#------------------------------------------------------------------------------ #$Date: 2018-11-08 05:52:15 +0200 (Thu, 08 Nov 2018) $ #$Revision: 211856 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/27/2242714.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242714 _cell_angle_alpha 90.000 _cell_angle_beta 100.444 _cell_angle_gamma 90.000 _cell_length_a 11.6979 _cell_length_b 25.7716 _cell_length_c 14.1055 _exptl_crystal_F_000 1888.33 _reflns_d_resolution_high 0.7951 _cod_data_source_file sj5565IIIsup4.hkl _cod_data_source_block III _shelx_title ' f22cga' _shelx_refln_list_code 4 _shelx_f_calc_maximum 370.19 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28511.40 30350.99 1786.34 o 4 0 0 780.26 1113.13 188.55 o 6 0 0 2483.36 2306.49 335.12 o 8 0 0 34.64 231.40 147.95 o 10 0 0 1733.92 1929.06 400.84 o 12 0 0 881.81 1261.13 360.33 o 14 0 0 103.85 29.00 137.67 o 1 1 0 64.26 37.00 8.60 o 2 1 0 335.45 436.39 59.93 o 3 1 0 2566.91 2521.98 214.19 o 4 1 0 305.81 287.80 102.71 o 5 1 0 121.33 165.83 68.30 o 6 1 0 136.53 206.37 73.14 o 7 1 0 61.68 84.76 117.38 o 8 1 0 179.29 141.26 87.89 o 9 1 0 434.15 296.05 115.30 o 10 1 0 1391.22 2226.95 316.56 o 11 1 0 406.88 556.91 194.14 o 12 1 0 4149.06 4620.95 658.98 o 13 1 0 460.97 562.45 149.35 o 14 1 0 525.37 854.03 184.60 o 0 2 0 7897.70 7526.27 224.23 o 1 2 0 16970.04 16876.04 217.13 o 2 2 0 2.05 7.83 10.50 o 3 2 0 278.49 320.42 52.31 o 4 2 0 983.87 842.68 72.72 o 5 2 0 6.50 4.58 27.14 o 6 2 0 83.28 40.36 43.93 o 7 2 0 1329.06 1419.81 207.14 o 8 2 0 20.41 -16.60 137.17 o 9 2 0 1098.67 941.25 198.05 o 10 2 0 35.28 138.99 84.35 o 11 2 0 234.85 187.80 93.42 o 12 2 0 400.53 357.25 116.73 o 13 2 0 239.37 152.75 60.40 o 14 2 0 0.13 48.34 53.13 o 1 3 0 324.67 415.29 25.51 o 2 3 0 28.15 52.85 21.96 o 3 3 0 1508.92 1348.94 89.34 o 4 3 0 2994.18 3149.47 157.16 o 5 3 0 2306.86 2211.32 125.03 o 6 3 0 53.98 -11.90 35.82 o 7 3 0 8213.58 8670.87 502.96 o 8 3 0 186.43 413.79 120.96 o 9 3 0 379.01 483.04 140.18 o 10 3 0 123.59 1091.45 210.07 o 11 3 0 561.62 556.79 129.66 o 12 3 0 119.33 74.87 63.70 o 13 3 0 1800.57 2220.70 291.19 o 14 3 0 11.72 -28.35 97.13 o 0 4 0 47.63 113.58 16.04 o 1 4 0 84.98 87.13 13.69 o 2 4 0 2777.94 2773.71 79.82 o 3 4 0 2903.23 2745.43 188.88 o 4 4 0 3286.05 3014.82 153.42 o 5 4 0 334.79 555.99 88.84 o 6 4 0 369.66 417.82 52.60 o 7 4 0 7062.74 7580.52 377.59 o 8 4 0 1684.49 1649.18 190.14 o 9 4 0 2.04 43.01 62.19 o 10 4 0 661.94 642.15 142.45 o 11 4 0 238.24 195.96 80.24 o 12 4 0 41.82 9.21 51.79 o 13 4 0 3.34 -67.63 76.71 o 14 4 0 19.58 -81.31 109.67 o 1 5 0 5140.15 4912.90 122.01 o 2 5 0 106.81 249.43 32.01 o 3 5 0 2877.35 2909.83 129.60 o 4 5 0 84.71 47.12 26.36 o 5 5 0 394.97 410.50 66.77 o 6 5 0 6.08 6.89 39.97 o 7 5 0 1366.98 1162.15 150.56 o 8 5 0 5551.25 5457.14 343.06 o 9 5 0 61.35 52.84 41.16 o 10 5 0 6614.52 6513.24 480.62 o 11 5 0 2552.57 2747.48 287.22 o 12 5 0 392.30 338.01 105.84 o 13 5 0 168.88 181.63 91.48 o 14 5 0 1732.29 1851.98 271.97 o 0 6 0 4387.06 5242.79 123.22 o 1 6 0 17523.72 17429.10 194.25 o 2 6 0 13319.47 12965.84 244.91 o 3 6 0 2586.33 2523.83 86.68 o 4 6 0 1876.26 1604.01 143.77 o 5 6 0 230.87 245.77 48.90 o 6 6 0 3126.63 2930.36 186.51 o 7 6 0 233.54 368.10 81.76 o 8 6 0 9620.50 10670.11 478.81 o 9 6 0 106.30 198.36 60.72 o 10 6 0 1251.44 1265.25 271.45 o 11 6 0 188.17 197.51 89.50 o 12 6 0 131.99 135.08 95.04 o 13 6 0 25.50 11.96 56.62 o 14 6 0 212.91 420.22 133.83 o 1 7 0 3590.44 3472.04 91.16 o 2 7 0 21564.16 20856.93 244.68 o 3 7 0 3866.67 3748.24 116.41 o 4 7 0 944.72 870.31 81.26 o 5 7 0 275.98 220.54 48.66 o 6 7 0 284.90 223.08 55.40 o 7 7 0 617.90 695.62 138.49 o 8 7 0 1254.79 1395.62 175.67 o 9 7 0 406.86 303.24 82.23 o 10 7 0 115.91 82.07 39.97 o 11 7 0 711.36 736.13 149.31 o 12 7 0 96.43 61.62 46.05 o 13 7 0 2.13 75.50 69.98 o 14 7 0 64.05 -64.11 70.06 o 0 8 0 7406.55 7793.01 170.63 o 1 8 0 42.29 64.28 13.85 o 2 8 0 382.23 420.57 36.30 o 3 8 0 4890.81 4552.33 129.12 o 4 8 0 162.36 378.05 46.32 o 5 8 0 8077.43 7207.17 332.49 o 6 8 0 158.03 76.95 49.12 o 7 8 0 338.10 305.45 68.82 o 8 8 0 1.76 43.41 48.74 o 9 8 0 1132.35 964.86 150.60 o 10 8 0 428.16 295.54 173.50 o 11 8 0 487.98 466.75 121.98 o 12 8 0 26.72 3.16 64.70 o 13 8 0 498.60 535.75 155.92 o 14 8 0 30.06 -34.16 111.95 o 1 9 0 469.87 529.73 35.57 o 2 9 0 11126.90 11469.01 178.60 o 3 9 0 38.60 742.03 145.74 o 4 9 0 1033.30 1274.49 78.80 o 5 9 0 756.67 839.53 91.81 o 6 9 0 1734.07 1696.67 141.42 o 7 9 0 2113.10 2032.31 168.36 o 8 9 0 15.01 -6.21 32.67 o 9 9 0 3012.26 3033.83 268.79 o 10 9 0 234.36 195.90 83.08 o 11 9 0 171.06 228.88 88.65 o 12 9 0 598.04 630.01 220.48 o 13 9 0 29.50 118.98 63.20 o 0 10 0 49.04 40.33 16.36 o 1 10 0 493.22 654.65 40.09 o 2 10 0 444.52 536.35 43.39 o 3 10 0 3627.10 3698.44 120.54 o 4 10 0 19274.19 19301.87 303.54 o 5 10 0 360.62 340.38 50.26 o 6 10 0 3154.65 2578.90 171.92 o 7 10 0 301.94 412.34 71.98 o 8 10 0 2165.79 2007.57 159.81 o 9 10 0 1536.06 1527.31 159.94 o 10 10 0 101.14 197.22 74.35 o 11 10 0 708.38 889.24 156.56 o 12 10 0 384.21 378.42 104.90 o 13 10 0 22.93 102.92 66.29 o 1 11 0 119.07 133.73 21.09 o 2 11 0 7279.07 7585.73 167.36 o 3 11 0 603.40 931.64 102.45 o 4 11 0 5460.94 5877.26 166.87 o 5 11 0 137.22 72.10 21.70 o 6 11 0 2402.39 2248.48 144.25 o 7 11 0 73.54 53.62 24.49 o 8 11 0 4600.45 4250.76 207.16 o 9 11 0 60.81 58.38 30.93 o 10 11 0 1323.76 1292.43 192.97 o 11 11 0 890.17 1277.80 191.75 o 12 11 0 720.81 744.32 156.00 o 13 11 0 340.59 416.91 126.75 o 0 12 0 978.18 895.44 71.04 o 1 12 0 563.11 445.16 40.30 o 2 12 0 4056.93 3870.14 130.87 o 3 12 0 11140.43 11773.19 205.56 o 4 12 0 1454.31 1256.70 77.43 o 5 12 0 1879.21 1738.95 110.16 o 6 12 0 1364.60 1292.54 111.95 o 7 12 0 108.32 204.37 113.36 o 8 12 0 2421.51 2416.33 172.78 o 9 12 0 1858.22 1834.69 158.22 o 10 12 0 3475.12 4307.08 252.53 o 11 12 0 130.81 99.23 46.09 o 12 12 0 289.11 372.44 93.83 o 13 12 0 172.51 -13.43 93.19 o 1 13 0 22.02 16.27 13.89 o 2 13 0 107.36 185.06 24.81 o 3 13 0 1876.47 1944.35 114.40 o 4 13 0 1430.56 1704.75 92.10 o 5 13 0 70.91 78.81 24.03 o 6 13 0 101.73 110.44 34.36 o 7 13 0 1561.21 1496.70 127.54 o 8 13 0 32.75 69.65 43.45 o 9 13 0 857.46 707.23 95.47 o 10 13 0 543.92 750.41 119.03 o 11 13 0 475.02 498.28 119.42 o 12 13 0 525.13 528.10 147.55 o 13 13 0 101.25 154.70 126.18 o 0 14 0 212.39 138.36 38.44 o 1 14 0 15716.89 15298.61 256.04 o 2 14 0 6061.53 6298.75 158.61 o 3 14 0 2354.92 2178.70 99.96 o 4 14 0 2463.09 2625.42 108.56 o 5 14 0 1740.09 1638.83 104.75 o 6 14 0 6.82 57.56 24.39 o 7 14 0 2028.03 2068.55 151.95 o 8 14 0 679.30 634.60 89.19 o 9 14 0 51.56 25.86 37.65 o 10 14 0 114.30 62.85 48.45 o 11 14 0 1959.50 2279.93 317.87 o 12 14 0 30.78 -14.47 83.54 o 13 14 0 309.47 565.96 296.22 o 1 15 0 113.70 133.56 25.15 o 2 15 0 0.09 45.82 20.10 o 3 15 0 104.08 129.10 26.77 o 4 15 0 47.13 55.93 16.58 o 5 15 0 267.58 285.54 47.56 o 6 15 0 617.89 501.25 95.69 o 7 15 0 1304.54 1395.93 124.83 o 8 15 0 205.93 265.49 69.84 o 9 15 0 75.35 79.46 48.45 o 10 15 0 560.42 553.04 107.51 o 11 15 0 2150.25 2628.42 346.63 o 12 15 0 106.50 198.84 227.81 o 0 16 0 6760.54 7248.30 308.31 o 1 16 0 738.65 631.65 54.84 o 2 16 0 4130.04 4206.69 135.63 o 3 16 0 16.07 34.03 13.70 o 4 16 0 1032.86 978.39 73.86 o 5 16 0 374.38 381.93 48.61 o 6 16 0 1972.46 1857.45 114.88 o 7 16 0 316.42 361.85 69.20 o 8 16 0 3685.29 3599.45 211.54 o 9 16 0 7.37 86.26 68.94 o 10 16 0 1603.20 1435.57 172.57 o 11 16 0 204.28 291.10 126.60 o 12 16 0 504.00 609.77 182.92 o 1 17 0 159.71 321.78 87.35 o 2 17 0 1665.19 1713.78 121.06 o 3 17 0 4.99 -3.95 12.95 o 4 17 0 1.72 4.14 15.51 o 5 17 0 1.25 73.49 29.63 o 6 17 0 5.24 31.06 22.60 o 7 17 0 28.92 107.02 32.13 o 8 17 0 1075.39 1435.91 135.48 o 9 17 0 234.20 148.53 51.99 o 10 17 0 571.25 638.11 100.14 o 11 17 0 211.41 199.43 129.18 o 12 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113.14 o 7 27 0 4.40 94.37 61.04 o 8 27 0 911.58 1085.69 280.77 o 0 28 0 3591.04 4912.87 665.22 o 1 28 0 353.05 244.67 117.58 o 2 28 0 447.80 668.24 135.55 o 3 28 0 74.45 4.33 51.23 o 4 28 0 3188.66 3696.10 326.99 o 5 28 0 175.01 137.82 69.41 o 6 28 0 2188.91 2536.93 283.31 o 7 28 0 152.63 196.23 101.10 o 1 29 0 167.51 258.29 195.17 o 2 29 0 168.80 96.48 68.88 o 3 29 0 574.94 535.52 129.36 o 4 29 0 8.78 -14.48 73.20 o 5 29 0 168.33 298.96 153.06 o 6 29 0 159.74 184.15 129.52 o 0 30 0 420.50 510.74 214.75 o 1 30 0 6.69 -43.37 43.37 o 2 30 0 4.65 38.89 40.98 o 3 30 0 2408.23 2981.41 311.54 o 4 30 0 1.35 86.38 50.46 o 5 30 0 153.12 33.84 131.54 o 1 31 0 59.50 -8.15 109.42 o 2 31 0 1293.05 1542.68 232.16 o 3 31 0 131.39 181.69 80.25 o 4 31 0 0.30 62.68 121.47 o 0 32 0 277.77 433.38 209.72 o 1 32 0 2.81 78.85 61.37 o 2 32 0 243.09 171.55 204.47 o -13 0 1 2400.00 2378.28 526.05 o -11 0 1 4842.11 4662.37 666.00 o -9 0 1 2573.00 2312.50 427.87 o -7 0 1 1269.73 1723.59 323.20 o -5 0 1 15637.79 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