Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 2243977
Preview
Coordinates | 2243977.cif |
---|---|
Structure factors | 2243977.hkl |
Original paper (by DOI) | HTML |
Chemical name | Bis[3,5-bis(trifluoromethyl)phenyl-2κ<i>C</i>^1^](fluorido-1κ<i>I</i>)(hydrido-2κ<i>H</i>)bis[1,1(η^5^)-pentamethylcyclopentadienyl]germaniumuranium(<i>Ge</i>—<i>U</i>) |
---|---|
Formula | C37 H39 F13 Ge U |
Calculated formula | C37 H39 F13 Ge U |
Title of publication | Crystal structures of metallocene complexes with uranium–germanium bonds |
Authors of publication | Tarlton, Michael L.; Kelley, Steven P.; Walensky, Justin R. |
Journal of publication | Acta Crystallographica Section E |
Year of publication | 2021 |
Journal volume | 77 |
Journal issue | 12 |
Pages of publication | 1258 - 1262 |
a | 34.16 ± 0.003 Å |
b | 13.5237 ± 0.0011 Å |
c | 16.2986 ± 0.0013 Å |
α | 90° |
β | 95.028 ± 0.002° |
γ | 90° |
Cell volume | 7500.5 ± 1.1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0736 |
Residual factor for significantly intense reflections | 0.0412 |
Weighted residual factors for significantly intense reflections | 0.0838 |
Weighted residual factors for all reflections included in the refinement | 0.0941 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | Yes |
Revision | Date | Message | Files |
---|---|---|---|
271898 (current) | 2022-01-07 | cif/ hkl/ Adding structures of 2243976, 2243977 via cif-deposit CGI script. |
2243977.cif 2243977.hkl |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.