#------------------------------------------------------------------------------ #$Date: 2020-12-16 07:55:03 +0200 (Wed, 16 Dec 2020) $ #$Revision: 259927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/37/2243707.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243707 _cell_angle_alpha 102.011 _cell_angle_beta 90.426 _cell_angle_gamma 109.827 _cell_length_a 9.6582 _cell_length_b 9.8765 _cell_length_c 13.0748 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file wm5591complex2sup5.hkl _cod_data_source_block complex2 _shelx_title ' 160617_off1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 219.95 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 48379.19 48990.23 1508.47 o 3 0 0 109.36 127.72 4.33 o 4 0 0 5027.16 5025.58 82.27 o 5 0 0 819.79 851.82 22.86 o 6 0 0 6115.90 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