#------------------------------------------------------------------------------ #$Date: 2020-11-18 07:09:10 +0200 (Wed, 18 Nov 2020) $ #$Revision: 259160 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/36/2243677.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243677 _cell_angle_alpha 90.000 _cell_angle_beta 97.226 _cell_angle_gamma 90.000 _cell_length_a 13.2962 _cell_length_b 6.2300 _cell_length_c 12.9294 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.8233 _cod_data_source_file hb7952IIsup2.hkl _cod_data_source_block II _shelx_title ' wa1324 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.61 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 9507.80 8870.39 135.27 o 4 0 0 183.47 182.24 5.21 o 5 0 0 919.99 864.26 13.96 o 6 0 0 200.78 195.39 5.89 o 7 0 0 346.72 379.53 6.23 o 8 0 0 105.69 109.30 3.55 o 9 0 0 31.92 35.22 4.20 o 10 0 0 186.76 189.94 7.97 o 11 0 0 990.93 973.38 17.29 o 12 0 0 541.67 522.31 7.06 o 13 0 0 939.75 944.39 70.22 o 14 0 0 80.76 90.67 6.23 o 15 0 0 3.97 8.33 3.01 o 16 0 0 0.15 7.94 6.91 o 1 1 0 914.94 909.61 13.03 o 2 1 0 2019.17 1995.88 53.96 o 3 1 0 7589.69 7270.54 310.49 o 4 1 0 3551.67 3439.54 53.82 o 5 1 0 8711.91 8660.83 131.09 o 6 1 0 1552.77 1518.86 30.87 o 7 1 0 351.26 305.19 4.75 o 8 1 0 1554.38 1659.64 31.14 o 9 1 0 597.49 642.72 11.31 o 10 1 0 2707.98 2670.81 55.83 o 11 1 0 94.65 92.83 2.77 o 12 1 0 254.49 249.12 5.63 o 13 1 0 313.41 317.26 10.44 o 14 1 0 18.91 19.78 2.73 o 15 1 0 7.96 10.08 2.25 o 0 2 0 1262.73 1236.30 51.18 o 1 2 0 1256.14 1216.98 25.10 o 2 2 0 3274.54 3250.13 43.89 o 3 2 0 195.05 147.36 6.49 o 4 2 0 1033.71 1033.49 39.87 o 5 2 0 5146.38 5712.29 158.59 o 6 2 0 123.17 121.54 3.61 o 7 2 0 0.77 6.16 2.53 o 8 2 0 4.08 9.65 3.93 o 9 2 0 1.99 3.43 1.92 o 10 2 0 21.00 24.55 2.19 o 11 2 0 0.54 0.78 2.49 o 12 2 0 32.09 31.15 2.62 o 13 2 0 61.28 61.64 4.05 o 14 2 0 29.54 30.50 2.71 o 15 2 0 353.58 324.46 8.04 o 1 3 0 125.57 132.11 4.09 o 2 3 0 14.33 15.73 3.19 o 3 3 0 814.38 959.22 15.87 o 4 3 0 24.19 30.16 3.74 o 5 3 0 826.25 960.62 27.43 o 6 3 0 144.02 153.10 19.56 o 7 3 0 163.19 170.83 15.92 o 8 3 0 454.07 486.15 23.67 o 9 3 0 376.51 392.15 23.07 o 10 3 0 419.71 455.36 25.59 o 11 3 0 502.65 489.36 21.86 o 12 3 0 694.64 678.30 23.79 o 13 3 0 63.63 64.47 4.11 o 14 3 0 89.67 90.89 4.97 o 0 4 0 45.04 36.76 4.62 o 1 4 0 474.43 488.73 16.44 o 2 4 0 787.59 856.91 14.33 o 3 4 0 11.85 6.33 2.99 o 4 4 0 34.30 29.20 2.76 o 5 4 0 715.54 773.21 36.07 o 6 4 0 713.78 723.16 88.29 o 7 4 0 186.43 210.25 17.77 o 8 4 0 303.74 289.82 47.22 o 9 4 0 181.68 188.34 12.38 o 10 4 0 15.88 15.16 3.34 o 11 4 0 0.43 1.47 3.34 o 12 4 0 90.67 99.88 7.52 o 13 4 0 157.91 143.83 6.38 o 1 5 0 4.31 4.31 2.92 o 2 5 0 174.40 171.48 4.66 o 3 5 0 14.60 15.94 2.72 o 4 5 0 150.28 148.89 6.83 o 5 5 0 201.71 211.18 6.39 o 6 5 0 53.12 58.58 6.43 o 7 5 0 562.21 581.28 45.02 o 8 5 0 213.36 196.46 22.43 o 9 5 0 194.33 195.67 13.88 o 10 5 0 880.59 994.74 83.07 o 11 5 0 279.67 291.21 31.50 o 12 5 0 5.43 2.73 3.84 o 0 6 0 2295.85 2295.12 44.56 o 1 6 0 27.86 24.81 2.82 o 2 6 0 67.68 66.90 3.65 o 3 6 0 1035.76 1011.41 13.35 o 4 6 0 472.91 461.21 5.68 o 5 6 0 181.80 172.63 3.90 o 6 6 0 223.33 207.78 16.73 o 7 6 0 18.32 17.64 3.41 o 8 6 0 18.88 20.11 4.97 o 9 6 0 9.89 11.00 2.89 o 1 7 0 111.31 106.87 3.38 o 2 7 0 12.60 12.32 2.78 o 3 7 0 0.15 1.25 2.80 o 4 7 0 68.62 63.38 3.31 o 5 7 0 365.66 333.45 11.24 o 6 7 0 146.69 116.87 5.91 o -15 1 1 25.65 21.21 2.75 o -14 1 1 1.91 2.63 2.73 o -13 1 1 23.15 21.32 2.28 o -12 1 1 490.46 500.02 14.54 o -11 1 1 842.74 825.83 16.99 o -10 1 1 614.25 628.38 16.80 o -9 1 1 54.83 53.32 2.30 o -8 1 1 641.95 667.58 9.53 o -7 1 1 429.03 463.13 9.33 o -6 1 1 32.99 40.88 2.41 o -5 1 1 1547.54 1703.81 44.62 o -4 1 1 1645.92 1692.54 44.24 o -3 1 1 2628.84 2739.63 101.46 o -2 1 1 786.91 807.11 29.03 o -1 1 1 35.73 33.72 3.36 o 0 1 1 1035.18 983.88 17.83 o 1 1 1 755.14 676.72 8.18 o 2 1 1 33.88 38.56 3.22 o 3 1 1 128.99 115.47 3.34 o 4 1 1 0.00 1.21 2.01 o 5 1 1 15.06 13.96 1.92 o 6 1 1 94.41 97.12 3.09 o 7 1 1 1034.45 1072.79 28.45 o 8 1 1 556.66 574.79 15.39 o 9 1 1 167.16 168.84 5.11 o 10 1 1 693.42 693.85 16.89 o 11 1 1 0.14 1.31 1.92 o 12 1 1 570.08 575.43 12.66 o 13 1 1 50.87 50.35 2.22 o 14 1 1 23.24 21.24 2.22 o 15 1 1 22.99 28.74 2.85 o -15 2 1 152.33 136.44 3.79 o -14 2 1 166.31 169.63 7.18 o -13 2 1 21.75 16.74 3.22 o -12 2 1 290.97 261.44 3.94 o -11 2 1 204.36 209.65 6.19 o -10 2 1 415.99 440.38 11.41 o -9 2 1 77.68 88.57 2.57 o -8 2 1 75.06 78.61 2.85 o -7 2 1 105.07 102.98 8.14 o -6 2 1 214.43 218.73 16.86 o -5 2 1 569.28 632.73 57.45 o -4 2 1 187.18 220.92 10.12 o -3 2 1 137.03 145.23 7.41 o -2 2 1 130.89 130.35 4.85 o -1 2 1 1358.31 1415.54 17.76 o 0 2 1 0.28 4.16 3.72 o 1 2 1 199.16 186.49 4.38 o 2 2 1 3715.90 3599.90 106.98 o 3 2 1 9.87 5.92 3.61 o 4 2 1 24.44 16.04 2.29 o 5 2 1 1898.09 2180.99 59.46 o 6 2 1 805.84 846.43 40.62 o 7 2 1 873.13 885.82 29.89 o 8 2 1 0.09 4.65 2.42 o 9 2 1 425.51 442.34 20.80 o 10 2 1 1.42 3.20 2.33 o 11 2 1 122.59 120.67 4.38 o 12 2 1 397.02 403.07 25.58 o 13 2 1 62.19 66.78 5.64 o 14 2 1 4.83 7.96 2.30 o 15 2 1 5.92 5.02 3.17 o -14 3 1 9.11 5.94 2.55 o -13 3 1 4.01 8.81 2.74 o -12 3 1 24.34 28.22 2.73 o -11 3 1 159.16 169.09 6.50 o -10 3 1 0.15 3.65 2.54 o -9 3 1 3.56 4.01 2.73 o -8 3 1 0.36 -2.78 4.64 o -7 3 1 6.44 9.81 3.92 o -6 3 1 24.49 29.48 4.85 o -5 3 1 323.08 414.62 49.73 o -4 3 1 13.86 21.78 3.45 o -3 3 1 40.66 47.01 3.54 o -2 3 1 1210.93 1322.46 30.22 o -1 3 1 1647.81 1732.53 36.51 o 0 3 1 919.49 907.87 9.46 o 1 3 1 1151.16 1185.04 19.82 o 2 3 1 966.33 1046.65 28.47 o 3 3 1 237.73 277.16 9.94 o 4 3 1 0.29 0.59 3.11 o 5 3 1 17.03 18.48 3.72 o 6 3 1 14.58 19.70 2.28 o 7 3 1 103.95 127.72 3.33 o 8 3 1 73.80 74.72 3.05 o 9 3 1 175.41 180.12 5.71 o 10 3 1 535.17 585.47 29.23 o 11 3 1 352.46 358.55 21.98 o 12 3 1 98.18 102.57 5.24 o 13 3 1 61.18 58.67 2.97 o 14 3 1 14.59 13.38 2.90 o -13 4 1 63.69 64.46 5.96 o -12 4 1 0.07 4.77 2.69 o -11 4 1 54.90 54.55 2.79 o -10 4 1 183.35 193.91 10.28 o -9 4 1 0.12 3.89 3.51 o -8 4 1 34.72 43.08 5.04 o -7 4 1 125.66 130.91 16.16 o -6 4 1 5.93 16.27 4.68 o -5 4 1 109.56 119.17 9.68 o -4 4 1 333.90 365.73 10.61 o -3 4 1 235.73 252.11 4.32 o -2 4 1 381.16 397.98 7.59 o -1 4 1 48.68 43.54 3.16 o 0 4 1 56.18 64.37 3.35 o 1 4 1 139.82 146.15 3.71 o 2 4 1 151.57 172.18 3.41 o 3 4 1 845.04 874.12 27.02 o 4 4 1 1389.48 1498.38 63.47 o 5 4 1 217.32 208.46 8.17 o 6 4 1 291.65 300.88 19.78 o 7 4 1 157.17 195.37 6.85 o 8 4 1 1143.23 1140.35 104.84 o 9 4 1 1064.12 1144.56 95.24 o 10 4 1 14.17 27.20 4.07 o 11 4 1 1.23 2.31 2.94 o 12 4 1 11.33 9.75 3.41 o 13 4 1 0.03 -0.05 2.67 o -12 5 1 23.77 24.99 2.61 o -11 5 1 0.21 1.73 2.49 o -10 5 1 539.15 523.07 37.16 o -9 5 1 27.64 34.44 4.49 o -8 5 1 735.26 679.06 83.40 o -7 5 1 124.02 117.21 11.30 o -6 5 1 574.17 551.58 35.73 o -5 5 1 472.70 465.46 26.01 o -4 5 1 359.75 350.65 5.55 o -3 5 1 92.56 85.03 3.26 o -2 5 1 608.66 617.03 9.42 o -1 5 1 132.19 136.87 3.56 o 0 5 1 343.51 351.18 4.72 o 1 5 1 10.19 10.42 2.98 o 2 5 1 76.58 78.75 3.00 o 3 5 1 456.27 468.41 7.80 o 4 5 1 208.18 219.71 4.00 o 5 5 1 141.87 151.27 5.53 o 6 5 1 12.22 10.13 3.29 o 7 5 1 21.60 20.35 3.53 o 8 5 1 95.08 89.33 7.67 o 9 5 1 701.57 744.70 70.74 o 10 5 1 5.94 7.00 2.76 o 11 5 1 38.85 43.28 5.33 o -9 6 1 96.74 94.16 4.89 o -8 6 1 194.65 183.54 25.84 o -7 6 1 224.24 211.18 4.76 o -6 6 1 81.93 70.26 3.78 o -5 6 1 49.07 44.86 3.88 o -4 6 1 155.15 153.12 3.38 o -3 6 1 0.51 1.91 2.32 o -2 6 1 441.08 408.31 10.60 o -1 6 1 1874.25 1815.87 12.42 o 0 6 1 284.61 270.88 4.31 o 1 6 1 38.51 37.68 2.54 o 2 6 1 21.93 22.67 2.41 o 3 6 1 264.97 259.43 5.26 o 4 6 1 487.18 485.96 6.21 o 5 6 1 62.63 63.84 3.38 o 6 6 1 53.82 48.64 3.29 o 7 6 1 1.35 6.14 4.33 o 8 6 1 444.15 422.53 34.51 o 9 6 1 129.02 106.92 8.10 o -6 7 1 554.89 467.96 9.18 o -5 7 1 1034.12 930.64 47.34 o -4 7 1 308.91 280.56 12.84 o -3 7 1 57.17 57.79 2.94 o -2 7 1 407.88 379.90 14.04 o -1 7 1 205.66 196.61 7.55 o 0 7 1 188.99 182.96 5.76 o 1 7 1 17.70 15.47 2.91 o 2 7 1 53.47 49.77 2.83 o 3 7 1 35.70 36.45 3.09 o 4 7 1 145.42 130.61 7.07 o 5 7 1 27.75 23.34 3.74 o -16 0 2 592.65 596.59 85.56 o -15 0 2 135.23 119.09 14.24 o -14 0 2 411.78 381.50 29.33 o -13 0 2 270.75 266.05 12.94 o -12 0 2 519.36 513.97 27.53 o -11 0 2 1618.19 1609.03 53.29 o -10 0 2 653.73 690.25 27.99 o -9 0 2 2392.97 2517.62 125.37 o -8 0 2 1363.45 1259.44 25.43 o -7 0 2 1936.00 1887.64 34.44 o -6 0 2 3106.00 3204.31 52.86 o -5 0 2 622.75 723.41 8.38 o -4 0 2 1740.31 1890.69 72.86 o -3 0 2 2566.17 2561.52 76.03 o -2 0 2 427.99 428.13 9.25 o 2 0 2 1523.51 1244.46 59.19 o 3 0 2 331.42 286.10 19.26 o 4 0 2 979.71 908.89 51.33 o 5 0 2 145.14 135.75 4.89 o 6 0 2 60.55 50.54 3.34 o 7 0 2 1337.96 1336.24 42.22 o 8 0 2 237.09 225.48 8.67 o 9 0 2 1659.44 1664.71 12.60 o 10 0 2 43.39 46.47 3.13 o 11 0 2 90.30 93.98 3.41 o 12 0 2 5016.39 5111.19 75.08 o 13 0 2 1020.98 1106.38 66.68 o 14 0 2 13.68 11.11 2.99 o 15 0 2 30.81 35.98 6.18 o -15 1 2 190.98 174.09 3.63 o -14 1 2 210.70 196.64 7.51 o -13 1 2 135.26 136.58 4.55 o -12 1 2 31.45 40.56 2.89 o -11 1 2 13.48 13.84 2.25 o -10 1 2 45.44 48.22 2.16 o -9 1 2 7.55 9.60 2.59 o -8 1 2 94.36 83.48 2.91 o -7 1 2 758.66 808.15 22.55 o -6 1 2 5049.23 5218.62 110.27 o -5 1 2 302.00 261.00 8.25 o -4 1 2 304.17 277.95 7.43 o -3 1 2 2201.67 2092.06 65.64 o -2 1 2 482.87 466.76 21.21 o -1 1 2 12539.14 11468.50 515.55 o 0 1 2 3397.66 3093.43 51.91 o 1 1 2 1943.17 1754.60 46.75 o 2 1 2 12680.08 10855.43 151.40 o 3 1 2 4326.35 3876.09 64.53 o 4 1 2 3963.36 3640.23 56.35 o 5 1 2 562.36 442.78 4.62 o 6 1 2 436.52 360.56 5.70 o 7 1 2 637.56 671.60 16.39 o 8 1 2 350.72 371.19 15.90 o 9 1 2 23.13 27.20 1.95 o 10 1 2 10.43 14.00 1.87 o 11 1 2 60.80 65.11 2.31 o 12 1 2 321.95 333.34 8.49 o 13 1 2 36.26 38.08 2.51 o 14 1 2 6.28 8.15 2.39 o 15 1 2 395.21 371.92 20.84 o -15 2 2 37.67 29.94 2.81 o -14 2 2 18.23 16.31 2.47 o -13 2 2 161.40 151.77 4.77 o -12 2 2 262.20 254.14 9.79 o -11 2 2 1227.81 1264.51 33.20 o -10 2 2 8.89 13.42 1.83 o -9 2 2 21.37 25.38 1.91 o -8 2 2 639.56 588.45 21.41 o -7 2 2 805.59 810.52 20.78 o -6 2 2 1927.21 2021.83 67.25 o -5 2 2 1599.17 1682.51 61.12 o -4 2 2 2234.34 2436.63 78.51 o -3 2 2 3497.81 3634.45 89.25 o -2 2 2 1877.44 1841.61 32.38 o -1 2 2 115.33 108.07 3.73 o 0 2 2 78.15 72.45 3.38 o 1 2 2 89.97 88.40 3.29 o 2 2 2 728.23 702.86 6.67 o 3 2 2 1.19 3.75 1.97 o 4 2 2 669.16 711.05 11.03 o 5 2 2 55.61 38.91 2.07 o 6 2 2 119.32 84.56 3.80 o 7 2 2 5958.27 6216.99 423.75 o 8 2 2 2355.13 2431.63 138.02 o 9 2 2 732.27 711.76 34.87 o 10 2 2 773.86 761.38 28.29 o 11 2 2 274.48 297.37 19.18 o 12 2 2 189.85 196.35 7.51 o 13 2 2 98.59 92.84 5.97 o 14 2 2 136.28 144.34 10.15 o 15 2 2 1.60 4.38 2.60 o -14 3 2 87.19 89.18 8.04 o -13 3 2 148.62 152.94 8.13 o -12 3 2 41.53 44.65 2.48 o -11 3 2 102.74 105.46 6.97 o -10 3 2 455.15 462.88 13.78 o -9 3 2 313.20 319.56 15.82 o -8 3 2 0.17 0.00 2.73 o -7 3 2 241.43 263.37 23.91 o -6 3 2 99.19 90.94 10.77 o -5 3 2 211.08 291.72 16.37 o -4 3 2 7.63 22.81 4.18 o -3 3 2 7983.20 9074.45 326.85 o -2 3 2 3121.68 3285.07 39.15 o -1 3 2 530.69 435.23 5.82 o 0 3 2 6415.37 6330.85 117.45 o 1 3 2 4097.51 4008.47 70.09 o 2 3 2 1775.05 1702.92 25.67 o 3 3 2 1978.39 2021.47 61.07 o 4 3 2 2316.46 2558.35 116.17 o 5 3 2 565.92 575.49 26.17 o 6 3 2 322.87 348.18 13.15 o 7 3 2 394.57 422.15 18.12 o 8 3 2 10.62 13.01 2.21 o 9 3 2 48.80 50.77 4.49 o 10 3 2 177.09 182.61 7.55 o 11 3 2 189.68 210.06 12.42 o 12 3 2 18.91 20.51 2.21 o 13 3 2 45.20 49.01 3.33 o 14 3 2 315.30 329.03 16.87 o -13 4 2 59.57 61.61 2.71 o -12 4 2 15.62 19.23 2.51 o -11 4 2 183.88 197.32 12.57 o -10 4 2 0.24 4.74 2.82 o -9 4 2 86.97 82.98 7.54 o -8 4 2 2542.97 2612.65 290.63 o -7 4 2 885.22 944.23 90.00 o -6 4 2 858.14 884.06 36.19 o -5 4 2 1070.86 1079.66 47.89 o -4 4 2 458.60 453.47 14.91 o -3 4 2 971.73 1003.49 20.11 o -2 4 2 561.15 568.46 6.88 o -1 4 2 436.14 449.60 6.53 o 0 4 2 49.73 47.20 2.91 o 1 4 2 291.26 300.27 4.22 o 2 4 2 169.28 152.70 6.32 o 3 4 2 735.72 743.01 29.15 o 4 4 2 1508.73 1587.02 91.20 o 5 4 2 572.91 577.68 42.46 o 6 4 2 395.12 428.74 18.64 o 7 4 2 518.64 537.71 31.45 o 8 4 2 95.06 108.52 6.87 o 9 4 2 0.25 3.45 2.50 o 10 4 2 310.10 299.70 23.17 o 11 4 2 259.68 223.11 17.43 o 12 4 2 15.03 19.05 2.75 o 13 4 2 178.44 193.18 19.78 o -12 5 2 20.18 24.50 2.55 o -11 5 2 328.79 306.11 19.64 o -10 5 2 92.10 94.23 4.98 o -9 5 2 25.89 34.25 8.97 o -8 5 2 2.95 2.00 3.49 o -7 5 2 182.29 189.99 9.32 o -6 5 2 213.32 212.32 18.89 o -5 5 2 146.16 135.63 18.64 o -4 5 2 327.79 306.81 7.29 o -3 5 2 631.61 620.01 8.85 o -2 5 2 656.54 635.05 9.51 o -1 5 2 1190.12 1204.97 15.14 o 0 5 2 319.73 303.17 9.95 o 1 5 2 201.88 197.23 5.05 o 2 5 2 1959.46 1953.93 30.61 o 3 5 2 166.34 168.80 4.06 o 4 5 2 80.14 78.41 3.26 o 5 5 2 53.21 55.60 3.25 o 6 5 2 192.98 200.46 11.08 o 7 5 2 23.08 24.18 2.96 o 8 5 2 103.52 107.84 4.86 o 9 5 2 5.16 5.73 3.65 o 10 5 2 84.56 93.39 5.72 o 11 5 2 45.61 44.70 6.49 o -9 6 2 151.46 136.07 13.06 o -8 6 2 77.63 84.43 4.41 o -7 6 2 40.20 38.55 3.96 o -6 6 2 320.23 291.59 16.79 o -5 6 2 153.26 145.06 4.93 o -4 6 2 16.31 15.50 2.48 o -3 6 2 249.52 239.83 4.13 o -2 6 2 23.64 23.36 2.79 o -1 6 2 29.17 30.44 2.75 o 0 6 2 10.81 9.84 2.39 o 1 6 2 220.96 210.59 3.70 o 2 6 2 511.08 492.33 10.17 o 3 6 2 120.17 111.34 3.34 o 4 6 2 33.09 35.10 2.78 o 5 6 2 0.23 0.79 2.53 o 6 6 2 4.73 7.90 3.71 o 7 6 2 7.05 12.62 3.02 o 8 6 2 51.81 54.61 3.32 o 9 6 2 324.87 328.54 23.10 o -5 7 2 26.98 24.05 4.32 o -4 7 2 0.29 1.61 2.37 o -3 7 2 11.98 13.32 2.83 o -2 7 2 272.88 236.51 12.03 o -1 7 2 984.05 932.72 19.16 o 0 7 2 52.96 51.61 2.75 o 1 7 2 19.65 19.79 2.80 o 2 7 2 118.33 111.22 3.38 o 3 7 2 108.03 104.51 3.46 o 4 7 2 29.77 35.35 3.21 o 5 7 2 10.27 9.58 3.73 o -15 1 3 2.67 4.98 2.74 o -14 1 3 11.17 10.64 2.94 o -13 1 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