#------------------------------------------------------------------------------ #$Date: 2022-11-11 05:06:44 +0200 (Fri, 11 Nov 2022) $ #$Revision: 279232 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/42/2244218.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244218 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.8413 _cell_length_b 15.9517 _cell_length_c 18.5099 _exptl_crystal_F_000 1008.00 _reflns_d_resolution_high 0.7675 _cod_data_source_file yk2177Isup2.hkl _cod_data_source_block I _shelx_title ' pure_disulfide_0m_a_a.res in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.36 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13346.24 14278.64 105.35 o 4 0 0 15822.73 17098.16 123.87 o 6 0 0 15313.86 15662.28 190.85 o 8 0 0 4569.66 4749.21 99.34 o 10 0 0 1415.23 1385.73 75.88 o 2 1 0 30826.40 32569.77 159.28 o 4 1 0 991.55 958.05 21.23 o 6 1 0 4665.85 4896.49 62.02 o 8 1 0 782.99 827.36 37.75 o 10 1 0 156.24 149.82 31.12 o 0 2 0 8162.21 7673.60 149.30 o 2 2 0 2839.80 3109.32 24.55 o 4 2 0 360.70 342.86 13.66 o 6 2 0 939.64 862.10 33.52 o 8 2 0 145.71 133.81 25.28 o 10 2 0 62.79 40.68 31.31 o 2 3 0 3150.98 3684.65 30.83 o 4 3 0 2712.50 3073.72 44.56 o 6 3 0 524.40 429.47 22.48 o 8 3 0 390.84 414.02 30.30 o 10 3 0 387.92 334.88 35.39 o 0 4 0 4299.27 4132.45 40.13 o 2 4 0 6627.35 6755.41 40.13 o 4 4 0 232.66 312.52 13.42 o 6 4 0 449.92 458.07 22.83 o 8 4 0 18.13 47.96 23.61 o 10 4 0 22.75 70.50 46.59 o 2 5 0 15392.56 15751.89 81.15 o 4 5 0 5702.61 6237.42 54.87 o 6 5 0 9053.11 9232.31 84.21 o 8 5 0 610.23 656.40 34.59 o 0 6 0 42997.74 43897.36 304.09 o 2 6 0 3011.74 3039.13 27.90 o 4 6 0 739.83 796.17 20.40 o 6 6 0 8707.64 8116.28 78.55 o 8 6 0 3422.04 3274.49 59.76 o 2 7 0 52.56 95.59 17.17 o 4 7 0 351.55 354.73 17.50 o 6 7 0 1271.97 1275.37 30.27 o 8 7 0 7.13 21.00 23.64 o 0 8 0 724.21 1296.94 31.27 o 2 8 0 399.32 495.98 17.06 o 4 8 0 294.27 313.85 14.66 o 6 8 0 598.97 594.98 22.76 o 8 8 0 31.87 49.63 22.76 o 2 9 0 367.98 465.71 16.35 o 4 9 0 1814.49 1682.67 28.62 o 6 9 0 107.64 99.85 15.60 o 8 9 0 2083.09 1913.71 47.47 o 0 10 0 15552.45 15588.30 157.24 o 2 10 0 1992.47 1906.03 31.44 o 4 10 0 5414.99 5119.46 50.52 o 6 10 0 90.02 104.21 15.07 o 8 10 0 164.19 156.96 23.70 o 2 11 0 3221.88 3285.29 47.28 o 4 11 0 2222.10 2235.64 55.46 o 6 11 0 1792.88 1821.71 45.97 o 8 11 0 56.47 59.03 21.72 o 0 12 0 884.38 830.41 44.88 o 2 12 0 4619.68 4450.92 79.48 o 4 12 0 3630.11 3449.98 43.30 o 6 12 0 71.93 69.92 16.48 o 8 12 0 941.85 1020.44 108.44 o 2 13 0 1606.41 1572.11 70.04 o 4 13 0 5.65 20.17 17.07 o 6 13 0 2742.36 2518.84 95.32 o 0 14 0 4804.51 4538.77 94.26 o 2 14 0 2519.17 2581.95 55.11 o 4 14 0 1400.65 1328.63 34.47 o 6 14 0 410.48 328.84 32.55 o 2 15 0 0.04 -25.88 25.88 o 4 15 0 258.39 307.32 28.51 o 6 15 0 131.17 42.12 27.99 o 0 16 0 63.71 35.14 46.15 o 2 16 0 11.85 -2.51 24.17 o 4 16 0 27.02 -14.68 29.88 o 6 16 0 23.78 -2.18 27.48 o 2 17 0 19.83 -29.92 29.92 o 4 17 0 879.95 817.59 43.60 o 0 18 0 367.48 339.23 87.72 o 2 18 0 465.86 490.96 34.04 o 4 18 0 104.50 41.34 31.44 o 2 19 0 1228.81 1099.05 81.40 o 4 19 0 2395.75 2438.14 92.22 o 0 20 0 79.66 -27.67 42.46 o 2 20 0 426.63 420.18 50.00 o 1 1 1 13325.80 13376.31 64.21 o 2 1 1 191.80 204.86 6.54 o 3 1 1 4616.38 4859.06 24.52 o 4 1 1 280.87 304.56 10.24 o 5 1 1 1101.37 1069.91 18.76 o 6 1 1 2691.49 2665.53 33.27 o 7 1 1 11.86 3.82 16.07 o 8 1 1 178.47 209.47 18.81 o 9 1 1 1459.04 1532.18 37.95 o 10 1 1 303.51 294.10 24.14 o 0 2 1 2905.44 2980.44 33.19 o 1 2 1 4091.58 4186.92 19.49 o 2 2 1 1263.41 1326.84 11.80 o 3 2 1 2256.43 2634.05 17.56 o 4 2 1 883.36 964.05 14.41 o 5 2 1 1425.58 1620.47 21.39 o 6 2 1 2056.63 1960.40 29.49 o 7 2 1 5.83 6.77 16.03 o 8 2 1 11.81 -3.50 16.20 o 9 2 1 20.09 24.37 17.97 o 10 2 1 429.42 456.37 28.79 o 1 3 1 3437.17 3531.83 18.34 o 2 3 1 4434.73 4481.49 23.30 o 3 3 1 572.47 674.13 11.33 o 4 3 1 18.47 13.50 8.04 o 5 3 1 1651.70 1693.38 20.48 o 6 3 1 1286.97 1394.66 25.82 o 7 3 1 170.34 206.23 17.03 o 8 3 1 132.70 145.39 18.85 o 9 3 1 107.75 105.40 22.21 o 10 3 1 14.48 27.23 22.36 o 0 4 1 37761.58 37348.45 181.10 o 1 4 1 6519.21 6504.14 28.53 o 2 4 1 184.12 212.67 6.56 o 3 4 1 2497.31 2391.37 16.91 o 4 4 1 2491.59 2502.17 19.87 o 5 4 1 567.31 579.69 13.90 o 6 4 1 2742.16 2613.22 31.80 o 7 4 1 438.50 466.65 19.91 o 8 4 1 428.03 478.60 22.08 o 9 4 1 0.71 -8.04 18.11 o 10 4 1 489.03 439.71 36.47 o 1 5 1 2303.39 2273.90 16.14 o 2 5 1 65.07 108.87 6.74 o 3 5 1 89.30 135.97 12.38 o 4 5 1 1034.25 1046.93 15.13 o 5 5 1 646.90 621.45 14.24 o 6 5 1 455.06 428.00 15.86 o 7 5 1 404.15 395.21 17.67 o 8 5 1 44.78 40.61 16.39 o 9 5 1 0.92 2.63 18.44 o 0 6 1 12235.75 12381.70 72.51 o 1 6 1 1591.20 1414.59 13.81 o 2 6 1 11.24 13.20 6.94 o 3 6 1 13333.86 13871.14 61.84 o 4 6 1 267.76 242.68 9.81 o 5 6 1 592.27 734.08 16.39 o 6 6 1 21.06 28.91 13.14 o 7 6 1 4595.13 4309.58 41.69 o 8 6 1 917.60 911.40 26.90 o 9 6 1 69.66 16.60 19.55 o 1 7 1 1733.27 1739.57 16.31 o 2 7 1 4036.97 3932.90 24.80 o 3 7 1 354.55 356.76 9.22 o 4 7 1 127.60 133.06 9.03 o 5 7 1 538.10 524.65 14.47 o 6 7 1 3174.93 3177.76 33.43 o 7 7 1 155.01 166.95 14.99 o 8 7 1 171.22 175.17 18.91 o 9 7 1 1771.81 1606.13 37.23 o 0 8 1 8.38 5.50 10.68 o 1 8 1 756.15 800.54 13.89 o 2 8 1 3485.64 3567.01 28.06 o 3 8 1 514.33 483.90 11.88 o 4 8 1 778.30 756.66 17.04 o 5 8 1 1245.79 1203.04 19.36 o 6 8 1 1700.19 1731.06 25.40 o 7 8 1 1654.14 1548.98 31.55 o 8 8 1 1566.99 1564.56 32.96 o 9 8 1 1557.17 1402.13 47.44 o 1 9 1 714.40 838.47 14.98 o 2 9 1 2569.54 2531.82 24.42 o 3 9 1 7.89 0.31 8.13 o 4 9 1 1256.57 1219.83 17.30 o 5 9 1 1569.86 1477.26 22.67 o 6 9 1 1084.84 1082.70 26.84 o 7 9 1 493.00 468.89 21.72 o 8 9 1 1206.72 1167.05 31.82 o 9 9 1 4.70 3.06 19.05 o 0 10 1 5383.75 5356.75 52.23 o 1 10 1 1.45 19.18 9.19 o 2 10 1 2896.31 2851.16 25.74 o 3 10 1 560.86 561.41 14.27 o 4 10 1 15.85 8.65 10.57 o 5 10 1 248.82 309.23 13.86 o 6 10 1 1362.14 1280.81 22.45 o 7 10 1 38.44 31.09 13.23 o 8 10 1 676.51 695.78 22.78 o 1 11 1 18.84 26.87 12.93 o 2 11 1 48.72 55.08 11.79 o 3 11 1 1006.58 953.03 20.00 o 4 11 1 336.80 287.88 18.27 o 5 11 1 334.17 302.88 15.80 o 6 11 1 152.60 169.53 14.21 o 7 11 1 1448.48 1354.10 30.11 o 8 11 1 500.34 471.86 22.84 o 0 12 1 2292.18 2167.83 47.67 o 1 12 1 0.35 -4.76 12.35 o 2 12 1 24.42 70.58 16.77 o 3 12 1 826.62 921.05 22.02 o 4 12 1 60.96 51.67 12.02 o 5 12 1 58.80 60.24 13.44 o 6 12 1 664.24 724.54 29.44 o 7 12 1 46.71 45.79 14.49 o 8 12 1 338.88 353.15 30.99 o 1 13 1 450.38 459.22 18.27 o 2 13 1 230.68 293.46 27.68 o 3 13 1 1.22 2.43 12.05 o 4 13 1 948.80 991.27 24.73 o 5 13 1 460.79 484.29 24.57 o 6 13 1 6.57 10.35 15.67 o 7 13 1 141.57 171.86 17.53 o 0 14 1 2037.18 1884.77 47.41 o 1 14 1 236.52 270.63 20.60 o 2 14 1 449.98 531.73 20.75 o 3 14 1 2035.57 1806.32 31.00 o 4 14 1 1189.59 1220.52 28.60 o 5 14 1 2.53 31.03 18.50 o 6 14 1 725.76 743.23 28.46 o 7 14 1 71.36 25.07 18.96 o 1 15 1 757.95 725.14 33.33 o 2 15 1 1172.83 1110.11 30.16 o 3 15 1 301.51 289.73 19.54 o 4 15 1 3170.89 3080.91 41.43 o 5 15 1 10.44 1.13 20.68 o 6 15 1 402.73 332.54 23.68 o 7 15 1 41.39 63.53 30.00 o 0 16 1 193.55 180.09 38.41 o 1 16 1 1429.62 1262.47 32.08 o 2 16 1 1918.91 1877.17 34.94 o 3 16 1 22.85 43.98 17.07 o 4 16 1 248.47 259.52 32.70 o 5 16 1 729.73 647.32 28.60 o 6 16 1 1008.60 1109.04 38.86 o 1 17 1 539.27 464.32 23.31 o 2 17 1 395.83 400.19 22.80 o 3 17 1 1.49 -15.42 16.47 o 4 17 1 5.74 12.03 18.94 o 5 17 1 29.19 27.99 21.74 o 0 18 1 698.69 694.02 55.41 o 1 18 1 547.06 572.72 29.60 o 2 18 1 1325.84 1400.31 42.40 o 3 18 1 2.98 26.77 22.36 o 4 18 1 11.34 14.98 21.10 o 5 18 1 563.64 549.75 84.18 o 1 19 1 0.19 -20.02 20.02 o 2 19 1 46.12 -5.25 27.49 o 3 19 1 20.24 28.84 24.39 o 4 19 1 420.57 451.75 46.73 o 0 20 1 33.30 -6.42 49.94 o 1 20 1 192.60 100.95 24.95 o 2 20 1 221.74 202.27 26.68 o 1 0 2 916.88 939.12 12.93 o 2 0 2 26125.44 27622.94 139.10 o 3 0 2 16489.24 17046.26 91.98 o 4 0 2 66.76 111.68 11.39 o 5 0 2 703.81 856.98 28.81 o 6 0 2 68.81 63.40 25.72 o 7 0 2 2162.91 2111.70 60.33 o 8 0 2 72.87 84.56 25.88 o 9 0 2 125.95 159.40 29.25 o 10 0 2 6.18 -4.86 27.22 o 1 1 2 12425.41 12714.49 47.91 o 2 1 2 1594.75 1687.36 13.21 o 3 1 2 11.56 8.56 6.86 o 4 1 2 553.32 677.16 11.81 o 5 1 2 456.40 464.25 14.11 o 6 1 2 841.48 910.06 23.96 o 7 1 2 537.16 565.88 22.33 o 8 1 2 5.28 -0.94 16.21 o 9 1 2 336.25 344.86 22.28 o 10 1 2 4.45 -14.87 20.35 o 0 2 2 4825.87 4727.36 28.99 o 1 2 2 16675.83 16721.87 63.96 o 2 2 2 21642.25 22608.35 79.27 o 3 2 2 8533.67 8616.59 38.70 o 4 2 2 171.86 160.99 8.46 o 5 2 2 281.87 300.64 12.27 o 6 2 2 488.96 550.19 17.84 o 7 2 2 909.24 984.51 30.45 o 8 2 2 779.69 799.92 25.60 o 9 2 2 0.16 6.56 20.58 o 10 2 2 210.67 197.81 21.51 o 1 3 2 7662.38 7432.31 32.48 o 2 3 2 20287.89 20647.72 76.18 o 3 3 2 6566.50 6771.15 32.05 o 4 3 2 16806.77 18070.36 74.94 o 5 3 2 3935.47 3819.23 31.60 o 6 3 2 2592.73 2613.53 31.32 o 7 3 2 1.66 -5.74 15.02 o 8 3 2 64.63 71.95 17.12 o 9 3 2 2080.16 2097.78 38.90 o 10 3 2 564.65 508.70 26.38 o 0 4 2 1306.17 1210.57 18.26 o 1 4 2 2400.80 2247.23 15.86 o 2 4 2 4.46 2.85 6.07 o 3 4 2 439.98 504.33 10.28 o 4 4 2 905.01 916.56 14.21 o 5 4 2 2420.63 2377.44 22.71 o 6 4 2 333.44 354.01 15.44 o 7 4 2 4.27 1.96 13.15 o 8 4 2 350.94 336.30 20.68 o 9 4 2 696.10 674.07 26.93 o 1 5 2 1603.89 1603.19 13.51 o 2 5 2 445.23 569.45 10.63 o 3 5 2 532.70 451.14 12.34 o 4 5 2 0.70 13.91 7.71 o 5 5 2 2952.63 2839.29 24.43 o 6 5 2 104.95 114.36 12.66 o 7 5 2 90.69 92.81 14.11 o 8 5 2 60.80 51.66 17.55 o 9 5 2 1840.89 1780.53 37.31 o 0 6 2 783.76 768.83 17.80 o 1 6 2 1.75 -4.06 6.50 o 2 6 2 58.87 29.09 6.89 o 3 6 2 2490.44 2390.64 20.91 o 4 6 2 393.74 427.53 10.99 o 5 6 2 13.45 2.77 8.81 o 6 6 2 0.32 10.54 12.46 o 7 6 2 92.68 102.96 15.36 o 8 6 2 5.38 14.53 15.95 o 9 6 2 443.69 441.12 22.34 o 1 7 2 948.70 997.66 12.96 o 2 7 2 199.99 220.49 9.82 o 3 7 2 1690.25 1693.01 19.33 o 4 7 2 4.27 -7.57 7.57 o 5 7 2 101.48 96.32 14.89 o 6 7 2 62.21 66.75 11.62 o 7 7 2 1758.61 1727.87 33.76 o 8 7 2 34.44 22.02 16.28 o 9 7 2 912.06 867.17 27.92 o 0 8 2 1878.71 1870.80 39.33 o 1 8 2 5439.45 5602.75 29.50 o 2 8 2 8224.15 8706.31 44.49 o 3 8 2 5797.37 5462.55 36.71 o 4 8 2 29.48 39.25 10.40 o 5 8 2 64.79 50.38 9.43 o 6 8 2 487.01 513.16 17.30 o 7 8 2 1272.99 1234.03 24.84 o 8 8 2 586.47 577.63 23.11 o 9 8 2 2.45 -16.03 18.46 o 1 9 2 1083.16 996.43 16.14 o 2 9 2 396.49 358.28 11.47 o 3 9 2 61.05 74.27 10.64 o 4 9 2 2200.70 2161.04 25.31 o 5 9 2 130.52 90.09 12.35 o 6 9 2 7.98 12.99 10.97 o 7 9 2 657.59 675.37 22.84 o 8 9 2 412.31 369.41 22.27 o 9 9 2 16.31 -2.52 22.22 o 0 10 2 317.64 299.42 17.77 o 1 10 2 953.47 870.49 16.70 o 2 10 2 172.71 201.66 11.15 o 3 10 2 4207.87 4095.01 36.73 o 4 10 2 13.87 -0.10 11.24 o 5 10 2 19.39 7.23 12.72 o 6 10 2 0.02 11.37 18.94 o 7 10 2 682.72 673.97 21.64 o 8 10 2 304.45 255.77 23.13 o 1 11 2 2139.06 2061.65 28.05 o 2 11 2 106.99 74.36 10.49 o 3 11 2 745.94 718.25 19.90 o 4 11 2 197.68 151.72 14.45 o 5 11 2 193.40 172.24 14.09 o 6 11 2 639.15 644.39 22.83 o 7 11 2 174.58 210.29 18.38 o 8 11 2 408.97 359.56 23.65 o 0 12 2 228.85 262.11 22.73 o 1 12 2 1280.44 1237.43 29.02 o 2 12 2 784.69 772.71 19.58 o 3 12 2 294.02 297.17 15.76 o 4 12 2 158.64 165.16 13.43 o 5 12 2 1302.46 1247.95 27.42 o 6 12 2 22.28 19.90 18.47 o 7 12 2 2.80 18.26 18.12 o 8 12 2 70.33 39.69 25.92 o 1 13 2 11.46 -2.82 13.44 o 2 13 2 203.35 283.49 21.92 o 3 13 2 464.64 485.30 19.85 o 4 13 2 17.22 22.91 12.41 o 5 13 2 30.89 49.86 14.01 o 6 13 2 210.12 215.49 18.72 o 7 13 2 185.05 223.05 23.31 o 0 14 2 1482.55 1425.07 42.87 o 1 14 2 1686.76 1541.00 29.66 o 2 14 2 147.66 93.10 18.98 o 3 14 2 5.58 -8.72 16.18 o 4 14 2 19.84 7.07 15.95 o 5 14 2 2138.92 2096.22 42.18 o 6 14 2 557.53 512.99 24.46 o 7 14 2 86.07 95.22 28.37 o 1 15 2 725.94 715.27 26.10 o 2 15 2 143.81 123.35 31.11 o 3 15 2 156.10 148.07 19.91 o 4 15 2 94.65 113.78 18.15 o 5 15 2 484.12 444.41 24.42 o 6 15 2 55.50 33.37 19.96 o 0 16 2 518.39 595.01 39.30 o 1 16 2 0.00 20.80 16.92 o 2 16 2 959.40 920.47 25.72 o 3 16 2 596.10 597.07 25.79 o 4 16 2 12.65 24.12 20.61 o 5 16 2 141.01 156.69 19.93 o 6 16 2 68.77 131.13 24.86 o 1 17 2 309.69 365.46 21.97 o 2 17 2 61.60 59.65 19.28 o 3 17 2 2.37 -19.70 19.70 o 4 17 2 369.40 378.50 24.23 o 5 17 2 99.09 53.32 20.44 o 0 18 2 38.17 32.71 27.00 o 1 18 2 243.18 306.73 27.50 o 2 18 2 5.15 11.84 20.00 o 3 18 2 1054.44 1069.38 47.66 o 4 18 2 9.84 -17.48 21.16 o 1 19 2 204.19 206.59 24.65 o 2 19 2 23.05 -7.49 39.30 o 3 19 2 0.87 -26.73 26.73 o 0 20 2 583.49 535.64 56.32 o 1 20 2 1182.46 1076.44 34.72 o 2 20 2 35.46 4.41 21.65 o 1 1 3 1.06 3.18 4.46 o 2 1 3 177.10 198.73 6.72 o 3 1 3 729.25 649.18 10.97 o 4 1 3 4314.28 4488.53 27.21 o 5 1 3 1031.12 983.15 17.36 o 6 1 3 428.10 438.68 17.82 o 7 1 3 0.79 -3.59 15.01 o 8 1 3 697.65 768.91 25.66 o 9 1 3 1177.87 1270.36 34.72 o 10 1 3 363.55 411.77 24.66 o 0 2 3 3706.21 3709.28 24.53 o 1 2 3 483.97 487.23 8.61 o 2 2 3 12897.18 12949.40 52.12 o 3 2 3 1093.87 957.06 12.07 o 4 2 3 64.23 67.53 8.00 o 5 2 3 843.37 852.40 18.98 o 6 2 3 233.73 211.25 14.43 o 7 2 3 477.99 524.20 21.06 o 8 2 3 43.85 45.62 17.81 o 9 2 3 14.85 57.48 18.52 o 10 2 3 159.22 124.96 21.05 o 1 3 3 6101.20 6307.24 28.78 o 2 3 3 56.84 78.26 6.62 o 3 3 3 3576.85 3886.35 21.42 o 4 3 3 38.14 54.11 8.16 o 5 3 3 359.06 406.88 15.05 o 6 3 3 116.55 111.36 13.19 o 7 3 3 13.06 26.01 14.40 o 8 3 3 117.56 139.90 17.98 o 9 3 3 817.80 790.20 27.29 o 10 3 3 329.35 327.25 27.33 o 0 4 3 3232.13 3309.21 26.60 o 1 4 3 2010.81 1918.09 14.03 o 2 4 3 776.37 740.74 12.69 o 3 4 3 12928.48 12915.33 56.70 o 4 4 3 685.28 632.37 12.21 o 5 4 3 1092.88 1137.91 18.05 o 6 4 3 372.04 377.01 17.03 o 7 4 3 1795.73 1767.53 28.85 o 8 4 3 261.55 294.85 18.76 o 9 4 3 0.88 2.08 17.75 o 1 5 3 139.91 157.71 7.23 o 2 5 3 0.11 8.87 6.75 o 3 5 3 884.87 950.34 16.70 o 4 5 3 54.62 53.66 7.30 o 5 5 3 14.32 20.86 9.53 o 6 5 3 46.92 71.47 12.34 o 7 5 3 101.11 74.07 13.88 o 8 5 3 17.36 7.90 14.33 o 9 5 3 45.48 62.87 18.87 o 0 6 3 1582.33 1573.44 20.93 o 1 6 3 2282.85 2172.42 16.77 o 2 6 3 2552.92 2447.32 19.70 o 3 6 3 6840.69 6743.10 37.93 o 4 6 3 3449.33 3444.12 25.27 o 5 6 3 1133.32 1152.80 18.19 o 6 6 3 467.30 469.57 15.39 o 7 6 3 910.15 897.29 32.98 o 8 6 3 811.02 842.74 27.96 o 9 6 3 915.83 846.79 27.41 o 1 7 3 7324.26 7325.59 40.18 o 2 7 3 970.67 999.53 15.25 o 3 7 3 1169.36 1128.69 16.90 o 4 7 3 651.27 652.75 14.18 o 5 7 3 161.49 124.68 9.72 o 6 7 3 56.60 44.76 14.83 o 7 7 3 148.02 160.72 12.68 o 8 7 3 73.98 92.73 20.36 o 9 7 3 1822.22 1708.84 42.24 o 0 8 3 314.84 283.46 14.81 o 1 8 3 881.60 808.02 13.42 o 2 8 3 1182.34 1180.47 18.40 o 3 8 3 81.03 115.15 10.02 o 4 8 3 55.99 42.71 9.72 o 5 8 3 243.46 229.85 14.26 o 6 8 3 4.35 -10.90 13.91 o 7 8 3 402.45 411.88 23.45 o 8 8 3 60.37 59.56 18.54 o 9 8 3 43.07 14.53 23.72 o 1 9 3 2644.52 2793.43 27.05 o 2 9 3 22.19 23.28 9.51 o 3 9 3 2112.41 2020.49 23.34 o 4 9 3 976.53 912.34 19.31 o 5 9 3 2642.65 2524.15 36.89 o 6 9 3 55.39 70.78 17.76 o 7 9 3 145.26 118.00 17.17 o 8 9 3 507.28 479.45 27.02 o 9 9 3 1165.09 1154.98 38.48 o 0 10 3 730.83 690.09 24.15 o 1 10 3 2.91 -8.53 8.53 o 2 10 3 329.29 340.49 11.84 o 3 10 3 3055.00 2898.19 30.32 o 4 10 3 490.42 525.08 16.49 o 5 10 3 1542.57 1457.66 28.82 o 6 10 3 56.56 41.72 17.75 o 7 10 3 39.31 38.73 21.63 o 8 10 3 1.10 21.40 21.74 o 1 11 3 461.42 547.24 18.87 o 2 11 3 364.35 394.87 12.78 o 3 11 3 90.04 109.66 12.99 o 4 11 3 987.94 873.22 22.57 o 5 11 3 187.59 185.59 13.99 o 6 11 3 642.67 688.45 26.51 o 7 11 3 86.07 84.03 17.86 o 8 11 3 549.03 564.11 30.49 o 0 12 3 4.03 -12.00 18.47 o 1 12 3 193.66 199.69 14.22 o 2 12 3 3416.38 3375.95 33.93 o 3 12 3 1508.38 1450.79 44.01 o 4 12 3 386.76 367.63 17.60 o 5 12 3 290.61 304.40 17.08 o 6 12 3 32.70 28.18 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5 12 11 2440.91 2499.88 57.83 o 6 12 11 7.87 5.44 26.86 o 1 13 11 2380.90 2299.74 31.92 o 2 13 11 132.20 141.41 17.59 o 3 13 11 103.74 106.15 25.56 o 4 13 11 11.08 4.11 23.57 o 5 13 11 0.64 24.82 24.99 o 6 13 11 117.91 121.29 28.41 o 0 14 11 353.77 393.44 37.64 o 1 14 11 96.74 106.05 16.29 o 2 14 11 389.19 385.17 20.51 o 3 14 11 1.24 4.39 23.79 o 4 14 11 172.79 149.24 25.95 o 5 14 11 225.59 208.11 29.27 o 1 15 11 991.17 995.61 27.94 o 2 15 11 60.40 94.03 20.72 o 3 15 11 118.11 113.09 26.75 o 4 15 11 3.29 2.88 23.98 o 5 15 11 194.53 192.00 30.14 o 0 16 11 14.98 41.84 25.74 o 1 16 11 4.77 7.30 15.96 o 2 16 11 1086.60 1032.85 31.49 o 3 16 11 1926.49 1871.21 51.26 o 4 16 11 871.87 909.83 38.40 o 1 17 11 46.31 43.40 19.62 o 2 17 11 6.92 3.91 21.50 o 3 17 11 15.25 30.31 26.23 o 0 18 11 156.76 167.20 33.49 o 1 18 11 133.07 122.40 22.83 o 0 0 12 277.20 272.78 23.03 o 1 0 12 3.18 7.71 12.46 o 2 0 12 164.45 144.90 14.61 o 3 0 12 6022.01 5795.41 75.44 o 4 0 12 382.94 386.07 17.85 o 5 0 12 875.61 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6 4 12 357.82 349.99 26.66 o 7 4 12 76.32 105.34 22.68 o 8 4 12 188.94 250.56 28.60 o 1 5 12 1967.64 1904.60 25.93 o 2 5 12 3.29 4.82 10.58 o 3 5 12 293.48 318.29 14.35 o 4 5 12 2123.64 2087.48 46.29 o 5 5 12 9.85 9.94 17.05 o 6 5 12 44.49 76.09 17.86 o 7 5 12 83.51 123.86 24.80 o 8 5 12 1356.19 1417.01 44.97 o 0 6 12 12.88 9.60 13.69 o 1 6 12 501.47 571.03 15.11 o 2 6 12 780.32 823.38 20.19 o 3 6 12 1657.00 1636.05 27.14 o 4 6 12 0.11 -15.72 15.72 o 5 6 12 725.78 749.97 27.42 o 6 6 12 107.65 104.70 19.58 o 7 6 12 455.58 485.97 35.54 o 8 6 12 191.75 205.39 28.58 o 1 7 12 0.07 5.16 9.60 o 2 7 12 243.91 249.36 18.10 o 3 7 12 136.34 151.49 16.42 o 4 7 12 370.44 319.26 17.33 o 5 7 12 0.01 -12.49 20.46 o 6 7 12 855.06 847.14 40.19 o 7 7 12 3.53 14.67 24.13 o 8 7 12 164.14 203.58 29.34 o 0 8 12 1094.41 1078.72 31.71 o 1 8 12 190.84 207.54 11.96 o 2 8 12 3434.41 3151.51 34.29 o 3 8 12 789.87 866.27 28.38 o 4 8 12 1043.81 1068.90 33.43 o 5 8 12 851.16 814.94 33.41 o 6 8 12 64.43 68.76 25.50 o 7 8 12 149.98 155.95 28.46 o 1 9 12 2370.15 2253.53 27.09 o 2 9 12 130.29 123.46 15.25 o 3 9 12 40.76 28.53 19.03 o 4 9 12 699.55 654.33 29.24 o 5 9 12 13.39 18.10 21.50 o 6 9 12 35.65 45.60 25.27 o 7 9 12 739.13 774.36 37.57 o 0 10 12 463.81 523.35 24.42 o 1 10 12 225.31 294.65 16.03 o 2 10 12 461.78 513.01 19.03 o 3 10 12 50.83 32.56 19.98 o 4 10 12 611.54 560.83 30.28 o 5 10 12 0.67 -18.53 23.19 o 6 10 12 169.56 138.40 28.15 o 7 10 12 64.35 44.82 26.89 o 1 11 12 1207.51 1158.25 23.26 o 2 11 12 7.44 27.05 15.91 o 3 11 12 380.22 398.61 25.57 o 4 11 12 57.06 85.78 26.88 o 5 11 12 12.87 -14.87 31.48 o 6 11 12 20.75 25.80 24.50 o 0 12 12 323.48 336.89 26.68 o 1 12 12 272.22 328.40 18.01 o 2 12 12 484.45 462.50 21.56 o 3 12 12 2.77 -8.74 21.61 o 4 12 12 361.59 355.63 32.33 o 5 12 12 379.07 456.84 31.94 o 6 12 12 92.30 94.54 29.25 o 1 13 12 91.77 117.41 15.22 o 2 13 12 1.07 -10.97 16.72 o 3 13 12 144.69 162.91 26.40 o 4 13 12 50.72 92.71 24.13 o 5 13 12 93.40 60.81 26.64 o 6 13 12 25.20 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13 430.03 490.39 14.95 o 2 3 13 26.39 23.38 10.68 o 3 3 13 906.95 950.94 23.31 o 4 3 13 3.98 7.31 12.25 o 5 3 13 420.50 390.42 22.68 o 6 3 13 192.13 147.25 22.42 o 7 3 13 59.51 104.68 26.57 o 8 3 13 1.09 40.95 31.23 o 0 4 13 3.27 0.67 14.00 o 1 4 13 1280.04 1328.77 20.13 o 2 4 13 2767.53 2668.75 26.62 o 3 4 13 3994.89 3933.94 40.94 o 4 4 13 65.73 56.59 13.40 o 5 4 13 42.93 25.96 19.76 o 6 4 13 25.24 21.71 18.67 o 7 4 13 947.64 1002.55 41.04 o 8 4 13 353.45 440.10 33.49 o 1 5 13 995.74 981.36 20.23 o 2 5 13 164.49 173.67 13.96 o 3 5 13 213.23 210.96 13.96 o 4 5 13 1464.47 1362.71 31.15 o 5 5 13 72.55 64.93 17.57 o 6 5 13 491.14 480.34 34.15 o 7 5 13 146.59 201.02 26.55 o 8 5 13 149.20 137.33 26.75 o 0 6 13 176.45 184.22 18.23 o 1 6 13 362.10 385.12 14.55 o 2 6 13 1463.29 1324.05 25.42 o 3 6 13 1308.86 1243.33 23.30 o 4 6 13 735.69 684.54 24.40 o 5 6 13 73.83 61.39 16.70 o 6 6 13 162.47 171.75 27.02 o 7 6 13 0.42 5.36 19.92 o 8 6 13 878.72 843.19 39.38 o 1 7 13 1324.89 1230.54 22.64 o 2 7 13 421.27 499.71 17.71 o 3 7 13 965.23 923.89 25.62 o 4 7 13 19.37 -15.98 15.98 o 5 7 13 268.93 324.35 26.55 o 6 7 13 81.12 107.56 27.45 o 7 7 13 145.18 141.69 25.83 o 0 8 13 163.16 194.18 18.81 o 1 8 13 639.17 697.89 18.64 o 2 8 13 537.09 521.22 19.95 o 3 8 13 1761.89 1775.52 30.48 o 4 8 13 1.78 -14.14 19.67 o 5 8 13 881.51 876.80 35.00 o 6 8 13 117.11 93.00 25.59 o 7 8 13 65.14 104.29 29.09 o 1 9 13 615.15 656.91 27.62 o 2 9 13 2.17 14.41 14.04 o 3 9 13 351.43 364.62 24.31 o 4 9 13 1948.94 1891.84 43.49 o 5 9 13 1146.08 1082.39 39.60 o 6 9 13 13.92 -7.33 25.74 o 7 9 13 0.27 15.68 26.15 o 0 10 13 736.21 708.15 28.45 o 1 10 13 123.06 123.90 14.36 o 2 10 13 2047.79 2006.87 45.18 o 3 10 13 1149.22 1125.77 35.38 o 4 10 13 47.72 36.61 22.79 o 5 10 13 904.28 942.81 39.52 o 6 10 13 57.24 26.64 24.92 o 7 10 13 37.73 74.37 28.39 o 1 11 13 630.21 646.44 24.72 o 2 11 13 16.47 32.44 12.78 o 3 11 13 7.18 13.75 20.81 o 4 11 13 24.87 54.07 24.75 o 5 11 13 3.60 -8.05 24.50 o 6 11 13 7.66 30.75 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