#------------------------------------------------------------------------------ #$Date: 2019-10-24 07:12:52 +0300 (Thu, 24 Oct 2019) $ #$Revision: 219488 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/31/2243146.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243146 _cell_angle_alpha 90.000 _cell_angle_beta 93.024 _cell_angle_gamma 90.000 _cell_length_a 13.7704 _cell_length_b 14.3398 _cell_length_c 28.4102 _exptl_crystal_F_000 2480.00 _reflns_d_resolution_high 0.7988 _cod_data_source_file wm55193sup4.hkl _cod_data_source_block 3 _shelx_title ' tac237 in P21/c No14' _shelx_refln_list_code 4 _shelx_f_calc_maximum 489.85 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3991.46 3610.47 94.33 o 3 0 0 169305.06 181332.83 1549.70 o 4 0 0 2707.72 3425.65 72.44 o 5 0 0 5222.87 4712.66 94.70 o 6 0 0 2301.32 1639.87 73.58 o 7 0 0 12321.44 12250.37 190.93 o 8 0 0 34824.58 33986.01 475.22 o 9 0 0 12470.22 14188.16 232.49 o 10 0 0 6678.16 6656.55 160.94 o 11 0 0 433.69 914.69 82.29 o 12 0 0 4531.21 4699.93 193.12 o 13 0 0 991.04 1146.45 76.63 o 14 0 0 565.49 456.22 56.93 o 15 0 0 4.94 110.28 56.98 o 16 0 0 126.09 449.14 93.90 o 17 0 0 8.85 107.22 59.13 o 2 1 0 171.62 120.47 24.05 o 3 1 0 352.41 506.44 17.36 o 4 1 0 2200.49 2257.46 37.36 o 5 1 0 32305.24 29054.53 351.47 o 6 1 0 4.89 57.72 10.98 o 7 1 0 11637.34 10029.45 118.61 o 8 1 0 1551.44 1839.35 57.25 o 9 1 0 276.92 159.96 19.98 o 10 1 0 132.83 173.10 22.22 o 11 1 0 8209.30 8363.74 138.86 o 12 1 0 3232.76 3012.70 88.26 o 13 1 0 4942.39 5079.39 119.88 o 14 1 0 1215.44 1280.19 64.65 o 15 1 0 170.09 131.16 37.28 o 16 1 0 202.76 172.17 54.85 o 17 1 0 1763.72 2141.55 136.16 o 0 2 0 127.70 180.19 19.51 o 1 2 0 6002.88 6611.91 84.07 o 2 2 0 47209.88 50095.13 253.58 o 3 2 0 28737.36 34144.00 170.91 o 4 2 0 22611.74 21945.85 142.17 o 5 2 0 634.72 684.85 18.73 o 6 2 0 57951.81 53085.68 292.44 o 7 2 0 3263.52 3334.25 54.04 o 8 2 0 39.78 89.41 12.77 o 9 2 0 3405.89 3163.70 82.01 o 10 2 0 1550.99 1565.67 60.82 o 11 2 0 226.65 97.15 17.53 o 12 2 0 7554.61 7405.36 118.86 o 13 2 0 51.12 80.00 18.00 o 14 2 0 163.60 274.32 34.58 o 15 2 0 1369.10 1231.33 81.56 o 16 2 0 6.02 -35.01 35.01 o 17 2 0 1171.37 1320.17 124.36 o 1 3 0 25554.34 25495.89 165.61 o 2 3 0 34909.84 40659.21 215.05 o 3 3 0 1016.77 757.60 26.77 o 4 3 0 567.87 340.87 14.98 o 5 3 0 16954.20 16649.12 118.26 o 6 3 0 149.33 170.97 18.72 o 7 3 0 5184.14 4119.34 95.77 o 8 3 0 170.98 131.57 13.34 o 9 3 0 1808.20 1698.16 49.47 o 10 3 0 4911.22 4860.47 94.28 o 11 3 0 3580.44 3717.85 79.45 o 12 3 0 1176.47 1060.82 44.01 o 13 3 0 7295.93 7202.88 117.51 o 14 3 0 811.68 872.39 50.43 o 15 3 0 885.04 858.02 115.32 o 16 3 0 634.00 596.42 106.57 o 0 4 0 61419.09 64766.29 462.45 o 1 4 0 80531.59 79093.95 353.94 o 2 4 0 5554.89 5314.56 73.89 o 3 4 0 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10 0 2812.02 2877.02 80.25 o 9 10 0 1103.84 1161.15 57.56 o 10 10 0 1314.34 1210.60 55.17 o 11 10 0 1897.71 2198.89 113.67 o 12 10 0 1872.88 2441.36 155.68 o 13 10 0 580.55 693.32 73.10 o 14 10 0 58.85 -20.68 42.97 o 1 11 0 7288.27 6977.16 82.56 o 2 11 0 7189.75 6758.56 80.72 o 3 11 0 2918.83 2565.32 47.14 o 4 11 0 113.71 91.48 12.15 o 5 11 0 314.74 269.42 20.88 o 6 11 0 3615.08 3776.26 98.32 o 7 11 0 358.19 372.51 35.12 o 8 11 0 37.01 68.39 15.74 o 9 11 0 1750.22 1502.52 68.03 o 10 11 0 3578.19 3765.61 183.34 o 11 11 0 288.08 321.14 94.12 o 12 11 0 98.44 117.34 40.56 o 13 11 0 203.83 144.46 42.87 o 0 12 0 2763.89 3328.58 92.75 o 1 12 0 3473.69 3835.21 63.24 o 2 12 0 660.52 629.43 29.35 o 3 12 0 1327.84 1777.44 64.79 o 4 12 0 485.73 655.08 28.26 o 5 12 0 6971.24 7058.15 111.28 o 6 12 0 2613.50 2699.09 81.87 o 7 12 0 1105.30 889.48 69.35 o 8 12 0 32.12 65.73 23.51 o 9 12 0 4703.40 4711.33 181.47 o 10 12 0 2038.18 2367.25 183.85 o 11 12 0 806.98 749.23 163.38 o 12 12 0 908.34 753.16 169.29 o 1 13 0 486.65 502.72 45.05 o 2 13 0 36.81 119.80 25.72 o 3 13 0 1149.16 1182.25 44.30 o 4 13 0 2251.87 2203.90 53.92 o 5 13 0 2209.28 2036.94 77.55 o 6 13 0 18.01 47.73 45.12 o 7 13 0 218.32 238.78 38.35 o 8 13 0 2726.36 2307.90 117.94 o 9 13 0 16.51 37.95 41.03 o 10 13 0 214.64 202.95 58.99 o 11 13 0 3.98 80.45 58.18 o 0 14 0 179.98 409.99 44.92 o 1 14 0 2220.52 2035.83 54.39 o 2 14 0 397.45 456.36 31.91 o 3 14 0 8138.31 8402.56 117.98 o 4 14 0 1329.75 1041.26 48.29 o 5 14 0 256.96 179.26 26.80 o 6 14 0 168.75 111.41 33.40 o 7 14 0 12.80 43.46 35.83 o 8 14 0 15.78 81.56 51.35 o 9 14 0 1064.78 941.79 81.23 o 10 14 0 1612.69 1648.79 123.42 o 1 15 0 369.92 330.98 26.93 o 2 15 0 6365.85 6068.95 133.82 o 3 15 0 110.52 254.93 36.96 o 4 15 0 1785.09 1931.41 96.27 o 5 15 0 121.63 79.83 31.40 o 6 15 0 48.47 63.95 29.95 o 7 15 0 554.13 431.44 53.98 o 8 15 0 1469.14 1666.58 117.57 o 9 15 0 6.14 200.57 61.21 o 0 16 0 365.50 478.93 129.81 o 1 16 0 484.29 412.62 61.47 o 2 16 0 35.67 7.14 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