#------------------------------------------------------------------------------ #$Date: 2020-12-12 07:51:53 +0200 (Sat, 12 Dec 2020) $ #$Revision: 259832 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/37/2243704.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243704 _cell_angle_alpha 105.024 _cell_angle_beta 105.935 _cell_angle_gamma 102.999 _cell_length_a 12.7166 _cell_length_b 14.4366 _cell_length_c 16.4038 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.7682 _cod_data_source_file mw2170Isup2.hkl _cod_data_source_block I _shelx_title ' k13kcm24' _shelx_refln_list_code 4 _shelx_f_calc_maximum 293.06 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 168.60 205.14 55.02 o 3 0 0 6292.56 6812.87 124.47 o 4 0 0 6074.56 5890.54 111.28 o 5 0 0 107.75 116.72 13.52 o 6 0 0 2369.41 2424.24 47.95 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