#------------------------------------------------------------------------------ #$Date: 2022-01-29 05:00:37 +0200 (Sat, 29 Jan 2022) $ #$Revision: 272343 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/40/2244021.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244021 _cell_angle_alpha 90.000 _cell_angle_beta 96.323 _cell_angle_gamma 90.000 _cell_length_a 18.2782 _cell_length_b 19.1455 _cell_length_c 24.6978 _exptl_crystal_F_000 3584.00 _reflns_d_resolution_high 0.7991 _cod_data_source_file wm5633Isup2.hkl _cod_data_source_block I _shelx_title ' SKM285_0m_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 566.99 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 47822.69 42738.65 1388.18 o 4 0 0 25091.45 23087.54 677.17 o 6 0 0 1714.39 1803.99 53.25 o 8 0 0 40.34 67.10 14.82 o 10 0 0 1363.83 1483.96 114.98 o 12 0 0 7.60 -2.07 14.86 o 14 0 0 4831.44 4953.60 96.69 o 16 0 0 8990.17 9652.07 177.64 o 18 0 0 2970.31 3212.71 79.68 o 20 0 0 139.12 161.21 20.94 o 22 0 0 323.49 286.92 21.42 o 1 1 0 2646.74 2489.46 63.06 o 2 1 0 121.82 99.23 10.48 o 3 1 0 2320.21 2130.55 39.00 o 4 1 0 247.22 355.81 11.48 o 5 1 0 11308.44 10624.08 179.44 o 6 1 0 383.79 409.26 15.86 o 7 1 0 1082.49 1081.96 32.98 o 8 1 0 5812.63 6237.21 114.36 o 9 1 0 311.06 199.94 22.30 o 10 1 0 1756.08 1684.06 63.14 o 11 1 0 534.81 423.76 27.20 o 12 1 0 125.20 63.12 9.67 o 13 1 0 29.29 28.03 9.84 o 14 1 0 878.75 933.12 23.23 o 15 1 0 1414.21 1420.89 30.78 o 16 1 0 2175.23 2147.07 39.56 o 17 1 0 22.88 24.15 10.15 o 18 1 0 228.36 193.33 17.71 o 19 1 0 670.99 705.18 22.26 o 20 1 0 10.09 21.34 7.80 o 21 1 0 40.18 48.99 8.95 o 22 1 0 140.81 115.24 15.95 o 0 2 0 28253.31 29176.79 904.04 o 1 2 0 2334.34 2364.36 58.89 o 2 2 0 5404.27 5616.03 94.69 o 3 2 0 49314.22 49240.39 801.98 o 4 2 0 254604.09 246439.83 8121.92 o 5 2 0 43464.51 45479.42 807.06 o 6 2 0 29439.84 30126.28 603.71 o 7 2 0 36081.99 36144.42 689.66 o 8 2 0 5905.78 6222.30 114.80 o 9 2 0 3876.20 3680.85 77.63 o 10 2 0 4289.25 3994.72 88.84 o 11 2 0 7.90 7.68 10.41 o 12 2 0 23.57 59.86 9.54 o 13 2 0 1434.60 1374.59 27.72 o 14 2 0 8.76 16.92 11.50 o 15 2 0 149.85 140.33 13.15 o 16 2 0 4583.77 4710.40 71.04 o 17 2 0 3658.31 3804.02 59.65 o 18 2 0 2276.43 2549.70 47.27 o 19 2 0 594.61 570.25 20.87 o 20 2 0 198.57 192.84 13.75 o 21 2 0 1.58 14.32 6.89 o 22 2 0 57.97 29.25 6.31 o 1 3 0 9738.49 9050.54 175.84 o 2 3 0 1430.38 1363.83 48.40 o 3 3 0 26.42 24.57 7.06 o 4 3 0 15571.54 14586.32 244.27 o 5 3 0 1634.81 1582.56 34.45 o 6 3 0 4011.67 3831.32 72.29 o 7 3 0 2108.71 2009.93 45.36 o 8 3 0 29794.35 30532.35 657.40 o 9 3 0 1174.28 1051.69 39.05 o 10 3 0 4424.62 4499.70 127.30 o 11 3 0 2249.65 2140.19 37.52 o 12 3 0 1818.50 1662.88 32.96 o 13 3 0 17.35 10.02 9.37 o 14 3 0 191.12 156.45 24.64 o 15 3 0 105.59 96.83 10.81 o 16 3 0 1863.72 1926.18 39.71 o 17 3 0 50.29 33.75 8.68 o 18 3 0 463.28 594.58 21.27 o 19 3 0 116.20 118.14 12.08 o 20 3 0 311.91 315.13 16.26 o 21 3 0 169.55 140.16 13.43 o 22 3 0 18.01 -2.59 6.09 o 0 4 0 57427.99 60347.66 1966.43 o 1 4 0 33852.10 34769.71 752.96 o 2 4 0 268963.34 240452.77 11423.91 o 3 4 0 100690.23 108560.71 2500.07 o 4 4 0 41208.80 40569.05 768.35 o 5 4 0 314.65 314.36 31.21 o 6 4 0 14795.96 14158.31 578.72 o 7 4 0 18541.98 18728.91 365.77 o 8 4 0 89.14 106.74 15.48 o 9 4 0 23.23 26.51 18.02 o 10 4 0 6275.54 6042.90 176.33 o 11 4 0 1341.29 1163.51 28.37 o 12 4 0 3462.04 3244.92 52.08 o 13 4 0 10923.56 10541.86 140.72 o 14 4 0 23.81 26.74 9.78 o 15 4 0 4.51 14.12 9.06 o 16 4 0 165.37 145.80 14.06 o 17 4 0 2299.17 2673.30 45.41 o 18 4 0 2969.88 3249.31 49.54 o 19 4 0 179.16 184.09 17.12 o 20 4 0 22.86 16.77 8.60 o 21 4 0 292.03 317.93 21.01 o 22 4 0 88.82 79.14 11.56 o 1 5 0 12850.13 12637.06 245.76 o 2 5 0 16397.74 15929.31 269.39 o 3 5 0 5856.12 5913.64 124.50 o 4 5 0 155.24 152.35 18.43 o 5 5 0 1140.41 1115.45 33.24 o 6 5 0 1952.91 1958.04 51.07 o 7 5 0 5605.19 6123.70 131.64 o 8 5 0 779.64 839.44 39.74 o 9 5 0 2247.54 2113.49 68.50 o 10 5 0 1520.99 1442.38 45.74 o 11 5 0 551.80 516.65 22.87 o 12 5 0 671.86 825.58 25.32 o 13 5 0 6.99 13.90 9.85 o 14 5 0 0.28 -8.30 11.19 o 15 5 0 1124.35 1172.88 38.80 o 16 5 0 622.34 713.24 32.73 o 17 5 0 1491.27 1548.08 31.20 o 18 5 0 410.30 386.53 36.64 o 19 5 0 0.08 15.50 8.06 o 20 5 0 1025.22 1017.49 26.15 o 21 5 0 48.44 52.55 9.49 o 22 5 0 82.70 89.14 10.87 o 0 6 0 71548.40 71991.66 2354.28 o 1 6 0 3845.29 3366.17 83.33 o 2 6 0 1073.74 1042.62 26.93 o 3 6 0 48818.75 50848.47 834.72 o 4 6 0 12989.53 12981.83 256.27 o 5 6 0 1696.50 1773.20 48.26 o 6 6 0 21491.18 22838.83 444.01 o 7 6 0 1440.33 1298.69 45.68 o 8 6 0 14394.49 14519.57 299.80 o 9 6 0 2008.70 2005.34 75.60 o 10 6 0 2464.55 2179.24 42.53 o 11 6 0 75.13 95.00 13.82 o 12 6 0 230.59 285.56 20.01 o 13 6 0 947.84 938.38 41.85 o 14 6 0 1607.13 1693.25 36.63 o 15 6 0 462.01 494.36 20.03 o 16 6 0 2792.12 2893.88 48.45 o 17 6 0 177.16 222.54 17.69 o 18 6 0 324.80 336.75 19.35 o 19 6 0 648.80 660.70 20.31 o 20 6 0 210.50 189.41 15.85 o 21 6 0 307.67 348.97 15.95 o 1 7 0 1568.43 1793.29 58.82 o 2 7 0 4600.69 4262.53 87.68 o 3 7 0 14553.45 14244.63 244.37 o 4 7 0 5341.60 5365.67 101.80 o 5 7 0 78.71 69.91 18.09 o 6 7 0 246.84 190.70 30.98 o 7 7 0 2551.57 2721.39 114.69 o 8 7 0 3165.58 3030.47 109.94 o 9 7 0 878.12 834.50 30.66 o 10 7 0 235.93 208.06 20.40 o 11 7 0 859.06 804.88 24.28 o 12 7 0 186.91 227.26 16.30 o 13 7 0 2088.96 2201.43 40.09 o 14 7 0 59.62 21.66 10.04 o 15 7 0 1495.24 1572.40 36.12 o 16 7 0 43.57 15.80 9.30 o 17 7 0 537.73 487.21 22.93 o 18 7 0 241.22 258.87 17.15 o 19 7 0 107.17 161.66 13.97 o 20 7 0 1039.13 1099.20 28.18 o 21 7 0 14.49 2.77 7.82 o 0 8 0 8183.01 8658.20 215.20 o 1 8 0 143.41 138.05 20.39 o 2 8 0 63.02 45.19 14.90 o 3 8 0 6917.93 7488.10 110.58 o 4 8 0 2662.65 2558.74 45.95 o 5 8 0 4803.31 4376.97 76.59 o 6 8 0 11469.94 11916.15 211.94 o 7 8 0 465.77 394.76 64.73 o 8 8 0 342.91 318.62 25.33 o 9 8 0 166.74 142.63 19.06 o 10 8 0 2.77 26.57 11.27 o 11 8 0 4142.36 4227.49 74.97 o 12 8 0 2415.49 2341.90 70.26 o 13 8 0 18.49 29.14 10.22 o 14 8 0 544.90 561.20 31.04 o 15 8 0 54.75 56.38 11.55 o 16 8 0 2230.71 2509.43 51.03 o 17 8 0 321.46 219.82 21.73 o 18 8 0 28.73 18.76 8.42 o 19 8 0 1018.60 1114.17 26.63 o 20 8 0 73.28 65.04 15.68 o 21 8 0 141.72 173.31 13.98 o 1 9 0 5096.28 5503.89 103.04 o 2 9 0 4981.96 4869.07 84.48 o 3 9 0 21.18 122.05 25.99 o 4 9 0 92.90 93.53 13.31 o 5 9 0 6622.37 6591.11 133.52 o 6 9 0 945.44 906.07 32.24 o 7 9 0 6.31 29.51 13.58 o 8 9 0 785.49 807.52 30.03 o 9 9 0 301.64 328.33 23.43 o 10 9 0 1244.13 1197.83 37.06 o 11 9 0 4642.95 4456.53 78.92 o 12 9 0 1212.28 1133.72 33.96 o 13 9 0 191.56 219.88 18.19 o 14 9 0 488.25 499.04 23.22 o 15 9 0 1059.66 1079.30 30.20 o 16 9 0 1159.74 1167.68 30.53 o 17 9 0 228.94 236.95 17.97 o 18 9 0 39.89 27.97 7.37 o 19 9 0 70.83 79.72 10.00 o 20 9 0 96.66 62.87 11.21 o 21 9 0 18.48 72.38 19.42 o 0 10 0 28022.63 30895.01 1020.05 o 1 10 0 2908.19 3137.66 116.44 o 2 10 0 757.31 883.02 45.89 o 3 10 0 40.92 41.15 21.77 o 4 10 0 599.63 655.26 43.26 o 5 10 0 14136.19 13888.24 278.74 o 6 10 0 1650.35 1347.98 33.97 o 7 10 0 867.55 1020.74 27.21 o 8 10 0 1225.79 1043.64 33.46 o 9 10 0 5.32 5.44 19.15 o 10 10 0 657.71 684.65 27.07 o 11 10 0 929.54 1019.13 34.49 o 12 10 0 2950.81 2929.62 79.53 o 13 10 0 17.41 30.39 12.52 o 14 10 0 256.47 262.02 18.34 o 15 10 0 3.89 -10.57 10.57 o 16 10 0 86.89 71.93 13.33 o 17 10 0 26.92 12.43 8.05 o 18 10 0 8.08 -3.70 7.33 o 19 10 0 426.24 426.39 15.35 o 20 10 0 108.26 130.41 14.92 o 1 11 0 1.85 8.83 21.64 o 2 11 0 136.40 175.50 26.80 o 3 11 0 370.91 240.34 23.17 o 4 11 0 807.04 1044.95 34.39 o 5 11 0 2082.34 2262.41 66.40 o 6 11 0 9907.78 10124.64 157.22 o 7 11 0 562.36 510.32 27.49 o 8 11 0 1531.07 1374.33 34.47 o 9 11 0 1184.74 1156.87 31.35 o 10 11 0 457.96 552.93 39.29 o 11 11 0 11.48 10.28 10.27 o 12 11 0 1020.81 965.46 28.43 o 13 11 0 0.87 9.94 9.81 o 14 11 0 0.21 14.15 9.41 o 15 11 0 747.64 760.56 24.67 o 16 11 0 957.66 988.20 26.51 o 17 11 0 0.37 -4.16 7.44 o 18 11 0 144.55 150.02 15.20 o 19 11 0 98.09 74.36 12.87 o 20 11 0 171.60 176.58 19.56 o 0 12 0 4243.25 4335.37 116.76 o 1 12 0 1486.25 1619.77 38.88 o 2 12 0 1316.66 1237.47 38.17 o 3 12 0 429.01 431.36 26.01 o 4 12 0 3021.43 3216.12 55.31 o 5 12 0 5207.04 5208.15 86.78 o 6 12 0 5404.28 5345.56 88.84 o 7 12 0 2677.23 2913.69 60.82 o 8 12 0 4627.69 4410.64 77.04 o 9 12 0 2962.91 2912.36 62.61 o 10 12 0 537.26 408.33 21.90 o 11 12 0 1252.43 1313.82 33.27 o 12 12 0 6.68 22.10 9.95 o 13 12 0 978.47 1062.14 29.12 o 14 12 0 396.23 423.29 20.39 o 15 12 0 1940.61 1930.41 40.54 o 16 12 0 18.95 1.24 8.04 o 17 12 0 71.59 73.99 9.73 o 18 12 0 67.44 12.36 7.06 o 19 12 0 167.90 199.79 13.51 o 1 13 0 577.42 424.24 17.99 o 2 13 0 1095.70 993.64 24.74 o 3 13 0 366.59 310.89 17.06 o 4 13 0 1830.37 1903.59 36.32 o 5 13 0 438.24 406.41 20.43 o 6 13 0 1906.98 1985.76 41.26 o 7 13 0 155.29 141.47 22.47 o 8 13 0 2147.63 2300.79 51.51 o 9 13 0 299.72 366.84 25.80 o 10 13 0 4231.26 4316.13 76.08 o 11 13 0 543.51 557.97 23.33 o 12 13 0 1601.09 1585.19 36.76 o 13 13 0 63.83 55.74 10.35 o 14 13 0 2.81 25.66 16.04 o 15 13 0 11.08 6.02 8.51 o 16 13 0 8.38 -1.74 7.28 o 17 13 0 0.37 -7.00 7.00 o 18 13 0 0.02 8.27 7.52 o 19 13 0 216.22 305.54 28.26 o 0 14 0 236.12 275.29 23.36 o 1 14 0 94.35 129.51 15.25 o 2 14 0 1857.91 1909.03 37.27 o 3 14 0 9.52 9.70 8.53 o 4 14 0 46.70 43.29 9.62 o 5 14 0 3747.00 3978.79 118.28 o 6 14 0 27.34 63.61 16.66 o 7 14 0 532.83 594.59 25.05 o 8 14 0 577.02 597.60 26.37 o 9 14 0 259.87 264.84 27.72 o 10 14 0 49.00 54.56 10.26 o 11 14 0 647.65 615.49 23.59 o 12 14 0 192.01 236.25 18.35 o 13 14 0 130.27 193.07 22.64 o 14 14 0 66.17 56.81 11.86 o 15 14 0 12.99 13.58 7.65 o 16 14 0 194.37 159.55 14.52 o 17 14 0 390.29 359.30 16.39 o 18 14 0 178.13 220.26 22.78 o 1 15 0 165.12 132.14 12.58 o 2 15 0 290.18 285.30 22.17 o 3 15 0 2234.27 2239.81 50.65 o 4 15 0 81.31 65.46 11.19 o 5 15 0 2906.31 2967.16 61.74 o 6 15 0 2140.54 2092.43 47.75 o 7 15 0 1774.11 1694.85 42.87 o 8 15 0 2235.35 2247.46 46.36 o 9 15 0 3610.62 3773.89 67.90 o 10 15 0 1094.99 1147.86 36.23 o 11 15 0 124.48 110.77 14.66 o 12 15 0 261.06 270.64 23.62 o 13 15 0 27.64 24.97 8.40 o 14 15 0 326.71 375.24 19.44 o 15 15 0 25.97 28.58 8.45 o 16 15 0 29.03 25.89 8.03 o 17 15 0 31.35 22.95 8.15 o 0 16 0 928.13 994.54 43.74 o 1 16 0 142.98 168.93 20.12 o 2 16 0 496.74 515.26 24.01 o 3 16 0 1.17 -6.94 12.48 o 4 16 0 867.85 879.52 29.75 o 5 16 0 25.89 21.73 10.54 o 6 16 0 4.79 11.81 10.69 o 7 16 0 202.10 248.55 20.32 o 8 16 0 1203.67 1339.84 32.70 o 9 16 0 282.08 343.17 19.90 o 10 16 0 1095.96 1193.61 37.38 o 11 16 0 122.29 150.12 21.55 o 12 16 0 834.50 741.27 24.04 o 13 16 0 327.36 349.62 22.18 o 14 16 0 30.88 30.25 8.03 o 15 16 0 71.21 33.86 7.77 o 16 16 0 10.58 11.23 7.77 o 1 17 0 99.01 91.22 13.09 o 2 17 0 1715.44 1708.47 42.31 o 3 17 0 472.71 425.86 25.04 o 4 17 0 24.38 21.44 10.90 o 5 17 0 270.70 292.07 35.94 o 6 17 0 24.21 35.01 11.64 o 7 17 0 38.31 21.85 9.26 o 8 17 0 101.59 149.48 16.89 o 9 17 0 509.81 515.38 26.68 o 10 17 0 192.54 211.46 18.27 o 11 17 0 3.66 2.43 8.43 o 12 17 0 100.35 95.80 16.25 o 13 17 0 10.15 11.88 8.45 o 14 17 0 709.25 765.87 49.31 o 15 17 0 316.15 326.55 15.23 o 16 17 0 7.23 -5.30 14.12 o 0 18 0 80.83 140.24 27.36 o 1 18 0 8.65 7.75 10.12 o 2 18 0 2.14 -10.01 10.01 o 3 18 0 902.57 899.96 28.47 o 4 18 0 1576.06 1685.63 51.05 o 5 18 0 61.03 49.20 9.93 o 6 18 0 886.12 919.36 29.82 o 7 18 0 38.81 25.28 9.73 o 8 18 0 426.80 389.17 20.84 o 9 18 0 121.26 142.11 15.44 o 10 18 0 288.00 288.33 20.25 o 11 18 0 71.12 109.22 15.22 o 12 18 0 3.70 -0.64 7.77 o 13 18 0 23.96 31.31 8.03 o 14 18 0 342.67 357.95 28.04 o 15 18 0 5.43 -12.36 12.36 o 1 19 0 542.29 655.19 33.40 o 2 19 0 180.15 206.47 25.00 o 3 19 0 1.16 -0.76 13.55 o 4 19 0 122.45 161.17 18.71 o 5 19 0 0.73 -11.59 11.59 o 6 19 0 740.67 781.10 22.79 o 7 19 0 240.27 268.47 17.39 o 8 19 0 226.39 226.15 17.62 o 9 19 0 414.77 432.37 22.88 o 10 19 0 928.91 953.77 33.21 o 11 19 0 1058.27 1004.03 56.25 o 12 19 0 1.67 23.30 8.98 o 13 19 0 140.15 117.12 17.66 o 0 20 0 280.22 246.65 27.39 o 1 20 0 637.88 723.57 24.73 o 2 20 0 213.18 235.31 16.83 o 3 20 0 178.01 166.86 19.69 o 4 20 0 162.52 117.54 12.24 o 5 20 0 0.42 -9.85 9.85 o 6 20 0 95.67 148.78 19.62 o 7 20 0 22.67 17.46 7.77 o 8 20 0 475.62 551.72 21.69 o 9 20 0 260.66 252.37 16.75 o 10 20 0 1.75 -5.43 7.83 o 11 20 0 2.35 2.47 9.30 o 12 20 0 210.65 209.37 16.23 o 1 21 0 47.39 35.39 11.48 o 2 21 0 23.74 7.83 13.67 o 3 21 0 21.96 22.08 10.15 o 4 21 0 251.62 234.06 15.45 o 5 21 0 25.80 27.92 8.07 o 6 21 0 49.96 61.71 15.53 o 7 21 0 100.17 71.35 15.01 o 8 21 0 28.53 28.49 10.59 o 9 21 0 93.06 119.47 19.08 o 10 21 0 96.96 91.56 24.72 o 0 22 0 138.45 131.75 20.57 o 1 22 0 99.62 90.16 11.59 o 2 22 0 114.50 137.44 17.08 o 3 22 0 203.73 219.99 15.80 o 4 22 0 84.75 72.46 13.25 o 5 22 0 76.45 59.54 10.67 o 6 22 0 7.71 -8.04 8.04 o 7 22 0 15.95 4.48 8.04 o 8 22 0 101.20 33.55 12.36 o 9 22 0 2.39 2.04 15.00 o 1 23 0 37.52 68.21 11.75 o 3 23 0 299.70 314.87 16.24 o 4 23 0 2.02 10.59 7.49 o 6 23 0 95.66 101.42 13.73 o -21 0 1 1040.41 1063.89 39.35 o -19 0 1 0.03 2.65 12.81 o -17 0 1 793.74 769.85 35.91 o -15 0 1 4331.57 4322.26 87.29 o -13 0 1 13744.83 13061.39 226.69 o -11 0 1 6128.90 7901.38 514.78 o -9 0 1 7727.27 8039.40 204.77 o -7 0 1 6456.32 7021.95 174.53 o -5 0 1 33276.59 31770.34 735.72 o -3 0 1 91918.27 75606.95 2453.78 o 1 0 1 29585.97 29985.59 977.45 o 3 0 1 57155.04 60053.83 1955.39 o 5 0 1 3015.90 2911.21 78.65 o 7 0 1 9275.32 9046.62 224.39 o 9 0 1 137.96 105.36 32.66 o 11 0 1 2576.74 2491.68 58.51 o 13 0 1 1902.61 1832.42 46.02 o 15 0 1 2928.80 2837.04 62.96 o 17 0 1 1931.91 2088.01 60.94 o 19 0 1 64.03 47.50 12.15 o 21 0 1 858.39 762.96 35.13 o -22 1 1 22.88 16.62 8.55 o -21 1 1 3.53 0.11 7.11 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