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Information card for entry 2243144
Preview
| Coordinates | 2243144.cif |
|---|---|
| Structure factors | 2243144.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis[bis(1,3-dibenzyl-4,5-diphenylimidazol-2-ylidene)silver(I)] tris(thiocyanato)argentate(I) diethyl ether disolvate |
|---|---|
| Formula | C127 H116 Ag3 N11 O2 S3 |
| Calculated formula | C123 H106 Ag3 N11 O S3 |
| Title of publication | Unexpected reactions of NHC*—Cu^I^ and —Ag^I^ bromides with potassium thio- or selenocyanate |
| Authors of publication | Tacke, Matthias; Marhöfer, Daniel; Althani, Hessah; Müller-Bunz, Helge |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2019 |
| Journal volume | 75 |
| Journal issue | 11 |
| Pages of publication | 1657 - 1663 |
| a | 14.86462 ± 0.00008 Å |
| b | 19.3714 ± 0.0001 Å |
| c | 19.85451 ± 0.00009 Å |
| α | 102.771 ± 0.0004° |
| β | 100.827 ± 0.0004° |
| γ | 99.5778 ± 0.0004° |
| Cell volume | 5345.84 ± 0.05 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0368 |
| Residual factor for significantly intense reflections | 0.0298 |
| Weighted residual factors for significantly intense reflections | 0.0759 |
| Weighted residual factors for all reflections included in the refinement | 0.0803 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.027 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 219488 (current) | 2019-10-24 | cif/ hkl/ Adding structures of 2243144, 2243145, 2243146 via cif-deposit CGI script. |
2243144.cif 2243144.hkl |
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Users of the data should acknowledge the original authors of the
structural data.