#------------------------------------------------------------------------------ #$Date: 2022-04-13 05:00:04 +0300 (Wed, 13 Apr 2022) $ #$Revision: 274505 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/40/2244071.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244071 _cell_angle_alpha 67.018 _cell_angle_beta 77.677 _cell_angle_gamma 84.220 _cell_length_a 8.7856 _cell_length_b 13.1738 _cell_length_c 14.0096 _exptl_crystal_F_000 720.00 _reflns_d_resolution_high 0.7826 _cod_data_source_file wm5639Isup2.hkl _cod_data_source_block I _shelx_title ' [SbS4]2 [Zn(cylam)]3 * 2 H2O * 2 MeCN at 200 K in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.56 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2693.01 3140.31 66.27 o 2 0 0 6798.03 6835.85 273.69 o 3 0 0 795.74 740.77 26.15 o 4 0 0 7606.74 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