#------------------------------------------------------------------------------ #$Date: 2020-04-04 08:03:05 +0300 (Sat, 04 Apr 2020) $ #$Revision: 250121 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/33/2243336.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243336 _cell_angle_alpha 93.915 _cell_angle_beta 103.120 _cell_angle_gamma 97.600 _cell_length_a 10.9053 _cell_length_b 14.1157 _cell_length_c 16.2324 _exptl_crystal_F_000 1090.00 _reflns_d_resolution_high 0.6200 _cod_data_source_file ex20301bsup3.hkl _cod_data_source_block 1b _shelx_title ' bufbd01 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.85 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2362.86 2437.43 51.52 o 2 0 0 1889.11 1963.49 38.74 o 3 0 0 2728.05 2834.94 56.12 o 4 0 0 3140.66 2997.73 61.04 o 5 0 0 489.36 414.68 16.41 o 6 0 0 2280.40 2330.93 53.16 o 7 0 0 650.69 737.78 30.09 o 8 0 0 119.15 96.88 14.12 o 9 0 0 1839.12 1868.47 50.92 o 10 0 0 23.08 25.92 14.78 o 11 0 0 27.86 31.16 18.12 o 12 0 0 46.90 64.99 21.85 o 13 0 0 363.70 385.55 38.95 o 14 0 0 347.41 322.06 51.80 o 15 0 0 394.90 383.96 57.32 o 16 0 0 31.63 68.19 49.82 o -17 1 0 13.38 38.52 39.10 o -16 1 0 13.31 34.22 39.87 o -15 1 0 351.41 321.12 53.91 o -14 1 0 141.35 165.38 50.74 o -13 1 0 0.20 -8.17 26.80 o -12 1 0 141.86 158.38 25.68 o -11 1 0 275.97 305.83 23.73 o -10 1 0 791.95 742.25 31.09 o -9 1 0 21.36 37.98 11.85 o -8 1 0 931.08 913.40 36.42 o -7 1 0 74.67 67.03 11.17 o -6 1 0 1924.69 1785.81 43.48 o -5 1 0 3299.79 3783.96 76.88 o -4 1 0 571.91 557.83 17.70 o -3 1 0 3262.10 3198.42 62.49 o -2 1 0 31430.61 32578.71 572.75 o -1 1 0 33869.37 36079.36 897.24 o 1 1 0 6005.19 7192.10 256.44 o 2 1 0 746.29 991.12 22.03 o 3 1 0 1422.76 1351.12 30.20 o 4 1 0 92.71 93.58 8.24 o 5 1 0 166.97 170.04 11.38 o 6 1 0 2826.45 2970.93 70.80 o 7 1 0 2749.65 2628.81 60.62 o 8 1 0 211.49 201.61 16.08 o 9 1 0 135.91 148.53 16.03 o 10 1 0 1152.71 1231.24 51.28 o 11 1 0 740.54 705.69 41.10 o 12 1 0 471.26 432.60 38.29 o 13 1 0 2.06 16.49 21.41 o 14 1 0 80.01 20.33 31.55 o 15 1 0 106.14 55.32 48.45 o 16 1 0 84.58 35.90 49.60 o -17 2 0 84.87 94.92 43.51 o -16 2 0 146.90 157.26 46.56 o -15 2 0 74.54 147.82 43.00 o -14 2 0 222.24 237.04 44.84 o -13 2 0 21.84 41.59 29.22 o -12 2 0 595.36 856.91 110.85 o -11 2 0 4.64 -2.36 12.84 o -10 2 0 172.91 200.41 27.05 o -9 2 0 973.75 993.08 36.68 o -8 2 0 1752.50 1714.24 46.20 o -7 2 0 1644.27 1566.24 41.40 o -6 2 0 2419.46 2642.32 58.78 o -5 2 0 1444.00 1361.80 37.21 o -4 2 0 0.47 -0.08 5.38 o -3 2 0 16254.50 16940.01 302.22 o -2 2 0 7455.62 8104.11 146.14 o -1 2 0 4095.53 4120.44 106.82 o 0 2 0 9757.64 10543.75 187.09 o 1 2 0 17567.67 18795.78 473.10 o 2 2 0 1164.92 1407.87 30.11 o 3 2 0 5147.40 5608.16 105.24 o 4 2 0 4723.54 4615.31 89.80 o 5 2 0 2.16 -0.58 7.26 o 6 2 0 711.27 584.91 21.06 o 7 2 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32.13 o 7 3 0 874.58 864.08 28.02 o 8 3 0 10.29 26.32 9.33 o 9 3 0 78.32 91.79 19.74 o 10 3 0 97.60 53.69 18.55 o 11 3 0 144.22 118.90 28.43 o 12 3 0 378.37 336.73 36.15 o 13 3 0 185.32 177.17 30.37 o 14 3 0 129.72 129.66 31.01 o 15 3 0 33.12 -1.38 33.27 o 16 3 0 163.04 224.60 50.85 o -17 4 0 192.23 218.28 53.58 o -16 4 0 9.72 28.27 36.60 o -15 4 0 323.82 401.27 57.83 o -14 4 0 15.22 28.25 30.91 o -13 4 0 161.96 91.44 43.10 o -12 4 0 276.54 305.00 33.16 o -11 4 0 812.10 815.49 43.53 o -10 4 0 144.50 193.98 28.91 o -9 4 0 1869.93 1801.54 49.32 o -8 4 0 5872.33 5796.94 119.06 o -7 4 0 241.02 231.17 15.14 o -6 4 0 3198.76 3175.83 68.39 o -5 4 0 7259.63 8004.21 151.42 o -4 4 0 3126.20 3042.65 62.42 o -3 4 0 9381.00 9565.32 175.22 o -2 4 0 9023.50 9606.17 246.29 o -1 4 0 1232.18 1232.98 27.69 o 0 4 0 1336.48 1567.63 33.81 o 1 4 0 1152.64 1053.17 25.07 o 2 4 0 172.76 219.40 12.26 o 3 4 0 3745.32 3817.70 75.75 o 4 4 0 148.24 144.80 18.67 o 5 4 0 4720.28 4861.32 97.16 o 6 4 0 342.88 301.75 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8 5 0 403.00 415.94 68.62 o 9 5 0 313.83 348.74 30.71 o 10 5 0 915.99 815.47 69.38 o 11 5 0 15.16 -9.23 17.80 o 12 5 0 41.65 57.47 23.13 o 13 5 0 935.90 1022.25 56.04 o 14 5 0 68.91 70.39 28.19 o 15 5 0 13.00 5.65 33.60 o -17 6 0 97.04 175.69 51.04 o -16 6 0 144.03 84.82 114.28 o -15 6 0 100.25 20.81 56.00 o -14 6 0 64.50 30.03 24.21 o -13 6 0 73.91 74.45 25.84 o -12 6 0 82.59 100.15 23.91 o -11 6 0 1545.55 1726.04 65.31 o -10 6 0 13.94 1.15 15.59 o -9 6 0 38.44 8.28 14.99 o -8 6 0 617.71 663.81 51.52 o -7 6 0 2609.55 2624.22 60.11 o -6 6 0 3996.90 3809.02 79.90 o -5 6 0 1946.40 1936.34 44.88 o -4 6 0 6130.35 6351.12 122.49 o -3 6 0 419.13 448.40 17.08 o -2 6 0 5830.11 6013.27 131.94 o -1 6 0 432.34 500.30 20.72 o 0 6 0 5682.38 6414.49 121.68 o 1 6 0 255.21 343.75 16.50 o 2 6 0 6114.15 6122.91 168.37 o 3 6 0 6595.12 6365.79 154.10 o 4 6 0 187.25 174.38 14.84 o 5 6 0 246.73 260.66 15.51 o 6 6 0 1536.31 1579.21 41.12 o 7 6 0 1017.10 1015.96 42.34 o 8 6 0 56.21 38.54 16.01 o 9 6 0 171.79 173.88 25.11 o 10 6 0 660.91 689.96 40.91 o 11 6 0 817.74 827.44 46.38 o 12 6 0 105.98 65.26 23.80 o 13 6 0 207.65 162.48 42.39 o 14 6 0 20.76 -3.08 30.64 o 15 6 0 185.14 220.20 48.76 o -16 7 0 44.87 5.73 41.14 o -15 7 0 0.39 -4.00 30.85 o -14 7 0 41.07 24.90 23.78 o -13 7 0 871.56 904.70 51.48 o -12 7 0 74.11 50.80 22.17 o -11 7 0 5.95 13.53 18.89 o -10 7 0 442.46 423.39 32.31 o -9 7 0 193.44 226.72 39.43 o -8 7 0 2333.81 2320.07 71.58 o -7 7 0 198.39 180.79 21.22 o -6 7 0 57.08 26.84 15.70 o -5 7 0 1275.17 1404.71 38.46 o -4 7 0 2609.97 2428.69 72.51 o -3 7 0 550.91 484.39 27.01 o -2 7 0 857.06 926.36 33.03 o -1 7 0 9.49 26.26 6.99 o 0 7 0 519.57 528.90 18.82 o 1 7 0 4833.19 4466.01 89.53 o 2 7 0 21.36 12.34 14.17 o 3 7 0 1084.69 1268.30 59.84 o 4 7 0 350.97 362.61 17.58 o 5 7 0 4055.23 4042.98 102.36 o 6 7 0 354.00 370.49 19.11 o 7 7 0 550.92 517.93 44.94 o 8 7 0 1436.15 1251.27 51.06 o 9 7 0 45.12 40.76 18.07 o 10 7 0 1215.96 1268.27 56.13 o 11 7 0 1.06 6.67 19.20 o 12 7 0 22.12 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246.85 45.03 o -9 11 0 184.79 182.66 26.59 o -8 11 0 316.64 316.28 31.29 o -7 11 0 751.28 741.12 39.12 o -6 11 0 932.45 973.73 69.04 o -5 11 0 818.34 896.36 57.75 o -4 11 0 302.08 311.75 20.64 o -3 11 0 3129.30 3140.96 104.02 o -2 11 0 774.76 812.86 33.99 o -1 11 0 80.56 93.98 13.21 o 0 11 0 712.36 724.84 27.97 o 1 11 0 2257.26 2260.41 113.57 o 2 11 0 1727.01 1677.93 103.08 o 3 11 0 1.06 -8.60 13.70 o 4 11 0 141.91 154.80 18.86 o 5 11 0 432.45 449.58 31.05 o 6 11 0 3114.23 3223.53 95.84 o 7 11 0 433.94 423.82 33.89 o 8 11 0 84.57 27.79 25.51 o 9 11 0 148.81 171.84 38.77 o 10 11 0 71.63 72.37 68.34 o 11 11 0 344.00 364.20 53.49 o 12 11 0 22.33 8.65 32.47 o 13 11 0 1.15 -32.18 32.18 o -15 12 0 83.02 54.87 39.56 o -14 12 0 33.88 82.31 30.69 o -13 12 0 502.36 603.61 49.04 o -12 12 0 1.27 -0.51 20.70 o -11 12 0 3.48 12.82 20.44 o -10 12 0 192.08 191.28 30.14 o -9 12 0 1151.27 1223.25 55.60 o -8 12 0 156.66 155.52 25.62 o -7 12 0 70.69 78.29 20.38 o -6 12 0 526.66 549.65 42.39 o -5 12 0 112.60 95.26 19.72 o -4 12 0 296.15 288.36 25.87 o -3 12 0 886.65 952.80 48.49 o -2 12 0 1.30 6.88 13.26 o -1 12 0 265.41 278.65 34.43 o 0 12 0 3131.66 3021.58 72.02 o 1 12 0 456.50 468.41 27.73 o 2 12 0 88.39 92.31 45.94 o 3 12 0 14.75 6.80 13.44 o 4 12 0 660.57 639.88 32.92 o 5 12 0 3953.78 4036.53 112.24 o 6 12 0 163.17 157.78 23.73 o 7 12 0 1.89 -13.57 13.57 o 8 12 0 104.96 90.25 32.63 o 9 12 0 350.85 329.68 57.60 o 10 12 0 1.52 43.90 32.01 o 11 12 0 50.01 46.27 35.01 o 12 12 0 0.91 29.79 34.01 o -15 13 0 139.45 163.96 48.58 o -14 13 0 1.51 -0.01 33.61 o -13 13 0 61.53 98.22 30.82 o -12 13 0 4.87 -5.62 22.15 o -11 13 0 215.94 169.47 30.04 o -10 13 0 448.70 478.13 46.54 o -9 13 0 0.71 14.24 19.70 o -8 13 0 442.29 542.81 51.45 o -7 13 0 136.46 125.99 23.82 o -6 13 0 415.33 425.72 31.98 o -5 13 0 21.90 15.51 15.97 o -4 13 0 395.95 391.08 30.29 o -3 13 0 66.18 39.24 19.31 o -2 13 0 1495.15 1388.89 50.13 o -1 13 0 613.98 681.47 34.22 o 0 13 0 139.87 191.66 27.61 o 1 13 0 231.60 254.08 26.16 o 2 13 0 566.91 537.58 62.17 o 3 13 0 1021.16 1057.85 43.92 o 4 13 0 231.30 305.19 42.05 o 5 13 0 21.94 8.01 14.53 o 6 13 0 171.87 224.88 62.17 o 7 13 0 407.61 300.91 71.08 o 8 13 0 679.18 625.04 60.78 o 9 13 0 37.59 62.63 33.29 o 10 13 0 143.29 136.59 48.00 o 11 13 0 10.77 -0.73 48.00 o 12 13 0 183.66 124.00 74.28 o -14 14 0 94.75 119.81 44.46 o -13 14 0 29.69 23.34 35.25 o -12 14 0 357.65 267.64 38.07 o -11 14 0 1.70 25.15 22.67 o -10 14 0 3.33 0.61 22.88 o -9 14 0 551.84 600.61 52.91 o -8 14 0 7.74 10.79 20.06 o -7 14 0 296.06 256.35 30.99 o -6 14 0 175.01 158.72 30.57 o -5 14 0 1051.67 1108.60 49.68 o -4 14 0 38.77 50.03 19.31 o -3 14 0 2623.75 2443.11 93.42 o -2 14 0 30.16 34.09 35.88 o -1 14 0 315.60 349.29 28.96 o 0 14 0 519.99 564.97 32.53 o 1 14 0 247.28 265.54 32.89 o 2 14 0 613.27 683.43 45.08 o 3 14 0 30.95 12.28 16.07 o 4 14 0 1630.49 1501.13 110.62 o 5 14 0 79.04 24.54 26.36 o 6 14 0 1182.72 1067.90 128.22 o 7 14 0 0.38 -11.57 27.63 o 8 14 0 50.58 7.30 29.69 o 9 14 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