#------------------------------------------------------------------------------ #$Date: 2019-05-25 07:55:10 +0300 (Sat, 25 May 2019) $ #$Revision: 215532 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/29/2242960.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242960 _cell_angle_alpha 90.000 _cell_angle_beta 105.923 _cell_angle_gamma 90.000 _cell_length_a 13.9361 _cell_length_b 15.5006 _cell_length_c 15.9885 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.8300 _cod_data_source_file is5512Isup2.hkl _cod_data_source_block I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 253.82 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -18 0 410.95 958.89 437.19 o 1 -18 0 105.26 281.58 352.41 o 2 -18 0 2.63 30.06 277.98 o 3 -18 0 5.65 170.31 302.84 o 4 -18 0 21.89 -1.62 213.45 o 1 -17 0 88.17 123.86 313.74 o 2 -17 0 14.72 2.56 175.62 o 3 -17 0 66.58 123.39 270.98 o 4 -17 0 116.35 214.03 305.88 o 5 -17 0 81.26 153.05 319.87 o 6 -17 0 9.54 327.52 395.64 o 0 -16 0 3.73 409.52 339.55 o 1 -16 0 4.14 84.30 269.75 o 2 -16 0 22.86 262.06 231.79 o 3 -16 0 8.76 74.36 211.39 o 4 -16 0 6.44 108.43 165.62 o 5 -16 0 18.38 149.11 298.14 o 6 -16 0 59.43 113.59 427.81 o 7 -16 0 16.12 195.98 428.96 o 8 -16 0 51.24 -48.67 463.94 o 1 -15 0 1754.21 2603.27 392.62 o 2 -15 0 184.50 656.92 229.28 o 3 -15 0 34.98 221.12 249.83 o 4 -15 0 28.91 39.91 48.15 o 5 -15 0 21.57 -5.04 96.32 o 6 -15 0 2.08 32.79 258.57 o 7 -15 0 132.42 406.89 360.76 o 8 -15 0 125.00 81.99 353.55 o 9 -15 0 1.17 117.39 426.89 o 0 -14 0 518.04 848.12 299.98 o 1 -14 0 286.59 221.61 167.70 o 2 -14 0 17.80 125.59 245.12 o 3 -14 0 11.19 120.50 222.00 o 4 -14 0 61.16 68.98 559.07 o 5 -14 0 33.25 190.08 279.74 o 6 -14 0 102.37 322.67 361.23 o 7 -14 0 56.55 198.59 277.64 o 8 -14 0 11.49 51.93 843.95 o 9 -14 0 2.32 24.20 2810.30 o 10 -14 0 10.76 65.73 249.10 o 1 -13 0 18.75 7.36 453.58 o 2 -13 0 234.12 407.82 152.79 o 3 -13 0 145.10 235.17 190.39 o 4 -13 0 223.01 374.70 214.83 o 5 -13 0 212.77 391.44 218.59 o 6 -13 0 36.04 85.17 281.96 o 7 -13 0 21.29 92.67 269.57 o 8 -13 0 175.74 330.16 314.76 o 9 -13 0 36.64 230.18 390.39 o 10 -13 0 5.30 161.37 651.95 o 0 -12 0 824.93 1043.07 246.99 o 1 -12 0 78.68 57.02 132.99 o 2 -12 0 250.18 430.26 185.42 o 3 -12 0 1197.94 1804.16 182.37 o 4 -12 0 429.70 659.62 190.90 o 5 -12 0 18.64 39.59 102.52 o 6 -12 0 570.96 936.97 225.47 o 7 -12 0 332.19 751.68 245.47 o 8 -12 0 28.52 71.80 117.48 o 9 -12 0 1.97 108.12 142.07 o 10 -12 0 21.95 95.53 184.19 o 1 -11 0 127.22 127.91 24.15 o 2 -11 0 2802.03 3416.54 293.52 o 3 -11 0 459.04 440.84 57.00 o 4 -11 0 174.83 210.64 179.89 o 5 -11 0 100.07 149.84 206.59 o 6 -11 0 213.53 250.10 195.02 o 7 -11 0 7.91 72.88 231.58 o 8 -11 0 17.34 156.73 195.13 o 9 -11 0 45.26 149.36 207.54 o 10 -11 0 59.84 310.66 259.59 o 11 -11 0 20.59 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1664.56 1764.06 71.31 o 5 -8 0 217.72 206.13 27.65 o 6 -8 0 394.89 329.70 37.79 o 7 -8 0 17.19 5.83 26.81 o 8 -8 0 448.90 700.08 182.54 o 9 -8 0 59.46 133.81 194.60 o 10 -8 0 232.26 729.39 261.10 o 11 -8 0 116.88 537.34 478.06 o 12 -8 0 47.19 268.73 1002.95 o 13 -8 0 7.66 339.12 790.43 o 14 -8 0 3.94 268.33 738.77 o 1 -7 0 186.21 179.48 20.71 o 2 -7 0 285.30 302.01 25.65 o 3 -7 0 2924.14 3369.89 109.84 o 4 -7 0 574.26 585.38 38.64 o 5 -7 0 369.02 401.04 29.69 o 6 -7 0 210.17 189.94 20.47 o 7 -7 0 55.28 53.52 11.84 o 8 -7 0 102.86 69.84 101.87 o 9 -7 0 114.33 211.14 59.31 o 10 -7 0 335.22 276.74 121.78 o 11 -7 0 305.23 374.10 302.82 o 12 -7 0 17.01 -36.08 36.08 o 13 -7 0 0.97 411.40 989.44 o 14 -7 0 1.57 162.34 1243.52 o 0 -6 0 18075.22 26551.55 3944.09 o 1 -6 0 11112.91 14666.60 773.18 o 2 -6 0 1720.55 1921.56 57.65 o 3 -6 0 1492.89 1565.02 66.91 o 4 -6 0 841.91 899.21 36.39 o 5 -6 0 179.01 199.96 18.07 o 6 -6 0 165.62 164.71 17.62 o 7 -6 0 787.20 1047.11 48.75 o 8 -6 0 5.92 5.15 7.90 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111.62 o 14 -4 0 6.89 -219.66 910.80 o 15 -4 0 4.37 92.42 324.60 o 1 -3 0 25541.28 33813.01 1454.50 o 2 -3 0 1429.25 1792.34 70.35 o 3 -3 0 3288.93 3448.49 147.99 o 4 -3 0 4852.59 5642.75 182.03 o 5 -3 0 5643.14 6958.94 108.48 o 6 -3 0 2322.02 2710.89 62.73 o 7 -3 0 793.86 671.03 35.09 o 8 -3 0 42.31 56.90 18.35 o 9 -3 0 27.83 24.31 10.63 o 10 -3 0 2.98 24.06 24.91 o 11 -3 0 6.28 20.45 21.64 o 12 -3 0 21.32 29.06 95.78 o 13 -3 0 1.02 -1.18 85.42 o 14 -3 0 1.33 396.17 369.29 o 15 -3 0 1.22 332.56 402.12 o 0 -2 0 24760.88 35612.24 2647.62 o 1 -2 0 172.56 163.71 9.35 o 2 -2 0 5449.12 6677.50 292.11 o 3 -2 0 149.07 179.32 12.91 o 4 -2 0 3070.93 3641.67 110.33 o 5 -2 0 2306.93 2396.10 86.69 o 6 -2 0 6819.61 8807.34 233.66 o 7 -2 0 2512.66 2797.55 100.58 o 8 -2 0 348.65 367.40 38.63 o 9 -2 0 151.53 132.30 27.46 o 10 -2 0 1.21 25.64 49.38 o 11 -2 0 13.40 37.87 132.29 o 12 -2 0 195.00 288.79 53.52 o 13 -2 0 23.37 47.31 29.70 o 14 -2 0 26.50 232.50 373.70 o 15 -2 0 10.80 279.88 417.42 o 16 -2 0 8.29 17.66 165.08 o 1 -1 0 240.20 272.43 8.79 o 2 -1 0 6017.64 6529.66 228.13 o 3 -1 0 50.38 62.69 4.85 o 4 -1 0 5468.95 5186.96 90.96 o 5 -1 0 6967.87 7381.08 166.50 o 6 -1 0 41.08 41.93 15.34 o 7 -1 0 2720.06 4223.20 328.23 o 8 -1 0 88.14 282.36 104.29 o 9 -1 0 4.89 33.43 16.43 o 10 -1 0 71.41 170.61 37.48 o 11 -1 0 2.37 15.28 128.91 o 12 -1 0 5.81 0.00 22.45 o 13 -1 0 7.14 -23.17 23.17 o 14 -1 0 0.18 124.84 468.96 o 15 -1 0 4.25 281.38 382.89 o 16 -1 0 2.32 545.35 756.71 o 1 0 0 62871.02 74643.11 2084.30 o 2 0 0 64424.23 73629.60 2003.37 o 3 0 0 1445.43 2056.29 45.20 o 4 0 0 11665.93 12862.84 183.02 o 5 0 0 8576.65 9781.63 168.64 o 6 0 0 4624.34 5193.05 181.37 o 7 0 0 6223.31 7959.23 110.12 o 8 0 0 1869.71 1887.21 88.06 o 9 0 0 640.82 483.76 37.43 o 10 0 0 169.47 273.63 40.95 o 11 0 0 27.05 -6.82 73.16 o 12 0 0 378.96 749.72 238.89 o 13 0 0 24.42 40.18 140.23 o 14 0 0 19.21 105.17 336.52 o 15 0 0 12.19 3.67 53.45 o 16 0 0 10.92 47.30 539.25 o 1 1 0 240.36 287.30 10.53 o 2 1 0 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159.62 681.06 o 0 8 0 752.78 694.89 36.60 o 1 8 0 58.20 51.45 4.01 o 2 8 0 3.83 5.70 6.65 o 3 8 0 2129.91 2101.75 49.81 o 4 8 0 1661.57 1696.81 55.60 o 5 8 0 216.15 211.99 20.71 o 6 8 0 394.61 387.82 45.71 o 7 8 0 17.38 5.23 15.72 o 8 8 0 449.25 546.47 55.81 o 9 8 0 59.71 106.16 94.81 o 10 8 0 232.37 416.56 82.31 o 11 8 0 116.60 90.23 52.17 o 12 8 0 46.94 -45.60 211.27 o 13 8 0 7.68 188.07 567.48 o 14 8 0 3.85 -28.57 283.40 o 1 9 0 1095.92 1140.10 36.56 o 2 9 0 48.16 47.86 11.57 o 3 9 0 429.70 420.47 26.68 o 4 9 0 71.39 89.56 12.35 o 5 9 0 482.36 513.93 36.02 o 6 9 0 418.54 392.74 43.41 o 7 9 0 118.14 89.15 26.36 o 8 9 0 321.08 305.20 69.89 o 9 9 0 581.51 645.92 223.48 o 10 9 0 187.00 220.42 39.96 o 11 9 0 406.10 270.94 243.53 o 12 9 0 12.30 260.52 697.47 o 13 9 0 2.26 347.72 808.71 o 14 9 0 0.36 384.73 946.24 o 0 10 0 787.84 812.53 86.13 o 1 10 0 83.85 94.98 11.89 o 2 10 0 430.31 496.74 35.06 o 3 10 0 220.62 215.84 17.28 o 4 10 0 168.99 212.07 19.65 o 5 10 0 546.92 532.91 45.54 o 6 10 0 29.04 42.21 22.52 o 7 10 0 2.29 22.80 34.59 o 8 10 0 11.19 5.92 57.43 o 9 10 0 71.84 78.31 49.49 o 10 10 0 10.43 18.55 263.50 o 11 10 0 3.33 113.83 1216.05 o 12 10 0 7.73 256.94 851.50 o 13 10 0 0.56 429.64 622.12 o 1 11 0 127.41 139.10 17.81 o 2 11 0 2804.04 3078.69 181.22 o 3 11 0 459.16 493.09 46.04 o 4 11 0 174.48 136.01 48.40 o 5 11 0 100.92 101.73 48.20 o 6 11 0 214.78 197.85 27.17 o 7 11 0 7.68 26.65 36.30 o 8 11 0 18.29 68.95 25.03 o 9 11 0 45.39 119.79 50.84 o 10 11 0 59.48 55.59 272.10 o 1 12 0 78.11 40.99 18.51 o 2 12 0 250.78 211.10 76.61 o 3 12 0 1198.18 1279.57 254.75 o 4 12 0 429.85 422.12 136.39 o 5 12 0 18.59 12.99 29.16 o 6 12 0 573.16 756.16 322.52 o 7 12 0 332.67 719.09 284.77 o 8 12 0 28.79 267.67 331.10 o 9 12 0 2.10 158.27 483.44 o 2 13 0 233.49 627.55 339.40 o 3 13 0 144.19 214.69 316.72 o 4 13 0 223.67 412.59 293.68 o 5 13 0 212.84 343.83 356.48 o 6 13 0 36.04 125.67 255.26 o 7 13 0 21.32 55.84 192.89 o 8 13 0 175.27 585.64 373.76 o 1 14 0 286.68 394.70 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