2 1 200.18 183.91 40.95 o 10 2 1 1050.04 1053.60 11.62 o 12 2 1 25.93 33.99 3.14 o 14 2 1 63.59 59.75 5.89 o 16 2 1 157.04 154.75 7.55 o 18 2 1 28.08 22.22 5.84 o -19 3 1 147.59 136.04 63.18 o -17 3 1 255.39 223.54 42.08 o -15 3 1 65.73 58.31 4.50 o -13 3 1 417.83 431.64 17.34 o -11 3 1 387.51 406.16 15.81 o -9 3 1 545.04 541.98 27.68 o -7 3 1 2508.34 2517.15 68.21 o -5 3 1 36.41 49.79 15.43 o -3 3 1 560.73 522.19 12.45 o -1 3 1 6695.93 7063.62 49.95 o 1 3 1 2627.33 2782.37 257.37 o 3 3 1 3760.22 3920.58 69.59 o 5 3 1 259.20 239.05 7.10 o 7 3 1 449.46 482.27 5.58 o 9 3 1 140.12 136.68 3.82 o 11 3 1 330.73 310.04 9.35 o 13 3 1 78.70 76.56 5.60 o 15 3 1 93.63 87.53 10.51 o 17 3 1 199.05 200.72 30.40 o 19 3 1 51.99 30.87 17.32 o -18 4 1 66.41 63.27 21.32 o -16 4 1 132.22 93.15 14.97 o -14 4 1 465.49 480.85 17.75 o -12 4 1 501.17 498.23 32.97 o -10 4 1 999.70 1022.93 17.64 o -8 4 1 159.34 151.94 8.45 o -6 4 1 83.13 80.48 6.42 o -4 4 1 367.98 357.04 8.55 o -2 4 1 1227.64 1290.79 6.56 o 0 4 1 1895.83 1888.76 18.12 o 2 4 1 13.14 9.06 1.87 o 4 4 1 1212.39 1173.49 21.80 o 6 4 1 895.33 883.28 13.69 o 8 4 1 100.82 76.21 6.96 o 10 4 1 106.55 98.05 7.99 o 12 4 1 698.20 717.35 14.02 o 14 4 1 208.29 209.67 5.98 o 16 4 1 21.71 15.98 11.39 o 18 4 1 8.50 14.46 8.22 o -17 5 1 126.76 133.99 22.99 o -15 5 1 75.97 65.22 19.66 o -13 5 1 86.98 83.99 10.16 o -11 5 1 496.49 506.76 16.68 o -9 5 1 242.38 244.39 17.24 o -7 5 1 688.85 687.20 20.57 o -5 5 1 275.39 258.99 9.41 o -3 5 1 1293.92 1293.31 12.58 o -1 5 1 2091.88 2045.18 18.53 o 1 5 1 853.67 783.59 71.99 o 3 5 1 1448.72 1444.37 17.28 o 5 5 1 196.39 207.61 8.58 o 7 5 1 574.48 530.83 19.36 o 9 5 1 474.88 468.22 20.57 o 11 5 1 851.59 805.00 40.23 o 13 5 1 37.71 46.09 10.53 o 15 5 1 93.87 116.77 12.57 o -14 6 1 124.49 88.02 18.15 o -12 6 1 68.97 85.02 21.78 o -10 6 1 57.67 55.31 9.72 o -8 6 1 127.20 118.37 10.53 o -6 6 1 458.15 453.10 11.17 o -4 6 1 37.93 28.47 5.35 o -2 6 1 94.68 87.14 3.44 o 0 6 1 349.79 299.03 30.45 o 2 6 1 461.40 446.25 9.15 o 4 6 1 296.59 294.28 9.87 o 6 6 1 496.96 489.02 22.87 o 8 6 1 93.99 81.49 10.02 o 10 6 1 359.52 368.49 20.41 o 12 6 1 374.37 444.32 20.84 o 14 6 1 86.94 126.73 19.96 o -11 7 1 32.66 34.11 14.97 o -9 7 1 119.31 102.78 9.06 o -7 7 1 59.70 81.43 8.11 o -5 7 1 51.46 46.77 6.32 o -3 7 1 35.27 33.53 6.71 o -1 7 1 462.33 456.71 10.24 o 1 7 1 69.39 64.48 3.86 o 3 7 1 37.00 28.40 4.29 o 5 7 1 583.12 584.90 25.11 o 7 7 1 235.77 266.23 13.56 o 9 7 1 206.56 241.25 15.86 o 11 7 1 169.57 224.48 43.86 o -6 8 1 2.70 -5.60 10.27 o -4 8 1 60.43 53.56 23.74 o -2 8 1 173.28 117.15 47.24 o 0 8 1 50.57 31.69 11.28 o 2 8 1 168.61 123.51 39.13 o 4 8 1 11.72 8.28 7.44 o 6 8 1 144.86 88.92 66.09 o -6 -8 2 72.48 95.23 26.16 o -4 -8 2 86.08 72.26 10.69 o -2 -8 2 81.34 110.10 13.12 o 0 -8 2 42.17 48.43 6.63 o 2 -8 2 75.19 88.37 5.75 o 4 -8 2 155.28 162.08 13.93 o 6 -8 2 9.17 19.08 16.48 o -11 -7 2 8.67 26.93 10.33 o -9 -7 2 59.12 58.66 9.51 o -7 -7 2 72.81 74.05 8.01 o -5 -7 2 72.90 94.02 9.17 o -3 -7 2 11.09 16.05 4.85 o -1 -7 2 632.22 654.17 18.27 o 1 -7 2 6.59 9.72 4.27 o 3 -7 2 159.52 148.54 6.76 o 5 -7 2 785.39 809.70 8.58 o 7 -7 2 238.62 234.08 12.77 o 9 -7 2 438.36 459.89 16.33 o 11 -7 2 69.23 78.10 10.76 o -14 -6 2 149.30 153.25 15.73 o -12 -6 2 0.55 0.97 7.72 o -10 -6 2 79.47 87.41 12.33 o -8 -6 2 110.28 101.85 7.09 o -6 -6 2 18.66 22.33 5.21 o -4 -6 2 635.98 636.89 21.77 o -2 -6 2 329.83 311.36 15.28 o 0 -6 2 285.20 290.85 6.31 o 2 -6 2 275.82 271.28 11.61 o 4 -6 2 985.52 981.68 9.27 o 6 -6 2 9.10 19.11 2.70 o 8 -6 2 353.20 330.75 15.15 o 10 -6 2 93.19 109.63 10.30 o 12 -6 2 19.65 26.39 8.13 o 14 -6 2 331.98 369.21 20.73 o -17 -5 2 38.03 51.10 19.53 o -15 -5 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46.67 12.22 o -17 -3 2 150.07 162.94 7.77 o -15 -3 2 275.68 283.19 18.87 o -13 -3 2 872.34 855.83 16.02 o -11 -3 2 98.71 94.68 3.54 o -9 -3 2 234.03 219.02 6.99 o -7 -3 2 258.12 248.69 7.76 o -5 -3 2 500.54 539.27 8.26 o -3 -3 2 526.82 527.27 7.28 o -1 -3 2 1290.07 1272.70 12.48 o 1 -3 2 37.45 41.96 1.91 o 3 -3 2 993.83 1131.75 10.08 o 5 -3 2 1515.22 1575.24 21.13 o 7 -3 2 121.95 137.94 5.34 o 9 -3 2 433.24 409.09 12.88 o 11 -3 2 936.82 936.43 21.65 o 13 -3 2 81.51 83.64 6.94 o 15 -3 2 285.65 298.89 9.74 o 17 -3 2 106.21 105.36 8.16 o -20 -2 2 223.46 257.81 14.83 o -18 -2 2 136.54 157.70 13.49 o -16 -2 2 215.56 226.46 7.90 o -14 -2 2 28.94 29.69 3.44 o -12 -2 2 2115.98 2128.06 40.73 o -10 -2 2 9.98 13.54 1.94 o -8 -2 2 7320.20 7745.71 132.76 o -6 -2 2 661.20 645.43 16.23 o -4 -2 2 1509.46 1572.70 12.79 o -2 -2 2 10464.66 10913.21 106.49 o 0 -2 2 932.61 878.78 6.28 o 2 -2 2 2262.99 2328.23 25.82 o 4 -2 2 818.22 774.60 8.73 o 6 -2 2 353.80 334.62 4.58 o 8 -2 2 98.48 99.94 3.60 o 10 -2 2 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