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Information card for entry 2243919
Preview
| Coordinates | 2243919.cif |
|---|---|
| Structure factors | 2243919.hkl |
| Original IUCr paper | HTML |
| Chemical name | Tetrakis(1,3-dimethylimidazolium-2-ylidene)palladium(II) hexadecacarbonyltetrarhenium diethyl ether disolvate |
|---|---|
| Formula | C44 H52 N8 O18 Pd Re4 |
| Calculated formula | C44 H52 N8 O18 Pd Re4 |
| Title of publication | Crystal structure of the new palladium complexes tetrakis(1,3-dimethylimidazolium-2-ylidene)palladium(II) hexadecacarbonyltetrarhenium diethyl ether disolvate and octa-μ-carbonyl-dicarbonyltetrakis(triphenylphosphane)palladiumdirhenium (unknown solvate) |
| Authors of publication | Shapovalov, Sergey; Tikhonova, Olga; Skabitsky, Ivan |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2021 |
| Journal volume | 77 |
| Journal issue | 10 |
| a | 21.1079 ± 0.0009 Å |
| b | 14.0026 ± 0.0006 Å |
| c | 19.4346 ± 0.0008 Å |
| α | 90° |
| β | 109.342 ± 0.001° |
| γ | 90° |
| Cell volume | 5420 ± 0.4 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0434 |
| Residual factor for significantly intense reflections | 0.028 |
| Weighted residual factors for significantly intense reflections | 0.0598 |
| Weighted residual factors for all reflections included in the refinement | 0.0651 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.058 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 269149 (current) | 2021-09-15 | cif/ hkl/ Adding structures of 2243919, 2243920 via cif-deposit CGI script. |
2243919.cif 2243919.hkl |
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Users of the data should acknowledge the original authors of the
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