#------------------------------------------------------------------------------ #$Date: 2022-01-15 04:36:22 +0200 (Sat, 15 Jan 2022) $ #$Revision: 272052 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/40/2244010.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244010 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6878 _cell_length_b 18.0941 _cell_length_c 26.9604 _exptl_crystal_F_000 2304.00 _reflns_d_resolution_high 0.8393 _cod_data_source_file wm56312sup7.hkl _cod_data_source_block 2 _shelx_title ' kp16_a.res in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 407.54 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 104660.09 105441.95 894.91 o 4 0 0 39730.15 40080.99 406.28 o 6 0 0 8634.17 8929.78 156.82 o 8 0 0 1379.03 1368.53 84.14 o 10 0 0 12104.08 11691.16 376.49 o 12 0 0 391.21 289.37 112.90 o 2 1 0 33541.61 32640.78 176.25 o 4 1 0 20868.71 20479.99 164.34 o 6 1 0 31.57 31.39 32.34 o 8 1 0 2378.01 2487.88 70.70 o 10 1 0 2306.56 2387.28 83.02 o 12 1 0 165.23 206.13 68.08 o 0 2 0 314.02 223.73 27.27 o 2 2 0 543.69 412.79 38.69 o 4 2 0 2.41 17.34 23.38 o 6 2 0 2235.20 2157.93 61.11 o 8 2 0 38.39 64.33 29.03 o 10 2 0 3992.92 3888.10 99.52 o 12 2 0 884.71 876.60 101.43 o 2 3 0 3113.83 3122.00 108.92 o 4 3 0 922.88 912.24 41.56 o 6 3 0 517.09 562.99 41.40 o 8 3 0 4363.43 3955.43 85.93 o 10 3 0 7020.46 6579.75 164.97 o 12 3 0 32.01 68.41 60.34 o 0 4 0 32903.56 31343.75 248.27 o 2 4 0 6509.50 6454.65 60.02 o 4 4 0 774.16 882.16 38.40 o 6 4 0 6610.96 6214.51 100.28 o 8 4 0 392.16 444.55 44.36 o 10 4 0 5.20 57.26 42.34 o 12 4 0 1115.88 1255.42 152.09 o 2 5 0 3459.10 3368.93 48.62 o 4 5 0 43.69 19.60 24.54 o 6 5 0 3976.08 3964.20 75.10 o 8 5 0 2177.47 1997.30 73.16 o 10 5 0 56.02 235.12 69.06 o 12 5 0 2612.80 2512.11 134.03 o 0 6 0 7552.30 7270.75 79.90 o 2 6 0 113173.54 106122.56 556.39 o 4 6 0 6.75 -24.29 24.29 o 6 6 0 3270.46 3005.17 66.45 o 8 6 0 2065.49 1760.68 69.21 o 10 6 0 7752.74 7167.53 190.28 o 12 6 0 2322.35 2481.25 202.40 o 2 7 0 46014.34 44298.76 291.91 o 4 7 0 150.28 117.80 25.17 o 6 7 0 340.20 379.08 41.67 o 8 7 0 3672.40 3236.18 82.82 o 10 7 0 622.47 677.29 75.68 o 12 7 0 65.55 159.75 73.30 o 0 8 0 65.88 144.02 45.09 o 2 8 0 1033.60 1029.20 53.65 o 4 8 0 4810.90 4745.37 66.26 o 6 8 0 136.79 88.60 27.60 o 8 8 0 4419.48 4132.03 95.78 o 10 8 0 156.70 257.86 59.67 o 12 8 0 30.04 32.31 69.68 o 2 9 0 6915.62 7301.87 105.40 o 4 9 0 146.21 133.07 38.41 o 6 9 0 314.43 346.21 35.14 o 8 9 0 447.13 614.49 51.69 o 10 9 0 92.84 61.91 50.66 o 12 9 0 43.39 121.25 66.87 o 0 10 0 5036.08 4774.93 174.99 o 2 10 0 112.93 533.88 84.34 o 4 10 0 464.08 581.40 52.65 o 6 10 0 236.39 283.94 33.59 o 8 10 0 12.76 29.95 36.84 o 10 10 0 40.16 28.23 45.77 o 12 10 0 14.26 88.82 63.91 o 2 11 0 15571.90 14538.72 159.13 o 4 11 0 214.60 158.05 38.21 o 6 11 0 364.42 420.36 36.61 o 8 11 0 6.90 -36.30 36.30 o 10 11 0 289.89 296.84 58.46 o 0 12 0 13.29 -38.07 48.78 o 2 12 0 2695.03 2315.60 67.23 o 4 12 0 3683.94 3322.97 91.30 o 6 12 0 113.67 208.30 48.88 o 8 12 0 45.56 4.80 39.50 o 10 12 0 164.02 115.58 52.67 o 2 13 0 152.55 200.49 35.74 o 4 13 0 1593.74 1476.91 96.85 o 6 13 0 1041.66 1007.87 90.57 o 8 13 0 0.15 -33.63 33.63 o 10 13 0 840.31 854.96 76.97 o 0 14 0 4262.08 3811.00 210.39 o 2 14 0 3928.59 3361.29 83.37 o 4 14 0 1522.68 1577.20 81.53 o 6 14 0 13.51 31.77 53.05 o 8 14 0 21.05 -47.69 63.08 o 10 14 0 149.57 180.57 74.97 o 2 15 0 2023.59 1773.00 66.91 o 4 15 0 3961.46 3425.22 201.52 o 6 15 0 3.74 -14.65 52.59 o 8 15 0 600.84 579.44 97.28 o 10 15 0 1.80 109.43 81.83 o 0 16 0 1224.24 1521.77 243.44 o 2 16 0 7285.88 6202.97 220.30 o 4 16 0 1744.28 1685.16 99.86 o 6 16 0 96.57 92.81 59.31 o 8 16 0 247.33 279.54 86.86 o 2 17 0 119.62 95.13 40.49 o 4 17 0 236.28 173.54 56.51 o 6 17 0 109.09 88.72 62.24 o 8 17 0 1650.57 1752.53 158.64 o 0 18 0 1943.92 1910.31 240.22 o 2 18 0 28.00 24.60 35.54 o 4 18 0 2777.49 2397.59 104.93 o 6 18 0 168.44 134.60 67.25 o 2 19 0 267.20 325.57 62.04 o 4 19 0 557.64 523.13 70.04 o 6 19 0 62.14 163.90 69.86 o 0 20 0 1753.70 1542.73 309.54 o 2 20 0 39.65 51.12 81.49 o 4 20 0 1754.18 1578.16 97.34 o 2 21 0 450.88 831.74 230.55 o 1 1 1 1219.01 783.65 41.48 o 2 1 1 562.81 623.95 19.43 o 3 1 1 68587.55 64959.31 216.41 o 4 1 1 15861.89 14690.17 83.47 o 5 1 1 786.79 845.60 34.60 o 6 1 1 7058.34 6870.56 77.22 o 7 1 1 3.84 26.12 18.56 o 8 1 1 34.88 24.64 19.85 o 9 1 1 1186.05 1216.53 52.45 o 10 1 1 66.36 205.62 31.48 o 11 1 1 173.47 224.53 63.71 o 12 1 1 152.19 155.89 47.83 o 13 1 1 0.17 57.26 44.58 o 0 2 1 840.71 702.99 28.03 o 1 2 1 13427.53 12155.31 56.00 o 2 2 1 25062.24 22884.52 97.91 o 3 2 1 122.49 120.73 13.32 o 4 2 1 8006.69 7621.01 58.29 o 5 2 1 1112.43 1193.84 36.42 o 6 2 1 1261.05 1196.41 36.91 o 7 2 1 234.94 223.40 24.96 o 8 2 1 598.19 646.15 34.56 o 9 2 1 1599.81 1474.25 50.40 o 10 2 1 8357.58 7883.01 103.00 o 11 2 1 726.94 846.05 72.62 o 12 2 1 1703.46 1620.30 87.70 o 13 2 1 1.55 46.97 44.37 o 1 3 1 337.75 351.45 12.68 o 2 3 1 166092.92 158025.77 468.34 o 3 3 1 559.46 558.47 18.35 o 4 3 1 10888.77 10351.07 78.04 o 5 3 1 1151.51 1183.73 36.18 o 6 3 1 2695.26 2461.14 44.51 o 7 3 1 136.30 165.05 22.59 o 8 3 1 270.83 236.75 26.17 o 9 3 1 1146.97 1185.21 65.54 o 10 3 1 229.48 336.22 36.20 o 11 3 1 485.55 348.67 51.55 o 12 3 1 351.58 353.33 55.80 o 13 3 1 58.07 58.44 43.52 o 1 4 1 327.26 372.84 21.84 o 2 4 1 15246.06 16079.13 72.74 o 3 4 1 2.52 7.21 9.32 o 4 4 1 3012.67 3178.17 40.00 o 5 4 1 846.14 943.13 42.76 o 6 4 1 25.12 28.79 17.37 o 7 4 1 652.89 714.29 34.12 o 8 4 1 2550.38 2524.46 50.80 o 9 4 1 50.71 60.89 25.05 o 10 4 1 483.29 599.98 46.22 o 11 4 1 35.89 60.61 40.35 o 12 4 1 326.47 332.21 53.86 o 13 4 1 28.48 69.25 45.53 o 1 5 1 53087.61 49698.21 200.38 o 2 5 1 7252.37 6825.54 46.24 o 3 5 1 481.74 504.02 19.26 o 4 5 1 1185.30 1148.11 31.35 o 5 5 1 11.71 16.84 18.88 o 6 5 1 1262.34 1396.11 36.10 o 7 5 1 55.08 9.68 16.87 o 8 5 1 1889.08 1968.29 51.45 o 9 5 1 3919.26 3709.94 65.22 o 10 5 1 2402.26 2413.58 83.45 o 11 5 1 91.87 71.03 38.39 o 12 5 1 1793.22 1788.21 91.37 o 13 5 1 211.25 193.14 56.24 o 0 6 1 14950.72 14220.31 88.74 o 1 6 1 14933.08 14020.49 85.93 o 2 6 1 3657.69 3809.22 90.49 o 3 6 1 613.08 723.50 23.40 o 4 6 1 427.78 500.87 27.42 o 5 6 1 1.41 -16.38 16.38 o 6 6 1 38.47 35.83 17.13 o 7 6 1 1.53 3.70 18.88 o 8 6 1 1231.77 1292.34 46.61 o 9 6 1 0.22 23.53 22.78 o 10 6 1 2123.26 2034.66 87.96 o 11 6 1 0.57 -17.84 34.47 o 12 6 1 2341.74 2294.38 95.49 o 13 6 1 0.06 128.52 47.96 o 1 7 1 6478.73 6286.49 57.49 o 2 7 1 5158.70 4659.13 57.50 o 3 7 1 16303.78 16073.21 83.69 o 4 7 1 10.71 -15.10 15.10 o 5 7 1 2049.33 1739.21 35.36 o 6 7 1 27.62 5.97 17.05 o 7 7 1 0.52 0.36 17.80 o 8 7 1 657.61 658.49 36.87 o 9 7 1 25.94 44.20 25.40 o 10 7 1 1139.91 1029.05 62.81 o 11 7 1 17.80 -7.44 34.60 o 12 7 1 907.43 933.17 76.54 o 13 7 1 131.53 244.41 52.46 o 0 8 1 4865.05 4953.43 58.39 o 1 8 1 4906.30 4963.87 54.83 o 2 8 1 1112.45 1106.81 39.03 o 3 8 1 6805.44 6664.96 76.90 o 4 8 1 569.19 635.81 24.07 o 5 8 1 17.29 0.17 14.54 o 6 8 1 436.59 483.69 27.80 o 7 8 1 744.02 775.75 36.67 o 8 8 1 1985.53 1941.13 51.65 o 9 8 1 132.79 107.58 32.03 o 10 8 1 72.34 104.86 35.61 o 11 8 1 20.65 -31.50 35.49 o 12 8 1 7.39 112.14 52.77 o 1 9 1 3489.53 3555.28 49.09 o 2 9 1 8789.77 8276.21 79.11 o 3 9 1 1055.93 1128.13 42.91 o 4 9 1 1239.71 1369.39 34.38 o 5 9 1 406.55 540.87 25.40 o 6 9 1 8.53 -7.94 16.73 o 7 9 1 191.98 172.63 27.02 o 8 9 1 71.76 85.77 25.82 o 9 9 1 140.07 114.56 36.32 o 10 9 1 300.79 328.04 43.92 o 11 9 1 12.07 10.50 33.85 o 12 9 1 2136.86 2168.78 148.95 o 0 10 1 300.69 321.75 29.49 o 1 10 1 176.09 219.05 22.01 o 2 10 1 26172.92 24300.34 149.10 o 3 10 1 154.75 148.68 24.43 o 4 10 1 3398.76 3041.58 62.08 o 5 10 1 424.56 484.70 23.35 o 6 10 1 364.26 420.03 26.42 o 7 10 1 471.41 548.62 33.53 o 8 10 1 1367.15 1475.22 54.88 o 9 10 1 212.12 202.26 36.00 o 10 10 1 50.23 26.84 35.27 o 11 10 1 670.21 699.95 54.58 o 12 10 1 204.36 330.85 54.36 o 1 11 1 2495.09 2360.94 42.28 o 2 11 1 2294.38 2072.52 45.24 o 3 11 1 1118.06 1202.38 53.19 o 4 11 1 78.43 69.14 22.93 o 5 11 1 260.20 297.52 32.84 o 6 11 1 115.88 87.51 19.90 o 7 11 1 865.13 910.50 36.89 o 8 11 1 1151.87 1159.99 52.10 o 9 11 1 244.89 235.22 36.16 o 10 11 1 0.50 -7.65 31.46 o 11 11 1 10.60 77.45 39.41 o 0 12 1 221.89 237.82 53.61 o 1 12 1 666.16 723.27 31.22 o 2 12 1 4920.40 4520.14 63.37 o 3 12 1 2163.10 1952.29 48.50 o 4 12 1 1465.24 1444.70 49.93 o 5 12 1 1.23 1.95 24.61 o 6 12 1 396.42 496.46 35.84 o 7 12 1 5.94 19.80 21.66 o 8 12 1 102.83 85.87 29.49 o 9 12 1 199.67 194.82 35.04 o 10 12 1 235.59 229.23 40.25 o 11 12 1 175.07 122.67 43.48 o 1 13 1 130.71 196.75 22.20 o 2 13 1 65.49 48.25 20.56 o 3 13 1 59.01 116.52 28.01 o 4 13 1 2446.11 2175.89 56.25 o 5 13 1 319.70 347.77 36.90 o 6 13 1 375.56 390.46 49.28 o 7 13 1 1.49 -4.65 36.87 o 8 13 1 8.38 19.95 25.04 o 9 13 1 116.33 120.41 36.16 o 10 13 1 402.17 416.41 43.87 o 11 13 1 6.70 97.36 37.57 o 0 14 1 3302.87 2917.20 121.24 o 1 14 1 1774.81 1575.29 39.01 o 2 14 1 142.91 196.13 26.56 o 3 14 1 2690.54 2145.61 58.13 o 4 14 1 664.37 835.45 47.23 o 5 14 1 783.15 883.52 60.26 o 6 14 1 75.77 112.19 39.85 o 7 14 1 71.87 123.69 41.70 o 8 14 1 58.01 16.70 49.41 o 9 14 1 129.52 142.92 31.39 o 10 14 1 89.11 96.98 44.16 o 1 15 1 5.76 -1.26 20.23 o 2 15 1 1424.61 1237.69 47.06 o 3 15 1 1968.84 1744.50 79.44 o 4 15 1 532.92 537.17 50.88 o 5 15 1 1193.49 1195.29 71.90 o 6 15 1 521.51 674.47 59.98 o 7 15 1 1020.43 983.15 69.51 o 8 15 1 3.37 9.35 46.48 o 9 15 1 113.48 33.81 51.91 o 0 16 1 5967.21 5094.20 237.69 o 1 16 1 15.33 2.48 33.65 o 2 16 1 11.15 -0.75 29.38 o 3 16 1 786.99 856.75 56.57 o 4 16 1 133.50 134.02 36.83 o 5 16 1 46.98 102.49 36.38 o 6 16 1 129.31 196.97 43.88 o 7 16 1 193.46 244.53 57.91 o 8 16 1 0.03 67.40 48.23 o 9 16 1 0.03 61.24 53.43 o 1 17 1 433.53 446.11 85.35 o 2 17 1 795.45 806.02 46.76 o 3 17 1 234.89 207.18 36.32 o 4 17 1 38.05 43.53 33.65 o 5 17 1 71.73 86.98 38.61 o 6 17 1 251.83 199.46 46.55 o 7 17 1 2.49 29.11 48.47 o 8 17 1 41.76 61.20 57.56 o 0 18 1 2.44 58.24 73.86 o 1 18 1 18.02 37.77 67.02 o 2 18 1 6.19 12.93 24.12 o 3 18 1 39.50 57.44 35.02 o 4 18 1 781.93 801.06 55.90 o 5 18 1 705.91 674.63 58.43 o 6 18 1 482.99 411.78 53.75 o 7 18 1 46.51 55.96 53.22 o 1 19 1 40.78 51.31 60.19 o 2 19 1 1.95 -0.12 41.49 o 3 19 1 829.34 753.04 52.40 o 4 19 1 313.61 230.40 39.91 o 5 19 1 65.06 63.65 71.83 o 6 19 1 3.07 -45.22 45.22 o 0 20 1 0.71 -21.73 83.51 o 1 20 1 24.59 -47.28 52.49 o 2 20 1 673.41 546.31 93.48 o 3 20 1 214.16 95.81 42.52 o 4 20 1 292.27 395.56 51.90 o 5 20 1 0.65 66.73 47.80 o 1 21 1 75.00 64.46 63.99 o 2 21 1 984.41 889.26 121.47 o 3 21 1 265.15 278.57 53.52 o 1 0 2 103.66 124.28 13.50 o 2 0 2 16154.83 16198.97 99.10 o 3 0 2 23811.53 22543.48 145.00 o 4 0 2 1963.80 1889.96 42.95 o 5 0 2 2918.19 2922.39 66.01 o 6 0 2 3866.51 4137.11 77.72 o 7 0 2 666.64 849.42 51.70 o 8 0 2 664.44 780.24 50.24 o 9 0 2 738.51 690.82 58.59 o 10 0 2 479.01 458.94 52.09 o 11 0 2 3354.18 3252.51 170.57 o 12 0 2 277.22 234.27 101.92 o 13 0 2 8.60 1.88 62.15 o 1 1 2 2749.22 2444.12 19.42 o 2 1 2 3833.13 3471.94 31.71 o 3 1 2 25385.22 23595.50 102.06 o 4 1 2 3532.19 3314.25 38.83 o 5 1 2 1102.23 1124.06 38.50 o 6 1 2 417.08 560.03 33.36 o 7 1 2 4316.04 4274.66 58.58 o 8 1 2 804.31 922.71 39.47 o 9 1 2 0.00 -0.10 23.25 o 10 1 2 217.44 291.63 33.36 o 11 1 2 283.74 363.99 66.54 o 12 1 2 33.62 61.68 43.18 o 13 1 2 0.02 46.08 45.70 o 0 2 2 5973.45 5335.09 43.89 o 1 2 2 18578.41 17214.52 67.48 o 2 2 2 1591.54 1406.55 22.64 o 3 2 2 6371.21 6032.78 50.95 o 4 2 2 399.76 439.98 26.55 o 5 2 2 9874.90 9446.81 76.27 o 6 2 2 33.78 57.65 21.80 o 7 2 2 10750.61 9771.01 86.61 o 8 2 2 25.05 35.43 20.79 o 9 2 2 48.77 66.71 24.58 o 10 2 2 8780.64 8093.59 106.00 o 11 2 2 3551.84 3369.13 114.62 o 12 2 2 1669.10 1605.31 89.26 o 13 2 2 207.74 113.02 48.87 o 1 3 2 1075.34 942.86 15.98 o 2 3 2 7759.92 6924.93 51.84 o 3 3 2 4008.88 3623.38 38.18 o 4 3 2 1227.86 1221.64 29.57 o 5 3 2 3768.27 3225.03 48.80 o 6 3 2 76.92 92.43 20.79 o 7 3 2 2617.50 2446.58 46.56 o 8 3 2 2298.91 2165.39 48.20 o 9 3 2 598.34 655.18 38.33 o 10 3 2 3798.76 3797.01 76.52 o 11 3 2 43.51 91.80 45.70 o 12 3 2 122.85 146.21 47.08 o 13 3 2 73.18 151.29 48.95 o 0 4 2 374.48 364.24 16.91 o 1 4 2 97808.30 96851.05 374.24 o 2 4 2 6148.50 5823.63 39.71 o 3 4 2 3536.69 3250.47 38.15 o 4 4 2 1534.03 1599.98 31.35 o 5 4 2 4352.26 4597.29 63.85 o 6 4 2 555.11 607.12 38.33 o 7 4 2 478.40 576.98 31.05 o 8 4 2 69.63 98.68 23.34 o 9 4 2 6.17 102.44 27.79 o 10 4 2 491.06 551.33 45.22 o 11 4 2 141.21 146.49 44.35 o 12 4 2 87.20 108.87 45.39 o 13 4 2 40.81 85.84 44.08 o 1 5 2 67243.85 67054.38 242.04 o 2 5 2 32.31 64.51 9.08 o 3 5 2 1034.17 924.82 21.91 o 4 5 2 140.84 149.98 19.92 o 5 5 2 587.14 750.62 31.48 o 6 5 2 191.01 239.81 24.05 o 7 5 2 84.54 56.46 17.56 o 8 5 2 0.27 25.09 20.67 o 9 5 2 1759.01 1832.50 51.83 o 10 5 2 8.97 88.13 37.92 o 11 5 2 667.48 632.15 53.79 o 12 5 2 135.67 163.49 46.99 o 13 5 2 187.41 197.67 52.68 o 0 6 2 2151.16 1986.71 30.08 o 1 6 2 280.16 477.23 22.76 o 2 6 2 400.63 512.15 19.52 o 3 6 2 946.06 1008.31 25.54 o 4 6 2 2069.29 1950.80 39.40 o 5 6 2 331.86 286.39 23.57 o 6 6 2 189.53 220.47 22.13 o 7 6 2 1756.11 1778.98 43.72 o 8 6 2 577.27 683.40 39.83 o 9 6 2 3429.12 2999.82 66.11 o 10 6 2 846.30 930.99 71.10 o 11 6 2 434.02 413.85 48.33 o 12 6 2 292.80 326.43 54.47 o 13 6 2 0.85 95.41 45.76 o 1 7 2 5081.48 4758.67 50.68 o 2 7 2 6.49 -6.28 18.42 o 3 7 2 1695.34 1510.91 28.36 o 4 7 2 0.34 -5.45 15.32 o 5 7 2 1165.90 1126.71 31.97 o 6 7 2 14.82 -0.33 17.11 o 7 7 2 0.44 5.02 18.62 o 8 7 2 208.11 247.06 28.49 o 9 7 2 294.06 284.82 32.26 o 10 7 2 174.07 206.73 41.64 o 11 7 2 1.02 22.08 35.63 o 12 7 2 711.24 633.42 65.74 o 13 7 2 79.21 125.83 47.13 o 0 8 2 10513.05 10256.25 80.60 o 1 8 2 7.60 18.42 18.30 o 2 8 2 3600.78 3582.29 56.52 o 3 8 2 5487.51 5378.24 69.81 o 4 8 2 0.03 -2.46 13.40 o 5 8 2 103.96 87.94 17.54 o 6 8 2 955.69 1063.40 35.27 o 7 8 2 4.69 23.97 20.59 o 8 8 2 2588.53 2455.34 54.25 o 9 8 2 111.26 73.94 31.56 o 10 8 2 1089.17 1176.71 63.27 o 11 8 2 509.50 559.20 53.21 o 12 8 2 77.40 152.75 53.09 o 1 9 2 18541.42 17518.19 112.26 o 2 9 2 2482.16 2278.94 45.14 o 3 9 2 2139.56 2005.66 45.44 o 4 9 2 437.68 550.93 28.33 o 5 9 2 1031.28 989.74 40.04 o 6 9 2 573.89 643.73 30.30 o 7 9 2 1.65 2.10 20.82 o 8 9 2 3690.96 3514.08 61.07 o 9 9 2 0.37 2.81 29.59 o 10 9 2 262.99 267.81 40.58 o 11 9 2 82.95 132.02 39.06 o 12 9 2 2196.13 2153.77 92.82 o 0 10 2 3074.82 3006.75 54.93 o 1 10 2 766.76 900.75 45.19 o 2 10 2 525.86 749.27 34.75 o 3 10 2 120.82 189.69 25.96 o 4 10 2 1891.36 1836.83 47.82 o 5 10 2 119.88 160.70 17.47 o 6 10 2 769.67 843.92 34.75 o 7 10 2 274.07 329.09 29.77 o 8 10 2 245.93 312.20 33.65 o 9 10 2 88.10 33.26 30.66 o 10 10 2 15.20 -10.67 30.88 o 11 10 2 939.13 997.21 94.95 o 12 10 2 70.46 189.73 48.22 o 1 11 2 248.76 289.25 23.59 o 2 11 2 849.35 1117.84 41.65 o 3 11 2 12217.12 11046.18 114.33 o 4 11 2 1.82 -14.75 20.83 o 5 11 2 134.71 119.03 26.87 o 6 11 2 5.94 -2.23 17.04 o 7 11 2 1126.68 1194.07 40.23 o 8 11 2 378.34 422.50 38.44 o 9 11 2 211.52 218.34 39.41 o 10 11 2 399.70 362.93 44.07 o 11 11 2 29.20 50.03 39.51 o 0 12 2 19.89 17.47 24.26 o 1 12 2 181.46 271.70 23.38 o 2 12 2 711.01 737.91 36.84 o 3 12 2 3241.91 3071.77 60.07 o 4 12 2 521.48 609.34 41.25 o 5 12 2 328.19 326.65 34.85 o 6 12 2 606.87 676.05 40.17 o 7 12 2 3134.76 2795.78 53.66 o 8 12 2 25.63 57.71 29.81 o 9 12 2 56.05 57.46 29.56 o 10 12 2 3.98 40.32 33.06 o 11 12 2 117.27 89.43 40.20 o 1 13 2 138.48 169.44 21.85 o 2 13 2 1968.39 1845.52 45.60 o 3 13 2 23.51 29.66 22.62 o 4 13 2 25.87 94.04 26.32 o 5 13 2 4491.39 4056.30 76.55 o 6 13 2 492.36 506.53 56.61 o 7 13 2 1185.40 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o 0 12 3 1039.62 1139.45 96.77 o 1 12 3 20.93 19.95 16.87 o 2 12 3 1029.82 1073.49 44.53 o 3 12 3 5310.98 4654.45 72.30 o 4 12 3 127.44 117.66 28.98 o 5 12 3 1072.56 1121.06 53.38 o 6 12 3 3675.52 3447.38 57.85 o 7 12 3 729.98 760.19 41.83 o 8 12 3 603.38 724.71 44.06 o 9 12 3 151.57 177.42 33.93 o 10 12 3 989.07 1084.00 58.69 o 11 12 3 785.59 669.75 55.79 o 1 13 3 119.49 173.46 22.32 o 2 13 3 159.59 195.18 25.55 o 3 13 3 398.31 407.39 38.23 o 4 13 3 2124.34 1963.52 54.83 o 5 13 3 222.18 272.17 34.80 o 6 13 3 4305.34 3845.47 91.12 o 7 13 3 1471.51 1556.67 56.42 o 8 13 3 902.63 978.18 46.97 o 9 13 3 98.74 123.57 33.91 o 10 13 3 4.76 56.03 33.77 o 11 13 3 183.02 219.63 42.44 o 0 14 3 30.51 118.07 50.49 o 1 14 3 421.69 447.95 29.39 o 2 14 3 0.00 27.60 22.03 o 3 14 3 108.30 115.34 28.62 o 4 14 3 928.79 1089.05 54.23 o 5 14 3 417.62 393.52 46.30 o 6 14 3 343.98 446.53 56.63 o 7 14 3 1191.57 1287.06 76.64 o 8 14 3 239.34 286.90 44.61 o 9 14 3 172.43 161.17 31.57 o 10 14 3 51.14 96.30 35.20 o 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10005.27 82.43 o 7 1 4 3217.61 3192.94 51.86 o 8 1 4 5.05 18.21 20.72 o 9 1 4 2501.36 2503.19 56.24 o 10 1 4 3627.35 3344.49 76.68 o 11 1 4 88.40 116.74 45.94 o 12 1 4 7.97 27.92 42.22 o 13 1 4 4.07 65.89 45.30 o 0 2 4 103.66 96.29 13.16 o 1 2 4 1846.73 1790.39 22.28 o 2 2 4 1201.84 959.36 18.85 o 3 2 4 746.60 689.10 18.45 o 4 2 4 836.94 845.74 24.74 o 5 2 4 2077.96 2171.53 40.77 o 6 2 4 3272.52 3142.84 51.59 o 7 2 4 6403.48 6245.37 69.92 o 8 2 4 156.85 155.10 24.06 o 9 2 4 2575.32 2485.03 55.31 o 10 2 4 771.59 736.52 49.82 o 11 2 4 565.60 507.17 64.81 o 12 2 4 158.85 171.71 49.80 o 13 2 4 215.67 132.10 48.26 o 1 3 4 4.34 4.17 7.94 o 2 3 4 5973.17 5509.05 42.92 o 3 3 4 1667.73 1773.06 29.02 o 4 3 4 0.57 -5.47 11.47 o 5 3 4 16791.01 16985.05 150.92 o 6 3 4 186.76 216.90 24.35 o 7 3 4 2594.24 2715.23 48.76 o 8 3 4 624.64 643.47 34.87 o 9 3 4 173.49 197.80 28.97 o 10 3 4 1426.66 1457.15 63.34 o 11 3 4 3.04 30.34 39.67 o 12 3 4 17.37 81.97 43.99 o 13 3 4 146.24 151.95 49.02 o 0 4 4 1413.69 1253.46 25.74 o 1 4 4 23351.00 23228.51 99.72 o 2 4 4 4382.08 4045.21 36.86 o 3 4 4 288.20 403.96 17.94 o 4 4 4 371.26 377.11 23.57 o 5 4 4 6147.71 6583.61 72.27 o 6 4 4 85.57 75.05 17.91 o 7 4 4 1109.53 1136.37 37.70 o 8 4 4 39.43 45.79 21.23 o 9 4 4 535.21 564.41 36.37 o 10 4 4 20.99 23.85 33.18 o 11 4 4 95.67 218.89 52.11 o 12 4 4 376.03 396.68 58.03 o 13 4 4 12.02 26.15 44.25 o 1 5 4 4.15 87.91 9.65 o 2 5 4 71.54 89.92 11.45 o 3 5 4 4940.54 5078.34 46.64 o 4 5 4 305.13 409.85 25.24 o 5 5 4 281.65 434.11 26.21 o 6 5 4 593.78 643.98 31.23 o 7 5 4 1.32 12.44 15.98 o 8 5 4 0.04 22.52 23.75 o 9 5 4 3289.04 3087.63 63.55 o 10 5 4 45.89 15.03 30.67 o 11 5 4 335.12 365.25 49.74 o 12 5 4 1416.49 1390.32 85.69 o 13 5 4 126.77 193.01 51.70 o 0 6 4 1450.76 1496.16 33.50 o 1 6 4 691.65 793.09 19.02 o 2 6 4 11844.40 11242.50 64.44 o 3 6 4 608.88 725.08 24.84 o 4 6 4 1177.01 1134.25 32.64 o 5 6 4 295.45 358.29 24.30 o 6 6 4 127.23 150.14 21.10 o 7 6 4 1233.55 1268.67 38.77 o 8 6 4 14.22 13.80 21.25 o 9 6 4 2200.77 1901.36 56.41 o 10 6 4 2.54 34.54 32.71 o 11 6 4 175.16 184.92 41.24 o 12 6 4 1993.13 1891.77 103.74 o 13 6 4 152.99 157.11 48.10 o 1 7 4 119.76 139.61 14.50 o 2 7 4 126.71 239.89 16.75 o 3 7 4 3400.09 3190.87 44.77 o 4 7 4 7212.33 7430.71 65.91 o 5 7 4 1583.17 1601.24 35.84 o 6 7 4 500.69 598.34 29.67 o 7 7 4 1806.36 1672.09 45.95 o 8 7 4 61.97 92.90 24.41 o 9 7 4 456.57 507.97 42.44 o 10 7 4 15.84 27.79 35.14 o 11 7 4 730.04 700.01 59.96 o 12 7 4 0.34 81.12 44.62 o 13 7 4 12.53 179.32 48.49 o 0 8 4 9700.93 9775.18 93.21 o 1 8 4 1970.23 1938.48 33.21 o 2 8 4 580.10 696.58 29.59 o 3 8 4 3781.41 3541.33 40.17 o 4 8 4 1858.30 2282.53 37.05 o 5 8 4 462.54 593.11 27.53 o 6 8 4 66.94 122.73 20.15 o 7 8 4 38.50 45.57 23.08 o 8 8 4 2066.19 2026.78 50.66 o 9 8 4 603.58 652.07 48.50 o 10 8 4 121.01 94.64 36.46 o 11 8 4 194.02 218.29 44.26 o 12 8 4 215.09 166.96 54.43 o 1 9 4 1694.89 1696.25 31.26 o 2 9 4 4585.62 4341.01 47.38 o 3 9 4 7523.65 7180.14 67.39 o 4 9 4 8.55 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8 10 360.58 319.74 46.15 o 11 8 10 76.60 97.55 44.09 o 12 8 10 195.40 232.03 55.78 o 1 9 10 568.00 652.93 27.54 o 2 9 10 1145.83 1279.37 33.56 o 3 9 10 1159.18 1147.71 32.32 o 4 9 10 887.16 1097.08 34.30 o 5 9 10 341.04 345.90 26.86 o 6 9 10 149.95 205.14 27.46 o 7 9 10 60.52 83.10 23.86 o 8 9 10 6.31 12.95 26.04 o 9 9 10 54.60 43.76 30.99 o 10 9 10 93.14 110.46 36.64 o 11 9 10 3.34 42.69 46.07 o 0 10 10 22.83 16.44 20.87 o 1 10 10 892.15 1019.33 48.30 o 2 10 10 298.69 332.44 22.32 o 3 10 10 324.82 388.80 24.42 o 4 10 10 45.74 37.01 16.82 o 5 10 10 215.44 186.03 22.05 o 6 10 10 28.50 55.15 22.03 o 7 10 10 207.19 204.95 30.83 o 8 10 10 11.14 35.03 28.90 o 9 10 10 279.65 279.20 39.29 o 10 10 10 253.61 219.98 44.27 o 11 10 10 15.48 57.17 41.77 o 1 11 10 647.02 844.36 37.28 o 2 11 10 494.78 574.03 28.51 o 3 11 10 676.96 833.79 34.62 o 4 11 10 7.57 28.53 18.28 o 5 11 10 83.86 78.07 21.08 o 6 11 10 56.85 30.70 24.62 o 7 11 10 703.99 691.44 40.74 o 8 11 10 210.04 202.53 37.73 o 9 11 10 80.75 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36.28 o 3 1 13 1292.13 1482.48 41.37 o 4 1 13 289.34 302.15 25.16 o 5 1 13 5145.19 4792.87 53.46 o 6 1 13 91.01 108.21 19.40 o 7 1 13 95.88 149.72 25.93 o 8 1 13 12.16 -11.47 21.92 o 9 1 13 25.23 17.16 33.70 o 10 1 13 18.12 33.79 33.62 o 11 1 13 129.88 63.88 37.95 o 12 1 13 62.41 149.73 58.96 o 0 2 13 3052.43 3048.48 52.08 o 1 2 13 2239.12 2618.05 47.82 o 2 2 13 97.44 104.14 20.74 o 3 2 13 1162.49 1281.11 39.22 o 4 2 13 1409.85 1371.85 30.28 o 5 2 13 343.40 418.01 25.94 o 6 2 13 57.75 59.51 18.43 o 7 2 13 62.12 46.92 22.04 o 8 2 13 45.41 66.31 23.93 o 9 2 13 483.52 510.50 45.18 o 10 2 13 1349.53 1201.03 64.63 o 11 2 13 540.96 599.76 54.05 o 12 2 13 611.13 668.05 70.80 o 1 3 13 19254.48 19802.38 103.28 o 2 3 13 13254.30 13785.01 89.59 o 3 3 13 1069.49 1151.67 32.41 o 4 3 13 2626.81 2473.15 39.31 o 5 3 13 217.98 206.94 20.95 o 6 3 13 182.47 198.96 24.53 o 7 3 13 24.90 20.11 20.68 o 8 3 13 433.16 410.61 33.16 o 9 3 13 0.47 12.75 30.93 o 10 3 13 195.84 183.38 39.77 o 11 3 13 187.06 241.52 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13 347.61 331.85 45.70 o 9 9 13 177.87 200.78 35.70 o 10 9 13 228.91 246.78 46.23 o 11 9 13 1.69 0.60 43.97 o 0 10 13 1085.88 1083.72 56.05 o 1 10 13 0.37 36.95 16.65 o 2 10 13 2656.34 2355.85 43.31 o 3 10 13 932.50 1023.71 37.62 o 4 10 13 223.49 254.56 26.34 o 5 10 13 0.47 22.05 21.15 o 6 10 13 84.82 63.01 24.08 o 7 10 13 247.45 259.37 36.46 o 8 10 13 87.03 33.88 34.63 o 9 10 13 161.07 144.48 43.47 o 10 10 13 124.06 122.12 44.36 o 1 11 13 2130.06 1847.63 42.63 o 2 11 13 69.31 95.30 20.11 o 3 11 13 0.01 3.88 20.99 o 4 11 13 1.60 29.74 20.81 o 5 11 13 59.44 79.85 23.89 o 6 11 13 104.44 112.49 27.43 o 7 11 13 28.25 25.87 29.37 o 8 11 13 201.58 156.07 34.31 o 9 11 13 27.69 49.13 50.50 o 10 11 13 1.57 44.09 45.75 o 0 12 13 66.89 108.05 29.32 o 1 12 13 116.42 169.95 23.78 o 2 12 13 606.89 608.62 32.52 o 3 12 13 49.73 57.11 21.40 o 4 12 13 14.97 39.60 24.20 o 5 12 13 3.30 32.85 25.54 o 6 12 13 74.61 120.01 28.86 o 7 12 13 4.56 81.52 28.84 o 8 12 13 138.05 172.01 37.52 o 9 12 13 146.05 178.13 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41.67 o 0 10 21 43.85 45.81 32.58 o 1 10 21 48.12 79.45 24.20 o 2 10 21 4.66 23.21 24.49 o 3 10 21 943.25 1070.75 49.30 o 4 10 21 14.80 42.16 27.13 o 5 10 21 204.99 340.32 39.10 o 6 10 21 697.08 808.78 51.42 o 7 10 21 37.91 106.38 48.32 o 8 10 21 641.67 749.73 60.47 o 1 11 21 1032.37 1247.33 48.12 o 2 11 21 368.62 488.98 36.18 o 3 11 21 93.32 169.77 30.83 o 4 11 21 209.26 269.65 36.79 o 5 11 21 1010.31 1020.48 53.12 o 6 11 21 0.30 106.50 39.31 o 7 11 21 103.72 131.38 44.17 o 0 12 21 3432.34 3256.55 120.80 o 1 12 21 133.81 198.36 32.00 o 2 12 21 2820.65 2415.93 61.45 o 3 12 21 20.02 87.36 31.77 o 4 12 21 523.23 800.48 61.14 o 5 12 21 395.34 568.92 47.35 o 6 12 21 202.88 317.98 43.94 o 7 12 21 262.85 359.43 77.77 o 1 13 21 55.29 123.76 31.91 o 2 13 21 613.68 693.97 52.83 o 3 13 21 33.15 117.30 56.51 o 4 13 21 0.04 52.93 37.18 o 5 13 21 12.92 129.38 37.04 o 6 13 21 84.97 161.10 49.92 o 0 14 21 2676.17 2314.54 104.07 o 1 14 21 1136.23 1261.27 58.01 o 2 14 21 17.85 52.68 38.86 o 3 14 21 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46.34 o 4 2 22 5432.54 4528.62 98.86 o 5 2 22 3246.98 2741.00 88.15 o 6 2 22 83.35 112.89 41.91 o 7 2 22 810.87 806.92 68.31 o 8 2 22 36.29 73.29 58.80 o 9 2 22 85.08 121.29 62.68 o 10 2 22 143.36 150.35 48.96 o 1 3 22 274.91 340.61 34.61 o 2 3 22 88.29 125.86 26.77 o 3 3 22 789.79 842.77 53.14 o 4 3 22 2925.06 2582.67 81.90 o 5 3 22 63.91 116.12 40.23 o 6 3 22 3269.12 2934.22 97.50 o 7 3 22 224.06 230.55 56.25 o 8 3 22 679.54 736.26 86.24 o 9 3 22 159.56 223.66 60.65 o 0 4 22 67.71 89.50 41.94 o 1 4 22 43.69 105.90 26.21 o 2 4 22 671.98 685.79 50.94 o 3 4 22 477.19 523.79 44.06 o 4 4 22 389.75 505.92 53.33 o 5 4 22 749.56 750.18 61.88 o 6 4 22 1113.97 1073.93 77.57 o 7 4 22 133.76 203.78 61.40 o 8 4 22 20.55 78.07 57.70 o 9 4 22 2.52 27.15 43.80 o 1 5 22 997.68 982.54 48.67 o 2 5 22 1360.08 1568.32 63.44 o 3 5 22 1980.93 1970.11 65.22 o 4 5 22 305.72 400.73 47.12 o 5 5 22 2288.79 2076.47 90.63 o 6 5 22 85.48 36.33 48.07 o 7 5 22 127.19 224.77 71.23 o 8 5 22 259.22 254.58 60.59 o 9 5 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60.11 o 1 15 22 62.20 147.53 41.84 o 2 15 22 34.93 184.88 46.83 o 3 15 22 115.44 335.85 53.99 o 1 1 23 162.23 148.40 25.86 o 2 1 23 527.65 555.72 48.30 o 3 1 23 107.18 133.62 37.06 o 4 1 23 1687.26 1475.77 70.30 o 5 1 23 131.81 175.90 49.97 o 6 1 23 57.29 142.27 44.62 o 7 1 23 316.43 251.13 58.84 o 8 1 23 22.82 52.08 49.52 o 9 1 23 202.94 252.49 68.73 o 0 2 23 49.57 74.73 72.37 o 1 2 23 67.91 40.87 25.23 o 2 2 23 204.36 189.49 35.06 o 3 2 23 304.84 263.12 42.73 o 4 2 23 629.03 618.91 58.10 o 5 2 23 216.76 233.81 43.99 o 6 2 23 1127.76 1184.48 73.78 o 7 2 23 45.37 46.65 49.63 o 8 2 23 341.56 274.04 62.72 o 9 2 23 175.45 170.76 76.92 o 1 3 23 416.44 380.29 35.18 o 2 3 23 187.38 179.39 34.00 o 3 3 23 154.65 120.38 45.34 o 4 3 23 55.77 81.55 37.91 o 5 3 23 192.66 168.67 43.50 o 6 3 23 993.45 982.33 71.03 o 7 3 23 436.58 327.85 63.18 o 8 3 23 215.01 213.99 67.43 o 9 3 23 35.16 16.67 58.16 o 0 4 23 4.91 32.34 39.19 o 1 4 23 14.62 28.01 28.19 o 2 4 23 1522.90 1499.76 67.95 o 3 4 23 503.65 627.12 55.27 o 4 4 23 0.24 61.61 40.49 o 5 4 23 44.53 45.67 39.68 o 6 4 23 27.92 47.76 40.80 o 7 4 23 0.24 49.39 50.44 o 8 4 23 184.97 162.97 64.14 o 9 4 23 26.79 -18.03 57.95 o 1 5 23 629.03 538.03 50.50 o 2 5 23 1626.83 1506.73 75.94 o 3 5 23 77.30 85.84 39.09 o 4 5 23 386.15 406.09 60.34 o 5 5 23 24.83 40.19 41.63 o 6 5 23 6.83 -38.00 38.00 o 7 5 23 276.66 280.03 63.13 o 8 5 23 34.86 122.10 61.87 o 9 5 23 10.79 41.37 73.34 o 0 6 23 3711.63 3176.47 74.62 o 1 6 23 144.67 176.97 29.95 o 2 6 23 71.85 64.93 33.68 o 3 6 23 135.58 161.87 42.94 o 4 6 23 856.71 918.89 77.21 o 5 6 23 231.66 244.20 50.49 o 6 6 23 642.47 715.65 70.89 o 7 6 23 578.30 449.70 66.33 o 8 6 23 0.84 33.26 59.28 o 1 7 23 59.73 131.81 27.13 o 2 7 23 193.83 270.45 35.27 o 3 7 23 289.85 428.09 43.20 o 4 7 23 41.02 30.77 45.78 o 5 7 23 1143.01 1196.11 84.70 o 6 7 23 25.13 -45.99 45.99 o 7 7 23 39.15 102.35 43.34 o 8 7 23 1330.11 1171.41 103.75 o 0 8 23 1924.71 1755.93 75.42 o 1 8 23 166.07 221.99 30.32 o 2 8 23 21.49 92.25 30.82 o 3 8 23 78.34 105.45 30.79 o 4 8 23 7.89 -25.54 29.75 o 5 8 23 780.35 781.99 72.89 o 6 8 23 203.71 172.94 48.27 o 7 8 23 348.02 451.75 67.90 o 8 8 23 1784.38 1814.07 119.85 o 1 9 23 690.93 848.95 45.38 o 2 9 23 283.55 389.78 36.91 o 3 9 23 7.65 64.95 37.85 o 4 9 23 371.19 419.69 44.69 o 5 9 23 28.19 37.11 40.01 o 6 9 23 53.83 65.74 42.34 o 7 9 23 183.97 380.64 54.99 o 0 10 23 1081.23 1084.17 78.29 o 1 10 23 776.93 922.52 50.15 o 2 10 23 127.32 226.31 36.60 o 3 10 23 817.69 1006.59 63.06 o 4 10 23 293.55 329.82 48.93 o 5 10 23 481.14 555.33 62.91 o 6 10 23 13.63 30.22 46.22 o 7 10 23 25.01 103.99 43.42 o 1 11 23 438.63 425.55 43.10 o 2 11 23 611.11 672.59 45.36 o 3 11 23 2.49 50.01 29.44 o 4 11 23 221.01 287.27 65.51 o 5 11 23 340.53 398.05 45.59 o 6 11 23 9.59 41.32 50.17 o 0 12 23 1197.82 1054.17 85.76 o 1 12 23 15.59 113.05 53.68 o 2 12 23 269.50 369.68 40.68 o 3 12 23 70.10 4.18 45.17 o 4 12 23 1.42 117.13 50.07 o 5 12 23 28.93 79.07 41.55 o 1 13 23 84.58 201.23 36.52 o 2 13 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