#------------------------------------------------------------------------------ #$Date: 2016-04-06 22:07:34 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181919 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/30/05/2300564.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2300564 _cell_angle_alpha 90.000 _cell_angle_beta 98.290 _cell_angle_gamma 90.000 _cell_length_a 8.8965 _cell_length_b 6.9130 _cell_length_c 16.4390 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.6965 _cod_data_source_file ks54942_uncorrsup7.hkl _cod_data_source_block 2_uncorr #BEGIN Tags that were not found in dictionaries: _shelx_title ' NoFilter_05_a.res in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 133.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 918.63 908.72 6.04 o 4 0 0 587.11 595.55 5.23 o 6 0 0 58.60 59.94 1.26 o 8 0 0 394.80 322.58 3.73 o 10 0 0 13.99 11.28 1.49 o 12 0 0 195.56 214.32 5.40 o 1 1 0 535.38 490.38 2.72 o 3 1 0 3008.32 3178.23 14.27 o 5 1 0 2.96 2.45 0.27 o 7 1 0 4.75 5.29 0.41 o 9 1 0 45.20 40.37 1.22 o 11 1 0 576.94 610.81 6.67 o 0 2 0 4274.93 4360.21 27.22 o 2 2 0 4957.58 5215.71 21.70 o 4 2 0 569.98 671.27 3.69 o 6 2 0 22.01 19.97 0.60 o 8 2 0 962.04 911.79 5.41 o 10 2 0 271.74 261.09 3.47 o 12 2 0 3.83 2.34 1.00 o 1 3 0 41.56 53.04 0.63 o 3 3 0 418.78 439.53 2.62 o 5 3 0 491.86 538.70 3.10 o 7 3 0 500.84 533.18 3.60 o 9 3 0 150.40 181.74 2.46 o 11 3 0 0.82 -0.55 0.71 o 0 4 0 12.83 11.03 0.60 o 2 4 0 342.79 343.07 2.04 o 4 4 0 361.06 406.56 2.74 o 6 4 0 669.64 648.57 3.89 o 8 4 0 212.70 202.42 2.19 o 10 4 0 16.39 15.50 1.71 o 1 5 0 100.72 109.97 1.13 o 3 5 0 269.10 301.67 2.25 o 5 5 0 10.38 17.35 0.69 o 7 5 0 8.83 11.11 0.82 o 9 5 0 57.18 57.22 1.90 o 0 6 0 1919.46 1971.09 12.44 o 2 6 0 233.34 248.05 2.18 o 4 6 0 42.53 44.43 1.17 o 8 6 0 49.65 53.92 1.69 o 10 6 0 46.87 45.82 2.68 o 1 7 0 6.58 5.94 0.58 o 3 7 0 0.00 -0.04 0.49 o 5 7 0 0.04 -0.30 0.61 o 7 7 0 22.63 42.40 2.80 o 0 8 0 277.02 262.21 4.34 o 2 8 0 298.62 301.15 3.40 o 4 8 0 7.47 9.63 1.26 o 6 8 0 0.71 1.71 0.81 o 1 9 0 10.41 11.83 1.11 o 3 9 0 72.08 70.61 1.94 o 5 9 0 76.98 71.42 2.06 o -11 1 1 28.39 27.57 1.45 o -9 1 1 108.17 111.49 1.87 o -7 1 1 1.29 1.21 0.32 o -5 1 1 2104.28 2169.21 10.26 o -3 1 1 1301.21 1347.25 5.97 o -1 1 1 136.15 124.98 0.66 o 1 1 1 2787.20 2802.68 11.68 o 3 1 1 4307.52 4624.69 23.66 o 5 1 1 1241.30 1344.72 6.74 o 7 1 1 2229.76 2152.80 10.64 o 9 1 1 0.06 0.80 0.47 o 11 1 1 25.92 30.63 1.69 o -12 2 1 1.47 0.36 0.97 o -10 2 1 47.21 52.19 1.69 o -8 2 1 395.21 360.57 2.81 o -6 2 1 221.04 226.40 1.88 o -4 2 1 1334.81 1498.65 7.22 o -2 2 1 65.60 54.73 0.62 o 0 2 1 10943.58 11258.83 53.94 o 2 2 1 168.55 165.08 1.33 o 4 2 1 24.76 21.59 0.53 o 6 2 1 51.95 45.62 0.82 o 8 2 1 30.27 26.91 0.92 o 10 2 1 109.49 112.26 2.25 o 12 2 1 61.56 67.24 2.72 o -11 3 1 148.08 146.03 2.84 o -9 3 1 22.72 22.99 1.26 o -7 3 1 2417.98 2241.99 11.15 o -5 3 1 9.32 12.14 0.47 o -3 3 1 546.86 552.72 2.97 o -1 3 1 1670.21 1801.16 7.94 o 1 3 1 9.33 4.46 0.25 o 3 3 1 195.16 214.69 1.60 o 5 3 1 1183.30 1181.48 5.86 o 7 3 1 1118.06 1005.25 5.84 o 9 3 1 295.94 291.82 3.02 o 11 3 1 169.02 175.96 3.18 o -10 4 1 69.11 69.38 2.08 o -8 4 1 177.63 153.91 2.08 o -6 4 1 71.86 74.81 1.01 o -4 4 1 50.17 57.09 1.06 o -2 4 1 1260.51 1323.07 6.58 o 0 4 1 877.52 912.50 5.11 o 2 4 1 368.72 405.95 2.32 o 4 4 1 6.92 11.95 0.49 o 6 4 1 9.98 9.04 0.54 o 8 4 1 85.10 94.15 1.67 o 10 4 1 16.80 20.47 1.33 o -9 5 1 34.27 30.17 1.36 o -7 5 1 368.07 360.90 3.29 o -5 5 1 254.98 249.79 2.24 o -3 5 1 640.55 650.98 3.90 o -1 5 1 43.45 44.99 0.70 o 1 5 1 28.22 25.40 0.71 o 3 5 1 67.91 59.09 0.89 o 5 5 1 64.91 65.54 1.26 o 7 5 1 487.57 458.78 4.41 o 9 5 1 256.70 265.27 3.73 o -10 6 1 1.62 1.01 1.25 o -8 6 1 26.57 23.35 1.23 o -6 6 1 43.75 43.37 1.22 o -4 6 1 89.57 90.88 1.40 o -2 6 1 5.96 6.44 0.52 o 0 6 1 59.46 63.51 2.02 o 2 6 1 56.69 57.94 1.08 o 4 6 1 35.17 35.11 1.20 o 6 6 1 14.40 13.81 0.83 o 8 6 1 29.42 25.44 1.19 o -9 7 1 114.07 109.60 2.92 o -7 7 1 7.91 9.67 1.30 o -5 7 1 114.44 117.23 2.25 o -3 7 1 43.17 43.81 1.15 o -1 7 1 101.05 100.71 1.69 o 1 7 1 95.40 91.78 1.53 o 3 7 1 5.82 5.46 0.75 o 5 7 1 55.64 50.65 1.67 o 7 7 1 22.53 24.22 1.83 o -6 8 1 30.96 33.24 1.60 o -4 8 1 281.01 270.86 3.32 o -2 8 1 7.17 7.32 0.77 o 0 8 1 89.51 87.87 2.10 o 2 8 1 0.32 -0.28 0.59 o 4 8 1 70.70 66.92 1.75 o 6 8 1 44.65 40.87 1.76 o -5 9 1 290.18 299.33 3.82 o -3 9 1 11.61 12.60 1.15 o -1 9 1 176.23 158.88 2.79 o 1 9 1 58.08 54.12 1.91 o 3 9 1 13.17 15.36 1.15 o 5 9 1 61.62 70.30 2.24 o -12 0 2 24.90 39.47 2.91 o -10 0 2 17.96 13.62 1.90 o -8 0 2 500.98 472.12 4.81 o -6 0 2 405.81 388.49 3.07 o -4 0 2 3609.71 4267.55 26.83 o -2 0 2 4498.14 4856.12 32.22 o 0 0 2 2425.09 2331.71 17.89 o 2 0 2 7203.81 7315.20 40.79 o 4 0 2 61.44 57.96 1.05 o 6 0 2 69.85 84.57 1.50 o 8 0 2 1013.09 977.37 8.04 o 10 0 2 1304.69 1294.20 12.41 o 12 0 2 71.53 62.63 3.45 o -11 1 2 142.88 156.61 3.53 o -9 1 2 354.80 341.86 3.43 o -7 1 2 879.34 699.93 4.18 o -5 1 2 835.52 848.62 3.95 o -3 1 2 2411.99 2571.53 11.85 o -1 1 2 9437.67 9203.06 41.53 o 1 1 2 202.31 202.57 1.26 o 3 1 2 173.67 165.61 1.37 o 5 1 2 30.92 16.27 0.58 o 7 1 2 3868.55 3593.91 16.89 o 9 1 2 6.46 5.76 0.59 o 11 1 2 55.26 56.78 2.06 o -12 2 2 30.11 30.19 3.12 o -10 2 2 36.89 39.54 1.60 o -8 2 2 16.92 24.17 0.85 o -6 2 2 249.58 221.36 1.85 o -4 2 2 7.10 16.33 0.40 o -2 2 2 1718.65 1744.54 7.60 o 0 2 2 17937.03 18430.24 73.78 o 2 2 2 1013.60 1054.70 4.82 o 4 2 2 74.02 79.22 0.97 o 6 2 2 421.65 409.82 2.81 o 8 2 2 58.65 66.86 1.29 o 10 2 2 2.03 4.65 0.70 o 12 2 2 123.88 128.18 3.63 o -11 3 2 63.30 64.85 2.06 o -9 3 2 2.26 0.96 0.69 o -7 3 2 3.23 5.95 0.54 o -5 3 2 127.26 132.00 1.27 o -3 3 2 72.96 74.65 0.83 o -1 3 2 27.96 28.45 0.41 o 1 3 2 1740.54 1908.08 9.58 o 3 3 2 2197.57 2398.08 12.85 o 5 3 2 231.65 237.94 1.91 o 7 3 2 29.38 26.57 0.87 o 9 3 2 40.37 38.17 1.14 o 11 3 2 69.95 73.81 2.18 o -10 4 2 138.22 132.85 2.40 o -8 4 2 149.20 160.34 2.27 o -6 4 2 20.06 22.07 0.66 o -4 4 2 0.01 1.23 0.30 o -2 4 2 226.63 232.91 1.75 o 0 4 2 183.99 178.01 1.25 o 2 4 2 0.95 2.65 0.22 o 4 4 2 805.29 835.94 4.68 o 6 4 2 44.16 45.22 1.04 o 8 4 2 86.27 86.16 1.62 o 10 4 2 116.13 112.04 3.86 o -11 5 2 185.85 180.88 3.83 o -9 5 2 47.55 41.77 1.55 o -7 5 2 1489.90 1466.63 8.76 o -5 5 2 0.18 0.05 0.31 o -3 5 2 23.65 29.33 0.67 o -1 5 2 156.13 171.13 1.39 o 1 5 2 167.07 177.98 1.68 o 3 5 2 87.33 89.71 1.23 o 5 5 2 168.68 174.61 2.07 o 7 5 2 195.37 186.08 2.94 o 9 5 2 47.31 50.02 1.91 o -10 6 2 3.53 4.08 1.30 o -8 6 2 181.33 187.27 2.76 o -6 6 2 125.92 123.84 1.87 o -4 6 2 1.90 2.76 0.44 o -2 6 2 43.48 43.71 1.05 o 0 6 2 17.43 21.61 0.72 o 2 6 2 535.60 550.66 4.75 o 4 6 2 132.79 133.48 1.97 o 6 6 2 36.83 37.39 1.23 o 8 6 2 6.72 4.33 0.73 o -9 7 2 105.49 106.90 2.90 o -7 7 2 287.61 302.39 4.42 o -5 7 2 344.55 341.19 3.61 o -3 7 2 33.70 36.24 1.12 o -1 7 2 142.22 139.28 2.14 o 1 7 2 25.83 25.63 0.97 o 3 7 2 0.18 0.67 0.50 o 5 7 2 104.32 107.13 1.98 o 7 7 2 332.45 320.66 3.72 o -6 8 2 4.32 6.03 0.87 o -4 8 2 66.77 68.66 1.77 o -2 8 2 132.99 133.45 2.14 o 0 8 2 109.91 104.21 1.91 o 2 8 2 3.32 2.16 0.64 o 4 8 2 0.01 -0.65 0.65 o 6 8 2 11.37 13.14 1.18 o -5 9 2 380.03 371.25 4.76 o -3 9 2 40.48 38.04 1.71 o -1 9 2 3.63 4.64 0.78 o 1 9 2 40.89 37.26 2.92 o 3 9 2 75.84 72.72 1.95 o 5 9 2 17.87 19.81 1.45 o -11 1 3 134.18 147.27 2.74 o -9 1 3 30.46 33.95 1.33 o -7 1 3 10.51 10.65 0.49 o -5 1 3 271.55 258.00 1.60 o -3 1 3 97.14 90.99 0.69 o -1 1 3 524.76 465.60 2.73 o 1 1 3 3470.27 3514.18 14.65 o 3 1 3 2659.20 2770.11 10.70 o 5 1 3 1204.22 1253.73 6.37 o 7 1 3 354.93 359.80 2.69 o 9 1 3 49.95 48.50 1.86 o 11 1 3 134.89 131.78 2.92 o -12 2 3 125.86 150.47 4.01 o -10 2 3 11.03 9.86 0.99 o -8 2 3 504.30 399.14 3.25 o -6 2 3 241.65 246.53 1.94 o -4 2 3 54.94 62.24 0.70 o -2 2 3 1432.08 1475.69 5.63 o 0 2 3 13593.07 14058.24 75.20 o 2 2 3 1178.80 1212.96 6.99 o 4 2 3 623.02 638.76 3.39 o 6 2 3 586.32 559.28 3.33 o 8 2 3 305.93 299.98 2.64 o 10 2 3 80.01 80.67 1.82 o 12 2 3 18.82 15.52 2.40 o -11 3 3 512.08 531.78 5.66 o -9 3 3 0.26 10.94 1.02 o -7 3 3 340.15 336.14 2.86 o -5 3 3 390.60 419.10 2.46 o -3 3 3 1702.64 1714.18 7.37 o -1 3 3 925.66 998.97 4.39 o 1 3 3 116.89 116.85 1.03 o 3 3 3 873.83 933.31 5.16 o 5 3 3 334.36 344.80 2.72 o 7 3 3 35.41 37.06 0.98 o 9 3 3 55.07 89.20 1.57 o 11 3 3 31.13 36.00 2.41 o -10 4 3 1.68 1.30 0.80 o -8 4 3 1402.86 1350.38 8.86 o -6 4 3 0.02 0.11 0.27 o -4 4 3 115.63 115.47 1.18 o -2 4 3 261.31 254.93 1.57 o 0 4 3 6464.64 6876.42 31.62 o 2 4 3 835.16 892.71 4.39 o 4 4 3 1.41 0.08 0.26 o 6 4 3 0.64 -0.05 0.44 o 8 4 3 2.01 2.88 0.66 o 10 4 3 58.59 66.79 3.13 o -11 5 3 368.06 368.13 5.33 o -9 5 3 0.05 -0.75 0.75 o -7 5 3 106.99 106.60 1.70 o -5 5 3 718.29 718.32 3.96 o -3 5 3 13.98 16.68 0.55 o -1 5 3 31.28 26.54 0.58 o 1 5 3 4.86 1.13 0.30 o 3 5 3 71.87 76.21 1.19 o 5 5 3 103.38 102.19 1.61 o 7 5 3 17.90 16.66 1.10 o 9 5 3 10.24 11.51 1.00 o -10 6 3 1.36 1.07 1.25 o -8 6 3 78.18 79.28 1.89 o -6 6 3 263.07 253.48 3.53 o -4 6 3 425.87 436.06 3.25 o -2 6 3 588.41 600.04 3.89 o 0 6 3 98.59 199.52 4.32 o 2 6 3 54.86 58.82 1.12 o 4 6 3 24.96 27.32 1.09 o 6 6 3 53.68 56.18 1.40 o 8 6 3 2.77 2.67 0.72 o -9 7 3 9.52 10.26 1.52 o -7 7 3 249.84 257.00 3.62 o -5 7 3 366.96 365.17 3.71 o -3 7 3 312.50 312.39 2.96 o -1 7 3 118.67 121.44 1.88 o 1 7 3 0.03 0.01 0.43 o 3 7 3 158.68 152.80 2.21 o 5 7 3 0.38 -0.25 0.55 o 7 7 3 21.19 22.10 1.23 o -6 8 3 11.01 7.68 1.21 o -4 8 3 82.11 84.19 1.89 o -2 8 3 14.12 15.58 0.97 o 0 8 3 211.45 214.16 2.78 o 2 8 3 122.36 124.15 2.19 o 4 8 3 26.04 26.51 1.43 o 6 8 3 168.27 163.80 3.02 o -5 9 3 240.89 231.66 4.16 o -3 9 3 1.96 11.02 1.21 o -1 9 3 4.80 3.50 0.97 o 1 9 3 13.36 12.34 1.01 o 3 9 3 59.11 62.39 2.27 o -12 0 4 6.76 12.09 1.96 o -10 0 4 0.53 0.40 0.81 o -8 0 4 677.66 505.49 5.97 o -6 0 4 56.41 43.06 0.81 o -4 0 4 1018.90 1214.52 6.81 o -2 0 4 5985.33 5931.77 34.37 o 0 0 4 967.28 957.41 4.73 o 2 0 4 3649.20 3758.73 21.10 o 4 0 4 1250.05 1298.55 9.17 o 6 0 4 2597.67 2498.35 16.96 o 8 0 4 695.30 679.64 8.94 o 10 0 4 0.96 2.27 0.81 o 12 0 4 95.81 92.38 3.66 o -11 1 4 37.75 37.53 1.55 o -9 1 4 60.11 56.44 1.64 o -7 1 4 147.96 98.78 1.49 o -5 1 4 1147.50 1264.37 5.62 o -3 1 4 1.61 1.23 0.12 o -1 1 4 2905.65 3073.23 11.60 o 1 1 4 3297.87 3426.47 19.72 o 3 1 4 387.24 415.90 2.18 o 5 1 4 345.00 311.91 1.90 o 7 1 4 2502.56 2286.76 11.37 o 9 1 4 127.93 124.56 1.87 o 11 1 4 23.78 26.75 2.27 o -12 2 4 49.68 54.08 2.08 o -10 2 4 48.35 43.29 1.42 o -8 2 4 32.29 16.85 0.90 o -6 2 4 1.20 0.77 0.20 o -4 2 4 974.78 1097.14 4.74 o -2 2 4 34.79 46.92 0.49 o 0 2 4 2733.40 2867.70 11.51 o 2 2 4 44.86 45.34 0.60 o 4 2 4 415.82 402.97 2.36 o 6 2 4 8.33 4.87 0.42 o 8 2 4 293.40 281.84 2.59 o 10 2 4 766.13 759.34 5.64 o -11 3 4 31.37 25.04 1.48 o -9 3 4 108.32 93.26 1.81 o -7 3 4 7.32 7.00 0.54 o -5 3 4 44.08 39.67 0.67 o -3 3 4 313.62 338.27 1.87 o -1 3 4 1302.22 1367.24 6.34 o 1 3 4 10.20 8.44 0.29 o 3 3 4 2.58 2.20 0.21 o 5 3 4 9.20 6.74 0.51 o 7 3 4 252.17 248.36 2.49 o 9 3 4 5.54 4.34 0.64 o 11 3 4 146.65 154.92 3.34 o -10 4 4 0.17 0.45 0.76 o -8 4 4 7.42 9.22 0.71 o -6 4 4 12.88 15.84 0.60 o -4 4 4 84.84 82.93 0.99 o -2 4 4 473.72 500.72 2.46 o 0 4 4 4036.25 4275.64 17.27 o 2 4 4 1018.38 1065.12 5.54 o 4 4 4 5.48 11.18 0.67 o 6 4 4 13.75 10.68 0.76 o 8 4 4 17.85 20.79 1.11 o 10 4 4 25.28 30.65 1.63 o -11 5 4 158.46 152.28 3.44 o -9 5 4 13.89 12.82 1.01 o -7 5 4 140.86 144.80 1.70 o -5 5 4 404.95 399.42 2.61 o -3 5 4 11.29 10.59 0.46 o -1 5 4 573.62 605.88 3.43 o 1 5 4 182.53 196.67 1.87 o 3 5 4 332.53 339.89 3.07 o 5 5 4 2.68 2.91 0.50 o 7 5 4 190.83 181.70 2.93 o 9 5 4 160.05 170.92 2.75 o -10 6 4 51.37 47.10 2.15 o -8 6 4 456.83 446.08 4.04 o -6 6 4 9.11 9.00 0.69 o -4 6 4 237.66 227.20 2.26 o -2 6 4 24.90 23.69 0.82 o 0 6 4 527.11 551.55 3.88 o 2 6 4 256.18 253.76 2.65 o 4 6 4 214.06 217.62 2.74 o 6 6 4 60.71 51.00 1.62 o 8 6 4 70.39 72.49 1.76 o -9 7 4 43.72 50.41 4.98 o -7 7 4 306.47 289.50 3.85 o -5 7 4 430.58 433.34 3.87 o -3 7 4 129.47 124.60 1.95 o -1 7 4 72.46 70.56 1.36 o 1 7 4 43.89 42.21 1.41 o 3 7 4 0.02 0.42 0.49 o 5 7 4 160.73 156.04 2.41 o 7 7 4 223.29 220.20 3.11 o -6 8 4 746.19 739.00 7.90 o -4 8 4 82.87 79.95 2.29 o -2 8 4 52.70 48.74 1.72 o 0 8 4 93.02 110.58 2.01 o 2 8 4 129.57 129.01 2.26 o 4 8 4 0.14 -0.68 0.68 o 6 8 4 23.11 20.55 1.62 o -5 9 4 3.16 1.31 1.21 o -3 9 4 31.66 33.71 2.63 o -1 9 4 45.18 41.06 1.93 o 1 9 4 0.40 1.60 0.85 o 3 9 4 22.68 23.42 1.48 o -11 1 5 31.71 33.51 1.45 o -9 1 5 4.30 8.87 0.87 o -7 1 5 401.84 352.23 3.10 o -5 1 5 12.73 14.22 0.43 o -3 1 5 531.98 531.37 2.76 o -1 1 5 1764.27 1909.86 7.76 o 1 1 5 420.49 409.91 1.83 o 3 1 5 629.75 684.82 3.06 o 5 1 5 568.49 565.89 2.93 o 7 1 5 255.24 231.98 2.14 o 9 1 5 0.00 -0.47 0.47 o 11 1 5 135.76 133.51 2.24 o -12 2 5 255.57 283.38 4.07 o -10 2 5 0.00 -0.17 0.58 o -8 2 5 184.77 168.71 2.56 o -6 2 5 87.39 73.86 0.95 o -4 2 5 359.30 398.46 2.17 o -2 2 5 109.47 132.11 0.92 o 0 2 5 74.25 85.27 0.85 o 2 2 5 1314.37 1399.90 6.61 o 4 2 5 41.42 55.31 0.77 o 6 2 5 165.52 167.89 1.72 o 8 2 5 144.33 149.59 1.84 o 10 2 5 11.45 11.58 0.88 o -11 3 5 266.30 276.08 3.90 o -9 3 5 10.16 14.52 0.93 o -7 3 5 473.16 434.00 3.40 o -5 3 5 1743.78 1719.19 7.64 o -3 3 5 9.08 10.38 0.38 o -1 3 5 3321.95 3762.19 19.81 o 1 3 5 86.34 95.62 0.84 o 3 3 5 466.30 437.99 3.00 o 5 3 5 86.01 93.85 1.31 o 7 3 5 2508.26 2416.33 14.19 o 9 3 5 66.03 71.53 1.96 o 11 3 5 0.89 1.14 1.00 o -10 4 5 52.57 52.21 1.87 o -8 4 5 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