#------------------------------------------------------------------------------ #$Date: 2020-08-29 08:07:21 +0300 (Sat, 29 Aug 2020) $ #$Revision: 255742 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/35/2243561.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243561 _cell_angle_alpha 73.817 _cell_angle_beta 83.550 _cell_angle_gamma 88.865 _cell_length_a 9.6333 _cell_length_b 12.7701 _cell_length_c 17.9560 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.8300 _cod_data_source_file hb7941Isup2.hkl _cod_data_source_block I _shelx_title ' shelxl in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 319.70 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 300.33 250.82 23.74 o 3 0 0 25047.62 24357.75 321.03 o 4 0 0 1046.86 1286.00 36.86 o 5 0 0 29343.52 28933.97 453.63 o 6 0 0 175.81 183.47 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