#------------------------------------------------------------------------------ #$Date: 2019-01-30 06:00:47 +0200 (Wed, 30 Jan 2019) $ #$Revision: 213390 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/28/2242835.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242835 _cell_angle_alpha 90.000 _cell_angle_beta 109.455 _cell_angle_gamma 90.000 _cell_length_a 17.5353 _cell_length_b 22.4798 _cell_length_c 21.2031 _exptl_crystal_F_000 3056.00 _reflns_d_resolution_high 0.8176 _cod_data_source_file ex2018Isup2.hkl _cod_data_source_block I _shelx_title ' mefedrone P21/c Apex II 190K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 521.58 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10717.31 7665.13 121.42 o 3 0 0 5760.95 3712.76 69.58 o 4 0 0 40.47 167.80 20.23 o 5 0 0 33335.60 33620.73 514.30 o 6 0 0 52001.03 57633.09 997.13 o 7 0 0 17652.91 16485.47 271.13 o 8 0 0 1305.60 1492.31 56.33 o 9 0 0 2720.47 2658.03 76.09 o 10 0 0 28272.04 28826.82 531.63 o 11 0 0 653.11 675.42 47.24 o 12 0 0 114.43 72.23 54.72 o 13 0 0 322.22 266.20 43.71 o 14 0 0 150.78 148.86 43.49 o 15 0 0 0.70 46.93 40.67 o 16 0 0 78.68 25.23 53.28 o 17 0 0 335.53 218.66 67.90 o 18 0 0 858.10 742.57 116.56 o 19 0 0 352.58 348.82 77.34 o 20 0 0 211.02 265.55 102.60 o 1 1 0 1207.34 773.72 12.95 o 2 1 0 1718.91 1751.41 35.73 o 3 1 0 64892.86 58688.93 705.91 o 4 1 0 3089.47 1951.09 35.02 o 5 1 0 1333.08 1515.00 32.20 o 6 1 0 688.81 993.15 27.97 o 7 1 0 9560.92 10016.06 139.38 o 8 1 0 1446.20 1587.40 40.85 o 9 1 0 973.35 1400.22 47.98 o 10 1 0 355.89 438.66 34.68 o 11 1 0 6090.62 6067.96 94.98 o 12 1 0 18.23 46.14 23.81 o 13 1 0 1068.28 1002.86 42.75 o 14 1 0 0.21 -26.94 26.94 o 15 1 0 1203.48 1365.57 52.57 o 16 1 0 109.44 115.32 36.93 o 17 1 0 0.84 -28.18 39.43 o 18 1 0 37.61 43.28 62.01 o 19 1 0 42.84 29.80 51.90 o 20 1 0 670.66 702.24 103.60 o 1 2 0 1777.52 380.49 10.55 o 2 2 0 420.91 102.52 8.04 o 3 2 0 3802.65 3466.80 49.93 o 4 2 0 2834.24 5099.22 66.88 o 5 2 0 16723.32 14998.84 170.80 o 6 2 0 1022.20 1202.34 31.15 o 7 2 0 1682.10 1138.53 38.00 o 8 2 0 458.11 286.29 22.65 o 9 2 0 285.18 164.43 21.36 o 10 2 0 88.83 121.42 21.57 o 11 2 0 1319.12 1446.13 44.53 o 12 2 0 137.32 131.45 25.67 o 13 2 0 422.61 474.50 34.50 o 14 2 0 1.43 25.41 27.56 o 15 2 0 9.24 32.52 29.44 o 16 2 0 10.89 -11.91 33.43 o 17 2 0 311.52 329.37 50.10 o 18 2 0 34.72 -11.84 41.65 o 19 2 0 1.97 -14.28 51.20 o 20 2 0 0.93 -4.57 95.46 o 1 3 0 14104.44 7596.14 86.84 o 2 3 0 6170.72 8985.95 102.37 o 3 3 0 22.55 183.35 12.78 o 4 3 0 150.11 383.07 23.72 o 5 3 0 15224.27 18493.47 207.76 o 6 3 0 2478.46 3056.93 50.69 o 7 3 0 405.02 440.83 23.15 o 8 3 0 14251.36 13472.49 164.46 o 9 3 0 170.59 197.00 22.01 o 10 3 0 5.35 -15.08 18.98 o 11 3 0 129.56 134.50 24.16 o 12 3 0 1559.39 1826.05 52.66 o 13 3 0 3015.41 2884.50 79.23 o 14 3 0 2804.29 2714.38 67.92 o 15 3 0 457.42 459.32 42.48 o 16 3 0 22.09 -13.07 34.50 o 17 3 0 196.52 165.02 40.27 o 18 3 0 51.90 44.89 48.76 o 19 3 0 10.06 -32.13 44.49 o 20 3 0 382.70 461.58 80.90 o 0 4 0 158982.89 163822.97 2414.32 o 1 4 0 9753.60 2582.20 37.85 o 2 4 0 41534.18 63128.54 664.77 o 3 4 0 1158.86 1614.97 31.64 o 4 4 0 5248.13 4941.74 66.51 o 5 4 0 12205.45 10820.31 129.36 o 6 4 0 3204.69 2934.17 50.27 o 7 4 0 9347.32 11238.94 139.18 o 8 4 0 6762.53 8745.31 115.89 o 9 4 0 274.46 315.51 23.78 o 10 4 0 1048.97 911.49 34.63 o 11 4 0 2200.47 1798.02 49.03 o 12 4 0 60.34 92.90 25.33 o 13 4 0 92.47 47.27 27.29 o 14 4 0 417.31 525.86 37.66 o 15 4 0 52.50 50.71 34.20 o 16 4 0 229.32 185.43 38.86 o 17 4 0 48.61 139.99 39.13 o 18 4 0 109.46 120.57 44.50 o 19 4 0 0.71 -26.73 61.72 o 1 5 0 12479.75 16103.43 179.39 o 2 5 0 6585.54 13157.47 149.51 o 3 5 0 12809.21 10184.78 120.12 o 4 5 0 42.88 17.56 11.95 o 5 5 0 4211.15 3055.80 49.77 o 6 5 0 8.39 34.92 15.22 o 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124.06 51.05 o 17 8 0 61.13 78.51 52.50 o 18 8 0 13.74 -48.13 48.13 o 19 8 0 53.72 87.75 73.97 o 1 9 0 8008.91 8864.34 113.29 o 2 9 0 10286.85 9784.51 123.18 o 3 9 0 710.63 496.23 23.94 o 4 9 0 65.67 142.76 18.89 o 5 9 0 927.64 1024.16 32.99 o 6 9 0 8700.48 9397.81 123.94 o 7 9 0 300.04 439.68 28.33 o 8 9 0 892.07 877.07 56.66 o 9 9 0 1662.78 1534.17 56.45 o 10 9 0 200.32 154.96 26.35 o 11 9 0 163.00 110.66 27.17 o 12 9 0 1112.78 1348.39 54.95 o 13 9 0 1167.52 1095.44 52.77 o 14 9 0 1106.30 1205.67 66.01 o 15 9 0 2.90 37.96 46.37 o 16 9 0 294.86 362.16 58.25 o 17 9 0 462.03 398.98 61.83 o 18 9 0 13.24 -47.03 47.03 o 19 9 0 13.58 -8.12 60.72 o 0 10 0 25998.40 33540.89 524.07 o 1 10 0 329.62 263.59 21.70 o 2 10 0 52.07 208.03 20.70 o 3 10 0 34.54 191.05 20.60 o 4 10 0 189.36 136.28 19.72 o 5 10 0 105.87 67.54 18.71 o 6 10 0 7.45 11.49 17.71 o 7 10 0 365.78 304.35 25.76 o 8 10 0 3288.18 3088.10 61.77 o 9 10 0 56.08 55.98 22.06 o 10 10 0 2223.78 2412.33 58.51 o 11 10 0 530.57 585.11 43.39 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