#------------------------------------------------------------------------------ #$Date: 2020-11-28 07:19:17 +0200 (Sat, 28 Nov 2020) $ #$Revision: 259272 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/36/2243688.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243688 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.0770 _cell_length_b 18.1608 _cell_length_c 7.9336 _exptl_crystal_F_000 936.00 _reflns_d_resolution_high 0.7355 _cod_data_source_file ru2071Ho_Molybdatesup4.hkl _cod_data_source_block Ho_Molybdate _shelx_title ' khomo2o8_a.res in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 502.57 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 152708.33 149273.47 3545.95 o 4 0 0 147523.89 148958.94 3549.90 o 6 0 0 33347.16 33653.41 1692.33 o 1 1 0 210.14 263.99 11.05 o 3 1 0 3709.48 3922.53 78.69 o 5 1 0 1941.55 1960.98 81.25 o 0 2 0 111018.30 96899.85 2299.04 o 2 2 0 25903.42 24416.79 417.11 o 4 2 0 48900.82 49158.15 898.43 o 6 2 0 11931.83 11732.02 381.04 o 1 3 0 122223.53 124974.87 2241.74 o 3 3 0 47108.58 47101.93 856.72 o 5 3 0 24278.32 24474.49 502.43 o 0 4 0 326.23 427.60 26.56 o 2 4 0 9176.41 9481.82 214.78 o 4 4 0 2007.21 1835.52 58.48 o 6 4 0 4106.28 3865.24 247.69 o 1 5 0 239956.94 232652.94 4172.15 o 3 5 0 141970.11 139372.06 2507.98 o 5 5 0 78140.63 78087.83 1685.90 o 0 6 0 3561.59 3654.91 102.87 o 2 6 0 3007.30 3404.75 74.71 o 4 6 0 415.20 425.77 35.43 o 6 6 0 1900.28 1847.96 126.08 o 1 7 0 55824.71 54424.38 921.18 o 3 7 0 28336.74 28080.34 562.39 o 5 7 0 16790.77 16726.66 439.13 o 0 8 0 82516.33 83904.50 2003.75 o 2 8 0 70488.73 69153.18 1250.32 o 4 8 0 49784.78 49541.50 1083.16 o 6 8 0 21922.35 21503.51 566.55 o 1 9 0 2029.46 2160.01 62.90 o 3 9 0 2550.01 2523.79 76.04 o 5 9 0 1245.02 1204.00 90.91 o 0 10 0 202500.98 210557.27 5007.39 o 2 10 0 91336.92 89151.56 1614.94 o 4 10 0 65496.73 67183.45 1632.13 o 6 10 0 23769.35 23342.45 711.96 o 1 11 0 1609.34 1771.71 52.71 o 3 11 0 441.96 411.29 45.32 o 5 11 0 383.86 389.89 66.70 o 0 12 0 36167.05 38499.98 937.41 o 2 12 0 28902.25 27827.30 703.66 o 4 12 0 19379.61 18881.68 495.52 o 1 13 0 73917.29 72720.81 1332.00 o 3 13 0 40751.34 38277.86 949.94 o 5 13 0 22040.20 20800.79 573.81 o 0 14 0 4510.62 4938.14 150.82 o 2 14 0 1586.32 1487.83 78.37 o 4 14 0 209.83 255.99 64.00 o 1 15 0 61137.80 62349.63 1140.25 o 3 15 0 43093.24 39534.31 1757.55 o 5 15 0 28858.53 27735.01 747.23 o 0 16 0 1196.14 1276.87 73.99 o 2 16 0 2266.81 2413.97 174.08 o 4 16 0 940.73 827.61 90.16 o 1 17 0 20816.56 22377.74 511.09 o 3 17 0 15350.36 15162.46 419.33 o 0 18 0 27095.45 28892.06 832.33 o 2 18 0 32496.30 34389.71 863.50 o 4 18 0 19640.13 19186.70 523.58 o 1 19 0 1111.07 1219.33 80.05 o 3 19 0 855.66 1159.56 99.28 o 0 20 0 42419.25 44981.16 2235.44 o 2 20 0 25139.44 26120.01 672.31 o 1 21 0 63.32 62.38 71.36 o 3 21 0 504.45 588.20 101.14 o 0 22 0 13296.69 13318.00 769.84 o 2 22 0 6698.64 6712.65 264.60 o 1 23 0 15183.78 14651.53 597.49 o 1 1 1 1166.02 1271.81 22.52 o 2 1 1 13.44 -0.99 6.88 o 3 1 1 379.92 426.41 15.49 o 4 1 1 1548.53 1498.47 34.24 o 5 1 1 228.32 303.62 28.64 o 6 1 1 3985.00 3727.70 131.80 o 0 2 1 1376.73 1399.27 33.15 o 1 2 1 1150.09 1115.50 22.24 o 2 2 1 326.58 364.84 12.66 o 3 2 1 2065.63 1824.20 33.04 o 4 2 1 149.67 153.29 15.38 o 5 2 1 8273.94 7920.96 135.23 o 6 2 1 0.58 148.49 46.86 o 1 3 1 10496.58 10231.63 145.91 o 2 3 1 6469.24 6212.58 89.97 o 3 3 1 6060.22 5979.09 83.17 o 4 3 1 5744.72 5490.22 84.21 o 5 3 1 1925.34 2025.62 58.69 o 6 3 1 6790.12 6377.14 172.26 o 0 4 1 2599.24 2753.95 57.39 o 1 4 1 1580.75 1521.69 29.08 o 2 4 1 2429.56 2548.34 43.00 o 3 4 1 5225.23 5039.83 75.02 o 4 4 1 481.73 575.10 25.69 o 5 4 1 1506.38 1636.65 63.78 o 6 4 1 553.89 673.35 61.23 o 1 5 1 52.46 53.30 9.49 o 2 5 1 81.75 87.82 11.60 o 3 5 1 10.87 -7.27 11.12 o 4 5 1 6.10 3.35 16.04 o 5 5 1 47.90 32.27 25.41 o 6 5 1 47.23 -20.10 48.30 o 0 6 1 204.29 218.63 15.64 o 1 6 1 10330.73 10745.14 162.09 o 2 6 1 763.60 799.52 24.71 o 3 6 1 671.88 592.32 23.15 o 4 6 1 534.45 540.05 28.70 o 5 6 1 4905.53 4711.69 98.54 o 6 6 1 295.29 301.54 52.56 o 1 7 1 4304.86 4334.99 66.95 o 2 7 1 7232.04 7297.39 112.03 o 3 7 1 1679.00 1706.60 38.02 o 4 7 1 5827.21 5604.81 106.73 o 5 7 1 1283.87 1359.48 52.57 o 6 7 1 5803.85 5305.70 140.86 o 0 8 1 17185.18 15519.64 310.01 o 1 8 1 8401.96 8674.34 146.63 o 2 8 1 9960.72 9845.21 147.63 o 3 8 1 354.52 290.01 22.14 o 4 8 1 6574.82 6509.72 121.44 o 5 8 1 9670.31 9225.40 188.48 o 6 8 1 2242.94 2364.84 142.09 o 1 9 1 1035.19 1090.49 28.61 o 2 9 1 10.35 16.91 14.09 o 3 9 1 1037.72 1070.63 37.59 o 4 9 1 830.71 818.04 39.73 o 5 9 1 815.26 936.00 78.09 o 6 9 1 2586.90 2537.92 112.20 o 0 10 1 1551.02 1523.19 67.65 o 1 10 1 194.98 202.76 16.65 o 2 10 1 207.66 220.92 20.11 o 3 10 1 1310.93 1410.16 44.51 o 4 10 1 819.20 885.03 44.92 o 5 10 1 46.13 56.40 37.48 o 6 10 1 243.05 178.84 81.51 o 1 11 1 7428.27 7343.41 111.52 o 2 11 1 467.90 456.94 28.06 o 3 11 1 5459.92 5465.19 106.91 o 4 11 1 1774.78 1619.50 66.46 o 5 11 1 2498.41 2631.48 91.05 o 6 11 1 3201.83 3100.32 225.81 o 0 12 1 8420.44 8315.28 158.83 o 1 12 1 193.41 194.31 18.57 o 2 12 1 6099.36 5914.53 97.09 o 3 12 1 1521.60 1390.22 60.68 o 4 12 1 4506.94 4410.80 111.30 o 5 12 1 5717.42 5603.70 137.66 o 1 13 1 8509.44 8202.63 191.40 o 2 13 1 1311.73 1249.84 43.59 o 3 13 1 6512.28 6213.61 151.19 o 4 13 1 3005.33 2889.55 91.37 o 5 13 1 3308.18 3390.34 109.17 o 0 14 1 1004.52 1096.15 54.93 o 1 14 1 898.75 891.88 60.29 o 2 14 1 1953.38 2086.79 73.57 o 3 14 1 843.85 895.02 60.12 o 4 14 1 650.50 620.15 51.48 o 5 14 1 1165.17 1033.05 69.16 o 1 15 1 3548.20 3558.88 72.00 o 2 15 1 57.21 64.31 32.61 o 3 15 1 2835.80 2690.82 85.26 o 4 15 1 30.48 61.86 42.39 o 5 15 1 2180.57 1703.50 121.17 o 0 16 1 10384.83 10880.41 222.22 o 1 16 1 281.55 264.84 29.47 o 2 16 1 12447.03 12241.22 238.96 o 3 16 1 1381.63 1286.50 73.33 o 4 16 1 6245.76 5660.88 157.41 o 1 17 1 6494.29 6731.40 123.65 o 2 17 1 2479.95 2517.06 98.79 o 3 17 1 4244.75 3997.83 181.20 o 4 17 1 3156.26 2784.15 111.76 o 0 18 1 5032.44 5324.83 143.10 o 1 18 1 513.99 521.02 59.17 o 2 18 1 4359.52 4399.40 146.71 o 3 18 1 1918.43 1865.45 82.40 o 4 18 1 3538.48 3224.31 115.50 o 1 19 1 2590.60 2642.97 88.14 o 2 19 1 68.89 94.09 43.23 o 3 19 1 2244.62 2351.05 94.55 o 4 19 1 302.77 42.18 181.91 o 0 20 1 8645.25 8985.40 276.92 o 1 20 1 348.97 390.05 56.80 o 2 20 1 4983.04 4863.93 137.02 o 3 20 1 85.50 55.34 54.29 o 1 21 1 10038.97 10546.67 251.47 o 2 21 1 554.19 565.72 80.38 o 3 21 1 8405.19 8567.78 271.47 o 0 22 1 3643.78 3751.40 374.38 o 1 22 1 663.17 740.42 83.82 o 2 22 1 2534.67 2559.67 105.73 o 1 23 1 3714.62 3970.88 349.95 o 2 23 1 284.43 215.82 101.01 o 0 24 1 3749.29 4518.34 429.74 o 1 24 1 388.42 515.07 128.27 o 0 0 2 384.22 430.50 32.73 o 1 0 2 86.49 339.85 30.26 o 2 0 2 739.96 898.98 28.67 o 3 0 2 132.84 477.99 94.91 o 4 0 2 4181.05 4001.46 93.94 o 5 0 2 414.79 1190.53 68.09 o 6 0 2 3005.15 3010.10 160.09 o 1 1 2 205291.67 210777.25 2670.83 o 2 1 2 1.47 7.23 7.48 o 3 1 2 109563.98 111020.61 1528.27 o 4 1 2 266.06 304.05 24.84 o 5 1 2 45559.50 46785.80 723.62 o 6 1 2 129.49 222.67 51.44 o 0 2 2 12159.13 12648.58 232.70 o 1 2 2 115.34 149.09 10.67 o 2 2 2 14997.74 15513.78 220.82 o 3 2 2 53.82 197.60 18.89 o 4 2 2 4246.03 4210.20 71.50 o 5 2 2 38.40 476.62 39.93 o 6 2 2 5703.58 5718.87 168.16 o 1 3 2 7683.63 7627.82 116.53 o 2 3 2 55.27 131.28 12.40 o 3 3 2 12866.70 12537.16 176.74 o 4 3 2 46.24 103.68 16.56 o 5 3 2 9853.65 9895.26 183.11 o 6 3 2 42.02 442.50 118.25 o 0 4 2 169955.50 168906.91 3274.20 o 1 4 2 67.14 64.83 10.26 o 2 4 2 216867.95 215914.53 2959.26 o 3 4 2 351.11 376.26 18.39 o 4 4 2 67824.95 68254.24 991.74 o 5 4 2 130.59 156.46 27.12 o 6 4 2 44534.16 43449.90 817.68 o 1 5 2 1937.55 2280.08 41.74 o 2 5 2 221.77 270.08 17.74 o 3 5 2 195.15 205.79 17.45 o 4 5 2 592.41 630.95 28.52 o 5 5 2 989.94 1048.73 48.82 o 6 5 2 115.04 523.35 60.99 o 0 6 2 74327.84 72337.51 1408.41 o 1 6 2 20.29 20.86 10.52 o 2 6 2 120269.21 117974.06 1621.63 o 3 6 2 249.70 251.73 18.78 o 4 6 2 45563.74 45613.98 670.73 o 5 6 2 156.63 222.13 30.51 o 6 6 2 29750.73 29462.42 613.81 o 1 7 2 9404.44 9415.92 146.57 o 2 7 2 4.82 14.19 12.86 o 3 7 2 9723.80 9748.61 149.58 o 4 7 2 15.36 4.50 19.18 o 5 7 2 7967.77 8020.49 149.30 o 6 7 2 20.98 98.69 52.77 o 0 8 2 30295.74 30679.71 562.66 o 1 8 2 5.56 16.14 12.95 o 2 8 2 13250.15 12991.98 191.80 o 3 8 2 303.20 270.32 22.29 o 4 8 2 7786.83 7779.73 133.77 o 5 8 2 6.03 82.70 30.61 o 6 8 2 4955.52 4499.13 146.64 o 1 9 2 142874.23 142949.86 1965.11 o 2 9 2 35.56 53.94 15.40 o 3 9 2 97265.78 96907.59 1341.85 o 4 9 2 289.69 226.38 28.96 o 5 9 2 46791.53 46932.25 732.04 o 6 9 2 72.36 98.29 61.75 o 0 10 2 169.44 233.34 27.14 o 1 10 2 63.39 75.55 14.93 o 2 10 2 4445.35 4456.32 78.69 o 3 10 2 192.51 210.36 23.32 o 4 10 2 1276.99 1313.93 54.76 o 5 10 2 222.42 226.77 37.70 o 6 10 2 133.72 -17.58 170.05 o 1 11 2 71553.05 72345.98 1004.64 o 2 11 2 1.65 9.84 18.00 o 3 11 2 42404.13 41519.90 695.85 o 4 11 2 148.17 106.39 30.37 o 5 11 2 19765.72 20278.69 377.70 o 6 11 2 97.41 -42.18 224.10 o 0 12 2 25208.38 23929.12 420.87 o 1 12 2 31.81 28.39 18.58 o 2 12 2 6805.74 6928.00 116.19 o 3 12 2 0.02 12.61 23.16 o 4 12 2 12641.72 12480.53 231.56 o 5 12 2 31.57 -0.61 40.53 o 1 13 2 7028.15 7184.69 118.94 o 2 13 2 5.83 42.34 22.95 o 3 13 2 8681.83 8627.90 200.85 o 4 13 2 47.56 48.61 36.70 o 5 13 2 6825.20 6789.68 161.08 o 0 14 2 90430.78 88882.34 1609.91 o 1 14 2 44.20 6.69 22.21 o 2 14 2 64392.77 65786.84 920.84 o 3 14 2 166.35 200.18 35.43 o 4 14 2 40084.70 39304.64 751.48 o 5 14 2 91.88 87.00 48.60 o 1 15 2 1860.97 1956.43 64.28 o 2 15 2 56.52 71.70 28.66 o 3 15 2 1745.33 1868.53 86.98 o 4 15 2 266.16 213.81 46.72 o 5 15 2 236.16 150.28 216.19 o 0 16 2 33265.18 34116.85 690.21 o 1 16 2 35.70 73.26 29.45 o 2 16 2 33751.20 34076.54 540.63 o 3 16 2 71.84 63.39 38.92 o 4 16 2 24336.47 23904.00 444.02 o 1 17 2 12250.16 12122.62 202.21 o 2 17 2 3.01 35.86 37.04 o 3 17 2 8673.96 8629.96 198.55 o 4 17 2 2.84 76.42 50.62 o 0 18 2 5152.06 5225.37 178.41 o 1 18 2 25.28 102.61 34.56 o 2 18 2 1974.77 2011.58 100.76 o 3 18 2 204.88 208.07 49.45 o 4 18 2 2077.44 2071.22 279.28 o 1 19 2 31976.61 33059.08 555.20 o 2 19 2 35.38 -37.12 45.45 o 3 19 2 28053.14 28193.30 559.48 o 4 19 2 180.44 -21.09 195.10 o 0 20 2 1449.39 1620.11 105.96 o 1 20 2 8.58 93.48 50.17 o 2 20 2 3680.67 3710.25 115.75 o 3 20 2 129.03 108.33 58.25 o 1 21 2 25776.58 26171.30 606.69 o 2 21 2 0.15 -23.94 52.30 o 3 21 2 17551.00 15975.43 682.41 o 0 22 2 7147.09 7842.04 375.82 o 1 22 2 14.27 45.53 67.52 o 2 22 2 4818.32 4912.07 155.50 o 1 23 2 53.26 67.35 83.47 o 2 23 2 0.05 -55.37 158.19 o 1 24 2 40.99 137.10 379.65 o 1 1 3 9411.82 9400.78 130.46 o 2 1 3 5.40 31.66 8.92 o 3 1 3 3129.31 3314.49 56.73 o 4 1 3 2190.65 2262.96 54.94 o 5 1 3 861.21 1155.73 57.07 o 6 1 3 2388.44 2651.49 103.46 o 0 2 3 3559.77 3625.43 74.52 o 1 2 3 6014.11 6862.99 94.58 o 2 2 3 6837.37 6694.31 103.28 o 3 2 3 10857.34 10812.15 155.01 o 4 2 3 760.04 1031.10 45.63 o 5 2 3 2457.15 2464.86 69.19 o 6 2 3 1004.84 1040.27 72.46 o 1 3 3 113.35 192.38 11.60 o 2 3 3 2509.01 2270.87 46.24 o 3 3 3 11.19 45.52 12.55 o 4 3 3 7043.63 7229.79 117.41 o 5 3 3 22.62 -9.05 25.91 o 6 3 3 3669.38 3626.17 120.09 o 0 4 3 3489.25 3464.07 79.86 o 1 4 3 1342.75 1602.06 33.32 o 2 4 3 8631.43 8172.93 124.44 o 3 4 3 10271.58 10262.24 155.62 o 4 4 3 2976.39 3155.12 63.24 o 5 4 3 202.33 163.49 31.13 o 6 4 3 1996.80 2197.37 93.48 o 1 5 3 65.35 58.97 11.99 o 2 5 3 38.44 44.92 13.84 o 3 5 3 27.65 36.48 14.87 o 4 5 3 2.11 -0.77 17.42 o 5 5 3 59.72 86.25 30.68 o 6 5 3 42.52 22.92 42.31 o 0 6 3 275.20 305.76 21.16 o 1 6 3 1019.25 1019.86 28.34 o 2 6 3 738.26 861.57 28.88 o 3 6 3 2708.20 2634.66 54.72 o 4 6 3 243.24 272.42 24.10 o 5 6 3 2312.23 2385.78 75.41 o 6 6 3 58.55 98.74 45.95 o 1 7 3 15242.17 14869.49 236.39 o 2 7 3 3407.53 3199.32 60.09 o 3 7 3 11762.04 11551.89 176.39 o 4 7 3 6985.95 6630.83 112.50 o 5 7 3 5576.96 5603.88 131.92 o 6 7 3 3301.73 3029.39 122.95 o 0 8 3 2183.23 2323.29 63.83 o 1 8 3 12.45 9.47 13.74 o 2 8 3 374.77 393.87 22.49 o 3 8 3 4716.79 4453.08 81.02 o 4 8 3 1129.54 1145.07 48.48 o 5 8 3 3536.68 3489.51 86.93 o 6 8 3 333.73 260.07 71.99 o 1 9 3 6188.04 6118.20 101.41 o 2 9 3 5.77 2.70 15.75 o 3 9 3 3210.99 3340.07 67.45 o 4 9 3 1297.26 1406.51 52.09 o 5 9 3 1500.55 1690.47 63.23 o 0 10 3 799.29 869.63 44.02 o 1 10 3 7.38 9.02 17.28 o 2 10 3 847.42 913.79 41.27 o 3 10 3 585.75 662.46 32.44 o 4 10 3 1046.50 1124.41 51.10 o 5 10 3 3.59 -31.69 33.84 o 1 11 3 797.79 856.16 33.08 o 2 11 3 218.15 275.96 24.61 o 3 11 3 885.68 906.46 48.09 o 4 11 3 2002.46 2087.49 81.01 o 5 11 3 852.73 794.74 52.95 o 0 12 3 22220.40 21106.71 535.45 o 1 12 3 1360.16 1466.35 43.76 o 2 12 3 21526.13 21856.30 320.01 o 3 12 3 5323.90 5123.82 95.86 o 4 12 3 8886.01 8871.95 175.21 o 5 12 3 2222.96 1996.63 79.91 o 1 13 3 896.03 993.46 41.50 o 2 13 3 574.32 633.68 35.17 o 3 13 3 760.39 813.83 43.29 o 4 13 3 3739.88 3616.69 95.61 o 5 13 3 873.80 780.17 63.72 o 0 14 3 2299.90 2308.39 105.11 o 1 14 3 89.42 126.61 26.72 o 2 14 3 4371.87 4456.80 88.06 o 3 14 3 2719.43 2813.03 76.50 o 4 14 3 2251.57 2470.73 86.32 o 5 14 3 185.02 137.57 83.80 o 1 15 3 5216.44 5081.52 102.87 o 2 15 3 25.22 34.31 28.02 o 3 15 3 3271.64 3473.38 93.41 o 4 15 3 16.39 96.16 44.16 o 0 16 3 4523.31 4548.50 166.49 o 1 16 3 1.14 18.58 29.56 o 2 16 3 3479.22 3732.15 88.05 o 3 16 3 2012.31 2009.12 78.25 o 4 16 3 2711.61 2676.19 95.76 o 1 17 3 14699.82 13858.46 409.39 o 2 17 3 1520.31 1495.43 69.31 o 3 17 3 12595.78 12626.46 315.32 o 4 17 3 3635.95 3390.05 112.76 o 0 18 3 1184.99 1307.50 122.44 o 1 18 3 180.15 141.73 42.92 o 2 18 3 309.95 318.71 48.53 o 3 18 3 4472.56 4398.47 134.50 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