#------------------------------------------------------------------------------
#$Date: 2019-07-31 07:41:19 +0300 (Wed, 31 Jul 2019) $
#$Revision: 217323 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/30/2243036.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243036
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   13.4770
_cell_length_b                   9.5617
_cell_length_c                   9.8500
_exptl_crystal_F_000             820.00
_reflns_d_resolution_high        0.8304
_cod_data_source_file            vn2151IIsup3.hkl
_cod_data_source_block           II
_shelx_title                     ' ABER110  RB/BR/ME-PIP            New: Amm2'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            516.12
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-x, y, z'
'x, -y, z'
'x, y+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'-x, y+1/2, z+1/2'
'x, -y+1/2, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 1 -11 3210.15 3354.84 173.93 o
1 1 -11 3001.58 3211.55 125.77 o
2 1 -11 1206.27 1250.15 95.19 o
3 1 -11 2970.86 3111.18 131.14 o
4 1 -11 4143.83 4316.32 164.66 o
5 1 -11 3089.58 3212.07 136.55 o
0 3 -11 105.98 132.85 126.00 o
1 3 -11 4673.53 5072.63 189.71 o
2 3 -11 9087.13 9708.30 399.77 o
3 3 -11 4548.54 4844.25 168.47 o
4 3 -11 103.12 167.23 93.22 o
0 0 -10 6652.65 6889.68 369.90 o
1 0 -10 10279.27 10460.06 341.56 o
2 0 -10 15709.29 16060.35 468.55 o
3 0 -10 8306.57 8480.25 226.01 o
4 0 -10 6863.34 6786.12 208.44 o
5 0 -10 7657.33 7755.86 223.64 o
6 0 -10 10595.79 11427.17 388.22 o
7 0 -10 8690.46 9450.87 412.43 o
8 0 -10 6667.66 7390.33 328.23 o
0 2 -10 9429.02 9972.20 391.08 o
1 2 -10 6005.18 6230.89 170.29 o
2 2 -10 13656.47 13879.20 269.89 o
3 2 -10 6618.72 6641.52 155.00 o
4 2 -10 7923.32 8254.22 171.58 o
5 2 -10 4137.64 4244.70 144.59 o
6 2 -10 12685.41 13293.68 415.82 o
7 2 -10 5829.56 6194.14 268.06 o
8 2 -10 4051.61 4275.60 159.10 o
0 4 -10 3860.18 4393.22 223.40 o
1 4 -10 4512.05 4700.48 185.10 o
2 4 -10 7129.60 7369.14 297.56 o
3 4 -10 1929.53 1986.93 128.05 o
4 4 -10 4077.22 4129.92 184.11 o
5 4 -10 5030.94 5183.56 239.50 o
6 4 -10 4153.85 4061.85 154.63 o
0 6 -10 1742.54 1944.01 236.65 o
1 6 -10 7873.62 8549.20 479.31 o
2 6 -10 12075.12 11925.37 325.31 o
0 1 -9 1210.31 1323.99 128.12 o
1 1 -9 629.77 690.05 79.18 o
2 1 -9 15225.95 14989.38 284.28 o
3 1 -9 334.77 379.09 64.02 o
4 1 -9 1846.77 1775.00 96.17 o
5 1 -9 1373.47 1510.35 95.99 o
6 1 -9 9871.13 10669.31 286.95 o
7 1 -9 363.95 358.65 79.80 o
8 1 -9 1800.63 2007.51 127.60 o
9 1 -9 868.76 961.67 95.56 o
10 1 -9 8543.65 9031.04 181.51 o
0 3 -9 2698.67 2738.59 152.41 o
1 3 -9 8942.14 9110.49 247.19 o
2 3 -9 11593.98 11501.56 283.96 o
3 3 -9 9036.88 9252.38 218.45 o
4 3 -9 788.00 865.61 95.08 o
5 3 -9 7293.68 7482.65 207.28 o
6 3 -9 8793.37 8815.02 194.55 o
7 3 -9 7521.57 7501.29 190.50 o
8 3 -9 640.83 621.35 106.12 o
9 3 -9 4719.19 4944.26 184.89 o
0 5 -9 2146.82 2298.70 185.61 o
1 5 -9 771.59 877.67 105.89 o
2 5 -9 19017.31 18851.49 315.67 o
3 5 -9 694.42 727.71 129.34 o
4 5 -9 3314.52 3281.38 136.26 o
5 5 -9 929.06 981.62 109.93 o
6 5 -9 12350.65 12586.51 355.52 o
7 5 -9 404.75 416.06 92.94 o
0 7 -9 769.68 844.24 148.00 o
1 7 -9 8016.50 9003.27 556.56 o
2 7 -9 6040.09 6748.57 389.34 o
3 7 -9 6902.54 7405.02 379.99 o
0 0 -8 285.97 364.15 138.63 o
1 0 -8 18011.41 17457.71 322.41 o
2 0 -8 27089.17 25570.67 414.15 o
3 0 -8 20141.20 19148.31 419.18 o
4 0 -8 1017.38 993.51 74.06 o
5 0 -8 15795.95 15250.10 330.52 o
6 0 -8 24126.62 23553.75 764.68 o
7 0 -8 15405.58 16118.45 427.45 o
8 0 -8 340.65 391.98 118.64 o
9 0 -8 8144.67 8586.23 245.83 o
10 0 -8 13579.40 14435.43 601.66 o
11 0 -8 12702.35 13648.98 536.37 o
0 2 -8 2708.96 2578.91 116.23 o
1 2 -8 16157.25 15728.88 286.63 o
2 2 -8 12284.99 12124.85 206.78 o
3 2 -8 14191.39 13723.96 210.13 o
4 2 -8 1851.24 1866.41 71.54 o
5 2 -8 13412.52 13075.96 210.07 o
6 2 -8 12721.10 12742.93 255.52 o
7 2 -8 9734.03 9907.49 286.82 o
8 2 -8 1366.81 1456.51 110.50 o
9 2 -8 12585.97 13162.15 301.88 o
10 2 -8 6945.21 7097.50 213.10 o
11 2 -8 4161.06 4364.80 180.53 o
0 4 -8 4961.58 4940.73 207.41 o
1 4 -8 6719.50 6745.95 149.94 o
2 4 -8 23866.25 23534.06 569.94 o
3 4 -8 7380.19 7380.32 188.97 o
4 4 -8 2620.03 2686.29 106.99 o
5 4 -8 5733.44 5693.07 168.47 o
6 4 -8 22227.29 22205.15 492.20 o
7 4 -8 6058.31 6270.50 190.98 o
8 4 -8 2139.90 2057.36 113.50 o
9 4 -8 3001.02 3011.98 149.58 o
10 4 -8 13451.44 13805.08 412.93 o
0 6 -8 4525.04 4864.57 323.21 o
1 6 -8 2350.29 2548.60 144.94 o
2 6 -8 1963.74 2101.30 108.23 o
3 6 -8 2748.75 2935.65 131.58 o
4 6 -8 5419.29 5714.38 211.44 o
5 6 -8 2172.35 2238.56 125.74 o
6 6 -8 2357.31 2293.26 119.41 o
7 6 -8 1203.33 1141.75 104.39 o
8 6 -8 3535.90 3454.22 129.66 o
0 8 -8 6246.41 6816.25 579.01 o
1 8 -8 329.60 389.02 109.64 o
2 8 -8 35543.43 36600.16 509.74 o
3 8 -8 167.86 202.99 98.50 o
4 8 -8 4050.76 4364.28 219.13 o
0 1 -7 2767.22 2763.56 87.06 o
1 1 -7 489.41 504.74 37.40 o
2 1 -7 26441.73 25004.52 290.32 o
3 1 -7 562.56 564.36 46.48 o
4 1 -7 1959.99 1936.02 74.34 o
5 1 -7 546.20 534.73 51.26 o
6 1 -7 22726.06 22579.66 341.78 o
7 1 -7 67.45 96.34 50.07 o
8 1 -7 1278.75 1320.96 84.22 o
9 1 -7 537.86 591.88 81.82 o
10 1 -7 14987.19 15678.79 407.92 o
11 1 -7 23.02 30.22 94.43 o
12 1 -7 697.81 767.34 102.96 o
13 1 -7 453.34 482.97 113.87 o
0 3 -7 5247.37 5088.18 187.42 o
1 3 -7 3471.76 3276.62 95.60 o
2 3 -7 12561.07 12193.42 195.09 o
3 3 -7 7801.75 7456.90 140.47 o
4 3 -7 6235.91 6161.13 124.62 o
5 3 -7 2402.45 2528.48 86.66 o
6 3 -7 9943.43 10111.47 148.94 o
7 3 -7 4132.93 4311.95 129.30 o
8 3 -7 3187.66 3192.58 142.41 o
9 3 -7 2699.85 2701.81 121.65 o
10 3 -7 5685.29 5711.60 147.82 o
11 3 -7 3266.04 3333.94 148.72 o
12 3 -7 1869.07 1954.24 117.16 o
0 5 -7 4032.14 4054.69 222.58 o
1 5 -7 4463.23 4588.49 127.82 o
2 5 -7 46010.63 46717.59 712.49 o
3 5 -7 1700.28 1728.19 75.47 o
4 5 -7 2924.77 2942.49 113.51 o
5 5 -7 4435.85 4407.90 149.32 o
6 5 -7 38255.96 39035.45 1194.57 o
7 5 -7 2079.64 2052.92 119.82 o
8 5 -7 2690.69 2610.86 123.97 o
9 5 -7 2760.83 2707.74 149.10 o
10 5 -7 24178.90 24271.72 580.45 o
11 5 -7 1079.09 1105.59 108.65 o
0 7 -7 1137.45 1210.25 128.02 o
1 7 -7 2860.33 3102.68 165.95 o
2 7 -7 2519.32 2695.56 115.84 o
3 7 -7 5474.07 5825.13 208.82 o
4 7 -7 1647.49 1737.93 110.81 o
5 7 -7 2317.53 2306.70 117.11 o
6 7 -7 2379.64 2372.97 129.33 o
7 7 -7 2776.24 2665.65 141.34 o
8 7 -7 971.36 1030.31 107.13 o
0 9 -7 2279.04 2355.74 159.28 o
1 9 -7 671.29 727.20 105.69 o
2 9 -7 13609.58 14879.06 526.22 o
3 9 -7 9.63 28.51 94.79 o
0 0 -6 60444.97 57806.04 1008.89 o
1 0 -6 7143.08 6879.64 139.17 o
2 0 -6 23667.40 22232.21 339.97 o
3 0 -6 4673.91 4376.42 113.84 o
4 0 -6 36011.51 34443.01 640.82 o
5 0 -6 6719.90 6463.46 172.19 o
6 0 -6 16624.85 16943.85 404.35 o
7 0 -6 5190.84 5312.84 155.40 o
8 0 -6 24133.53 24209.47 700.16 o
9 0 -6 2401.18 2540.56 181.59 o
10 0 -6 11829.53 13002.26 867.48 o
11 0 -6 4279.09 4261.33 332.46 o
12 0 -6 14499.83 14192.25 487.88 o
13 0 -6 2159.97 2124.83 232.80 o
14 0 -6 6263.75 6230.89 308.77 o
0 2 -6 13812.88 12831.17 240.97 o
1 2 -6 4595.21 4430.69 82.33 o
2 2 -6 72483.29 68389.01 819.80 o
3 2 -6 2508.45 2397.81 65.13 o
4 2 -6 17475.68 16718.97 307.37 o
5 2 -6 3343.33 3497.95 135.05 o
6 2 -6 48111.63 48523.27 678.28 o
7 2 -6 3983.95 4055.83 111.58 o
8 2 -6 11056.01 11377.64 191.40 o
9 2 -6 986.49 1068.76 87.60 o
10 2 -6 36394.43 37439.66 651.49 o
11 2 -6 2542.43 2609.63 107.21 o
12 2 -6 5706.39 5951.76 187.51 o
13 2 -6 748.29 769.09 105.74 o
0 4 -6 13205.07 13150.53 544.44 o
1 4 -6 2656.39 2654.52 87.91 o
2 4 -6 9467.63 9444.32 191.45 o
3 4 -6 1507.19 1503.92 78.65 o
4 4 -6 7632.40 7685.48 164.36 o
5 4 -6 4057.33 4029.97 113.78 o
6 4 -6 6884.39 6788.92 188.06 o
7 4 -6 535.58 529.10 99.74 o
8 4 -6 6310.68 6245.55 188.09 o
9 4 -6 2023.98 2074.17 118.50 o
10 4 -6 5313.78 5318.73 139.87 o
11 4 -6 606.63 596.32 87.30 o
12 4 -6 5191.16 5402.62 187.66 o
0 6 -6 399.08 454.54 65.88 o
1 6 -6 14958.03 15625.08 329.03 o
2 6 -6 30454.88 30957.22 865.09 o
3 6 -6 11928.37 12012.26 269.42 o
4 6 -6 1467.43 1508.45 78.44 o
5 6 -6 12371.63 11972.92 338.22 o
6 6 -6 19500.48 19282.31 543.87 o
7 6 -6 12348.84 12068.53 383.94 o
8 6 -6 907.62 921.54 92.42 o
9 6 -6 6286.29 6177.68 198.65 o
10 6 -6 16035.29 15877.67 439.55 o
11 6 -6 8286.78 8325.76 174.06 o
0 8 -6 4590.63 4837.26 189.85 o
1 8 -6 4387.09 4687.90 134.41 o
2 8 -6 10380.24 11052.79 261.84 o
3 8 -6 4591.26 4815.01 149.28 o
4 8 -6 1925.12 1975.67 111.85 o
5 8 -6 4842.16 4810.16 166.64 o
6 8 -6 5917.67 5875.25 192.39 o
7 8 -6 2010.29 1981.96 124.41 o
8 8 -6 1391.28 1424.98 107.06 o
0 1 -5 1525.24 1524.48 66.92 o
1 1 -5 4559.62 4336.38 92.86 o
2 1 -5 11573.66 10744.62 191.62 o
3 1 -5 3631.18 3462.37 70.68 o
4 1 -5 3200.28 3143.70 71.04 o
5 1 -5 2635.34 2598.31 61.09 o
6 1 -5 15239.75 15098.40 187.58 o
7 1 -5 3350.36 3499.26 88.75 o
8 1 -5 1779.96 1849.93 68.64 o
9 1 -5 2820.41 2930.47 90.13 o
10 1 -5 7139.11 7410.00 224.32 o
11 1 -5 2219.68 2325.62 121.74 o
12 1 -5 733.27 718.60 108.70 o
13 1 -5 1726.01 1750.73 129.13 o
14 1 -5 3395.47 3405.73 244.65 o
0 3 -5 8310.78 7918.58 212.66 o
1 3 -5 17674.41 16934.56 220.51 o
2 3 -5 36955.55 35289.59 417.75 o
3 3 -5 16881.58 16415.94 209.89 o
4 3 -5 7361.57 7304.04 120.09 o
5 3 -5 10594.15 10815.22 256.07 o
6 3 -5 34112.03 32941.72 734.20 o
7 3 -5 15287.01 15231.80 312.52 o
8 3 -5 6391.02 6361.45 180.37 o
9 3 -5 8671.22 8767.86 177.86 o
10 3 -5 17869.30 18214.09 353.60 o
11 3 -5 7683.19 7903.29 214.41 o
12 3 -5 1620.52 1667.77 104.46 o
13 3 -5 5235.07 5296.01 192.29 o
14 3 -5 10384.46 10219.56 277.96 o
0 5 -5 9423.34 9400.38 233.68 o
1 5 -5 828.81 906.10 67.36 o
2 5 -5 10445.77 10745.57 200.14 o
3 5 -5 1290.99 1318.21 75.70 o
4 5 -5 11442.42 11618.61 239.93 o
5 5 -5 678.15 728.48 71.42 o
6 5 -5 13287.85 12968.33 369.13 o
7 5 -5 1092.82 1119.60 93.69 o
8 5 -5 7281.98 7278.73 180.19 o
9 5 -5 218.00 240.81 76.32 o
10 5 -5 6310.05 6340.45 146.14 o
11 5 -5 1088.88 1102.87 93.32 o
12 5 -5 4663.53 4828.84 175.29 o
0 7 -5 4373.04 4637.65 191.47 o
1 7 -5 10513.87 11164.86 167.51 o
2 7 -5 23389.51 24341.20 371.25 o
3 7 -5 8391.87 8872.47 202.80 o
4 7 -5 3553.84 3590.17 121.92 o
5 7 -5 8918.82 8948.09 232.80 o
6 7 -5 21556.91 21137.93 592.24 o
7 7 -5 7114.44 6946.58 200.85 o
8 7 -5 4038.70 3947.37 144.85 o
9 7 -5 7916.00 7763.04 243.09 o
10 7 -5 12282.51 12193.09 336.89 o
0 9 -5 2318.09 2426.67 160.99 o
1 9 -5 1502.84 1554.18 97.28 o
2 9 -5 2522.75 2662.62 112.04 o
3 9 -5 1011.29 1013.95 90.61 o
4 9 -5 3122.20 3277.14 154.57 o
5 9 -5 1223.34 1232.90 111.54 o
6 9 -5 3937.26 3849.88 163.04 o
7 9 -5 1048.33 1008.52 112.40 o
0 0 -4 1827.18 1772.33 90.88 o
1 0 -4 59519.98 57258.75 1821.86 o
2 0 -4 63584.83 64756.54 1059.65 o
3 0 -4 78984.28 79224.61 1008.33 o
4 0 -4 2623.88 2674.51 95.37 o
5 0 -4 48547.03 48507.95 867.86 o
6 0 -4 33786.65 33985.75 496.75 o
7 0 -4 42467.27 42527.16 644.26 o
8 0 -4 5260.30 5588.11 158.95 o
9 0 -4 31377.83 32015.26 773.27 o
10 0 -4 22155.72 22657.34 525.69 o
11 0 -4 25762.64 25967.47 588.65 o
12 0 -4 885.73 892.01 148.13 o
13 0 -4 16850.38 16974.38 387.90 o
14 0 -4 14832.16 14710.51 542.51 o
15 0 -4 13302.44 13428.22 370.95 o
0 2 -4 42254.87 40415.37 538.96 o
1 2 -4 6652.38 6216.67 106.44 o
2 2 -4 4472.90 4266.48 93.13 o
3 2 -4 5575.65 5446.05 117.03 o
4 2 -4 33583.71 33186.72 389.02 o
5 2 -4 4018.65 4062.06 89.33 o
6 2 -4 5416.51 5505.47 106.98 o
7 2 -4 6298.17 6378.46 129.96 o
8 2 -4 17519.13 17641.14 259.29 o
9 2 -4 1270.27 1326.11 65.87 o
10 2 -4 2502.09 2694.06 96.31 o
11 2 -4 5608.84 5733.47 152.83 o
12 2 -4 13853.14 13658.95 355.51 o
13 2 -4 645.33 701.31 89.43 o
14 2 -4 688.00 679.39 111.35 o
15 2 -4 2460.15 2477.10 183.49 o
0 4 -4 9602.39 9923.94 252.06 o
1 4 -4 35518.43 35534.46 499.82 o
2 4 -4 22766.48 22957.47 330.22 o
3 4 -4 37281.16 37073.26 461.50 o
4 4 -4 8929.92 8872.18 173.15 o
5 4 -4 33188.09 32930.86 639.09 o
6 4 -4 13279.98 13181.36 266.41 o
7 4 -4 20718.88 20781.26 401.79 o
8 4 -4 6910.18 6934.34 171.44 o
9 4 -4 24655.57 24965.62 328.49 o
10 4 -4 9171.13 9225.73 215.58 o
11 4 -4 15542.73 15437.53 357.48 o
12 4 -4 1881.67 1970.00 104.41 o
13 4 -4 13737.54 13597.59 375.59 o
14 4 -4 6870.63 6541.54 206.00 o
0 6 -4 11867.34 12723.97 317.01 o
1 6 -4 308.21 333.36 50.68 o
2 6 -4 14120.04 14299.76 248.99 o
3 6 -4 694.11 733.24 61.96 o
4 6 -4 8918.02 8851.56 182.59 o
5 6 -4 399.53 408.36 55.04 o
6 6 -4 12085.29 11734.27 282.15 o
7 6 -4 60.33 120.90 74.15 o
8 6 -4 4253.60 4252.69 139.82 o
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10 6 -4 7732.27 7740.56 161.61 o
11 6 -4 219.55 206.13 75.66 o
12 6 -4 4886.17 4862.14 217.55 o
0 8 -4 15945.22 16588.15 500.20 o
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3 8 -4 16701.96 17121.46 418.73 o
4 8 -4 14934.23 15008.97 391.48 o
5 8 -4 14319.10 14178.87 331.82 o
6 8 -4 4855.87 4772.01 131.19 o
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0 10 -4 4630.29 4559.61 253.15 o
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3 10 -4 2956.23 2892.25 158.56 o
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0 1 -3 33759.12 31582.45 1057.83 o
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2 1 -3 4823.05 4781.21 90.41 o
3 1 -3 23487.31 23745.45 250.24 o
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5 1 -3 11142.48 11036.38 188.65 o
6 1 -3 1972.40 1997.55 59.91 o
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8 1 -3 14487.08 14607.07 189.83 o
9 1 -3 7496.28 7565.94 132.79 o
10 1 -3 1537.85 1549.95 62.35 o
11 1 -3 7669.32 7742.53 144.23 o
12 1 -3 6733.11 6761.69 235.50 o
13 1 -3 3997.85 4071.22 148.93 o
14 1 -3 415.39 461.17 95.97 o
15 1 -3 7055.64 6989.97 320.80 o
0 3 -3 9372.12 9736.06 227.60 o
1 3 -3 7083.55 6965.60 127.92 o
2 3 -3 19398.34 19430.68 249.75 o
3 3 -3 4055.03 4051.78 135.34 o
4 3 -3 4308.92 4287.42 111.80 o
5 3 -3 6844.52 6859.71 124.11 o
6 3 -3 13607.82 13719.09 196.23 o
7 3 -3 3461.55 3558.13 83.12 o
8 3 -3 4453.60 4506.82 106.17 o
9 3 -3 2808.22 2902.11 79.17 o
10 3 -3 9893.34 10190.57 196.92 o
11 3 -3 3251.50 3225.90 126.59 o
12 3 -3 2628.34 2636.00 125.51 o
13 3 -3 2317.71 2378.56 130.73 o
14 3 -3 4248.77 4259.42 174.46 o
15 3 -3 638.76 605.40 156.02 o
0 5 -3 31604.31 31491.09 565.61 o
1 5 -3 28097.15 28611.02 369.11 o
2 5 -3 2348.78 2390.02 75.74 o
3 5 -3 31943.87 32087.59 429.01 o
4 5 -3 23690.29 23655.20 323.33 o
5 5 -3 21713.30 21353.29 427.37 o
6 5 -3 886.23 883.10 59.17 o
7 5 -3 21428.23 20890.01 371.60 o
8 5 -3 20080.42 20097.52 348.56 o
9 5 -3 18629.79 18596.50 363.64 o
10 5 -3 946.13 976.30 84.96 o
11 5 -3 10396.00 10536.97 263.53 o
12 5 -3 11090.05 11301.94 251.35 o
13 5 -3 10164.30 10117.86 364.28 o
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