#------------------------------------------------------------------------------ #$Date: 2020-11-07 01:29:23 +0200 (Sat, 07 Nov 2020) $ #$Revision: 259019 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/36/2243669.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243669 _cell_angle_alpha 90.000 _cell_angle_beta 94.858 _cell_angle_gamma 90.000 _cell_length_a 13.5644 _cell_length_b 20.3405 _cell_length_c 17.4818 _exptl_crystal_F_000 2064.00 _reflns_d_resolution_high 0.8092 _cod_data_source_file zl2798Isup2.hkl _cod_data_source_block I _shelx_title ' shb4cg' _shelx_refln_list_code 4 _shelx_f_calc_maximum 341.93 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 169.12 359.47 27.68 o 4 0 0 63558.96 67021.87 477.14 o 6 0 0 40771.36 40467.83 216.70 o 8 0 0 139.34 158.41 47.42 o 10 0 0 152.82 295.92 63.19 o 12 0 0 477.19 519.91 92.72 o 14 0 0 469.78 510.00 107.53 o 16 0 0 436.25 317.27 102.38 o 2 1 0 8287.79 7633.01 80.35 o 3 1 0 48567.25 49205.64 249.02 o 4 1 0 48812.19 48275.22 285.81 o 5 1 0 17926.35 16897.16 156.79 o 6 1 0 34.08 19.81 14.58 o 7 1 0 5305.67 6110.40 90.06 o 8 1 0 9072.82 8677.85 112.98 o 9 1 0 715.88 737.20 60.34 o 10 1 0 152.34 148.61 34.25 o 11 1 0 1012.97 1056.80 80.70 o 12 1 0 304.03 299.68 54.24 o 13 1 0 1003.25 1040.42 93.18 o 14 1 0 318.47 401.77 68.98 o 15 1 0 685.02 711.20 94.61 o 16 1 0 155.50 128.01 64.81 o 1 2 0 12561.01 13314.42 128.62 o 2 2 0 6061.63 5251.39 108.47 o 3 2 0 16817.04 17660.63 246.20 o 4 2 0 4.73 44.13 15.28 o 5 2 0 1091.86 834.94 44.30 o 6 2 0 5459.80 4993.50 115.36 o 7 2 0 4352.31 4421.96 82.24 o 8 2 0 6028.93 5835.83 98.84 o 9 2 0 3402.56 3358.40 120.02 o 10 2 0 624.86 687.38 64.30 o 11 2 0 1.88 -16.73 36.69 o 12 2 0 1244.44 1137.21 89.12 o 13 2 0 562.51 591.18 73.69 o 14 2 0 483.42 533.20 74.69 o 15 2 0 6.47 -56.70 56.70 o 16 2 0 100.45 170.98 113.51 o 1 3 0 4067.97 3800.39 100.66 o 2 3 0 542.76 631.13 29.05 o 3 3 0 14722.45 13110.76 354.45 o 4 3 0 1907.45 1585.06 53.64 o 5 3 0 863.20 846.08 44.62 o 6 3 0 5808.15 5783.63 123.64 o 7 3 0 2221.86 1894.62 134.10 o 8 3 0 3952.80 4082.79 87.26 o 9 3 0 85.93 78.15 29.25 o 10 3 0 3761.11 3274.27 126.60 o 11 3 0 490.08 531.23 60.74 o 12 3 0 909.68 953.74 83.38 o 13 3 0 28.38 35.93 42.72 o 14 3 0 200.42 119.03 52.13 o 15 3 0 113.27 91.26 54.23 o 16 3 0 1.15 -66.74 68.95 o 0 4 0 758.40 1167.06 25.84 o 1 4 0 128.07 182.28 12.31 o 2 4 0 13541.59 14511.65 185.26 o 3 4 0 1454.94 1712.55 60.35 o 4 4 0 15378.54 15014.03 140.17 o 5 4 0 4715.23 4461.86 100.24 o 6 4 0 3482.58 3864.44 102.31 o 7 4 0 3720.10 3921.49 111.71 o 8 4 0 10.33 28.88 19.00 o 9 4 0 16.62 26.82 25.23 o 10 4 0 327.42 377.95 49.27 o 11 4 0 1098.18 1101.53 82.03 o 12 4 0 770.98 632.16 70.33 o 13 4 0 55.88 26.00 57.21 o 14 4 0 6.61 -13.39 47.94 o 15 4 0 541.94 410.27 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94.69 o 1 7 0 1805.01 1851.74 55.96 o 2 7 0 14.89 16.12 9.80 o 3 7 0 78.24 130.89 13.92 o 4 7 0 5753.22 5329.85 83.38 o 5 7 0 9848.44 10091.25 100.13 o 6 7 0 57.56 103.88 16.42 o 7 7 0 4394.81 4418.26 78.82 o 8 7 0 4191.24 3792.78 100.93 o 9 7 0 1571.83 1384.54 81.46 o 10 7 0 332.73 248.04 46.04 o 11 7 0 12.11 -22.97 34.65 o 12 7 0 355.62 268.94 49.82 o 13 7 0 745.28 873.47 88.62 o 14 7 0 3.32 67.35 72.29 o 15 7 0 226.06 335.43 106.18 o 16 7 0 113.14 -18.04 93.04 o 0 8 0 13765.32 14097.55 126.67 o 1 8 0 21071.01 21043.39 190.92 o 2 8 0 3517.54 3491.40 72.60 o 3 8 0 8254.18 9011.59 111.45 o 4 8 0 94.48 89.89 24.72 o 5 8 0 491.04 442.21 38.32 o 6 8 0 562.46 539.63 27.76 o 7 8 0 91.30 72.81 23.75 o 8 8 0 1.38 29.94 21.32 o 9 8 0 938.73 994.09 68.38 o 10 8 0 93.31 79.34 26.76 o 11 8 0 211.43 67.92 57.65 o 12 8 0 1659.27 2006.00 181.00 o 13 8 0 820.24 699.42 121.24 o 14 8 0 46.32 -34.42 70.17 o 15 8 0 52.31 126.36 97.15 o 1 9 0 11847.41 11925.61 157.44 o 2 9 0 190.27 259.99 13.79 o 3 9 0 7197.55 6605.74 77.33 o 4 9 0 291.41 398.89 26.11 o 5 9 0 308.30 291.01 29.33 o 6 9 0 200.92 137.21 22.04 o 7 9 0 2248.31 2193.08 73.63 o 8 9 0 1464.76 1588.76 67.99 o 9 9 0 204.42 141.37 61.23 o 10 9 0 2802.26 2648.46 186.80 o 11 9 0 2.54 49.03 55.25 o 12 9 0 1806.73 1613.61 167.37 o 13 9 0 684.25 623.64 122.52 o 14 9 0 156.39 116.92 81.67 o 15 9 0 428.96 444.66 121.37 o 0 10 0 2261.62 2949.77 228.62 o 1 10 0 7034.58 7436.57 81.81 o 2 10 0 4405.66 3423.47 87.69 o 3 10 0 102.76 69.52 11.26 o 4 10 0 1546.22 1578.27 40.31 o 5 10 0 600.59 692.55 75.93 o 6 10 0 128.84 74.21 42.17 o 7 10 0 3612.29 3508.39 127.13 o 8 10 0 54.10 107.83 49.88 o 9 10 0 312.76 335.95 78.56 o 10 10 0 221.93 278.40 81.03 o 11 10 0 2.20 12.15 63.72 o 12 10 0 179.60 178.40 76.92 o 13 10 0 170.92 167.98 79.52 o 14 10 0 405.26 528.31 127.26 o 15 10 0 6.05 -61.05 98.59 o 1 11 0 1505.53 1303.95 37.10 o 2 11 0 5346.94 5469.67 82.04 o 3 11 0 3894.00 3655.02 76.08 o 4 11 0 323.41 289.69 26.85 o 5 11 0 10.98 44.30 43.69 o 6 11 0 2442.19 2355.56 146.66 o 7 11 0 567.64 611.71 85.43 o 8 11 0 1020.10 1253.64 122.24 o 9 11 0 247.42 308.30 74.32 o 10 11 0 1669.19 1783.40 158.13 o 11 11 0 881.78 809.70 121.52 o 12 11 0 659.66 835.73 126.24 o 13 11 0 160.90 265.55 97.24 o 14 11 0 260.11 245.91 97.13 o 15 11 0 37.24 0.29 87.64 o 0 12 0 24558.33 25672.51 272.84 o 1 12 0 4327.70 4284.25 79.92 o 2 12 0 12.32 18.22 12.62 o 3 12 0 60.02 39.90 13.19 o 4 12 0 3988.35 3645.45 127.17 o 5 12 0 7402.57 7855.78 195.63 o 6 12 0 957.44 1064.96 97.05 o 7 12 0 4056.40 4141.31 207.94 o 8 12 0 520.32 604.14 93.01 o 9 12 0 93.70 50.07 51.43 o 10 12 0 21.58 -6.40 57.28 o 11 12 0 558.95 615.20 111.85 o 12 12 0 326.75 144.60 88.18 o 13 12 0 137.81 183.23 93.47 o 14 12 0 148.02 86.29 85.79 o 1 13 0 1348.34 1107.35 44.21 o 2 13 0 1504.57 1489.88 43.88 o 3 13 0 1573.13 1600.25 53.54 o 4 13 0 4996.87 5128.34 274.16 o 5 13 0 2465.48 2418.97 115.09 o 6 13 0 181.55 221.51 45.34 o 7 13 0 2743.33 2718.39 209.11 o 8 13 0 8298.34 8453.73 310.06 o 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328.32 97.82 o -16 1 1 333.43 303.07 71.49 o -15 1 1 279.22 164.57 113.25 o -14 1 1 578.48 592.87 78.12 o -13 1 1 181.68 138.40 88.85 o -12 1 1 1078.87 1184.30 91.80 o -11 1 1 2783.36 2853.27 128.18 o -10 1 1 45.14 101.02 37.06 o -9 1 1 1223.85 1424.89 81.56 o -8 1 1 2400.87 2590.21 78.71 o -7 1 1 3755.05 4225.34 65.41 o -6 1 1 538.84 523.83 33.71 o -5 1 1 3577.73 3346.01 84.07 o -4 1 1 3409.86 3805.36 59.72 o -3 1 1 116914.34 112613.95 1945.45 o -2 1 1 14623.29 14732.56 182.21 o 2 1 1 26693.99 26786.20 507.36 o 3 1 1 984.46 849.36 34.68 o 4 1 1 2652.78 2913.71 71.79 o 5 1 1 493.58 407.44 32.32 o 6 1 1 8081.76 7724.98 141.80 o 7 1 1 3189.70 3632.00 106.45 o 8 1 1 5188.47 4686.68 130.72 o 9 1 1 17.90 17.22 26.05 o 10 1 1 109.90 63.67 31.90 o 11 1 1 1825.71 1928.68 103.51 o 12 1 1 77.95 40.71 40.13 o 13 1 1 5.21 62.31 45.42 o 14 1 1 160.08 215.70 62.49 o 15 1 1 312.58 307.97 65.39 o 16 1 1 56.89 85.06 61.81 o -16 2 1 2.86 -66.36 95.88 o -15 2 1 185.87 157.04 60.99 o -14 2 1 105.30 70.02 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