#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/30/01/2300196.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2300196_Fobs
loop_
_publ_author_name
'Fan, Jiandong'
'Zhang, Huaijin'
'Yu, Wentao'
'Yu, Haohai'
'Wang, Jiyang'
'Jiang, Minhua'
_publ_section_title
;
 A Yb^3+^-doped NaY(WO~4~)~2~ crystal grown by the Czochralski
 technique
;
_journal_coeditor_code           AJ5103
_journal_issue                   3
_journal_name_full               'Journal of Applied Crystallography'
_journal_page_first              584
_journal_page_last               591
_journal_volume                  41
_journal_year                    2008
_space_group_IT_number           88
_symmetry_space_group_name_Hall  '-I 4ad'
_symmetry_space_group_name_H-M   'I 41/a :2'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   5.2039
_cell_length_b                   5.2039
_cell_length_c                   11.2838
_exptl_crystal_F_000             527.10
_reflns_d_resolution_high        0.6462
_[local]_cod_data_source_file    aj5103fanjd02sup2.hkl
_[local]_cod_data_source_block   fanjd02
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' fanjd02 in I4(1)/a'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            332.61
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-y+3/4, x+1/4, z+1/4'
'y+3/4, -x+3/4, z+3/4'
'x+1/2, y+1/2, z+1/2'
'-x+1, -y+1/2, z+1'
'-y+5/4, x+3/4, z+3/4'
'y+5/4, -x+5/4, z+5/4'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'y-3/4, -x-1/4, -z-1/4'
'-y-3/4, x-3/4, -z-3/4'
'-x+1/2, -y+1/2, -z+1/2'
'x, y+1/2, -z'
'y-1/4, -x+1/4, -z+1/4'
'-y-1/4, x-1/4, -z-1/4'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 2 0 66519.77 64016.19 2206.10 o
2 2 0 90620.60 86612.53 3039.70 o
-2 4 0 44254.94 45045.57 1470.61 o
0 4 0 52097.90 53621.46 1417.83 o
2 4 0 44949.50 43656.95 1724.84 o
4 4 0 21507.59 19701.87 2494.31 o
-4 6 0 15473.12 13992.89 1200.33 o
-2 6 0 18614.82 18536.11 708.63 o
0 6 0 23005.13 22932.67 883.63 o
2 6 0 17794.11 18003.04 696.93 o
4 6 0 16147.97 15339.40 797.25 o
0 8 0 10074.96 10360.37 891.91 o
0 1 1 20112.71 21414.50 601.52 o
-1 2 1 5417.40 5217.88 146.90 o
1 2 1 20414.55 20117.66 478.10 o
-2 3 1 6657.56 6731.48 139.14 o
0 3 1 8541.66 8325.16 182.92 o
2 3 1 14756.72 14133.76 340.61 o
-3 4 1 3998.64 3782.93 217.34 o
-1 4 1 10246.72 10163.77 210.84 o
1 4 1 5822.13 5719.11 135.15 o
3 4 1 6535.41 6230.67 188.25 o
-4 5 1 2629.41 2180.19 163.27 o
-2 5 1 5942.34 5734.73 146.08 o
0 5 1 6023.01 5983.30 142.02 o
2 5 1 3340.07 3437.04 108.86 o
4 5 1 3824.41 3820.54 121.64 o
-5 6 1 2088.45 1708.92 201.98 o
-3 6 1 2576.99 2302.63 166.39 o
-1 6 1 4127.32 3853.89 109.27 o
1 6 1 3125.85 3070.41 88.68 o
3 6 1 3260.56 3196.66 102.69 o
5 6 1 1747.18 1618.77 198.79 o
-2 7 1 1799.01 1728.89 60.70 o
0 7 1 2528.52 2424.94 72.43 o
2 7 1 2695.34 2702.36 80.68 o
1 1 2 110631.42 105211.30 2957.33 o
0 2 2 463.14 481.49 13.61 o
2 2 2 18.67 16.00 2.59 o
-1 3 2 58704.38 61655.20 1267.05 o
1 3 2 71651.91 73423.37 2116.34 o
3 3 2 44971.88 46242.55 1074.12 o
-2 4 2 353.86 357.39 10.48 o
0 4 2 797.64 750.26 20.91 o
2 4 2 135.10 126.88 6.88 o
4 4 2 12.26 7.92 15.16 o
-3 5 2 22120.84 19074.17 1445.27 o
-1 5 2 35853.72 36389.96 882.07 o
1 5 2 28250.06 28829.24 715.26 o
3 5 2 24363.54 24525.92 862.42 o
5 5 2 14107.20 15602.45 1351.00 o
-4 6 2 9.93 -14.91 44.68 o
-2 6 2 127.40 131.86 10.19 o
0 6 2 231.32 249.92 17.46 o
2 6 2 60.29 87.67 9.93 o
4 6 2 0.04 -6.02 7.99 o
-3 7 2 11151.04 9674.10 857.00 o
-1 7 2 12939.41 12346.57 356.65 o
1 7 2 14762.45 14354.17 395.22 o
3 7 2 10777.80 10778.12 385.09 o
0 8 2 10.27 0.49 38.76 o
0 1 3 19306.93 18510.87 764.17 o
-1 2 3 14890.24 15104.53 350.22 o
1 2 3 5172.20 5015.38 116.06 o
-2 3 3 13775.37 13847.71 261.50 o
0 3 3 7118.94 6888.34 143.31 o
2 3 3 7923.08 7814.95 157.56 o
-3 4 3 4904.01 5050.55 157.70 o
-1 4 3 6299.58 6166.73 145.46 o
1 4 3 10146.74 10131.35 252.15 o
3 4 3 3213.26 3450.94 93.68 o
-4 5 3 3585.07 4590.26 446.04 o
-2 5 3 3675.58 3549.91 105.66 o
0 5 3 5060.50 4964.82 126.02 o
2 5 3 5379.50 5333.11 178.38 o
4 5 3 2889.94 3112.56 440.88 o
-5 6 3 1425.30 1724.37 215.15 o
-3 6 3 3523.59 2820.02 297.74 o
-1 6 3 2899.41 2814.78 86.02 o
1 6 3 3280.63 3292.08 105.86 o
3 6 3 3057.28 3251.45 113.50 o
5 6 3 1767.56 2731.62 291.07 o
-2 7 3 2001.53 1915.18 125.42 o
0 7 3 3004.42 2797.93 87.29 o
2 7 3 1516.13 1466.27 57.18 o
0 0 4 75240.74 54157.69 3686.64 o
1 1 4 2898.00 3131.16 83.91 o
0 2 4 95300.83 93245.99 2198.95 o
2 2 4 58544.38 60799.72 1309.65 o
-1 3 4 130.22 140.53 7.20 o
1 3 4 123.25 123.83 8.67 o
3 3 4 31.35 56.23 5.42 o
-2 4 4 35712.94 37050.73 885.65 o
0 4 4 42579.25 42962.16 1036.36 o
2 4 4 35188.96 35975.96 866.82 o
4 4 4 25540.81 28008.65 2357.26 o
-3 5 4 76.19 86.62 23.21 o
-1 5 4 5.53 6.49 5.04 o
1 5 4 10.20 22.49 5.91 o
3 5 4 101.90 78.88 9.55 o
5 5 4 101.54 248.35 79.88 o
-4 6 4 11219.63 13476.09 1171.99 o
-2 6 4 18168.07 17126.47 847.54 o
0 6 4 20016.87 19510.05 633.59 o
2 6 4 18832.56 18837.21 616.08 o
4 6 4 10798.83 12077.78 1272.87 o
-3 7 4 4.49 3.52 60.56 o
-1 7 4 1.35 8.24 8.17 o
1 7 4 0.00 -0.62 9.14 o
3 7 4 21.38 26.72 11.08 o
0 1 5 8061.55 7775.35 216.50 o
-1 2 5 14693.94 14482.87 336.45 o
1 2 5 11636.92 11789.86 323.61 o
-2 3 5 5158.81 5193.33 128.41 o
0 3 5 12940.79 12438.05 281.34 o
2 3 5 3817.44 4017.63 90.36 o
-3 4 5 6296.37 6860.38 237.93 o
-1 4 5 4717.62 4750.73 116.85 o
1 4 5 5241.69 5060.93 125.26 o
3 4 5 5553.46 5681.98 156.87 o
-4 5 5 2948.19 3505.44 333.27 o
-2 5 5 3847.26 3880.50 130.13 o
0 5 5 4097.36 3978.90 123.99 o
2 5 5 4730.95 5009.54 169.58 o
4 5 5 2432.17 2888.34 158.40 o
-3 6 5 2075.68 2331.57 137.46 o
-1 6 5 3208.57 3133.15 110.61 o
1 6 5 3784.66 3603.78 125.11 o
3 6 5 1890.61 1837.78 69.18 o
-2 7 5 2538.68 2425.33 109.48 o
0 7 5 1778.21 1815.99 69.11 o
2 7 5 2167.89 2383.26 87.87 o
1 1 6 70234.13 70952.24 1938.08 o
0 2 6 1.35 3.54 4.75 o
2 2 6 2.78 4.70 4.72 o
-1 3 6 56646.11 58546.04 1382.32 o
1 3 6 40211.74 39578.45 1124.11 o
3 3 6 32316.39 34102.46 906.87 o
-2 4 6 6.45 9.38 8.54 o
0 4 6 3.76 13.55 4.56 o
2 4 6 0.09 4.28 5.55 o
4 4 6 1.41 15.97 23.19 o
-3 5 6 21499.27 22814.17 1768.26 o
-1 5 6 19116.38 18707.90 611.58 o
1 5 6 30548.43 30303.33 975.45 o
3 5 6 17811.18 18589.91 568.86 o
5 5 6 11003.40 12518.34 632.26 o
-4 6 6 0.42 45.65 53.32 o
-2 6 6 2.56 6.66 19.24 o
0 6 6 1.69 36.10 10.13 o
2 6 6 0.04 10.94 9.49 o
4 6 6 0.02 0.78 17.95 o
-1 7 6 13106.68 12951.83 423.81 o
1 7 6 10009.12 9769.13 325.39 o
0 1 7 6791.62 6769.05 174.85 o
-1 2 7 10212.09 9950.98 211.08 o
1 2 7 9701.40 9611.36 246.66 o
-2 3 7 4048.28 4391.81 118.62 o
0 3 7 9601.04 9629.94 258.26 o
2 3 7 3557.21 3636.04 89.80 o
-3 4 7 5142.53 5183.03 217.38 o
-1 4 7 4162.26 4321.24 127.66 o
1 4 7 3941.38 4142.20 104.23 o
3 4 7 4924.65 5976.25 250.39 o
-4 5 7 2359.23 2834.81 155.08 o
-2 5 7 3254.51 3414.87 285.88 o
0 5 7 3630.56 3611.32 124.46 o
2 5 7 3752.32 3659.09 126.18 o
4 5 7 2020.82 2080.03 120.27 o
-3 6 7 1671.36 1788.53 113.99 o
-1 6 7 2737.87 2745.98 99.39 o
1 6 7 3251.33 3236.36 112.70 o
3 6 7 1555.33 1751.76 81.01 o
-2 7 7 2201.49 2437.83 247.87 o
0 7 7 1400.80 1440.03 58.68 o
2 7 7 1944.12 1449.86 178.62 o
0 0 8 49641.70 51590.88 3447.52 o
1 1 8 1042.02 969.63 28.21 o
0 2 8 52217.41 52089.98 1399.93 o
2 2 8 38379.11 39826.50 1018.85 o
-1 3 8 71.58 85.07 9.43 o
1 3 8 62.79 77.40 10.55 o
3 3 8 17.38 24.45 10.24 o
-2 4 8 24544.97 25147.31 1257.28 o
0 4 8 28858.11 27915.48 916.78 o
2 4 8 24709.55 25554.80 781.60 o
4 4 8 17942.28 20646.97 794.50 o
-3 5 8 50.28 84.92 20.06 o
-1 5 8 2.83 19.30 11.21 o
1 5 8 9.66 9.23 8.83 o
3 5 8 86.15 142.07 25.98 o
5 5 8 83.63 98.99 54.53 o
-2 6 8 13422.58 14188.88 1239.10 o
0 6 8 14740.83 14695.05 573.39 o
2 6 8 13269.78 12868.19 422.56 o
-1 7 8 1.41 35.53 43.01 o
1 7 8 0.42 31.18 44.87 o
0 1 9 8242.82 7939.23 259.35 o
-1 2 9 6397.68 6338.21 151.64 o
1 2 9 3549.50 3510.91 131.44 o
-2 3 9 6703.53 6759.56 194.16 o
0 3 9 3665.37 3661.04 135.27 o
2 3 9 4729.53 5034.26 138.68 o
-3 4 9 2706.27 2893.37 126.21 o
-1 4 9 3625.15 3609.13 128.87 o
1 4 9 5247.68 5120.16 177.08 o
3 4 9 2039.32 1975.14 87.83 o
-4 5 9 2043.04 2244.25 129.68 o
-2 5 9 2225.96 2272.24 114.40 o
0 5 9 3127.67 3287.34 139.14 o
2 5 9 2893.30 3227.28 137.15 o
4 5 9 1835.19 2163.33 162.36 o
-3 6 9 2144.28 2095.99 158.59 o
-1 6 9 1848.91 2037.42 123.03 o
1 6 9 1905.10 1868.21 86.83 o
3 6 9 1869.44 1886.78 185.24 o
1 1 10 38205.91 41724.22 1170.16 o
0 2 10 47.30 72.46 9.29 o
2 2 10 0.35 2.91 8.52 o
-1 3 10 25001.83 22626.01 1229.13 o
1 3 10 29659.89 29169.63 1110.33 o
3 3 10 21776.76 22915.48 870.53 o
-2 4 10 69.58 64.59 18.47 o
0 4 10 170.17 125.76 15.78 o
2 4 10 45.46 89.49 15.32 o
4 4 10 1.31 4.59 15.79 o
-3 5 10 11378.89 11210.52 554.89 o
-1 5 10 18545.51 18280.70 983.83 o
1 5 10 14326.09 14550.86 576.17 o
3 5 10 12766.75 13332.28 1157.42 o
-2 6 10 38.29 46.35 27.10 o
0 6 10 79.75 122.68 21.04 o
2 6 10 26.12 5.71 17.06 o
0 1 11 5318.88 5637.83 129.71 o
-1 2 11 2807.33 2557.25 201.44 o
1 2 11 5042.73 5347.03 201.45 o
-2 3 11 2863.55 3061.27 153.81 o
0 3 11 3070.49 2855.29 198.51 o
2 3 11 4786.84 4514.94 289.94 o
-3 4 11 1649.25 1578.97 76.77 o
-1 4 11 3517.17 2755.06 141.73 o
1 4 11 2618.39 2714.71 126.57 o
3 4 11 2450.32 2663.39 117.64 o
-2 5 11 2432.00 2396.70 214.85 o
0 5 11 2428.22 2196.16 128.55 o
2 5 11 1441.00 1296.85 103.07 o
-1 6 11 1835.01 1845.50 230.47 o
1 6 11 1289.88 1465.50 75.24 o
0 0 12 37509.50 45989.11 2092.77 o
1 1 12 13.56 11.64 9.75 o
0 2 12 20707.61 20656.81 716.28 o
2 2 12 23842.42 22061.07 2278.18 o
-1 3 12 2.11 0.23 15.26 o
1 3 12 1.01 14.83 15.22 o
3 3 12 0.04 9.63 17.79 o
-2 4 12 15277.92 14500.97 647.48 o
0 4 12 17082.56 15469.87 872.91 o
2 4 12 15417.28 16728.79 738.10 o
4 4 12 8672.08 8651.78 341.93 o
-1 5 12 0.02 5.43 20.80 o
1 5 12 1.09 -0.68 15.40 o
0 1 13 3417.14 3509.07 116.43 o
-1 2 13 1979.28 1910.55 98.18 o
1 2 13 3905.38 3602.14 288.76 o
-2 3 13 1792.07 1465.51 82.69 o
0 3 13 2438.63 2352.09 150.05 o
2 3 13 3102.34 3223.72 159.42 o
-3 4 13 1337.79 1348.23 83.67 o
-1 4 13 2626.24 2247.83 118.58 o
1 4 13 1583.59 1523.63 121.12 o
3 4 13 1962.65 1976.81 108.37 o
0 5 13 1723.54 1656.24 90.26 o
1 1 14 18642.42 19728.59 702.61 o
0 2 14 22.76 13.81 15.89 o
2 2 14 2.13 -6.26 19.36 o
-1 3 14 14019.30 12796.52 935.15 o
1 3 14 15201.48 12253.97 761.12 o
3 3 14 11131.03 9725.90 960.08 o
-2 4 14 61.07 52.93 21.58 o
0 4 14 104.71 118.31 21.58 o
2 4 14 19.09 -2.98 20.60 o
0 1 15 2393.75 2569.46 103.30 o
-1 2 15 2302.94 2274.91 115.01 o
1 2 15 1378.73 1401.47 62.83 o
-2 3 15 2208.08 2033.41 106.60 o
0 3 15 1588.81 1136.05 159.00 o
2 3 15 1413.37 1303.06 219.00 o
0 0 16 11414.22 12195.20 762.32 o
1 1 16 63.97 78.14 22.25 o
0 2 16 13429.23 13393.88 974.20 o
2 2 16 10004.30 9553.97 428.46 o
0 1 17 1197.90 1375.91 62.66 o