data_2300571 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.9633 _cell_length_b 9.0417 _cell_length_c 18.4007 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.7494 _cod_data_source_file ks54945_corrsup14.hkl _cod_data_source_block 5_corr _shelx_title ' uncorr_a.res in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 96.09 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3840.54 3802.31 24.13 o 4 0 0 547.99 571.72 4.52 o 6 0 0 866.67 883.57 9.58 o 1 1 0 97.20 115.69 0.62 o 2 1 0 581.28 555.48 2.57 o 3 1 0 45.31 43.12 0.44 o 4 1 0 237.97 224.11 1.51 o 5 1 0 23.49 22.36 0.71 o 6 1 0 116.14 112.14 1.69 o 7 1 0 10.65 11.80 0.80 o 0 2 0 8.44 9.58 0.27 o 1 2 0 57.78 70.00 0.62 o 2 2 0 335.63 365.35 1.95 o 3 2 0 1.27 0.27 0.09 o 4 2 0 56.13 56.69 0.71 o 5 2 0 484.76 474.12 3.73 o 6 2 0 0.01 0.44 0.35 o 7 2 0 45.23 44.89 1.33 o 1 3 0 1680.39 1678.69 8.34 o 2 3 0 1759.32 1949.64 9.76 o 3 3 0 186.35 206.36 1.60 o 4 3 0 245.87 271.22 1.95 o 5 3 0 128.43 119.51 1.86 o 6 3 0 15.18 17.21 0.89 o 7 3 0 14.25 13.75 0.89 o 0 4 0 1542.39 1746.03 13.22 o 1 4 0 10.68 6.39 0.35 o 2 4 0 252.94 282.75 2.04 o 3 4 0 1412.39 1347.49 7.19 o 4 4 0 259.18 252.94 2.13 o 5 4 0 236.79 228.28 2.84 o 6 4 0 27.77 27.50 1.06 o 7 4 0 0.01 0.18 0.44 o 1 5 0 2173.73 2251.38 12.07 o 2 5 0 366.88 406.16 2.93 o 3 5 0 171.83 162.36 1.60 o 4 5 0 123.87 118.35 1.60 o 5 5 0 125.12 121.19 1.86 o 6 5 0 17.33 15.53 0.89 o 7 5 0 95.52 108.33 2.31 o 0 6 0 554.49 555.22 5.32 o 1 6 0 259.03 259.86 2.22 o 2 6 0 201.55 188.27 1.86 o 3 6 0 1038.73 994.03 7.19 o 4 6 0 15.75 16.41 0.71 o 5 6 0 71.59 70.80 1.60 o 6 6 0 31.82 36.02 1.42 o 1 7 0 8.70 6.12 0.44 o 2 7 0 187.58 186.58 1.95 o 3 7 0 7.64 8.25 0.62 o 4 7 0 91.83 93.33 1.69 o 5 7 0 67.95 68.23 1.69 o 6 7 0 62.05 56.16 1.77 o 0 8 0 192.27 193.59 2.93 o 1 8 0 12.11 12.86 0.62 o 2 8 0 76.58 77.63 1.51 o 3 8 0 124.95 115.87 1.95 o 4 8 0 0.03 0.62 0.44 o 5 8 0 1.79 1.60 0.62 o 1 9 0 19.95 20.85 1.15 o 2 9 0 93.11 87.30 2.22 o 3 9 0 4.87 5.23 0.71 o 4 9 0 45.74 44.80 1.95 o 5 9 0 1.78 1.33 0.71 o 0 10 0 347.41 348.14 5.59 o 1 10 0 68.94 74.17 1.95 o 2 10 0 0.38 0.71 0.62 o 3 10 0 112.88 125.27 2.84 o 4 10 0 0.07 -0.71 0.71 o 1 11 0 298.27 298.99 4.79 o 2 11 0 52.34 55.98 2.13 o 3 11 0 30.59 24.93 1.60 o 0 12 0 12.62 16.06 2.13 o 1 0 1 816.18 852.25 3.99 o 2 0 1 340.24 387.36 2.04 o 3 0 1 391.08 361.36 2.13 o 4 0 1 1.20 0.35 0.09 o 5 0 1 316.36 307.24 2.93 o 6 0 1 0.73 0.71 0.35 o 7 0 1 33.67 33.54 1.15 o -7 1 1 24.74 28.04 1.06 o -6 1 1 19.93 19.16 0.89 o -5 1 1 66.42 67.16 1.24 o -4 1 1 114.59 114.89 1.15 o -3 1 1 603.07 632.05 3.55 o -2 1 1 111.96 119.95 0.89 o -1 1 1 2417.74 2323.60 11.18 o 0 1 1 920.29 951.71 4.17 o 1 1 1 2462.50 2367.87 8.96 o 2 1 1 108.26 116.14 0.80 o 3 1 1 592.43 624.24 3.02 o 4 1 1 120.54 122.70 0.98 o 5 1 1 64.85 63.97 0.98 o 6 1 1 20.53 19.08 0.80 o 7 1 1 25.02 28.57 1.06 o -7 2 1 7.22 6.12 0.71 o -6 2 1 6.84 5.94 0.53 o -5 2 1 238.40 240.61 2.40 o -4 2 1 9.42 10.38 0.35 o -3 2 1 143.11 127.58 0.98 o -2 2 1 344.44 352.75 1.95 o -1 2 1 979.48 1001.75 5.32 o 0 2 1 1678.24 1614.63 7.10 o 1 2 1 967.03 988.00 4.97 o 2 2 1 357.14 361.45 1.86 o 3 2 1 151.75 136.01 0.98 o 4 2 1 9.71 10.74 0.27 o 5 2 1 243.28 245.40 2.13 o 6 2 1 6.09 6.12 0.53 o 7 2 1 7.59 7.81 0.71 o -7 3 1 1.54 1.95 0.62 o -6 3 1 219.95 210.53 2.84 o -5 3 1 148.07 146.92 1.95 o -4 3 1 194.16 184.72 1.51 o -3 3 1 111.59 107.35 0.98 o -2 3 1 31.46 35.22 0.53 o -1 3 1 111.31 114.36 1.06 o 0 3 1 272.66 264.74 1.69 o 1 3 1 106.78 109.30 0.98 o 2 3 1 36.14 37.80 0.53 o 3 3 1 111.58 108.42 0.98 o 4 3 1 183.80 173.98 1.42 o 5 3 1 149.67 143.46 1.51 o 6 3 1 219.12 210.89 2.75 o 7 3 1 1.52 2.22 0.53 o -7 4 1 9.11 8.25 0.89 o -6 4 1 21.20 19.16 0.98 o -5 4 1 199.89 182.59 2.31 o -4 4 1 9.83 9.14 0.44 o -3 4 1 96.97 91.21 1.06 o -2 4 1 372.56 386.82 2.66 o -1 4 1 188.99 207.87 1.69 o 0 4 1 2864.56 2814.49 14.64 o 1 4 1 190.28 209.74 1.60 o 2 4 1 360.57 370.23 2.48 o 3 4 1 97.38 88.72 0.98 o 4 4 1 9.60 8.34 0.44 o 5 4 1 200.72 180.90 2.40 o 6 4 1 21.45 20.49 0.89 o 7 4 1 8.98 8.25 0.80 o -7 5 1 17.19 18.99 1.24 o -6 5 1 48.83 51.46 1.60 o -5 5 1 30.91 28.30 0.98 o -4 5 1 16.16 14.82 0.62 o -3 5 1 44.99 44.72 0.80 o -2 5 1 58.45 51.28 0.80 o -1 5 1 600.61 610.49 3.90 o 0 5 1 320.64 362.25 2.57 o 1 5 1 600.30 609.69 3.64 o 2 5 1 62.83 56.43 0.80 o 3 5 1 46.63 46.22 0.80 o 4 5 1 15.41 15.53 0.62 o 5 5 1 31.31 29.46 0.98 o 6 5 1 47.78 47.29 1.33 o 7 5 1 17.92 18.90 0.98 o -6 6 1 4.64 5.23 0.71 o -5 6 1 58.77 58.20 1.51 o -4 6 1 44.61 43.30 1.06 o -3 6 1 83.50 84.99 1.24 o -2 6 1 111.25 113.47 1.42 o -1 6 1 120.01 128.73 1.42 o 0 6 1 151.80 139.82 1.51 o 1 6 1 116.08 127.31 1.42 o 2 6 1 115.90 117.47 1.33 o 3 6 1 77.86 79.41 1.33 o 4 6 1 44.64 44.72 0.98 o 5 6 1 61.26 63.26 1.51 o 6 6 1 4.14 5.23 0.62 o -6 7 1 1.74 1.24 0.62 o -5 7 1 12.52 13.40 0.89 o -4 7 1 13.43 13.13 0.80 o -3 7 1 123.65 126.69 1.86 o -2 7 1 155.98 152.51 1.77 o -1 7 1 316.88 314.78 2.66 o 0 7 1 34.17 33.09 0.80 o 1 7 1 322.87 321.17 2.66 o 2 7 1 154.81 148.96 1.86 o 3 7 1 125.32 129.27 1.86 o 4 7 1 13.75 13.75 0.80 o 5 7 1 12.40 12.15 0.89 o 6 7 1 1.73 0.98 0.62 o -5 8 1 73.01 76.39 1.86 o -4 8 1 8.14 7.19 0.62 o -3 8 1 117.91 116.93 1.95 o -2 8 1 138.46 138.94 1.95 o -1 8 1 24.67 22.54 0.71 o 0 8 1 147.50 167.86 1.86 o 1 8 1 24.59 22.54 0.71 o 2 8 1 140.18 146.03 2.13 o 3 8 1 117.30 117.91 2.13 o 4 8 1 8.34 8.25 0.89 o 5 8 1 73.03 73.02 2.04 o -5 9 1 0.69 1.24 0.80 o -4 9 1 75.47 75.77 2.48 o -3 9 1 54.43 49.51 1.77 o -2 9 1 70.50 76.48 2.13 o -1 9 1 89.32 89.79 1.77 o 0 9 1 69.48 70.09 1.42 o 1 9 1 83.58 84.11 1.69 o 2 9 1 71.13 76.30 1.77 o 3 9 1 53.99 50.13 1.51 o 4 9 1 75.12 69.91 2.04 o 5 9 1 0.84 1.77 0.71 o -4 10 1 8.92 9.49 1.24 o -3 10 1 8.97 11.00 1.06 o -2 10 1 98.32 96.08 2.48 o -1 10 1 13.93 11.36 0.98 o 0 10 1 113.29 118.35 2.22 o 1 10 1 14.34 14.37 1.24 o 2 10 1 101.03 99.99 2.57 o 3 10 1 9.32 9.40 1.06 o 4 10 1 8.87 10.74 1.33 o -3 11 1 11.46 11.00 1.15 o -2 11 1 61.88 61.48 2.22 o -1 11 1 21.46 19.61 1.51 o 0 11 1 49.07 45.25 1.95 o 1 11 1 21.31 19.78 1.51 o 2 11 1 61.69 62.37 2.22 o 3 11 1 11.70 11.80 1.24 o 0 12 1 56.64 58.20 2.40 o 0 0 2 825.53 797.96 4.08 o 1 0 2 251.17 265.28 1.24 o 2 0 2 2164.19 2198.42 11.27 o 3 0 2 175.72 181.08 1.24 o 4 0 2 139.64 132.55 1.06 o 5 0 2 19.46 20.85 0.71 o 6 0 2 37.20 37.44 0.98 o 7 0 2 2.26 2.84 0.53 o -7 1 2 16.45 14.91 0.80 o -6 1 2 200.34 192.88 2.48 o -5 1 2 92.31 94.84 1.42 o -4 1 2 876.07 855.27 4.79 o -3 1 2 238.03 266.61 1.77 o -2 1 2 2117.80 2156.72 9.94 o -1 1 2 5060.90 4997.38 24.84 o 0 1 2 3964.70 3746.86 17.57 o 1 1 2 5037.35 4991.97 18.81 o 2 1 2 2113.03 2154.77 9.05 o 3 1 2 233.35 263.06 1.51 o 4 1 2 871.08 844.62 4.26 o 5 1 2 92.73 92.45 1.15 o 6 1 2 197.41 190.75 2.22 o 7 1 2 16.21 15.70 0.98 o -7 2 2 38.27 38.24 1.24 o -6 2 2 107.57 109.22 1.95 o -5 2 2 70.16 65.92 1.24 o -4 2 2 90.77 94.31 1.06 o -3 2 2 76.43 77.63 0.80 o -2 2 2 358.08 370.85 2.22 o -1 2 2 4332.68 4295.87 20.32 o 0 2 2 9233.00 8202.34 34.87 o 1 2 2 4357.50 4284.25 16.86 o 2 2 2 367.60 380.79 2.13 o 3 2 2 71.51 71.07 0.62 o 4 2 2 91.06 93.33 0.89 o 5 2 2 67.32 61.93 0.89 o 6 2 2 108.08 110.72 1.60 o 7 2 2 37.07 37.71 1.15 o -7 3 2 85.93 87.57 2.22 o -6 3 2 18.17 19.16 0.98 o -5 3 2 84.76 82.95 1.42 o -4 3 2 28.22 27.15 0.53 o -3 3 2 401.73 422.40 2.31 o -2 3 2 13.68 12.86 0.35 o -1 3 2 2614.62 2699.96 13.93 o 0 3 2 98.19 103.71 0.80 o 1 3 2 2636.99 2681.50 12.33 o 2 3 2 12.63 12.24 0.27 o 3 3 2 411.37 430.30 2.31 o 4 3 2 26.48 26.00 0.62 o 5 3 2 85.07 82.07 1.06 o 6 3 2 18.74 19.96 0.80 o 7 3 2 88.20 94.40 1.86 o -7 4 2 7.13 6.03 0.80 o -6 4 2 4.55 3.82 0.62 o -5 4 2 358.43 346.01 3.46 o -4 4 2 22.53 20.14 0.62 o -3 4 2 764.71 760.78 4.79 o -2 4 2 54.69 52.88 0.80 o -1 4 2 620.05 664.25 4.08 o 0 4 2 147.76 168.92 1.42 o 1 4 2 619.26 660.08 3.55 o 2 4 2 55.49 54.30 0.71 o 3 4 2 760.54 764.06 4.35 o 4 4 2 22.22 19.70 0.62 o 5 4 2 358.01 337.58 3.55 o 6 4 2 4.59 3.90 0.44 o 7 4 2 7.61 7.45 0.62 o -7 5 2 41.50 42.59 1.69 o -6 5 2 55.37 53.23 1.69 o -5 5 2 68.70 63.97 1.51 o -4 5 2 283.93 270.87 2.57 o -3 5 2 174.05 187.29 1.86 o -2 5 2 153.29 163.96 1.60 o -1 5 2 696.22 646.51 4.08 o 0 5 2 90.42 90.58 1.06 o 1 5 2 693.56 645.18 3.82 o 2 5 2 159.52 170.08 1.42 o 3 5 2 172.41 184.18 1.95 o 4 5 2 276.16 262.97 2.75 o 5 5 2 69.30 68.67 1.42 o 6 5 2 53.73 54.03 1.33 o 7 5 2 41.69 46.67 2.04 o -6 6 2 19.59 21.03 1.24 o -5 6 2 88.15 90.05 1.86 o -4 6 2 1.95 3.55 0.44 o -3 6 2 270.64 260.84 2.48 o -2 6 2 242.26 232.54 2.13 o -1 6 2 117.20 110.01 1.33 o 0 6 2 934.46 918.17 5.59 o 1 6 2 114.36 111.88 1.33 o 2 6 2 247.50 239.10 1.95 o 3 6 2 272.96 261.99 2.57 o 4 6 2 1.87 2.75 0.44 o 5 6 2 89.43 93.78 1.77 o 6 6 2 19.16 18.01 0.89 o -6 7 2 42.98 43.92 1.69 o -5 7 2 3.85 3.90 0.62 o -4 7 2 208.01 207.25 2.57 o -3 7 2 76.78 78.34 1.51 o -2 7 2 325.86 310.08 2.75 o -1 7 2 55.52 50.39 0.98 o 0 7 2 151.40 168.92 1.77 o 1 7 2 55.61 48.62 0.89 o 2 7 2 330.22 314.34 2.93 o 3 7 2 76.80 75.32 1.42 o 4 7 2 209.31 205.30 2.57 o 5 7 2 3.73 4.26 0.62 o 6 7 2 40.53 41.79 1.60 o -5 8 2 11.04 8.61 0.98 o -4 8 2 21.64 19.78 1.06 o -3 8 2 27.75 27.15 1.15 o -2 8 2 70.26 73.55 1.42 o -1 8 2 43.76 43.92 1.06 o 0 8 2 272.92 270.51 2.75 o 1 8 2 44.58 43.47 1.06 o 2 8 2 68.17 74.08 1.69 o 3 8 2 26.95 25.46 1.06 o 4 8 2 21.66 19.34 1.15 o 5 8 2 11.09 10.56 1.06 o -5 9 2 1.15 1.51 0.89 o -4 9 2 26.16 28.39 1.51 o -3 9 2 30.59 27.50 1.24 o -2 9 2 64.19 68.14 1.69 o -1 9 2 192.57 200.24 2.48 o 0 9 2 203.53 199.00 2.48 o 1 9 2 189.83 198.11 2.75 o 2 9 2 63.11 66.36 1.69 o 3 9 2 29.76 27.33 1.24 o 4 9 2 27.22 34.07 1.60 o 5 9 2 1.15 0.53 0.71 o -4 10 2 13.84 16.68 1.51 o -3 10 2 137.85 132.82 2.93 o -2 10 2 81.93 81.80 2.31 o -1 10 2 10.77 11.27 0.98 o 0 10 2 64.55 66.19 1.86 o 1 10 2 10.48 11.98 1.15 o 2 10 2 81.87 82.69 2.31 o 3 10 2 135.83 129.44 2.93 o 4 10 2 13.70 15.08 1.42 o -3 11 2 13.04 12.86 1.24 o -2 11 2 0.06 0.18 0.71 o -1 11 2 72.83 79.41 2.84 o 0 11 2 44.61 44.54 1.77 o 1 11 2 70.18 73.11 2.40 o 2 11 2 0.07 0.62 0.71 o 3 11 2 12.41 12.24 1.24 o 0 12 2 1.15 1.42 1.06 o 1 0 3 2506.05 2410.90 11.53 o 2 0 3 3796.38 3711.29 16.86 o 3 0 3 348.09 313.98 1.95 o 4 0 3 165.18 164.05 1.33 o 5 0 3 364.71 348.76 2.75 o 6 0 3 1.97 1.77 0.35 o 7 0 3 4.73 5.68 0.62 o -7 1 3 78.41 81.98 2.04 o -6 1 3 113.24 113.30 1.86 o -5 1 3 142.01 136.81 1.77 o -4 1 3 86.90 88.63 0.98 o -3 1 3 98.40 112.41 0.98 o -2 1 3 116.20 125.27 1.06 o -1 1 3 7001.71 6564.82 29.19 o 0 1 3 1399.19 1482.08 6.48 o 1 1 3 6992.95 6565.79 25.64 o 2 1 3 117.43 126.16 0.89 o 3 1 3 103.96 119.24 0.89 o 4 1 3 87.79 90.41 0.89 o 5 1 3 142.57 140.00 1.42 o 6 1 3 112.21 110.19 1.60 o 7 1 3 78.03 82.60 1.86 o -7 2 3 20.11 20.67 1.15 o -6 2 3 31.42 29.19 1.15 o -5 2 3 91.59 96.08 1.60 o -4 2 3 105.85 108.95 1.24 o -3 2 3 370.10 385.05 2.48 o -2 2 3 749.91 789.44 4.52 o -1 2 3 143.11 158.81 1.42 o 0 2 3 9.25 13.04 0.27 o 1 2 3 147.00 162.98 0.98 o 2 2 3 773.03 805.94 3.82 o 3 2 3 370.58 394.45 2.48 o 4 2 3 105.37 107.97 0.98 o 5 2 3 86.51 89.25 1.06 o 6 2 3 29.60 29.63 0.89 o 7 2 3 20.39 20.23 0.89 o -7 3 3 1.53 2.04 0.62 o -6 3 3 64.26 62.55 1.77 o -5 3 3 97.01 96.62 1.77 o -4 3 3 325.28 304.14 2.84 o -3 3 3 386.55 395.34 2.31 o -2 3 3 168.89 166.35 1.42 o -1 3 3 783.65 852.96 4.88 o 0 3 3 68.63 71.86 0.62 o 1 3 3 778.67 851.63 3.90 o 2 3 3 157.15 155.88 1.15 o 3 3 3 384.53 397.03 2.13 o 4 3 3 334.71 314.16 2.31 o 5 3 3 98.95 99.63 1.33 o 6 3 3 64.75 62.81 1.24 o 7 3 3 1.34 0.98 0.62 o -7 4 3 13.53 14.37 1.15 o -6 4 3 39.97 39.48 1.42 o -5 4 3 61.32 60.51 1.24 o -4 4 3 96.66 101.05 1.42 o -3 4 3 122.28 116.67 1.33 o -2 4 3 571.46 582.36 3.73 o -1 4 3 422.13 438.73 2.93 o 0 4 3 659.85 628.50 3.46 o 1 4 3 419.29 434.91 2.57 o 2 4 3 567.79 584.49 3.19 o 3 4 3 121.45 116.14 1.15 o 4 4 3 95.99 102.65 1.33 o 5 4 3 62.88 60.24 1.15 o 6 4 3 41.34 42.85 1.69 o 7 4 3 13.89 14.82 1.33 o -7 5 3 38.83 39.92 1.69 o -6 5 3 26.40 26.71 1.33 o -5 5 3 33.90 35.84 1.15 o -4 5 3 494.84 463.57 3.73 o -3 5 3 178.92 177.18 1.77 o -2 5 3 878.55 874.26 5.41 o -1 5 3 545.67 577.40 3.82 o 0 5 3 40.91 49.06 0.71 o 1 5 3 541.83 574.20 3.37 o 2 5 3 874.04 872.22 4.70 o 3 5 3 182.30 179.84 1.69 o 4 5 3 487.91 463.92 3.99 o 5 5 3 34.61 36.02 0.98 o 6 5 3 26.35 27.68 1.51 o 7 5 3 39.79 40.55 2.13 o -6 6 3 57.21 63.17 1.95 o -5 6 3 228.54 215.50 3.02 o -4 6 3 39.93 36.82 1.06 o -3 6 3 226.92 228.90 2.31 o -2 6 3 173.31 173.80 1.77 o -1 6 3 232.33 243.10 2.13 o 0 6 3 497.00 508.55 3.55 o 1 6 3 233.81 245.49 2.13 o 2 6 3 172.23 173.01 1.77 o 3 6 3 223.43 225.26 2.31 o 4 6 3 39.03 38.24 0.98 o 5 6 3 230.48 221.18 2.84 o 6 6 3 57.17 59.09 1.33 o -6 7 3 3.06 3.37 0.80 o -5 7 3 46.46 46.05 1.42 o -4 7 3 3.10 4.17 0.53 o -3 7 3 257.78 253.48 2.66 o -2 7 3 25.49 25.02 0.71 o -1 7 3 163.09 167.77 1.86 o 0 7 3 7.33 8.78 0.44 o 1 7 3 172.69 177.35 1.77 o 2 7 3 26.40 26.44 0.80 o 3 7 3 263.44 256.94 2.66 o 4 7 3 3.29 4.26 0.53 o 5 7 3 45.21 41.52 1.42 o 6 7 3 2.89 2.31 0.53 o -5 8 3 17.80 18.28 1.24 o -4 8 3 6.67 7.01 0.71 o -3 8 3 48.33 49.60 1.42 o -2 8 3 217.28 214.44 2.48 o -1 8 3 26.15 29.81 0.89 o 0 8 3 20.57 24.93 0.89 o 1 8 3 28.00 31.05 1.06 o 2 8 3 220.30 215.24 3.02 o 3 8 3 46.57 48.89 1.42 o 4 8 3 6.88 6.83 0.80 o 5 8 3 17.47 17.39 1.24 o -5 9 3 1.83 1.33 0.80 o -4 9 3 85.00 84.82 2.04 o -3 9 3 43.68 46.40 1.51 o -2 9 3 87.47 90.32 1.95 o -1 9 3 88.85 90.58 1.69 o 0 9 3 64.81 65.83 1.42 o 1 9 3 87.80 89.52 1.77 o 2 9 3 88.93 88.90 1.95 o 3 9 3 42.51 43.56 1.42 o 4 9 3 83.52 80.12 2.22 o 5 9 3 1.82 1.06 0.71 o -4 10 3 2.66 2.48 0.80 o -3 10 3 16.88 16.95 1.33 o -2 10 3 89.22 90.85 2.48 o -1 10 3 67.71 68.14 1.69 o 0 10 3 303.22 305.02 4.17 o 1 10 3 66.37 65.83 2.13 o 2 10 3 89.88 87.75 2.40 o 3 10 3 17.37 18.01 1.33 o 4 10 3 2.75 2.93 0.89 o -3 11 3 21.41 23.33 1.60 o -2 11 3 40.31 43.03 1.95 o -1 11 3 36.40 39.21 2.31 o 0 11 3 34.38 40.37 1.69 o 1 11 3 36.67 40.19 1.86 o 2 11 3 40.32 46.49 2.04 o 3 11 3 21.41 21.65 1.60 o 0 0 4 1365.39 1234.37 6.83 o 1 0 4 18.96 18.01 0.27 o 2 0 4 329.78 317.98 1.86 o 3 0 4 0.08 1.06 0.18 o 4 0 4 133.63 148.16 1.33 o 5 0 4 66.40 60.95 0.98 o 6 0 4 70.17 69.82 1.69 o 7 0 4 0.01 0.62 0.53 o -7 1 4 3.15 2.75 0.71 o -6 1 4 56.28 57.76 1.69 o -5 1 4 81.84 84.73 1.42 o -4 1 4 692.49 685.81 4.61 o -3 1 4 10.06 8.34 0.27 o -2 1 4 650.27 656.89 3.64 o -1 1 4 2560.80 2657.37 12.60 o 0 1 4 399.92 418.14 2.04 o 1 1 4 2563.69 2620.99 11.45 o 2 1 4 661.99 669.75 3.19 o 3 1 4 9.36 9.76 0.27 o 4 1 4 691.02 680.31 3.99 o 5 1 4 80.03 80.38 1.06 o 6 1 4 59.26 59.71 1.42 o 7 1 4 3.17 2.57 0.62 o -7 2 4 4.17 4.52 0.71 o -6 2 4 109.36 109.93 2.31 o -5 2 4 187.66 176.73 2.57 o -4 2 4 31.64 31.76 0.80 o -3 2 4 968.81 1002.90 5.77 o -2 2 4 983.82 1070.60 6.48 o -1 2 4 2907.08 3020.77 13.75 o 0 2 4 301.93 307.60 1.86 o 1 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