#------------------------------------------------------------------------------ #$Date: 2018-10-11 05:50:07 +0300 (Thu, 11 Oct 2018) $ #$Revision: 211388 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/26/2242666.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242666 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1719 _cell_length_b 16.4260 _cell_length_c 4.0249 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8306 _cod_data_source_file qm21291sup2.hkl _cod_data_source_block 1 _shelx_title ' 564_a.res in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 91.19 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -4 15.62 12.65 1.01 o 6 0 -4 57.20 66.32 3.36 o 1 1 -4 40.41 32.00 1.25 o 2 1 -4 25.59 16.78 1.88 o 3 1 -4 11.89 11.25 1.70 o 6 1 -4 125.87 138.62 6.24 o 7 1 -4 81.41 87.33 2.86 o 0 2 -4 1.37 2.36 0.94 o 1 2 -4 24.88 19.13 0.99 o 2 2 -4 44.67 39.37 1.83 o 3 2 -4 3.53 2.99 0.72 o 4 2 -4 6.38 5.68 1.51 o 5 2 -4 19.26 23.23 1.70 o 6 2 -4 46.98 53.21 2.13 o 7 2 -4 69.59 77.85 2.06 o 1 3 -4 4.32 4.19 0.66 o 2 3 -4 5.01 4.88 0.85 o 3 3 -4 1.54 0.99 0.68 o 4 3 -4 31.53 29.52 2.22 o 5 3 -4 5.29 5.36 0.79 o 6 3 -4 19.16 22.29 1.06 o 7 3 -4 32.10 30.05 0.98 o 0 4 -4 43.07 43.82 2.00 o 1 4 -4 9.87 9.59 0.82 o 2 4 -4 1.29 1.76 0.76 o 3 4 -4 53.83 50.01 2.17 o 4 4 -4 12.68 11.33 0.75 o 5 4 -4 24.74 24.26 1.01 o 6 4 -4 12.34 12.70 0.68 o 7 4 -4 4.91 6.12 0.69 o 1 5 -4 18.10 16.50 0.86 o 2 5 -4 77.26 77.34 2.41 o 3 5 -4 19.25 20.35 0.98 o 4 5 -4 5.93 6.65 0.62 o 5 5 -4 38.63 39.17 1.35 o 6 5 -4 16.17 16.40 0.75 o 0 6 -4 90.87 89.88 3.53 o 1 6 -4 88.11 88.70 2.62 o 2 6 -4 110.47 108.67 3.12 o 3 6 -4 166.14 164.70 5.24 o 4 6 -4 48.74 46.91 1.55 o 5 6 -4 16.70 16.48 0.78 o 6 6 -4 4.00 4.92 0.37 o 1 7 -4 6.83 6.96 0.64 o 2 7 -4 30.64 29.51 1.54 o 3 7 -4 85.38 86.03 2.92 o 4 7 -4 10.44 9.17 0.89 o 5 7 -4 26.00 25.23 0.95 o 0 8 -4 11.79 11.77 1.93 o 1 8 -4 67.43 70.57 2.48 o 2 8 -4 17.25 17.35 0.86 o 3 8 -4 222.88 218.36 6.62 o 4 8 -4 5.03 4.73 0.57 o 5 8 -4 14.00 11.14 0.84 o 1 9 -4 54.85 52.44 1.50 o 2 9 -4 60.21 58.88 2.04 o 3 9 -4 8.96 8.55 0.66 o 4 9 -4 12.14 12.17 0.58 o 0 10 -4 5.23 5.53 0.73 o 1 10 -4 4.75 4.80 0.49 o 2 10 -4 7.46 6.59 0.50 o 3 10 -4 16.05 14.29 1.29 o 1 11 -4 4.66 4.08 0.48 o 2 0 -3 243.57 230.36 10.02 o 4 0 -3 381.73 364.57 15.40 o 6 0 -3 417.17 406.03 17.05 o 8 0 -3 14.80 12.43 0.85 o 10 0 -3 10.44 11.72 1.71 o 1 1 -3 43.92 41.20 1.78 o 2 1 -3 137.79 146.17 4.68 o 3 1 -3 67.56 65.03 3.51 o 4 1 -3 144.49 143.52 6.64 o 5 1 -3 215.12 209.85 9.30 o 6 1 -3 120.20 116.71 11.06 o 7 1 -3 53.75 56.25 2.15 o 8 1 -3 41.40 39.60 3.09 o 9 1 -3 6.99 7.89 0.62 o 10 1 -3 7.43 8.72 1.07 o 1 2 -3 168.17 149.45 7.13 o 2 2 -3 5.89 6.42 0.83 o 3 2 -3 3.26 3.44 0.99 o 4 2 -3 184.87 189.91 8.56 o 5 2 -3 255.64 259.11 11.35 o 6 2 -3 68.24 71.32 2.71 o 7 2 -3 41.01 41.16 1.42 o 8 2 -3 14.66 17.21 0.73 o 9 2 -3 7.44 8.88 0.80 o 10 2 -3 7.05 9.74 1.26 o 0 3 -3 150.57 133.23 6.65 o 1 3 -3 0.66 0.06 1.07 o 2 3 -3 25.16 25.30 1.44 o 3 3 -3 11.00 9.06 1.31 o 4 3 -3 8.66 11.22 1.41 o 5 3 -3 43.02 45.82 2.87 o 6 3 -3 26.54 29.81 2.28 o 7 3 -3 1.30 2.14 0.50 o 8 3 -3 18.92 19.59 0.94 o 9 3 -3 2.69 3.69 0.37 o 10 3 -3 2.65 2.97 0.58 o 1 4 -3 7.77 7.82 1.51 o 2 4 -3 40.68 39.72 1.92 o 3 4 -3 53.28 54.08 2.30 o 4 4 -3 2.57 3.14 1.11 o 5 4 -3 70.10 75.77 4.13 o 6 4 -3 38.52 42.97 1.94 o 7 4 -3 22.27 26.24 1.12 o 8 4 -3 32.45 38.94 1.12 o 9 4 -3 11.26 12.86 0.57 o 10 4 -3 20.20 25.97 1.07 o 0 5 -3 49.94 51.01 3.51 o 1 5 -3 44.74 39.12 1.66 o 2 5 -3 12.11 12.11 1.14 o 3 5 -3 64.25 60.79 3.12 o 4 5 -3 159.12 158.22 12.40 o 5 5 -3 7.20 9.09 1.17 o 6 5 -3 6.57 7.27 0.87 o 7 5 -3 77.42 89.53 2.57 o 8 5 -3 39.37 47.87 1.72 o 9 5 -3 1.43 2.56 0.54 o 10 5 -3 7.84 12.46 0.71 o 1 6 -3 10.72 9.68 0.98 o 2 6 -3 163.69 162.79 3.85 o 3 6 -3 40.34 39.03 2.08 o 4 6 -3 303.28 333.40 9.77 o 5 6 -3 120.64 130.66 4.77 o 6 6 -3 48.47 55.45 2.26 o 7 6 -3 16.23 18.61 0.77 o 8 6 -3 43.83 52.65 2.45 o 9 6 -3 4.57 5.05 0.37 o 0 7 -3 43.16 38.09 2.29 o 1 7 -3 195.03 194.80 4.52 o 2 7 -3 65.22 65.18 1.94 o 3 7 -3 382.92 392.79 7.51 o 4 7 -3 57.29 58.20 1.76 o 5 7 -3 310.45 323.36 12.13 o 6 7 -3 5.34 6.21 0.81 o 7 7 -3 45.26 50.91 1.43 o 8 7 -3 11.74 14.77 0.61 o 9 7 -3 43.67 50.41 1.41 o 1 8 -3 23.36 20.20 0.88 o 2 8 -3 28.35 30.89 1.28 o 3 8 -3 36.95 40.72 1.50 o 4 8 -3 122.61 124.13 3.47 o 5 8 -3 134.85 142.69 6.29 o 6 8 -3 4.47 4.18 0.47 o 7 8 -3 5.82 5.67 0.47 o 8 8 -3 23.70 31.21 0.88 o 9 8 -3 7.58 9.13 0.50 o 0 9 -3 33.48 35.05 1.85 o 1 9 -3 68.45 62.46 2.22 o 2 9 -3 2.28 2.34 0.53 o 3 9 -3 116.05 126.88 3.08 o 4 9 -3 87.95 87.79 3.61 o 5 9 -3 23.90 24.92 1.00 o 6 9 -3 10.77 10.79 0.58 o 7 9 -3 21.28 24.56 0.80 o 8 9 -3 17.49 18.82 0.64 o 1 10 -3 8.17 8.30 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1.27 0.42 o 1 7 -2 89.50 85.77 2.21 o 2 7 -2 49.78 54.14 1.80 o 3 7 -2 81.74 75.67 1.86 o 4 7 -2 38.77 34.26 0.96 o 5 7 -2 360.01 375.92 6.59 o 6 7 -2 88.64 94.40 2.21 o 7 7 -2 328.28 342.44 7.37 o 8 7 -2 1.94 1.63 0.40 o 9 7 -2 15.38 15.81 0.65 o 10 7 -2 5.67 6.62 0.41 o 11 7 -2 2.16 1.84 0.32 o 0 8 -2 18.03 21.67 1.36 o 1 8 -2 583.93 608.02 11.57 o 2 8 -2 33.64 33.44 1.43 o 3 8 -2 79.31 75.56 1.71 o 4 8 -2 36.29 33.94 1.21 o 5 8 -2 74.09 79.92 2.77 o 6 8 -2 79.13 83.91 2.04 o 7 8 -2 72.64 80.58 1.66 o 8 8 -2 16.20 16.29 0.54 o 9 8 -2 9.26 10.43 0.86 o 10 8 -2 5.56 6.72 0.40 o 1 9 -2 57.54 60.99 1.76 o 2 9 -2 3.49 2.27 0.56 o 3 9 -2 43.02 46.30 1.33 o 4 9 -2 48.44 47.35 1.23 o 5 9 -2 144.29 147.16 3.33 o 6 9 -2 434.47 454.79 11.98 o 7 9 -2 71.89 71.56 2.23 o 8 9 -2 14.34 14.65 0.84 o 9 9 -2 7.26 7.35 0.46 o 10 9 -2 20.44 25.15 1.10 o 0 10 -2 78.79 77.71 2.94 o 1 10 -2 18.25 19.25 0.95 o 2 10 -2 42.99 43.50 1.32 o 3 10 -2 152.38 145.86 3.09 o 4 10 -2 30.02 31.07 1.29 o 5 10 -2 284.13 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247.99 254.68 8.23 o 5 14 -2 12.82 13.83 0.58 o 6 14 -2 31.47 36.09 0.97 o 7 14 -2 14.22 16.95 0.59 o 1 15 -2 102.19 98.51 2.85 o 2 15 -2 21.95 22.79 0.66 o 3 15 -2 39.84 36.93 1.47 o 4 15 -2 96.68 107.47 3.42 o 5 15 -2 35.03 34.37 1.31 o 6 15 -2 32.79 34.19 1.02 o 0 16 -2 73.65 76.53 2.90 o 1 16 -2 6.64 5.99 0.53 o 2 16 -2 13.57 13.58 0.78 o 3 16 -2 70.76 75.69 2.49 o 4 16 -2 24.02 22.81 0.94 o 5 16 -2 23.76 25.81 0.83 o 1 17 -2 4.85 5.27 0.54 o 2 17 -2 93.55 92.76 2.67 o 3 17 -2 31.33 31.78 1.22 o 4 17 -2 37.61 34.74 2.09 o 2 0 -1 8315.70 8210.06 328.71 o 4 0 -1 697.09 706.26 12.93 o 6 0 -1 605.35 573.83 8.95 o 8 0 -1 152.08 159.07 3.70 o 10 0 -1 6.64 6.40 0.58 o 12 0 -1 7.42 5.30 0.49 o 0 1 -1 3582.74 3316.61 66.72 o 1 1 -1 195.11 196.69 2.35 o 2 1 -1 6574.08 6342.54 89.53 o 3 1 -1 16.45 19.45 0.45 o 4 1 -1 473.39 494.34 5.91 o 5 1 -1 273.96 279.60 3.36 o 6 1 -1 34.81 36.12 0.76 o 7 1 -1 24.32 23.32 0.60 o 8 1 -1 74.73 75.51 1.41 o 9 1 -1 34.72 40.96 0.91 o 10 1 -1 67.04 64.91 1.19 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10.77 0.52 o 2 17 0 26.76 26.19 1.12 o 3 17 0 4.24 3.31 0.36 o 4 17 0 58.85 59.85 2.36 o 5 17 0 1.14 0.74 0.33 o 6 17 0 10.33 7.50 0.40 o 0 18 0 123.83 129.54 4.37 o 1 18 0 23.59 29.91 1.02 o 2 18 0 1.44 1.35 0.40 o 3 18 0 6.99 6.39 0.48 o 4 18 0 0.35 0.28 0.36 o 5 18 0 18.88 15.79 1.01 o 1 19 0 52.02 54.24 2.03 o 2 19 0 5.54 6.37 0.51 o 3 19 0 41.85 45.93 2.84 o 2 0 1 8315.70 8112.73 187.63 o 4 0 1 697.09 694.06 10.10 o 6 0 1 605.35 574.05 5.79 o 8 0 1 152.08 152.98 2.73 o 10 0 1 6.64 6.40 0.48 o 12 0 1 7.42 5.46 0.55 o 0 1 1 3582.74 3402.22 78.07 o 1 1 1 195.11 201.92 2.51 o 2 1 1 6574.08 6490.86 105.94 o 3 1 1 16.45 19.61 0.43 o 4 1 1 473.39 486.96 4.59 o 5 1 1 273.96 276.07 2.23 o 6 1 1 34.81 35.48 0.43 o 7 1 1 24.32 22.52 0.42 o 8 1 1 74.73 72.47 0.92 o 9 1 1 34.72 37.62 0.63 o 10 1 1 67.04 60.85 1.21 o 11 1 1 47.69 42.05 1.01 o 12 1 1 2.65 2.02 0.29 o 13 1 1 4.26 4.55 0.44 o 1 2 1 3868.00 3690.66 55.69 o 2 2 1 290.09 298.42 3.92 o 3 2 1 100.05 102.67 1.78 o 4 2 1 712.72 696.57 5.78 o 5 2 1 649.04 635.78 4.94 o 6 2 1 92.72 89.21 0.98 o 7 2 1 283.56 280.65 2.97 o 8 2 1 84.16 87.70 1.13 o 9 2 1 33.47 32.15 0.72 o 10 2 1 37.76 35.02 0.77 o 11 2 1 31.38 32.27 0.78 o 12 2 1 8.02 6.76 0.42 o 13 2 1 8.95 7.26 0.42 o 0 3 1 999.41 957.97 17.00 o 1 3 1 121.27 108.14 1.81 o 2 3 1 971.23 935.00 11.94 o 3 3 1 63.60 68.84 1.11 o 4 3 1 108.59 112.61 1.07 o 5 3 1 27.24 26.71 0.38 o 6 3 1 19.07 19.20 0.40 o 7 3 1 136.18 127.79 1.47 o 8 3 1 66.32 64.00 0.94 o 9 3 1 37.70 38.65 0.98 o 10 3 1 133.82 125.34 2.83 o 11 3 1 37.83 37.14 0.94 o 12 3 1 0.45 0.98 0.31 o 13 3 1 7.74 7.31 0.55 o 1 4 1 1010.54 996.60 15.10 o 2 4 1 129.15 132.54 2.00 o 3 4 1 467.33 449.52 4.41 o 4 4 1 317.78 309.38 2.68 o 5 4 1 1.06 1.21 0.15 o 6 4 1 75.94 71.65 1.03 o 7 4 1 97.33 94.96 1.34 o 8 4 1 62.68 59.84 0.94 o 9 4 1 11.57 11.56 0.40 o 10 4 1 110.73 108.96 3.08 o 11 4 1 55.48 58.72 1.42 o 12 4 1 78.69 74.55 1.69 o 0 5 1 202.63 189.32 4.73 o 1 5 1 300.03 310.92 4.62 o 2 5 1 263.10 261.54 3.09 o 3 5 1 78.00 79.63 0.83 o 4 5 1 395.31 379.71 3.33 o 5 5 1 44.05 41.57 0.58 o 6 5 1 39.88 43.02 0.67 o 7 5 1 336.85 319.63 4.26 o 8 5 1 320.69 320.77 4.02 o 9 5 1 45.42 43.84 0.85 o 10 5 1 59.55 60.78 1.23 o 11 5 1 80.55 76.63 3.00 o 12 5 1 38.12 33.48 0.97 o 1 6 1 260.25 263.46 3.01 o 2 6 1 302.67 313.17 3.74 o 3 6 1 333.78 357.88 3.13 o 4 6 1 222.02 232.50 2.04 o 5 6 1 222.56 218.35 2.68 o 6 6 1 16.94 17.51 0.45 o 7 6 1 121.28 123.45 2.01 o 8 6 1 294.98 302.97 3.57 o 9 6 1 38.99 39.16 0.75 o 10 6 1 28.77 28.33 0.88 o 11 6 1 12.89 11.89 0.60 o 12 6 1 47.71 43.74 1.45 o 0 7 1 218.33 252.80 3.62 o 1 7 1 799.61 864.89 7.30 o 2 7 1 132.71 134.25 1.29 o 3 7 1 111.44 114.93 1.03 o 4 7 1 31.07 28.19 0.43 o 5 7 1 576.64 575.28 6.35 o 6 7 1 22.20 19.04 0.47 o 7 7 1 211.03 213.53 2.68 o 8 7 1 55.84 57.53 0.95 o 9 7 1 166.50 167.83 2.51 o 10 7 1 1.86 2.08 0.31 o 11 7 1 155.11 150.05 5.49 o 12 7 1 7.59 7.64 0.39 o 1 8 1 717.39 763.47 6.80 o 2 8 1 16.41 14.88 0.28 o 3 8 1 131.27 152.85 1.55 o 4 8 1 155.61 150.01 1.66 o 5 8 1 378.75 387.40 4.23 o 6 8 1 188.65 195.52 2.37 o 7 8 1 270.79 266.62 4.06 o 8 8 1 137.60 142.69 2.05 o 9 8 1 15.39 15.71 0.50 o 10 8 1 46.28 47.16 1.18 o 11 8 1 32.34 29.63 1.02 o 0 9 1 336.48 336.00 5.02 o 1 9 1 189.34 191.77 1.96 o 2 9 1 76.09 74.65 0.95 o 3 9 1 61.58 61.55 0.86 o 4 9 1 222.85 233.36 2.57 o 5 9 1 45.36 51.82 0.77 o 6 9 1 63.42 61.96 1.04 o 7 9 1 85.44 87.73 1.30 o 8 9 1 89.31 88.31 1.90 o 9 9 1 42.14 45.21 1.03 o 10 9 1 145.46 148.25 3.52 o 11 9 1 58.17 55.62 1.47 o 1 10 1 193.86 186.40 3.03 o 2 10 1 54.46 49.39 0.75 o 3 10 1 203.37 200.39 2.40 o 4 10 1 55.46 51.71 0.81 o 5 10 1 10.30 11.12 0.42 o 6 10 1 2.42 2.20 0.31 o 7 10 1 139.37 143.61 2.61 o 8 10 1 56.37 57.87 1.30 o 9 10 1 70.88 70.94 1.46 o 10 10 1 22.80 21.78 0.68 o 11 10 1 17.12 15.19 0.67 o 0 11 1 293.45 332.48 8.30 o 1 11 1 45.57 48.65 1.13 o 2 11 1 76.49 72.12 1.37 o 3 11 1 36.10 33.54 0.70 o 4 11 1 17.80 20.90 0.55 o 5 11 1 12.17 12.23 0.46 o 6 11 1 9.14 9.91 0.44 o 7 11 1 141.68 141.56 2.94 o 8 11 1 47.94 50.30 1.21 o 9 11 1 20.18 19.26 0.60 o 10 11 1 20.76 18.73 0.98 o 1 12 1 232.30 232.51 4.45 o 2 12 1 84.53 85.61 1.33 o 3 12 1 31.77 35.34 0.93 o 4 12 1 420.26 421.00 6.43 o 5 12 1 48.82 47.72 0.96 o 6 12 1 14.07 11.71 0.50 o 7 12 1 17.55 19.20 0.55 o 8 12 1 104.75 99.40 2.93 o 9 12 1 6.75 6.03 0.47 o 10 12 1 1.09 0.91 0.34 o 0 13 1 812.43 887.00 21.28 o 1 13 1 273.99 313.48 5.71 o 2 13 1 261.46 257.98 4.31 o 3 13 1 62.80 61.01 1.19 o 4 13 1 200.51 204.75 3.74 o 5 13 1 120.78 113.38 2.21 o 6 13 1 32.02 27.89 0.69 o 7 13 1 19.38 18.01 0.54 o 8 13 1 7.77 7.53 0.40 o 9 13 1 26.68 24.49 1.18 o 1 14 1 82.21 94.80 2.15 o 2 14 1 188.86 199.11 5.44 o 3 14 1 25.07 24.89 0.82 o 4 14 1 26.69 26.01 0.85 o 5 14 1 26.03 26.51 0.79 o 6 14 1 60.35 59.86 1.22 o 7 14 1 2.12 2.49 0.36 o 8 14 1 22.92 25.68 0.74 o 9 14 1 2.35 1.68 0.35 o 0 15 1 141.08 145.54 3.67 o 1 15 1 154.49 171.09 3.13 o 2 15 1 474.32 497.59 9.95 o 3 15 1 191.02 190.42 5.65 o 4 15 1 32.79 29.91 0.90 o 5 15 1 14.90 15.81 0.60 o 6 15 1 11.46 10.59 0.49 o 7 15 1 40.48 37.76 0.86 o 8 15 1 10.55 8.06 0.41 o 1 16 1 103.36 115.67 2.45 o 2 16 1 45.47 47.02 1.02 o 3 16 1 2.60 4.12 0.50 o 4 16 1 6.25 6.79 0.44 o 5 16 1 36.34 34.85 0.81 o 6 16 1 15.99 17.39 0.52 o 7 16 1 43.84 40.14 0.82 o 0 17 1 87.09 90.72 2.18 o 1 17 1 4.26 5.07 0.41 o 2 17 1 78.62 85.08 1.70 o 3 17 1 3.30 3.87 0.54 o 4 17 1 19.94 18.08 1.14 o 5 17 1 39.28 35.14 1.05 o 6 17 1 40.49 31.96 0.82 o 1 18 1 40.34 41.75 0.86 o 2 18 1 12.60 13.05 0.59 o 3 18 1 10.00 10.74 0.66 o 4 18 1 7.33 5.18 0.52 o 0 19 1 3.22 3.56 0.47 o 1 19 1 26.80 25.80 0.72 o 2 19 1 13.37 12.67 0.81 o 0 0 2 264.91 238.51 3.85 o 2 0 2 1623.50 1553.31 16.15 o 4 0 2 2702.27 2609.99 27.78 o 6 0 2 124.75 126.09 1.82 o 8 0 2 78.35 78.01 1.65 o 10 0 2 27.57 27.81 0.88 o 12 0 2 7.04 7.67 0.58 o 1 1 2 116.46 107.16 0.95 o 2 1 2 192.45 178.97 1.34 o 3 1 2 220.70 185.47 1.85 o 4 1 2 691.60 637.83 5.11 o 5 1 2 74.75 78.25 0.81 o 6 1 2 7.74 8.81 0.32 o 7 1 2 23.13 22.19 0.52 o 8 1 2 31.72 33.17 0.63 o 9 1 2 103.20 99.65 2.17 o 10 1 2 30.88 28.49 0.65 o 11 1 2 6.77 7.29 0.34 o 12 1 2 6.63 6.62 0.41 o 0 2 2 195.86 179.13 1.67 o 1 2 2 317.31 271.00 2.54 o 2 2 2 233.57 219.10 1.58 o 3 2 2 1528.65 1490.12 9.51 o 4 2 2 75.72 80.18 0.71 o 5 2 2 57.17 54.99 0.64 o 6 2 2 19.02 19.68 0.39 o 7 2 2 19.10 18.67 0.47 o 8 2 2 117.39 119.34 1.66 o 9 2 2 2.16 2.66 0.35 o 10 2 2 24.68 25.25 0.60 o 11 2 2 4.44 4.99 0.29 o 12 2 2 22.00 23.64 0.60 o 1 3 2 30.92 26.05 0.29 o 2 3 2 554.74 510.31 3.60 o 3 3 2 38.33 33.46 0.33 o 4 3 2 59.22 56.72 0.57 o 5 3 2 4.83 6.72 0.24 o 6 3 2 185.34 191.96 2.33 o 7 3 2 7.33 8.06 0.37 o 8 3 2 83.06 80.23 1.24 o 9 3 2 54.81 54.64 1.04 o 10 3 2 4.52 4.14 0.32 o 11 3 2 25.72 24.61 0.73 o 12 3 2 6.51 4.24 0.27 o 0 4 2 3.78 5.66 0.23 o 1 4 2 14.64 15.10 0.21 o 2 4 2 24.21 23.24 0.27 o 3 4 2 350.12 324.06 2.28 o 4 4 2 98.40 98.79 0.85 o 5 4 2 348.36 352.36 3.52 o 6 4 2 35.40 37.92 0.61 o 7 4 2 0.12 0.44 0.30 o 8 4 2 13.87 14.16 0.48 o 9 4 2 51.82 55.76 0.94 o 10 4 2 29.43 32.55 0.85 o 11 4 2 9.90 13.67 0.46 o 1 5 2 76.26 69.59 0.58 o 2 5 2 32.28 30.91 0.34 o 3 5 2 77.49 72.26 0.68 o 4 5 2 66.04 64.35 0.73 o 5 5 2 119.65 126.63 1.35 o 6 5 2 799.05 854.50 8.89 o 7 5 2 21.24 22.35 0.52 o 8 5 2 22.60 25.20 0.59 o 9 5 2 8.74 9.53 0.40 o 10 5 2 1.70 2.34 0.27 o 11 5 2 7.95 7.25 0.32 o 0 6 2 571.35 556.85 5.72 o 1 6 2 490.03 455.40 3.25 o 2 6 2 21.19 20.69 0.30 o 3 6 2 64.53 62.17 0.69 o 4 6 2 159.53 153.93 1.65 o 5 6 2 61.33 60.27 0.79 o 6 6 2 76.34 75.96 0.98 o 7 6 2 161.10 169.64 3.09 o 8 6 2 65.46 67.41 1.13 o 9 6 2 21.28 21.45 0.57 o 10 6 2 7.12 8.33 0.35 o 11 6 2 1.49 1.17 0.22 o 1 7 2 89.50 82.07 0.70 o 2 7 2 49.78 52.29 0.61 o 3 7 2 81.73 76.39 0.81 o 4 7 2 38.77 34.38 0.52 o 5 7 2 360.01 375.78 4.12 o 6 7 2 88.64 95.86 1.58 o 7 7 2 328.28 344.21 7.64 o 8 7 2 1.94 1.54 0.31 o 9 7 2 15.38 14.88 0.45 o 10 7 2 5.67 5.76 0.32 o 11 7 2 2.16 1.48 0.25 o 0 8 2 18.03 20.11 0.50 o 1 8 2 583.93 575.82 5.32 o 2 8 2 33.64 31.98 0.48 o 3 8 2 79.31 75.23 0.93 o 4 8 2 36.29 37.70 0.62 o 5 8 2 74.09 76.97 1.05 o 6 8 2 79.13 83.12 1.41 o 7 8 2 72.64 79.75 2.11 o 8 8 2 16.20 16.67 0.53 o 9 8 2 9.26 9.14 0.38 o 10 8 2 5.56 5.72 0.32 o 1 9 2 57.54 58.03 0.75 o 2 9 2 3.49 2.42 0.23 o 3 9 2 43.02 42.01 0.68 o 4 9 2 48.44 46.36 0.72 o 5 9 2 144.29 150.81 2.02 o 6 9 2 434.46 476.01 5.89 o 7 9 2 71.89 73.64 1.35 o 8 9 2 14.34 14.48 0.57 o 9 9 2 7.26 6.94 0.39 o 10 9 2 20.44 22.83 0.87 o 0 10 2 78.79 74.38 1.39 o 1 10 2 18.25 17.85 0.43 o 2 10 2 42.99 41.53 0.68 o 3 10 2 152.38 143.63 1.94 o 4 10 2 30.02 30.08 0.67 o 5 10 2 284.13 301.71 3.83 o 6 10 2 18.51 21.35 0.58 o 7 10 2 8.24 9.39 0.46 o 8 10 2 16.87 17.23 0.61 o 9 10 2 10.24 9.27 0.39 o 10 10 2 1.15 0.89 0.27 o 1 11 2 115.21 110.09 1.52 o 2 11 2 51.06 48.07 0.87 o 3 11 2 1.10 1.43 0.29 o 4 11 2 32.88 36.01 0.78 o 5 11 2 10.79 11.42 0.53 o 6 11 2 115.15 116.29 2.79 o 7 11 2 18.90 18.20 0.68 o 8 11 2 5.29 6.23 0.42 o 9 11 2 14.06 13.46 0.69 o 0 12 2 85.06 84.16 2.06 o 1 12 2 10.67 10.87 0.47 o 2 12 2 87.58 85.32 1.43 o 3 12 2 237.61 225.44 6.05 o 4 12 2 10.16 12.17 0.52 o 5 12 2 16.87 14.68 0.62 o 6 12 2 33.73 33.40 1.01 o 7 12 2 2.72 2.80 0.39 o 8 12 2 9.39 9.09 0.49 o 9 12 2 0.66 0.87 0.32 o 1 13 2 68.33 66.86 1.34 o 2 13 2 31.39 31.18 0.84 o 3 13 2 39.62 45.09 1.22 o 4 13 2 148.53 137.91 4.62 o 5 13 2 33.89 33.66 1.09 o 6 13 2 113.21 109.20 2.69 o 7 13 2 18.89 20.11 0.65 o 8 13 2 1.77 2.28 0.31 o 0 14 2 153.24 148.23 3.17 o 1 14 2 19.62 20.92 0.74 o 2 14 2 187.93 184.77 3.93 o 3 14 2 250.28 243.76 5.61 o 4 14 2 247.99 254.96 4.31 o 5 14 2 12.82 11.43 0.65 o 6 14 2 31.47 29.04 0.99 o 7 14 2 14.22 14.27 0.76 o 1 15 2 102.19 92.25 1.87 o 2 15 2 21.95 22.75 0.99 o 3 15 2 39.84 38.11 1.15 o 4 15 2 96.68 99.47 3.38 o 5 15 2 35.03 31.97 1.43 o 6 15 2 32.80 28.49 0.96 o 0 16 2 73.65 69.17 4.38 o 1 16 2 6.64 5.84 0.43 o 2 16 2 13.57 12.21 0.58 o 3 16 2 70.76 70.39 1.90 o 4 16 2 24.02 20.60 0.84 o 5 16 2 23.76 23.52 0.85 o 1 17 2 4.85 4.27 0.36 o 2 17 2 93.55 78.45 3.28 o 3 17 2 31.33 28.41 1.71 o 4 17 2 37.61 29.67 1.67 o 0 18 2 12.95 10.03 0.70 o 2 0 3 243.57 250.51 3.20 o 4 0 3 381.73 401.91 4.95 o 6 0 3 417.17 440.12 9.44 o 8 0 3 14.80 12.04 0.84 o 10 0 3 10.44 12.39 0.52 o 0 1 3 264.93 275.25 4.62 o 1 1 3 43.92 45.04 0.62 o 2 1 3 137.79 159.05 1.58 o 3 1 3 67.56 69.03 0.81 o 4 1 3 144.49 154.67 1.48 o 5 1 3 215.12 228.21 2.04 o 6 1 3 120.20 130.47 2.24 o 7 1 3 53.75 56.69 1.02 o 8 1 3 41.40 40.99 0.89 o 9 1 3 6.99 7.40 0.32 o 10 1 3 7.43 8.25 0.32 o 1 2 3 168.17 173.44 1.69 o 2 2 3 5.89 6.19 0.25 o 3 2 3 3.26 3.43 0.22 o 4 2 3 184.87 195.34 1.81 o 5 2 3 255.64 264.74 2.91 o 6 2 3 68.24 70.31 1.19 o 7 2 3 41.01 40.32 0.98 o 8 2 3 14.66 17.08 0.55 o 9 2 3 7.44 8.81 0.45 o 10 2 3 7.05 10.42 0.39 o 0 3 3 150.57 142.10 2.11 o 1 3 3 0.66 0.72 0.19 o 2 3 3 25.16 26.86 0.42 o 3 3 3 11.00 9.97 0.28 o 4 3 3 8.66 9.72 0.28 o 5 3 3 43.02 43.92 0.64 o 6 3 3 26.54 27.19 0.79 o 7 3 3 1.30 2.39 0.32 o 8 3 3 18.92 19.37 0.52 o 9 3 3 2.69 3.35 0.29 o 10 3 3 2.65 3.15 0.36 o 1 4 3 7.77 7.56 0.26 o 2 4 3 40.68 40.71 0.57 o 3 4 3 53.28 55.13 0.70 o 4 4 3 2.57 3.35 0.23 o 5 4 3 70.10 70.13 1.44 o 6 4 3 38.52 40.63 0.84 o 7 4 3 22.27 23.78 0.56 o 8 4 3 32.45 36.37 0.75 o 9 4 3 11.26 10.85 0.38 o 10 4 3 20.20 23.35 0.53 o 0 5 3 49.94 52.41 1.02 o 1 5 3 44.74 41.35 0.56 o 2 5 3 12.11 12.63 0.32 o 3 5 3 64.25 63.44 0.76 o 4 5 3 159.12 163.60 1.60 o 5 5 3 7.20 8.27 0.32 o 6 5 3 6.57 6.94 0.29 o 7 5 3 77.42 81.78 2.12 o 8 5 3 39.37 43.29 1.30 o 9 5 3 1.43 2.00 0.28 o 10 5 3 7.84 11.41 0.53 o 1 6 3 10.72 9.45 0.26 o 2 6 3 163.69 163.85 1.62 o 3 6 3 40.34 39.07 0.58 o 4 6 3 303.28 320.46 3.71 o 5 6 3 120.64 128.79 1.44 o 6 6 3 48.47 50.14 0.95 o 7 6 3 16.23 16.39 0.71 o 8 6 3 43.83 51.72 0.97 o 9 6 3 4.57 4.48 0.29 o 0 7 3 43.16 40.85 0.78 o 1 7 3 195.03 191.31 1.93 o 2 7 3 65.22 65.36 0.85 o 3 7 3 382.92 385.95 5.39 o 4 7 3 57.29 57.30 0.84 o 5 7 3 310.45 328.80 5.08 o 6 7 3 5.34 5.56 0.34 o 7 7 3 45.26 46.16 1.20 o 8 7 3 11.74 12.61 0.67 o 9 7 3 43.67 43.47 1.04 o 1 8 3 23.36 20.41 0.40 o 2 8 3 28.35 29.01 0.50 o 3 8 3 36.95 39.55 0.66 o 4 8 3 122.61 121.73 1.94 o 5 8 3 134.85 139.93 2.19 o 6 8 3 4.47 4.41 0.32 o 7 8 3 5.82 4.51 0.33 o 8 8 3 23.70 27.16 0.74 o 9 8 3 7.58 7.68 0.43 o 0 9 3 33.48 35.05 0.86 o 1 9 3 68.45 66.51 1.01 o 2 9 3 2.28 2.48 0.27 o 3 9 3 116.05 118.54 1.62 o 4 9 3 87.95 86.57 1.94 o 5 9 3 23.90 24.84 0.62 o 6 9 3 10.77 10.58 0.40 o 7 9 3 21.28 21.87 0.78 o 8 9 3 17.49 16.80 0.58 o 1 10 3 8.17 8.06 0.34 o 2 10 3 29.15 28.79 0.58 o 3 10 3 47.51 49.59 0.93 o 4 10 3 16.41 17.37 0.57 o 5 10 3 3.58 4.59 0.36 o 6 10 3 0.38 0.38 0.25 o 7 10 3 15.87 14.41 0.73 o 8 10 3 5.60 5.74 0.58 o 0 11 3 14.05 12.95 0.61 o 1 11 3 8.04 8.03 0.43 o 2 11 3 6.21 6.54 0.33 o 3 11 3 62.84 59.67 1.08 o 4 11 3 1.79 1.62 0.34 o 5 11 3 1.98 2.36 0.33 o 6 11 3 33.24 33.41 0.79 o 7 11 3 28.54 28.74 0.83 o 1 12 3 22.05 20.92 0.57 o 2 12 3 17.03 15.52 0.48 o 3 12 3 0.77 0.62 0.27 o 4 12 3 45.99 43.39 0.89 o 5 12 3 68.43 65.99 2.09 o 6 12 3 2.30 1.83 0.27 o 0 13 3 96.76 87.49 2.25 o 1 13 3 45.78 42.69 0.90 o 2 13 3 34.70 31.67 0.83 o 3 13 3 21.24 18.66 0.70 o 4 13 3 37.73 31.91 1.02 o 5 13 3 179.33 150.69 3.93 o 1 14 3 26.67 21.99 0.64 o 2 14 3 29.85 26.02 1.03 o 3 14 3 20.50 19.06 0.81 o 4 14 3 103.11 85.95 3.49 o 0 15 3 17.50 14.65 1.58 o 1 15 3 8.73 6.27 0.50 o 2 15 3 67.07 51.92 1.72 o 0 0 4 439.59 522.50 9.86 o 2 0 4 15.62 17.03 0.63 o 4 0 4 33.18 35.14 0.70 o 6 0 4 57.20 54.39 1.45 o 1 1 4 40.41 43.45 0.76 o 2 1 4 25.59 26.90 0.55 o 3 1 4 11.89 13.38 0.35 o 4 1 4 6.91 8.27 0.28 o 5 1 4 16.99 14.76 0.37 o 6 1 4 125.87 118.69 2.31 o 7 1 4 81.41 73.19 1.80 o 0 2 4 1.37 2.49 0.42 o 1 2 4 24.88 24.91 0.54 o 2 2 4 44.67 51.63 0.75 o 3 2 4 3.53 3.46 0.24 o 4 2 4 6.38 5.65 0.24 o 5 2 4 19.26 20.63 0.44 o 6 2 4 46.98 46.84 0.89 o 7 2 4 69.59 67.92 1.13 o 1 3 4 4.32 4.19 0.30 o 2 3 4 5.01 5.06 0.28 o 3 3 4 1.54 1.38 0.21 o 4 3 4 31.53 34.14 0.71 o 5 3 4 5.29 5.81 0.28 o 6 3 4 19.16 18.78 0.45 o 7 3 4 32.10 24.60 0.54 o 0 4 4 43.07 50.01 1.14 o 1 4 4 9.87 10.71 0.36 o 2 4 4 1.29 1.27 0.24 o 3 4 4 53.83 55.84 0.77 o 4 4 4 12.68 11.31 0.32 o 5 4 4 24.74 25.33 0.53 o 6 4 4 12.34 11.52 0.38 o 7 4 4 4.91 4.75 0.29 o 1 5 4 18.10 18.30 0.40 o 2 5 4 77.26 83.74 1.10 o 3 5 4 19.25 22.13 0.48 o 4 5 4 5.93 6.46 0.28 o 5 5 4 38.63 37.07 0.87 o 6 5 4 16.17 15.42 0.49 o 0 6 4 90.87 96.01 1.94 o 1 6 4 88.11 95.00 1.31 o 2 6 4 110.47 112.16 2.14 o 3 6 4 166.14 170.46 3.43 o 4 6 4 48.74 47.16 1.07 o 5 6 4 16.70 15.41 0.41 o 6 6 4 4.00 4.12 0.61 o 1 7 4 6.83 6.88 0.38 o 2 7 4 30.64 31.58 0.69 o 3 7 4 85.38 86.93 1.42 o 4 7 4 10.43 8.79 0.40 o 5 7 4 26.00 22.04 0.69 o 0 8 4 11.79 12.05 0.52 o 1 8 4 67.43 68.29 1.17 o 2 8 4 17.25 17.15 0.53 o 3 8 4 222.88 210.79 6.89 o 4 8 4 5.03 4.59 0.35 o 5 8 4 14.00 10.28 0.61 o 1 9 4 54.85 52.05 0.98 o 2 9 4 60.21 57.40 1.39 o 3 9 4 8.96 7.99 0.57 o 4 9 4 12.14 10.11 0.50 o 0 10 4 5.23 5.51 0.43 o 1 10 4 4.75 4.09 0.27 o 2 10 4 7.46 6.21 0.44 o 3 10 4 16.05 14.12 1.84 o 1 11 4 4.66 3.52 0.85 o