#------------------------------------------------------------------------------ #$Date: 2020-08-29 08:06:38 +0300 (Sat, 29 Aug 2020) $ #$Revision: 255741 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/35/2243558.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243558 _cell_angle_alpha 90 _cell_angle_beta 94.03(2) _cell_angle_gamma 90 _cell_length_a 3.9070(17) _cell_length_b 5.7872(17) _cell_length_c 11.317(5) _exptl_crystal_F_000 116 _reflns_d_resolution_high ? _cod_data_source_file wm5573IIsup3.hkl _cod_data_source_block II _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 55.73 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 172.48 175.96 2.17 o 2 0 0 1799.88 1795.50 19.23 o 3 0 0 0.72 1.03 0.74 < 4 0 0 189.16 199.15 3.77 o 1 1 0 2801.94 3106.39 32.60 o 2 1 0 12.52 15.33 0.67 o 3 1 0 334.28 334.77 3.43 o 4 1 0 0.12 1.00 0.81 < 5 1 0 54.31 60.70 2.47 o 0 2 0 314.90 298.19 3.25 o 1 2 0 0.16 0.22 0.55 < 2 2 0 208.88 219.67 2.16 o 3 2 0 7.10 10.24 0.80 o 4 2 0 50.53 52.28 1.63 o 5 2 0 0.65 7.88 2.10 o 1 3 0 190.38 195.45 2.39 o 2 3 0 11.31 13.21 0.85 o 3 3 0 66.03 79.66 1.78 o 5 3 0 19.68 25.96 2.58 o 0 4 0 695.57 727.09 8.63 o 1 4 0 8.85 10.92 0.89 o 2 4 0 270.62 278.87 3.55 o 3 4 0 2.18 2.95 1.14 < 1 5 0 579.76 601.06 7.12 o 2 5 0 1.28 2.84 0.97 < 3 5 0 169.74 171.65 3.94 o 4 5 0 0.12 3.60 1.74 < 0 6 0 285.11 292.98 7.91 o 1 6 0 0.01 2.57 2.58 < 2 6 0 177.24 176.11 3.72 o 3 6 0 0.03 3.09 4.27 < 1 7 0 61.41 60.25 2.94 o 0 8 0 27.56 30.57 6.44 o 1 8 0 0.39 5.19 5.69 < -4 0 1 124.35 122.92 2.79 o -3 0 1 8.79 8.96 1.02 o -2 0 1 589.73 623.17 8.33 o -1 0 1 138.53 162.63 2.25 o 1 0 1 909.15 981.44 9.62 o 2 0 1 1121.78 1185.01 11.88 o 3 0 1 4.76 3.89 0.91 o 4 0 1 149.57 153.67 3.84 o -5 1 1 29.64 37.00 1.94 o -4 1 1 15.96 19.13 1.14 o -3 1 1 145.82 146.02 1.90 o -2 1 1 25.71 23.88 0.86 o -1 1 1 541.94 607.26 4.41 o 0 1 1 104.09 107.85 1.04 o 1 1 1 1219.34 1275.99 10.35 o 2 1 1 0.04 0.01 0.54 < 3 1 1 286.05 288.51 2.97 o 4 1 1 5.68 8.23 1.02 o 5 1 1 47.27 46.41 2.83 o -5 2 1 12.19 15.36 1.89 o -4 2 1 15.01 36.42 4.16 o -3 2 1 72.65 72.55 1.42 o -2 2 1 40.84 35.31 0.91 o -1 2 1 211.26 235.32 2.39 o 0 2 1 317.46 322.64 2.47 o 1 2 1 353.43 388.19 3.59 o 2 2 1 193.17 191.62 1.98 o 3 2 1 68.36 64.12 1.39 o 4 2 1 76.36 77.52 2.10 o 5 2 1 12.69 13.99 2.34 o -5 3 1 6.85 8.93 2.38 o -4 3 1 32.26 35.52 1.60 o -3 3 1 12.60 16.01 1.12 o -2 3 1 128.18 129.81 2.07 o -1 3 1 39.82 35.18 1.18 o 0 3 1 235.06 239.06 2.17 o 1 3 1 151.97 151.91 2.08 o 2 3 1 126.38 130.27 1.97 o 3 3 1 107.36 106.68 1.78 o 4 3 1 31.65 35.08 1.80 o 5 3 1 29.16 33.57 3.77 o -3 4 1 25.38 25.83 1.49 o -2 4 1 80.49 82.24 2.12 o -1 4 1 18.59 18.71 1.17 o 0 4 1 189.51 190.13 2.22 o 1 4 1 0.67 0.09 0.80 < 2 4 1 235.24 239.21 3.24 o 3 4 1 9.49 10.36 1.20 o -4 5 1 3.10 5.42 7.61 < -3 5 1 87.30 90.13 3.12 o -2 5 1 1.70 1.67 0.94 < -1 5 1 193.98 199.60 3.44 o 0 5 1 9.66 12.30 1.22 o 1 5 1 267.75 288.75 4.45 o 2 5 1 3.87 4.49 1.21 o 3 5 1 124.51 125.90 3.10 o 4 5 1 0.12 0.46 2.22 < -3 6 1 4.85 7.82 1.74 o -2 6 1 74.18 73.51 2.50 o -1 6 1 1.22 1.67 1.65 < 0 6 1 138.96 152.47 3.99 o 1 6 1 0.21 -0.09 1.57 < 2 6 1 106.06 108.12 3.17 o 3 6 1 0.58 -2.58 9.40 < -2 7 1 17.13 13.63 2.80 o -1 7 1 26.63 28.41 2.82 o 0 7 1 21.16 22.34 2.37 o 1 7 1 41.69 39.22 2.63 o 2 7 1 14.34 14.86 13.64 < -1 8 1 20.86 21.69 5.32 o 0 8 1 13.39 8.74 3.69 < 1 8 1 18.92 11.46 2.80 o -5 0 2 8.74 13.82 2.68 o -4 0 2 4.94 8.75 1.32 o -3 0 2 12.39 12.94 1.05 o -2 0 2 61.17 52.29 1.59 o -1 0 2 151.45 138.68 2.11 o 0 0 2 43.67 44.67 0.80 o 1 0 2 13.87 11.54 0.54 o 2 0 2 11.73 17.12 0.94 o 3 0 2 0.20 0.78 0.81 < 4 0 2 5.35 8.73 1.65 o -5 1 2 0.40 7.82 7.86 < -4 1 2 39.06 41.28 1.42 o -3 1 2 14.72 15.54 1.00 o -2 1 2 199.56 203.49 2.61 o -1 1 2 24.74 21.69 0.59 o 0 1 2 499.69 508.09 4.45 o 1 1 2 5.25 7.08 0.42 o 2 1 2 48.74 44.49 0.90 o 3 1 2 8.57 8.92 0.78 o 4 1 2 9.87 12.06 1.21 o 5 1 2 6.94 17.37 10.08 < -5 2 2 41.11 43.73 2.34 o -3 2 2 310.63 309.14 3.55 o -2 2 2 8.03 7.80 0.58 o -1 2 2 1255.36 1325.88 9.54 o 0 2 2 12.95 14.25 0.60 o 1 2 2 748.15 746.31 5.86 o 2 2 2 55.31 53.97 1.02 o 3 2 2 128.60 128.17 2.14 o 4 2 2 20.63 24.34 1.82 o 5 2 2 15.54 19.49 3.00 o -5 3 2 0.01 3.05 2.47 < -4 3 2 98.02 101.21 2.30 o -3 3 2 7.57 6.72 0.96 o -2 3 2 580.96 592.98 5.51 o -1 3 2 12.75 12.47 0.81 o 0 3 2 1011.85 1099.76 8.50 o 1 3 2 27.79 30.11 0.99 o 2 3 2 287.59 287.45 2.92 o 3 3 2 27.54 30.91 1.26 o 4 3 2 40.49 117.58 11.41 o 5 3 2 11.02 12.50 3.08 o -3 4 2 61.89 63.65 2.05 o -2 4 2 18.75 18.42 1.20 o -1 4 2 214.98 221.13 2.82 o 0 4 2 4.54 4.80 0.79 o 1 4 2 131.21 136.92 2.42 o 2 4 2 1.77 4.16 1.05 o 3 4 2 19.58 21.22 1.29 o -4 5 2 8.22 9.86 2.57 o -3 5 2 5.79 6.97 1.46 o -2 5 2 18.71 20.02 1.46 o -1 5 2 6.39 7.54 1.21 o 0 5 2 20.72 22.26 1.41 o 1 5 2 0.05 0.89 1.19 < 2 5 2 3.17 2.62 1.27 < 3 5 2 1.39 7.31 1.80 o -3 6 2 21.00 20.54 2.21 o -2 6 2 4.05 5.40 1.38 o -1 6 2 33.68 37.23 1.60 o 0 6 2 2.26 2.95 2.12 < 1 6 2 19.66 20.04 2.08 o 2 6 2 2.16 2.67 3.59 < -2 7 2 71.49 59.22 2.69 o -1 7 2 3.61 2.03 1.65 < 0 7 2 83.85 78.63 2.94 o 1 7 2 5.84 6.31 2.10 o 2 7 2 40.77 35.38 3.05 o 0 8 2 3.87 0.58 3.51 < -5 0 3 33.09 31.54 2.29 o -4 0 3 57.81 53.92 2.16 o -3 0 3 74.04 75.86 2.81 o -2 0 3 381.16 391.80 5.60 o -1 0 3 46.12 35.36 1.17 o 0 0 3 281.86 316.52 3.60 o 1 0 3 598.04 539.18 5.80 o 2 0 3 291.16 299.63 4.66 o 3 0 3 147.72 148.86 3.01 o 4 0 3 55.46 58.74 3.05 o -5 1 3 13.47 11.97 1.37 o -4 1 3 75.68 74.53 2.15 o -3 1 3 56.03 55.61 1.34 o -2 1 3 231.54 233.92 2.39 o -1 1 3 119.27 117.46 1.86 o 0 1 3 780.82 780.15 6.04 o 1 1 3 149.95 139.16 1.53 o 2 1 3 373.27 366.96 3.42 o 3 1 3 56.31 56.82 1.56 o 4 1 3 57.29 62.11 2.17 o -5 2 3 64.99 63.68 2.26 o -4 2 3 5.46 5.55 1.04 o -3 2 3 226.27 223.33 2.88 o -2 2 3 13.45 14.65 0.66 o -1 2 3 1151.30 1190.73 8.92 o 0 2 3 21.34 28.86 0.92 o 1 2 3 931.25 963.11 8.31 o 2 2 3 0.03 -0.03 0.50 < 3 2 3 161.24 155.67 2.31 o 4 2 3 1.06 1.44 1.11 < 5 2 3 20.81 23.02 3.99 o -5 3 3 3.06 5.36 1.63 o -4 3 3 113.68 112.30 2.68 o -3 3 3 0.38 2.02 1.04 < -2 3 3 382.95 391.58 3.85 o -1 3 3 41.11 43.86 1.12 o 0 3 3 883.82 941.61 8.27 o 1 3 3 19.12 17.95 0.76 o 2 3 3 338.63 324.39 3.32 o 3 3 3 0.00 3.44 0.94 o 4 3 3 53.66 59.28 2.25 o -4 4 3 14.12 15.66 1.55 o -3 4 3 90.95 90.70 2.22 o -2 4 3 28.75 29.31 1.29 o -1 4 3 177.98 188.69 3.16 o 0 4 3 10.02 10.19 0.94 o 1 4 3 278.30 283.13 3.45 o 2 4 3 19.01 22.55 1.51 o 3 4 3 94.51 88.15 2.53 o 4 4 3 9.26 134.65 14.10 o -4 5 3 25.02 26.42 2.61 o -3 5 3 39.87 45.21 2.64 o -2 5 3 45.39 44.94 1.99 o -1 5 3 74.81 76.58 1.77 o 0 5 3 91.32 93.87 2.27 o 1 5 3 67.19 65.52 2.75 o 2 5 3 94.81 90.34 3.02 o 3 5 3 38.03 42.23 2.40 o 4 5 3 23.63 64.13 4.03 o -3 6 3 32.10 39.02 2.52 o -2 6 3 18.39 19.74 1.69 o -1 6 3 74.92 75.67 2.20 o 0 6 3 30.19 31.45 2.22 o 1 6 3 84.19 83.92 2.89 o 2 6 3 23.56 20.56 2.12 o 3 6 3 37.43 44.24 3.31 o -1 7 3 0.01 0.39 1.32 < 0 7 3 99.42 98.08 2.87 o 1 7 3 0.22 0.52 2.09 < 2 7 3 58.06 48.67 4.75 o 0 8 3 1.24 -0.71 4.24 < -5 0 4 31.77 28.19 2.25 o -4 0 4 94.41 89.11 2.77 o -3 0 4 185.49 179.31 3.86 o -2 0 4 735.78 728.66 10.08 o -1 0 4 871.23 856.94 9.86 o 0 0 4 2384.77 2418.21 30.10 o 1 0 4 459.69 470.63 5.79 o 2 0 4 334.22 328.75 4.47 o 3 0 4 209.65 201.61 3.60 o 4 0 4 53.23 58.21 3.13 o 5 0 4 44.68 38.43 4.54 o -5 1 4 16.89 17.92 1.57 o -4 1 4 78.41 76.21 2.15 o -3 1 4 150.98 145.27 2.47 o -2 1 4 289.38 284.18 3.00 o -1 1 4 710.56 712.56 6.11 o 0 1 4 425.77 414.68 3.45 o 1 1 4 330.76 334.26 3.03 o 2 1 4 271.78 254.76 2.69 o 3 1 4 64.62 60.82 1.67 o 4 1 4 80.02 78.06 2.34 o -5 2 4 31.44 29.51 1.97 o -4 2 4 10.50 10.97 1.23 o -3 2 4 109.59 108.21 1.86 o -2 2 4 45.15 41.83 1.07 o -1 2 4 91.44 86.06 1.89 o 0 2 4 0.36 2.63 0.66 o 1 2 4 182.13 178.06 2.42 o 2 2 4 6.34 5.36 0.78 o 3 2 4 76.96 76.70 1.99 o 4 2 4 10.96 9.43 1.51 o -5 3 4 1.72 3.97 1.89 < -4 3 4 58.66 57.77 1.98 o -3 3 4 13.96 14.65 0.99 o -2 3 4 106.00 104.02 1.85 o -1 3 4 11.45 12.13 0.84 o 0 3 4 82.54 79.53 1.47 o 1 3 4 0.11 0.10 0.65 < 2 3 4 78.15 83.96 1.77 o 3 3 4 5.58 7.19 1.17 o 4 3 4 32.80 34.81 2.57 o -4 4 4 21.94 26.84 1.83 o -3 4 4 87.92 79.90 2.71 o -2 4 4 100.83 95.12 2.41 o -1 4 4 161.88 161.32 2.53 o 0 4 4 152.96 144.38 2.04 o 1 4 4 102.81 107.71 1.90 o 2 4 4 39.20 40.73 1.75 o 3 4 4 71.83 73.59 2.38 o -4 5 4 33.02 36.44 2.74 o -3 5 4 86.48 81.16 2.63 o -2 5 4 102.31 98.81 2.66 o -1 5 4 221.05 216.68 3.36 o 0 5 4 137.38 133.60 2.50 o 1 5 4 153.71 149.02 2.86 o 2 5 4 100.17 100.79 2.98 o 3 5 4 43.58 45.32 2.50 o 4 5 4 42.25 41.63 6.13 o -3 6 4 38.12 34.01 3.17 o -2 6 4 77.46 200.42 14.03 o -1 6 4 60.92 59.62 2.02 o 0 6 4 80.16 73.38 2.33 o 1 6 4 75.41 71.66 2.85 o 2 6 4 41.73 39.88 2.58 o 3 6 4 44.46 41.48 3.19 o 0 7 4 27.78 26.85 1.68 o 1 7 4 7.34 4.74 2.30 < 2 7 4 24.44 20.69 2.96 o -4 0 5 65.53 63.51 3.43 o -3 0 5 62.00 57.20 2.11 o -2 0 5 270.16 251.70 4.23 o -1 0 5 630.08 695.58 8.52 o 0 0 5 593.87 615.62 6.89 o 1 0 5 566.25 546.17 6.16 o 2 0 5 240.33 234.06 3.60 o 3 0 5 63.50 59.92 2.12 o 4 0 5 24.88 26.51 2.89 o -5 1 5 19.10 17.82 1.65 o -4 1 5 3.46 2.58 1.03 < -3 1 5 81.45 80.91 2.24 o -2 1 5 87.04 85.04 1.81 o -1 1 5 339.55 353.34 3.83 o 0 1 5 256.01 252.00 2.69 o 1 1 5 375.67 361.68 3.86 o 2 1 5 49.81 48.80 1.27 o 3 1 5 64.43 63.35 1.53 o 4 1 5 13.88 15.00 1.58 o -4 2 5 9.45 10.87 1.40 o -3 2 5 0.01 2.81 1.26 < -2 2 5 63.68 62.74 1.56 o -1 2 5 0.21 -0.11 0.94 < 0 2 5 298.40 304.97 3.74 o 1 2 5 26.20 28.31 0.97 o 2 2 5 85.79 80.20 1.78 o 3 2 5 0.02 -0.24 0.94 < 4 2 5 19.99 18.17 2.06 o -4 3 5 2.37 4.25 1.32 o -3 3 5 13.09 14.05 1.40 o -2 3 5 0.19 0.24 1.10 < -1 3 5 97.34 90.45 1.93 o 0 3 5 7.91 9.33 0.72 o 1 3 5 135.67 127.74 2.13 o 2 3 5 6.19 6.91 0.98 o 3 3 5 37.12 37.41 1.98 o 4 3 5 0.35 12.59 5.47 < -4 4 5 20.96 24.78 2.08 o -2 4 5 59.45 57.62 1.68 o -1 4 5 33.31 32.77 1.37 o 0 4 5 128.51 121.37 2.09 o 1 4 5 32.51 32.65 1.31 o 2 4 5 87.41 86.14 2.27 o 3 4 5 7.04 5.90 1.51 o -4 5 5 5.62 5.35 1.94 < -3 5 5 51.35 50.89 2.14 o -2 5 5 46.19 43.55 2.07 o -1 5 5 114.91 115.76 2.73 o 0 5 5 95.27 91.18 2.18 o 1 5 5 111.29 102.54 2.71 o 2 5 5 43.25 50.81 3.40 o 3 5 5 31.14 31.86 2.26 o -3 6 5 8.24 4.30 2.19 < -2 6 5 54.03 165.98 15.21 o -1 6 5 29.42 28.80 1.62 o 0 6 5 86.37 86.71 3.16 o 1 6 5 21.99 19.77 1.87 o 2 6 5 40.04 35.46 2.83 o 3 6 5 10.71 7.50 3.07 < 0 7 5 0.20 1.36 3.24 < 1 7 5 31.79 27.20 2.88 o 2 7 5 0.15 0.95 2.85 < -4 0 6 41.81 35.24 2.35 o -3 0 6 3.73 5.88 1.71 o -2 0 6 72.59 71.85 2.11 o -1 0 6 2.04 6.01 1.36 o 0 0 6 7.79 7.83 0.99 o 1 0 6 12.89 10.64 1.14 o 2 0 6 21.39 21.43 1.23 o 3 0 6 0.65 1.77 1.14 < 4 0 6 12.14 17.91 2.35 o -5 1 6 28.56 26.43 2.06 o -4 1 6 24.96 24.31 1.36 o -3 1 6 67.90 63.68 1.62 o -2 1 6 48.73 49.53 1.44 o -1 1 6 78.27 72.81 1.85 o 0 1 6 12.03 12.28 0.89 o 1 1 6 90.91 86.54 1.57 o 2 1 6 2.14 2.17 0.69 o 3 1 6 43.29 44.16 1.38 o 4 1 6 2.53 11.77 2.32 o -5 2 6 27.58 31.71 2.12 o -4 2 6 61.07 57.91 1.96 o -3 2 6 159.49 151.34 2.17 o -2 2 6 98.29 93.98 1.91 o -1 2 6 219.85 207.11 2.86 o 0 2 6 221.10 217.13 2.48 o 1 2 6 80.72 76.36 1.58 o 2 2 6 182.73 177.20 2.57 o 3 2 6 26.62 28.95 1.42 o 4 2 6 33.94 37.34 3.02 o -4 3 6 63.04 59.04 2.68 o -3 3 6 78.93 76.43 2.21 o -2 3 6 206.13 204.47 3.33 o -1 3 6 123.37 120.61 2.31 o 0 3 6 147.29 150.71 2.14 o 1 3 6 180.40 178.42 2.67 o 2 3 6 44.56 45.58 1.49 o 3 3 6 74.28 71.81 2.22 o 4 3 6 9.92 21.74 3.53 o -4 4 6 29.98 27.62 2.39 o -3 4 6 29.02 31.13 1.57 o -2 4 6 60.89 58.95 1.79 o -1 4 6 41.78 45.10 1.70 o 0 4 6 53.93 56.08 1.58 o 1 4 6 10.93 12.43 0.98 o 2 4 6 41.13 45.68 1.53 o 3 4 6 3.05 5.11 1.71 < 4 4 6 14.14 27.30 5.14 o -3 5 6 24.75 24.26 1.87 o -1 5 6 24.47 28.78 1.52 o 0 5 6 0.01 -0.39 0.88 < 1 5 6 15.35 18.57 1.20 o 2 5 6 0.24 -0.72 1.67 < 3 5 6 10.60 9.74 2.52 o -3 6 6 7.60 12.09 3.29 o -2 6 6 20.83 193.71 17.44 o 0 6 6 23.88 21.95 1.51 o 1 6 6 0.28 -1.59 1.60 < 2 6 6 18.87 16.28 3.27 o 0 7 6 15.49 15.67 1.93 o 1 7 6 34.25 28.33 3.09 o -4 0 7 10.02 9.20 2.17 o -3 0 7 67.02 69.64 2.53 o -2 0 7 5.32 5.75 1.40 o -1 0 7 169.31 172.56 4.21 o 0 0 7 8.07 8.71 0.95 o 1 0 7 251.29 235.67 3.75 o 2 0 7 0.03 0.27 0.91 < 3 0 7 63.89 62.99 2.31 o 4 0 7 1.33 6.97 2.89 < -4 1 7 34.81 34.60 1.63 o -3 1 7 49.67 45.26 1.30 o -2 1 7 163.86 161.06 3.23 o -1 1 7 79.08 76.92 1.74 o 0 1 7 333.75 331.26 3.44 o 1 1 7 19.12 19.88 0.92 o 2 1 7 113.76 112.95 2.16 o 3 1 7 8.86 10.60 1.00 o 4 1 7 24.88 24.93 2.22 o -4 2 7 59.23 53.14 2.27 o -3 2 7 98.40 96.48 1.98 o -2 2 7 284.61 275.89 3.53 o -1 2 7 413.88 419.59 4.43 o 0 2 7 206.89 200.35 2.54 o 1 2 7 200.85 200.45 2.65 o 2 2 7 75.80 73.91 2.12 o 3 2 7 39.95 40.98 1.88 o 4 2 7 21.56 25.66 2.24 o -4 3 7 45.13 44.78 2.49 o -3 3 7 120.05 116.35 2.23 o -2 3 7 173.98 174.08 2.78 o -1 3 7 269.64 273.55 4.04 o 0 3 7 280.36 278.49 3.04 o 1 3 7 129.72 129.86 2.60 o 2 3 7 81.51 79.53 1.98 o 3 3 7 40.68 38.73 1.66 o 4 3 7 17.31 17.99 2.30 o -4 4 7 17.36 55.72 7.39 o -3 4 7 54.19 51.04 2.16 o -2 4 7 43.26 45.50 2.17 o -1 4 7 117.24 116.83 2.51 o 0 4 7 50.99 52.20 1.54 o 1 4 7 120.10 117.36 2.33 o 2 4 7 15.49 15.29 1.49 o 3 4 7 34.56 34.03 2.27 o -3 5 7 6.52 8.58 1.52 o -2 5 7 49.70 51.03 2.29 o -1 5 7 3.47 5.40 1.65 o 0 5 7 75.65 74.53 1.80 o 1 5 7 1.25 2.27 1.17 < 2 5 7 47.98 47.71 2.14 o 3 5 7 0.90 0.91 1.70 < -3 6 7 20.53 21.38 4.23 o -1 6 7 58.05 54.95 2.18 o 0 6 7 5.36 6.28 1.40 o 1 6 7 44.57 45.86 2.21 o 2 6 7 2.86 1.95 1.47 < -1 7 7 35.99 41.70 3.37 o 0 7 7 45.44 47.07 2.70 o 1 7 7 20.50 24.96 2.89 o -4 0 8 5.17 3.63 1.94 < -3 0 8 88.00 84.39 2.66 o -2 0 8 8.01 7.77 2.04 o -1 0 8 305.28 295.42 5.72 o 0 0 8 9.42 6.95 1.04 o 1 0 8 283.16 285.34 4.60 o 2 0 8 0.45 0.50 1.04 < 3 0 8 115.12 110.98 3.64 o 4 0 8 0.44 -1.66 2.40 < -4 1 8 36.06 32.87 1.68 o -3 1 8 0.37 0.13 0.85 < -2 1 8 94.62 96.50 2.29 o -1 1 8 4.44 4.68 1.05 o 0 1 8 208.54 210.61 2.90 o 1 1 8 11.68 12.23 0.95 o 2 1 8 150.98 147.02 2.48 o 3 1 8 2.69 3.32 0.95 o 4 1 8 37.96 38.23 2.55 o -4 2 8 2.67 3.10 1.44 < -3 2 8 23.76 26.29 1.47 o -2 2 8 30.70 31.35 1.51 o -1 2 8 22.14 23.54 1.44 o 0 2 8 147.55 143.33 2.20 o 1 2 8 99.57 98.08 2.25 o 2 2 8 27.75 28.42 1.33 o 3 2 8 39.77 37.13 1.73 o 4 2 8 3.74 5.72 2.67 < -4 3 8 19.86 23.01 2.30 o -3 3 8 11.01 11.01 1.34 o -2 3 8 21.37 22.34 1.53 o -1 3 8 72.47 68.43 1.91 o 0 3 8 40.10 39.52 1.33 o 1 3 8 69.80 68.01 2.21 o 2 3 8 50.09 49.28 1.77 o 3 3 8 10.37 8.62 1.83 o 4 3 8 14.64 13.83 2.33 o -4 4 8 0.05 3.09 1.90 < -3 4 8 38.07 37.58 2.07 o -2 4 8 2.45 13.71 8.42 < -1 4 8 82.78 83.79 2.53 o 0 4 8 7.06 6.56 0.99 o 1 4 8 79.26 77.45 2.13 o 2 4 8 7.71 6.34 1.12 o 3 4 8 42.43 38.90 2.68 o -3 5 8 2.27 1.34 1.52 < -2 5 8 62.56 59.51 2.46 o -1 5 8 0.50 4.08 1.63 < 0 5 8 109.21 106.22 2.35 o 1 5 8 0.04 0.14 1.13 < 2 5 8 75.50 68.71 2.20 o 3 5 8 0.28 -3.33 2.08 < -1 6 8 42.77 39.33 1.99 o 0 6 8 1.39 2.78 1.37 < 1 6 8 60.07 60.73 3.20 o 2 6 8 0.61 -0.19 1.96 < 0 7 8 17.02 17.87 1.99 o -4 0 9 23.47 19.44 2.79 o -3 0 9 89.20 85.59 3.70 o -2 0 9 52.80 48.06 3.09 o -1 0 9 190.24 199.72 5.32 o 0 0 9 26.39 25.30 1.92 o 1 0 9 150.11 151.31 4.07 o 2 0 9 3.36 4.16 1.21 o 3 0 9 39.76 41.33 2.64 o -4 1 9 30.13 30.26 2.16 o -3 1 9 33.49 30.64 1.62 o -2 1 9 77.76 74.28 2.70 o -1 1 9 58.54 54.70 1.84 o 0 1 9 65.91 67.97 1.96 o 1 1 9 11.56 12.22 1.10 o 2 1 9 36.13 35.90 1.43 o 3 1 9 0.39 1.10 1.14 < -4 2 9 6.66 11.09 10.84 < -3 2 9 15.88 17.45 1.40 o -2 2 9 44.16 45.40 2.34 o -1 2 9 4.32 3.68 1.36 < 0 2 9 49.32 47.05 1.50 o 1 2 9 0.22 1.37 0.98 < 2 2 9 2.17 3.31 1.08 o 3 2 9 5.24 4.02 1.59 < 4 2 9 0.49 1.27 1.69 < -3 3 9 12.07 11.21 1.76 o -2 3 9 7.44 8.09 1.51 o -1 3 9 38.53 36.46 1.66 o 0 3 9 0.06 -0.41 1.05 < 1 3 9 12.88 13.45 1.31 o 2 3 9 0.93 1.19 1.22 < 3 3 9 1.10 2.62 1.55 < -3 4 9 21.65 39.93 2.87 o -2 4 9 19.24 19.89 1.30 o -1 4 9 30.30 30.77 2.05 o 0 4 9 12.94 13.12 1.50 o 1 4 9 23.98 25.44 1.54 o 2 4 9 2.89 3.19 1.38 < 3 4 9 10.59 12.21 1.93 o -3 5 9 16.54 19.70 2.81 o -1 5 9 17.43 18.07 1.61 o 0 5 9 55.31 51.76 2.21 o 1 5 9 4.48 3.46 1.47 < 2 5 9 30.45 23.97 2.15 o -1 6 9 28.09 68.83 5.50 o 0 6 9 10.83 12.82 1.59 o 1 6 9 18.91 19.43 1.93 o -4 0 10 18.10 14.14 2.88 o -3 0 10 34.65 22.93 3.26 o -2 0 10 43.64 42.27 3.53 o -1 0 10 57.69 53.61 3.11 o 0 0 10 45.18 44.51 2.23 o 1 0 10 24.70 26.88 2.14 o 2 0 10 21.28 21.18 1.68 o 3 0 10 3.78 25.62 3.70 o 4 0 10 5.34 2.21 4.37 < -4 1 10 3.70 4.36 5.19 < -3 1 10 35.67 34.97 1.97 o -2 1 10 26.91 24.23 1.93 o -1 1 10 75.70 71.30 2.26 o 0 1 10 31.81 32.26 1.53 o 1 1 10 78.69 80.76 2.00 o 2 1 10 4.45 4.83 1.14 o 3 1 10 22.06 19.67 1.95 o -4 2 10 41.54 45.96 3.35 o -3 2 10 0.09 -1.01 1.18 < -2 2 10 74.77 72.28 2.45 o -1 2 10 9.10 8.73 1.58 o 0 2 10 171.23 168.67 3.56 o 1 2 10 2.94 3.88 1.18 o 2 2 10 96.83 91.64 2.42 o 3 2 10 0.02 -0.99 1.62 < -4 3 10 0.17 4.84 1.52 o -3 3 10 56.24 56.52 2.34 o -2 3 10 0.09 1.89 1.43 < -1 3 10 109.58 108.69 3.01 o 0 3 10 3.01 4.09 1.38 < 1 3 10 125.49 122.28 3.36 o 2 3 10 0.07 0.82 1.42 < 3 3 10 36.75 43.07 2.86 o -3 4 10 4.91 12.03 2.97 o -2 4 10 44.84 47.06 1.67 o -1 4 10 8.45 10.80 1.50 o 0 4 10 54.93 53.58 1.86 o 1 4 10 4.63 7.82 4.45 < 2 4 10 29.51 24.49 2.08 o 3 4 10 0.73 4.23 2.04 < -2 5 10 20.53 64.55 8.40 o -1 5 10 23.13 24.09 1.78 o 0 5 10 16.72 18.21 1.80 o 1 5 10 17.32 18.89 1.91 o 2 5 10 4.56 0.60 2.02 < 0 6 10 23.04 21.69 2.13 o 1 6 10 6.40 5.19 1.90 < -3 0 11 2.05 1.87 1.78 < -2 0 11 11.04 15.37 3.21 o -1 0 11 0.00 -1.19 2.06 < 1 0 11 0.04 8.93 6.39 < 2 0 11 24.52 19.39 3.90 o -3 1 11 41.02 45.47 2.74 o -2 1 11 2.51 1.47 1.91 < -1 1 11 40.56 41.95 2.04 o 0 1 11 0.00 -0.82 1.53 < 1 1 11 42.36 45.37 1.97 o 2 1 11 0.28 -1.13 1.42 < 3 1 11 26.81 23.55 2.28 o -4 2 11 51.72 52.07 3.02 o -3 2 11 0.81 0.82 2.96 < -2 2 11 123.38 128.00 3.20 o -1 2 11 4.20 5.03 1.92 < 0 2 11 85.32 87.43 2.83 o 1 2 11 2.40 6.75 8.13 < 2 2 11 64.58 62.72 2.56 o -3 3 11 76.52 85.06 2.98 o -2 3 11 1.54 1.63 0.95 < -1 3 11 109.44 120.84 3.09 o 0 3 11 0.02 3.41 1.80 < 1 3 11 77.16 77.81 2.47 o 2 3 11 1.58 5.22 1.94 < 3 3 11 37.81 14.64 3.90 o -3 4 11 1.05 2.26 1.59 < -2 4 11 30.77 35.80 2.12 o -1 4 11 0.05 1.35 1.27 < 0 4 11 41.91 40.10 2.18 o 0 5 11 0.03 2.16 1.57 < 1 5 11 12.05 12.11 2.18 o -3 0 12 14.57 17.97 2.51 o -2 0 12 15.73 19.89 4.15 o -1 0 12 58.61 62.78 5.38 o 0 0 12 6.56 13.65 2.34 o 1 0 12 27.23 26.44 3.53 o 2 0 12 7.41 27.77 4.16 o -3 1 12 12.48 14.30 2.00 o -2 1 12 13.08 12.15 2.01 o -1 1 12 27.76 35.77 2.16 o 0 1 12 26.63 27.48 1.84 o 1 1 12 13.04 14.35 2.22 o 2 1 12 7.27 5.82 1.85 o 3 1 12 6.48 2.53 2.10 < -3 2 12 0.15 0.43 1.48 < -2 2 12 37.78 43.87 1.95 o -1 2 12 0.43 4.73 1.65 < 0 2 12 52.30 58.81 2.02 o 1 2 12 4.08 31.57 13.74 < 2 2 12 12.39 12.30 2.07 o 3 2 12 0.05 -0.19 1.62 < -3 3 12 20.61 23.40 2.08 o -1 3 12 43.39 45.71 1.92 o 1 3 12 25.10 30.56 2.34 o 2 3 12 0.37 16.11 2.51 o -2 4 12 17.07 82.13 7.36 o -1 4 12 12.87 13.58 1.47 o 0 5 12 19.62 17.40 2.36 o 1 5 12 4.38 -0.07 4.51 < -3 0 13 32.35 40.17 3.24 o -1 0 13 42.05 43.11 2.98 o 0 0 13 7.90 15.16 2.53 o 1 0 13 45.84 44.36 3.70 o -3 1 13 0.88 2.90 1.96 < -2 1 13 23.20 22.05 1.83 o -1 1 13 0.46 5.68 2.02 < 0 1 13 24.08 28.23 2.26 o 1 1 13 2.95 4.91 1.97 < 2 1 13 16.60 41.48 4.49 o -2 2 13 1.49 8.49 4.82 < -1 2 13 4.61 8.93 2.30 o 0 2 13 0.02 0.39 6.25 < 2 2 13 0.39 17.53 6.59 < -2 3 13 4.85 41.94 3.73 o -1 3 13 0.15 -0.58 1.14 < 1 3 13 0.13 75.56 8.47 o -1 0 14 36.47 39.50 3.44 o 0 0 14 0.97 10.12 3.71 < 1 0 14 15.64 15.63 3.77 o 2 0 14 0.01 -5.11 3.72 < -2 1 14 39.76 48.06 2.24 o 0 1 14 24.03 36.27 1.73 o 1 1 14 2.45 8.11 12.45 < 2 1 14 9.83 9.34 2.50 o -1 2 14 27.45 31.32 2.21 o 0 2 14 16.41 27.20 2.69 o 1 2 14 12.90 23.05 3.16 o -1 3 14 13.01 33.04 3.13 o 0 0 15 2.13 5.51 2.39 < 0 1 15 13.95 40.53 2.92 o 1 1 15 4.67 46.97 15.51 o 0 2 15 7.57 170.86 20.19 o