#------------------------------------------------------------------------------ #$Date: 2020-08-29 08:06:38 +0300 (Sat, 29 Aug 2020) $ #$Revision: 255741 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/35/2243557.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243557 _cell_angle_alpha 90 _cell_angle_beta 111.2251 _cell_angle_gamma 90 _cell_length_a 7.1048 _cell_length_b 5.3003 _cell_length_c 11.9035 _exptl_crystal_F_000 200 _reflns_d_resolution_high 0.8077 _cod_data_source_file wm5573Isup2.hkl _cod_data_source_block I _shelx_title 'cu_jf_naprop2_fabry_0ma_a.res in p2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 86.66 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4874.46 5335.08 141.05 o 6 0 0 82.38 68.43 1.52 o 8 0 0 88.24 81.88 1.90 o 1 1 0 1.76 5.96 0.43 o 2 1 0 2702.57 2884.89 64.86 o 3 1 0 3.52 7.50 0.46 o 5 1 0 2.90 4.99 0.34 o 6 1 0 83.56 86.32 1.39 o 7 1 0 1.31 1.49 0.28 o 8 1 0 144.91 125.67 2.85 o 0 2 0 40.09 26.66 0.99 o 1 2 0 10.78 12.46 0.44 o 2 2 0 823.87 806.76 12.06 o 3 2 0 1.58 2.90 0.26 o 4 2 0 186.50 179.72 2.04 o 5 2 0 0.09 0.56 0.35 < 6 2 0 192.37 212.92 2.68 o 7 2 0 0.04 0.53 0.35 < 1 3 0 1.23 3.07 0.22 o 2 3 0 289.57 273.19 3.34 o 3 3 0 1.53 2.01 0.29 o 4 3 0 220.40 252.25 3.30 o 5 3 0 0.95 1.55 0.39 o 6 3 0 0.16 0.05 0.32 < 7 3 0 1.16 1.38 0.44 o 0 4 0 2419.01 2591.39 47.04 o 1 4 0 0.34 0.38 0.26 < 2 4 0 226.92 204.73 2.75 o 3 4 0 0.00 -0.15 0.27 < 4 4 0 2.66 9.70 0.48 o 5 4 0 0.01 -0.36 0.38 < 6 4 0 58.24 65.31 2.13 o 1 5 0 0.01 0.76 0.32 < 2 5 0 629.65 622.18 10.34 o 3 5 0 0.23 0.47 0.28 < 4 5 0 72.30 68.18 1.64 o 5 5 0 0.68 0.38 0.38 < 0 6 0 214.85 255.63 6.88 o 1 6 0 0.01 0.82 0.21 o 2 6 0 1.07 0.11 0.23 < 3 6 0 0.00 -0.15 0.30 < -8 0 1 167.25 132.61 3.12 o -6 0 1 281.68 264.37 4.59 o -4 0 1 3441.56 3325.17 84.95 o -2 0 1 813.46 828.97 25.47 o 2 0 1 536.22 704.97 18.58 o 4 0 1 542.10 675.78 11.20 o 6 0 1 421.18 397.96 6.74 o -8 1 1 9.78 11.28 0.46 o -7 1 1 0.00 0.53 0.26 < -6 1 1 52.57 52.63 0.96 o -5 1 1 1.39 1.27 0.22 o -3 1 1 11.69 15.95 0.63 o -2 1 1 5196.99 5584.59 104.13 o -1 1 1 68.40 71.47 1.66 o 0 1 1 870.26 1066.65 21.18 o 1 1 1 86.29 71.99 1.52 o 2 1 1 2.71 3.39 0.56 o 3 1 1 21.75 28.57 0.87 o 4 1 1 475.80 480.93 5.72 o 5 1 1 5.58 8.48 0.40 o 6 1 1 42.40 41.58 1.09 o 7 1 1 1.61 2.16 0.32 o -7 2 1 0.00 0.50 0.32 < -6 2 1 184.85 179.21 2.32 o -5 2 1 0.84 0.84 0.27 o -4 2 1 164.49 173.42 2.15 o -3 2 1 1.12 1.46 0.23 o -2 2 1 0.53 1.09 0.23 o -1 2 1 5.08 8.94 0.59 o 0 2 1 202.08 195.04 5.34 o 1 2 1 1.13 1.24 0.23 o 2 2 1 1280.66 1313.50 19.58 o 3 2 1 0.06 0.05 0.17 < 4 2 1 28.89 27.60 0.55 o 5 2 1 0.01 -0.17 0.28 < 6 2 1 220.14 206.68 2.60 o -7 3 1 0.00 0.58 0.41 < -6 3 1 53.93 58.47 1.22 o -5 3 1 0.26 0.55 0.35 < -3 3 1 3.66 5.31 0.31 o -2 3 1 374.35 337.77 4.54 o -1 3 1 19.46 19.57 0.56 o 0 3 1 86.97 88.79 1.83 o 1 3 1 21.63 23.40 0.67 o 2 3 1 7.86 6.09 0.35 o 3 3 1 8.56 9.76 0.35 o 4 3 1 652.68 674.59 11.30 o 5 3 1 3.83 4.77 0.48 o 6 3 1 8.43 8.18 0.48 o 7 3 1 1.13 1.00 0.35 < -6 4 1 58.41 58.17 1.35 o -5 4 1 0.12 -0.13 0.32 < -4 4 1 836.66 830.87 11.65 o -3 4 1 0.25 0.46 0.27 < -2 4 1 64.08 56.55 1.03 o -1 4 1 0.00 0.31 0.32 < 0 4 1 524.31 543.77 6.73 o 1 4 1 0.00 0.11 0.29 < 2 4 1 1.86 2.35 0.33 o 3 4 1 0.01 -0.28 0.29 < 4 4 1 79.89 96.12 1.58 o 5 4 1 0.02 0.06 0.30 < 6 4 1 172.47 166.56 4.53 o -5 5 1 0.30 -0.08 0.38 < -4 5 1 68.77 70.59 1.39 o -3 5 1 0.58 1.73 0.39 o -2 5 1 1199.52 1208.06 18.10 o -1 5 1 1.34 1.92 0.33 o 0 5 1 134.32 146.66 2.14 o 1 5 1 3.33 5.14 0.35 o 2 5 1 0.45 1.34 0.31 o 3 5 1 2.74 3.05 0.32 o 4 5 1 36.94 44.95 1.52 o 5 5 1 1.26 1.13 0.38 < -3 6 1 0.10 0.79 0.23 o -2 6 1 0.03 0.78 0.26 o -1 6 1 0.00 0.66 0.24 < 0 6 1 139.29 142.28 2.79 o 1 6 1 0.01 -0.17 0.29 < 2 6 1 8.71 9.69 0.38 o -8 0 2 58.22 60.56 2.87 o -6 0 2 34.93 43.00 1.03 o -4 0 2 3695.11 3841.75 138.85 o -2 0 2 1228.62 1394.07 40.72 o 0 0 2 121.00 126.61 2.14 o 2 0 2 353.91 341.64 13.12 o 4 0 2 550.36 536.85 8.22 o 6 0 2 221.63 214.24 3.45 o -8 1 2 5.56 8.98 0.37 o -7 1 2 2.54 3.17 0.49 o -6 1 2 603.62 597.93 6.72 o -5 1 2 10.82 12.51 0.34 o -4 1 2 66.53 71.19 1.70 o -3 1 2 46.07 53.19 1.26 o -2 1 2 814.51 929.99 23.96 o -1 1 2 148.99 126.84 3.41 o 0 1 2 242.98 307.96 5.75 o 1 1 2 98.76 80.76 1.61 o 2 1 2 128.23 130.42 3.24 o 3 1 2 20.99 23.42 0.79 o 4 1 2 615.55 611.64 6.59 o 5 1 2 4.46 4.19 0.31 o 6 1 2 26.30 28.38 0.70 o 7 1 2 0.87 1.00 0.28 o -8 2 2 49.50 58.00 3.24 o -7 2 2 0.04 -0.13 0.26 < -6 2 2 108.06 116.51 1.70 o -5 2 2 0.22 0.40 0.26 < -4 2 2 138.12 140.84 2.00 o -3 2 2 0.13 0.20 0.20 < -2 2 2 318.19 341.46 5.69 o -1 2 2 1.74 2.15 0.31 o 0 2 2 0.15 1.62 0.48 o 1 2 2 4.74 5.24 0.29 o 2 2 2 2465.00 2480.08 34.01 o 3 2 2 0.18 0.32 0.20 < 4 2 2 86.70 85.58 1.24 o 5 2 2 0.06 0.11 0.26 < 6 2 2 8.42 13.55 0.52 o 7 2 2 0.04 0.08 0.31 < -7 3 2 1.73 1.79 0.50 o -6 3 2 199.92 192.25 3.18 o -5 3 2 5.26 5.86 0.51 o -4 3 2 68.02 79.48 1.42 o -3 3 2 14.53 16.54 0.45 o -2 3 2 1.78 0.45 0.23 < -1 3 2 43.08 47.59 1.09 o 0 3 2 1684.67 1875.26 39.23 o 1 3 2 29.85 30.41 0.70 o 2 3 2 87.31 74.51 1.21 o 3 3 2 6.82 6.02 0.52 o 4 3 2 301.43 320.64 5.15 o 5 3 2 2.04 1.79 0.35 o 6 3 2 0.07 0.20 0.33 < -6 4 2 0.05 1.48 0.38 o -5 4 2 0.01 0.42 0.42 < -4 4 2 617.82 632.94 8.95 o -3 4 2 0.00 0.58 0.30 < -2 4 2 26.77 28.73 0.72 o -1 4 2 0.11 0.24 0.28 < 0 4 2 5.26 5.91 0.35 o 1 4 2 0.01 0.32 0.23 < 2 4 2 287.12 270.89 3.73 o 3 4 2 0.00 -0.06 0.29 < 4 4 2 35.37 35.84 0.74 o 5 4 2 0.04 0.32 0.30 < -5 5 2 1.18 0.45 0.39 < -4 5 2 7.48 10.09 0.57 o -3 5 2 4.50 7.35 0.53 o -2 5 2 403.98 389.33 5.60 o -1 5 2 4.82 5.97 0.41 o 0 5 2 21.22 20.44 0.56 o 2 5 2 121.34 116.68 2.04 o 3 5 2 3.27 4.09 0.34 o 4 5 2 167.53 168.16 3.77 o -3 6 2 0.00 -0.15 0.30 < -2 6 2 0.20 0.47 0.27 < -1 6 2 0.00 0.59 0.25 < 0 6 2 1.87 1.79 0.25 o 1 6 2 0.25 0.42 0.20 < 2 6 2 116.81 119.12 3.20 o -8 0 3 284.17 270.17 5.88 o -6 0 3 7.16 8.81 0.60 o -4 0 3 1354.96 1786.97 45.75 o -2 0 3 1.64 9.20 0.91 o 0 0 3 138.58 181.37 3.08 o 2 0 3 613.08 663.68 25.12 o 4 0 3 598.11 587.38 9.75 o 6 0 3 190.62 186.62 3.32 o -8 1 3 6.13 7.99 0.31 o -7 1 3 3.71 5.60 0.35 o -6 1 3 415.47 403.09 4.80 o -5 1 3 12.51 16.53 0.38 o -4 1 3 5.80 10.08 0.44 o -3 1 3 38.85 38.78 2.07 o -2 1 3 58.26 49.32 1.27 o -1 1 3 77.61 105.70 3.14 o 0 1 3 1238.78 1424.62 36.60 o 1 1 3 25.69 22.39 0.49 o 2 1 3 199.83 210.43 4.18 o 3 1 3 2.12 2.75 0.29 o 4 1 3 235.46 227.70 2.48 o 5 1 3 0.03 0.19 0.26 < 6 1 3 60.02 61.29 1.10 o 7 1 3 0.06 0.32 0.27 < -8 2 3 80.33 74.45 1.37 o -7 2 3 0.02 0.05 0.29 < -6 2 3 38.29 39.29 0.75 o -5 2 3 0.05 0.76 0.29 < -3 2 3 0.04 -0.12 0.19 < -2 2 3 2730.82 2927.30 76.99 o -1 2 3 19.01 21.27 0.94 o 0 2 3 290.94 347.98 9.21 o 1 2 3 3.99 3.59 0.27 o 2 2 3 841.85 854.50 9.93 o 3 2 3 0.95 0.81 0.24 o 4 2 3 4.52 8.78 0.41 o 5 2 3 0.07 -0.39 0.38 < 6 2 3 38.62 36.34 0.83 o 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0.23 < 2 6 3 119.01 103.03 4.00 o -8 0 4 198.50 196.54 3.90 o -6 0 4 5.10 3.39 0.51 o -4 0 4 370.57 697.17 31.43 o -2 0 4 279.04 337.65 12.60 o 0 0 4 5829.20 7509.93 199.85 o 2 0 4 2280.57 2239.73 40.63 o 4 0 4 58.12 57.17 1.36 o 6 0 4 1.46 3.08 0.54 o -8 1 4 0.81 2.10 0.28 o -7 1 4 2.09 2.37 0.34 o -6 1 4 176.66 173.58 2.30 o -5 1 4 3.53 4.65 0.28 o -4 1 4 227.31 224.60 3.88 o -3 1 4 4.79 3.33 1.55 < -2 1 4 17.63 16.59 0.83 o -1 1 4 0.10 2.94 0.30 o 0 1 4 755.71 714.11 15.14 o 1 1 4 3.64 2.95 0.25 o 2 1 4 552.68 515.89 5.78 o 3 1 4 2.98 2.68 0.27 o 4 1 4 99.62 104.21 1.38 o 5 1 4 1.90 1.73 0.35 o 6 1 4 12.73 13.76 0.45 o -8 2 4 9.77 8.12 0.54 o -7 2 4 0.08 0.23 0.26 < -6 2 4 90.72 98.07 1.45 o -5 2 4 0.38 0.81 0.32 < -3 2 4 0.28 0.17 0.20 < -2 2 4 3348.88 3624.04 79.91 o -1 2 4 3.76 4.64 0.39 o 0 2 4 667.75 884.73 16.28 o 1 2 4 0.26 0.08 0.18 < 2 2 4 19.74 20.02 0.37 o 3 2 4 0.03 -0.04 0.19 < 4 2 4 249.17 279.16 3.29 o 5 2 4 0.00 -0.49 0.26 < 6 2 4 10.40 11.62 0.44 o -7 3 4 1.21 2.41 0.47 o -6 3 4 0.70 1.66 0.40 o -5 3 4 1.02 2.31 0.50 o -4 3 4 836.22 842.93 11.84 o -3 3 4 0.16 1.58 0.30 o -2 3 4 161.27 148.60 2.00 o -1 3 4 0.92 1.07 0.30 o 0 3 4 397.17 430.14 5.11 o 1 3 4 2.34 1.78 0.26 o 2 3 4 34.43 27.24 0.57 o 3 3 4 1.51 0.73 0.29 < 5 3 4 0.87 0.91 0.29 o 6 3 4 50.05 45.78 1.41 o -6 4 4 15.74 12.02 0.58 o -5 4 4 0.02 0.48 0.35 < -3 4 4 0.00 0.05 0.29 < -2 4 4 41.06 52.19 1.05 o -1 4 4 0.01 -0.24 0.26 < 0 4 4 431.18 426.88 4.49 o 1 4 4 0.00 -0.14 0.23 < 2 4 4 409.32 362.54 4.84 o 3 4 4 0.06 0.19 0.35 < 4 4 4 18.28 21.69 0.70 o 5 4 4 0.14 0.28 0.23 < -5 5 4 0.77 0.96 0.51 < -4 5 4 1.97 9.43 0.56 o -3 5 4 0.51 1.38 0.36 o -2 5 4 77.87 65.45 1.07 o -1 5 4 0.00 0.75 0.26 < 0 5 4 171.99 172.74 3.09 o 1 5 4 0.14 0.25 0.22 < 2 5 4 206.83 185.84 2.52 o 3 5 4 0.30 0.23 0.27 < -3 6 4 0.00 1.11 0.50 < -2 6 4 151.77 143.24 2.78 o -1 6 4 0.15 0.36 0.21 < 1 6 4 0.02 0.00 0.26 < -8 0 5 313.78 275.55 6.01 o -6 0 5 49.60 40.10 0.98 o -4 0 5 617.73 599.68 12.88 o -2 0 5 1261.96 1262.96 46.08 o 0 0 5 2174.96 2602.40 76.72 o 2 0 5 1008.11 995.12 13.82 o 4 0 5 4.38 6.21 0.51 o 6 0 5 117.50 110.49 3.47 o -8 1 5 11.48 12.81 0.38 o -7 1 5 0.11 0.86 0.32 < -6 1 5 58.60 60.45 1.09 o -5 1 5 2.16 3.04 0.26 o -4 1 5 234.13 216.27 2.53 o -3 1 5 7.03 11.63 0.40 o -2 1 5 850.47 890.15 16.25 o -1 1 5 20.46 15.66 0.41 o 0 1 5 1118.49 1084.56 16.09 o 1 1 5 16.71 12.86 0.35 o 2 1 5 199.04 188.26 2.38 o 3 1 5 5.47 5.09 0.29 o 4 1 5 7.41 9.94 0.42 o 5 1 5 1.63 1.80 0.41 o 6 1 5 9.87 10.79 0.35 o -8 2 5 1.64 1.90 0.28 o -7 2 5 0.06 0.79 0.29 < -6 2 5 646.66 618.55 7.69 o -5 2 5 0.94 0.72 0.29 < -4 2 5 212.57 190.59 2.21 o -3 2 5 0.14 0.29 0.24 < -2 2 5 421.15 372.30 5.66 o -1 2 5 0.49 0.23 0.21 < 0 2 5 58.01 78.80 1.34 o 1 2 5 0.34 0.73 0.21 o 2 2 5 35.49 34.10 0.52 o 3 2 5 0.39 0.28 0.25 < 4 2 5 178.42 188.75 2.87 o 5 2 5 0.01 0.08 0.31 < 6 2 5 46.71 45.06 1.06 o -7 3 5 0.36 0.98 0.38 < -6 3 5 15.51 22.01 0.81 o -5 3 5 0.82 0.90 0.37 < -4 3 5 601.53 631.19 8.36 o -3 3 5 4.25 4.82 0.32 o -2 3 5 1.00 3.70 0.27 o -1 3 5 12.20 9.19 0.32 o 0 3 5 104.44 96.15 1.29 o 1 3 5 5.36 5.48 0.29 o 2 3 5 101.93 93.10 1.49 o 3 3 5 1.90 1.99 0.32 o 4 3 5 68.06 67.96 1.16 o 5 3 5 1.04 0.87 0.26 o -6 4 5 0.83 0.51 0.35 < -5 4 5 0.01 0.29 0.34 < -4 4 5 103.20 91.03 1.48 o -3 4 5 0.00 -0.44 0.29 < -2 4 5 388.10 349.83 4.24 o -1 4 5 0.10 0.05 0.23 < 0 4 5 233.54 241.11 2.72 o 1 4 5 0.18 0.20 0.26 < 2 4 5 130.78 116.32 1.83 o 3 4 5 0.00 0.17 0.38 < 4 4 5 0.04 0.78 0.31 < -5 5 5 0.47 1.00 0.48 < -4 5 5 2.14 9.22 0.48 o -3 5 5 1.53 1.56 0.29 o -2 5 5 354.95 331.00 4.42 o -1 5 5 1.46 2.14 0.33 o 0 5 5 347.22 368.40 5.21 o 1 5 5 2.86 3.30 0.27 o 2 5 5 28.63 28.22 0.67 o 3 5 5 2.58 1.76 0.31 o -2 6 5 51.38 48.38 1.73 o -1 6 5 0.06 0.68 0.38 < -8 0 6 11.78 26.15 0.97 o -6 0 6 9.51 13.33 0.71 o -4 0 6 1567.58 1522.25 56.41 o -2 0 6 3158.01 3213.85 67.10 o 0 0 6 18.31 14.07 0.61 o 2 0 6 1.32 2.56 0.29 o 4 0 6 2.90 4.36 0.45 o 6 0 6 97.32 89.20 2.10 o -8 1 6 5.61 7.46 0.34 o -7 1 6 3.75 5.46 0.44 o -6 1 6 54.34 60.04 0.95 o -5 1 6 7.59 8.26 0.32 o -4 1 6 613.09 588.29 7.31 o -3 1 6 15.58 17.27 0.48 o -2 1 6 550.81 576.86 7.47 o -1 1 6 25.09 20.59 0.48 o 0 1 6 271.99 301.77 4.60 o 1 1 6 10.98 9.01 0.26 o 2 1 6 40.44 40.85 0.57 o 3 1 6 3.25 3.52 0.36 o 4 1 6 203.56 201.65 2.72 o 5 1 6 1.01 1.36 0.29 o 6 1 6 46.93 43.72 1.01 o -8 2 6 4.34 3.66 0.38 o -7 2 6 0.01 0.30 0.32 < -6 2 6 387.47 380.61 5.17 o -5 2 6 0.02 0.35 0.29 < -4 2 6 3.38 6.03 0.31 o -3 2 6 0.29 0.48 0.27 < -2 2 6 100.49 84.69 1.16 o -1 2 6 4.94 3.97 0.29 o 0 2 6 139.98 157.48 2.12 o 1 2 6 0.41 0.27 0.18 < 2 2 6 294.27 279.55 3.57 o 3 2 6 0.07 0.21 0.23 < 4 2 6 239.57 243.69 3.42 o 5 2 6 0.00 -0.36 0.32 < -7 3 6 1.52 2.73 0.41 o -6 3 6 1.40 2.93 0.47 o -5 3 6 3.84 4.55 0.45 o -4 3 6 474.15 511.62 7.27 o -3 3 6 7.83 8.28 0.36 o -2 3 6 1.03 0.89 0.23 o -1 3 6 7.30 7.56 0.30 o 0 3 6 50.59 67.69 0.91 o 1 3 6 4.90 3.20 0.29 o 2 3 6 187.21 167.72 2.15 o 3 3 6 2.39 2.29 0.42 o 4 3 6 124.66 126.20 2.65 o -6 4 6 31.27 32.92 0.86 o -5 4 6 0.01 0.34 0.38 < -4 4 6 257.83 258.48 4.53 o -3 4 6 0.00 -0.14 0.29 < -2 4 6 467.58 413.75 4.94 o -1 4 6 0.25 0.37 0.24 < 0 4 6 22.28 31.77 0.58 o 1 4 6 0.68 0.22 0.29 < 2 4 6 37.84 31.93 0.68 o 3 4 6 0.20 0.63 0.29 < 4 4 6 24.69 22.08 0.63 o -5 5 6 2.06 2.09 0.45 o -4 5 6 116.89 110.34 2.02 o -3 5 6 4.12 5.34 0.41 o -2 5 6 252.29 256.79 3.71 o -1 5 6 5.25 7.57 0.34 o 0 5 6 198.77 206.82 3.26 o 1 5 6 2.76 2.89 0.24 o 2 5 6 3.62 3.04 0.39 o -8 0 7 126.49 149.58 3.45 o -6 0 7 374.54 347.74 5.92 o -4 0 7 561.12 537.13 8.89 o -2 0 7 412.57 381.45 8.23 o 0 0 7 36.01 32.90 0.74 o 2 0 7 263.17 241.36 4.67 o 4 0 7 12.12 12.82 0.55 o -8 1 7 61.73 60.97 0.95 o -7 1 7 3.27 5.05 0.38 o -6 1 7 174.06 168.07 2.24 o -5 1 7 6.77 7.44 0.34 o -4 1 7 588.22 567.52 6.12 o -3 1 7 10.83 8.21 0.35 o -2 1 7 61.12 54.73 0.75 o -1 1 7 6.50 5.42 0.29 o 0 1 7 228.29 240.22 2.47 o 1 1 7 0.84 1.49 0.19 o 2 1 7 191.57 179.26 1.92 o 3 1 7 0.00 0.32 0.24 < 4 1 7 75.19 81.20 1.13 o 5 1 7 0.09 0.16 0.26 < -8 2 7 5.12 11.24 0.59 o -7 2 7 0.03 0.39 0.33 < -6 2 7 382.73 356.65 6.89 o -5 2 7 0.12 0.21 0.31 < -4 2 7 5.67 9.59 0.37 o -3 2 7 0.13 0.46 0.24 < -2 2 7 182.36 169.90 2.37 o -1 2 7 2.34 1.42 0.26 o 0 2 7 446.43 471.78 4.74 o 1 2 7 0.03 0.25 0.25 < 2 2 7 349.18 338.21 3.92 o 3 2 7 0.09 -0.05 0.34 < 4 2 7 255.96 265.99 3.43 o 5 2 7 0.02 0.02 0.24 < -7 3 7 1.87 3.00 0.35 o -6 3 7 0.15 0.96 0.34 < -5 3 7 3.37 4.03 0.42 o -4 3 7 103.24 115.91 1.64 o -3 3 7 4.93 4.00 0.42 o -2 3 7 18.55 17.78 0.46 o -1 3 7 1.99 2.15 0.29 o 0 3 7 511.10 643.10 7.66 o 1 3 7 0.40 0.63 0.25 < 2 3 7 486.03 490.03 5.82 o 3 3 7 0.11 0.37 0.32 < 4 3 7 2.64 2.18 0.27 o -6 4 7 217.99 209.42 3.66 o -5 4 7 0.37 -0.12 0.32 < -4 4 7 45.69 50.70 0.96 o -3 4 7 0.65 0.43 0.32 < -2 4 7 28.95 25.99 0.57 o -1 4 7 0.19 0.19 0.27 < 0 4 7 41.87 45.81 0.80 o 1 4 7 0.05 -0.22 0.26 < 2 4 7 101.91 95.42 1.80 o 3 4 7 0.01 0.43 0.28 < -5 5 7 2.93 3.37 0.37 o -4 5 7 244.90 227.69 3.54 o -3 5 7 2.09 3.19 0.29 o -2 5 7 18.04 18.55 0.46 o -1 5 7 0.97 1.63 0.25 o 0 5 7 3.87 4.53 0.33 o 1 5 7 0.36 -0.30 0.17 < 2 5 7 4.01 2.98 0.41 o -8 0 8 83.26 95.69 2.32 o -6 0 8 259.38 251.88 4.86 o -4 0 8 231.57 247.36 4.25 o -2 0 8 4.55 4.77 0.35 o 0 0 8 1.77 1.92 0.30 o 2 0 8 366.20 378.50 5.94 o 4 0 8 1.22 1.18 0.33 o -8 1 8 196.27 187.92 3.23 o -7 1 8 1.01 4.40 0.41 o -6 1 8 24.13 24.71 0.63 o -5 1 8 0.45 0.69 0.25 < -3 1 8 0.00 0.89 0.20 o -2 1 8 309.04 285.47 3.45 o -1 1 8 2.94 2.61 0.23 o 0 1 8 278.57 311.91 2.88 o 1 1 8 4.79 4.07 0.34 o 2 1 8 90.35 87.35 1.10 o 3 1 8 2.27 1.49 0.26 o 4 1 8 8.68 10.41 0.33 o 5 1 8 0.85 0.89 0.28 o -8 2 8 1.34 3.88 0.41 o -7 2 8 0.00 -0.06 0.33 < -6 2 8 65.87 63.28 1.18 o -5 2 8 0.10 0.05 0.31 < -4 2 8 0.36 0.75 0.37 < -3 2 8 0.01 -0.11 0.30 < -2 2 8 1207.32 1154.93 12.23 o -1 2 8 0.22 0.83 0.28 < 0 2 8 1548.66 1710.58 16.11 o 1 2 8 0.02 0.21 0.23 < 2 2 8 17.49 17.23 1.09 o 3 2 8 0.07 0.20 0.29 < 4 2 8 12.51 13.61 0.56 o -7 3 8 0.71 0.78 0.29 < -6 3 8 31.63 28.81 0.77 o -5 3 8 0.61 0.41 0.34 < -4 3 8 191.46 183.89 2.65 o -3 3 8 0.27 0.53 0.35 < -2 3 8 511.03 495.26 5.88 o -1 3 8 1.82 1.34 0.27 o 0 3 8 161.33 202.52 2.53 o 1 3 8 1.06 1.37 0.23 o 2 3 8 180.95 174.71 2.93 o 3 3 8 0.96 0.70 0.28 < 4 3 8 9.17 8.22 0.41 o -6 4 8 63.39 71.81 1.56 o -5 4 8 0.01 0.88 0.48 < -4 4 8 55.59 59.98 1.06 o -3 4 8 0.01 -0.09 0.35 < -2 4 8 22.34 22.28 0.46 o -1 4 8 0.01 0.21 0.21 < 0 4 8 40.90 49.46 0.84 o 1 4 8 0.02 0.23 0.23 < 2 4 8 78.24 70.82 1.82 o -4 5 8 37.96 52.06 1.50 o -3 5 8 0.01 0.32 0.20 < -2 5 8 7.06 8.58 0.31 o -1 5 8 0.31 -0.10 0.23 < 0 5 8 78.06 77.79 1.37 o 1 5 8 0.95 0.38 0.30 < -8 0 9 73.23 73.01 1.83 o -6 0 9 66.73 63.80 1.52 o -4 0 9 59.57 52.68 1.34 o -2 0 9 143.71 132.27 1.80 o 0 0 9 2.58 4.62 0.43 o 2 0 9 202.50 220.32 5.11 o 4 0 9 8.90 8.39 0.46 o -8 1 9 25.62 24.83 0.70 o -7 1 9 0.90 1.87 0.38 o -6 1 9 64.89 63.58 1.01 o -5 1 9 3.46 3.95 0.34 o -4 1 9 125.31 128.07 1.90 o -3 1 9 7.68 7.41 0.34 o -2 1 9 330.27 304.70 2.94 o -1 1 9 9.13 8.43 0.38 o 0 1 9 66.29 66.50 1.38 o 1 1 9 4.22 3.61 0.29 o 2 1 9 23.32 20.59 0.46 o 3 1 9 1.37 1.78 0.33 o 4 1 9 37.00 39.21 0.75 o -7 2 9 0.03 -0.17 0.31 < -6 2 9 349.55 345.72 4.99 o -5 2 9 0.05 -0.29 0.35 < -4 2 9 874.82 820.25 9.13 o -3 2 9 0.14 0.35 0.26 < -2 2 9 74.01 69.17 1.08 o -1 2 9 0.35 0.41 0.23 < 0 2 9 206.72 234.76 2.56 o 1 2 9 0.00 0.00 0.58 < 2 2 9 10.83 11.19 0.41 o 3 2 9 0.05 0.26 0.26 < 4 2 9 122.17 120.32 2.77 o -7 3 9 0.48 1.03 0.26 o -6 3 9 21.20 18.74 0.62 o -5 3 9 1.80 1.61 0.38 o -4 3 9 325.23 313.55 3.61 o -3 3 9 3.37 3.26 0.38 o -2 3 9 658.73 658.22 7.37 o -1 3 9 3.62 3.39 0.37 o 0 3 9 0.15 0.43 0.25 < 1 3 9 2.25 2.19 0.31 o 2 3 9 14.12 14.60 0.56 o 3 3 9 0.81 0.69 0.28 < -6 4 9 1.61 4.65 0.44 o -5 4 9 0.00 0.32 0.29 < -4 4 9 51.51 53.02 1.15 o -3 4 9 0.00 0.31 0.23 < -2 4 9 94.34 93.35 1.23 o -1 4 9 0.04 0.10 0.20 < 0 4 9 15.04 18.56 0.44 o 1 4 9 0.01 0.05 0.38 < 2 4 9 36.74 33.68 1.09 o -3 5 9 2.20 1.18 0.25 o -2 5 9 15.45 16.26 0.40 o -1 5 9 1.81 1.38 0.31 o -8 0 10 69.67 76.40 4.15 o -6 0 10 0.00 2.15 0.83 < -4 0 10 2.74 1.21 0.33 o -2 0 10 408.35 404.38 5.42 o 0 0 10 16.77 15.40 0.54 o 2 0 10 146.52 140.29 2.54 o -8 1 10 16.10 23.47 0.73 o -7 1 10 3.22 3.71 0.50 o -6 1 10 224.54 213.72 2.79 o -5 1 10 4.44 4.14 0.37 o -4 1 10 34.92 37.32 0.94 o -3 1 10 5.49 5.54 0.32 o -2 1 10 0.46 0.87 0.26 o -1 1 10 4.48 4.04 0.30 o 0 1 10 151.87 175.54 2.02 o 1 1 10 1.79 1.61 0.29 o 2 1 10 44.10 42.77 0.81 o 3 1 10 0.57 0.51 0.29 < -7 2 10 0.00 0.17 0.29 < -6 2 10 192.32 192.26 2.93 o -5 2 10 0.11 0.29 0.31 < -4 2 10 648.32 609.37 9.38 o -3 2 10 0.10 0.16 0.29 < -2 2 10 6.52 7.26 0.35 o -1 2 10 0.45 0.23 0.24 < 0 2 10 62.57 69.50 1.06 o 1 2 10 0.01 0.09 0.26 < 2 2 10 25.40 26.73 0.58 o 3 2 10 0.01 0.66 0.30 < -6 3 10 252.91 242.57 3.50 o -5 3 10 2.33 2.36 0.37 o -4 3 10 47.27 48.97 0.76 o -3 3 10 3.08 3.60 0.28 o -2 3 10 89.92 87.77 1.15 o -1 3 10 1.82 2.14 0.33 o 0 3 10 0.50 0.32 0.24 < 1 3 10 1.43 1.36 0.35 o 2 3 10 88.19 81.20 1.38 o -5 4 10 0.15 0.45 0.27 < -4 4 10 31.03 31.23 0.64 o -3 4 10 0.17 0.05 0.23 < -2 4 10 70.47 67.82 1.01 o -1 4 10 0.33 0.83 0.24 o 0 4 10 5.75 7.75 0.33 o 1 4 10 0.52 0.87 0.25 o -6 0 11 17.37 21.35 0.76 o -4 0 11 27.02 20.71 0.68 o -2 0 11 416.76 401.50 6.89 o 0 0 11 9.49 11.75 0.61 o 2 0 11 26.45 29.87 1.05 o -7 1 11 1.37 2.61 0.38 o -6 1 11 41.77 40.46 0.76 o -5 1 11 2.29 2.39 0.35 o -4 1 11 99.58 105.50 1.40 o -3 1 11 2.60 1.90 0.37 o -2 1 11 27.90 26.32 0.54 o -1 1 11 0.80 0.63 0.28 < 0 1 11 115.21 136.09 1.73 o 1 1 11 0.08 0.40 0.27 < 2 1 11 19.03 18.28 0.44 o -7 2 11 0.00 0.85 0.51 < -6 2 11 12.78 14.04 0.46 o -5 2 11 0.00 0.75 0.26 < -4 2 11 36.38 45.88 0.91 o -3 2 11 0.02 0.18 0.28 < -2 2 11 16.03 19.57 0.51 o -1 2 11 0.01 0.26 0.26 < 0 2 11 87.14 88.78 1.18 o 1 2 11 0.01 0.11 0.23 < 2 2 11 4.09 3.73 0.26 o -6 3 11 151.43 140.13 1.95 o -5 3 11 1.89 1.42 0.32 o -4 3 11 9.95 17.00 0.45 o -3 3 11 1.34 1.16 0.23 o -2 3 11 6.35 5.82 0.29 o -1 3 11 0.93 1.17 0.46 < 0 3 11 5.27 5.95 0.41 o 1 3 11 0.29 0.57 0.23 < -4 4 11 0.02 0.25 0.29 < -3 4 11 0.51 0.14 0.20 < -2 4 11 83.05 72.10 1.46 o -1 4 11 0.15 0.11 0.35 < -6 0 12 103.17 100.04 2.17 o -4 0 12 46.87 45.67 1.11 o -2 0 12 273.29 265.27 4.23 o 0 0 12 0.67 0.92 0.50 < 2 0 12 19.81 21.19 0.94 o -7 1 12 0.23 0.94 0.57 < -6 1 12 0.57 1.04 0.29 o -5 1 12 0.01 0.28 0.31 < -4 1 12 148.32 144.43 1.98 o -3 1 12 0.30 0.35 0.26 < -2 1 12 23.33 19.80 0.48 o -1 1 12 1.20 1.32 0.28 o 0 1 12 6.18 6.80 0.43 o 1 1 12 1.17 1.48 0.28 o 2 1 12 36.25 24.89 1.51 o -6 2 12 33.71 32.63 0.66 o -5 2 12 0.00 0.01 0.27 < -3 2 12 0.03 0.51 0.27 < -2 2 12 6.43 10.73 0.43 o -1 2 12 0.08 0.02 0.26 < 0 2 12 261.92 322.08 3.83 o 1 2 12 0.00 0.35 0.39 < -5 3 12 0.17 0.45 0.26 < -4 3 12 1.64 1.85 0.26 o -3 3 12 0.08 0.38 0.21 < -2 3 12 83.48 80.12 1.05 o -1 3 12 0.63 0.84 0.30 < 0 3 12 4.34 4.92 0.45 o -6 0 13 228.11 222.41 6.00 o -4 0 13 0.12 0.84 0.48 < -2 0 13 6.70 6.71 0.64 o 0 0 13 20.72 26.43 0.75 o -6 1 13 1.29 2.78 0.33 o -5 1 13 2.23 2.40 0.36 o -4 1 13 25.69 21.01 0.72 o -3 1 13 3.06 3.12 0.35 o -2 1 13 88.20 99.58 1.71 o -1 1 13 2.01 2.53 0.28 o 0 1 13 2.59 4.63 0.33 o -5 2 13 0.00 0.59 0.29 < -4 2 13 154.81 151.09 2.24 o -3 2 13 0.05 -0.11 0.29 < -2 2 13 10.89 11.03 0.47 o -1 2 13 0.01 0.56 0.26 < 0 2 13 118.76 148.91 2.90 o -3 3 13 1.99 0.91 0.30 < -4 0 14 14.90 15.60 0.54 o -2 0 14 1.24 1.83 0.45 o -5 1 14 1.41 1.00 0.26 o -4 1 14 21.24 23.19 0.80 o -3 1 14 0.99 0.83 0.26 o -2 1 14 35.01 36.62 0.63 o -1 1 14 0.42 0.25 0.23 < -3 2 14 0.03 -0.08 0.30 <