data_2310155 _cell_angle_alpha 90.000 _cell_angle_beta 90.003 _cell_angle_gamma 90.000 _cell_length_a 13.3761 _cell_length_b 20.1111 _cell_length_c 19.8781 _exptl_crystal_F_000 2968.00 _reflns_d_resolution_high 0.7413 _[local]_cod_data_source_file bp5072str05h_twin_f_co2sup2.hkl _[local]_cod_data_source_block str05h_twin_f_co2 _shelx_title ' F_CO2_STR05h_twin in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 902.17 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 65737.16 66961.45 2729.55 o 4 0 0 15792.48 16098.00 423.48 o 6 0 0 35733.68 29601.99 466.90 o 8 0 0 247735.34 263925.84 3873.19 o 10 0 0 2008.45 2114.49 353.05 o 12 0 0 3761.79 4625.63 640.58 o 14 0 0 82916.09 89896.85 2818.31 o 16 0 0 617.93 54.20 731.52 o 1 1 0 162734.84 159293.19 1392.58 o 2 1 0 73943.21 70436.91 412.94 o 3 1 0 34093.69 35178.46 603.55 o 4 1 0 124627.27 130568.05 1736.06 o 5 1 0 9950.30 9157.38 209.89 o 6 1 0 14402.07 13262.62 305.51 o 7 1 0 755.83 1015.38 188.19 o 8 1 0 22756.15 24372.47 473.41 o 9 1 0 23286.48 23662.04 428.99 o 10 1 0 28298.33 29072.39 496.99 o 11 1 0 11022.64 10847.44 428.17 o 12 1 0 16998.82 16742.74 504.77 o 13 1 0 4668.30 5832.44 489.06 o 14 1 0 3311.65 3544.69 476.48 o 15 1 0 2650.95 2986.21 568.77 o 16 1 0 52.21 356.91 564.98 o 17 1 0 3.78 592.91 693.68 o 0 2 0 199293.89 173640.05 12022.51 o 1 2 0 4048.68 3500.51 78.25 o 2 2 0 38899.33 38219.58 951.87 o 3 2 0 32191.45 33958.60 556.73 o 4 2 0 12284.96 12006.51 197.30 o 5 2 0 10627.36 12077.76 213.61 o 6 2 0 2198.43 3154.58 171.46 o 7 2 0 17248.28 17858.36 305.47 o 8 2 0 512.08 657.24 173.04 o 9 2 0 11101.93 11781.82 375.98 o 10 2 0 7472.76 7834.87 346.01 o 11 2 0 1374.07 1413.62 300.37 o 12 2 0 4061.54 4753.36 401.84 o 13 2 0 1177.61 750.22 384.71 o 14 2 0 3628.02 4459.09 499.72 o 15 2 0 755.43 554.62 488.79 o 16 2 0 0.46 171.56 564.60 o 17 2 0 3050.66 3269.55 736.58 o 1 3 0 76065.80 71860.55 1917.31 o 2 3 0 985.26 1327.17 132.70 o 3 3 0 457674.53 486021.50 4313.81 o 4 3 0 2444.64 2455.57 154.79 o 5 3 0 59857.20 60258.37 849.41 o 6 3 0 5956.69 6487.08 200.41 o 7 3 0 32193.47 34313.52 389.82 o 8 3 0 1190.06 1666.81 190.82 o 9 3 0 10764.09 11467.53 390.89 o 10 3 0 1701.11 2102.25 293.02 o 11 3 0 17242.74 19237.14 475.23 o 12 3 0 43.25 19.95 339.19 o 13 3 0 566.21 1025.93 383.32 o 14 3 0 3161.34 3555.19 466.91 o 15 3 0 92.52 60.53 426.74 o 16 3 0 32.65 -326.65 537.27 o 17 3 0 7165.56 8951.74 3253.72 o 0 4 0 58540.56 56510.86 1045.46 o 1 4 0 5122.07 4827.62 261.40 o 2 4 0 400.59 634.51 113.24 o 3 4 0 7126.89 7105.53 259.57 o 4 4 0 2670.59 3440.97 145.15 o 5 4 0 422.41 1167.49 124.27 o 6 4 0 1641.72 3026.00 172.15 o 7 4 0 11734.14 12924.33 273.89 o 8 4 0 8.09 -16.51 161.62 o 9 4 0 141.96 563.01 221.19 o 10 4 0 1450.29 1528.19 276.11 o 11 4 0 17777.53 17129.88 574.40 o 12 4 0 5685.73 5872.22 482.87 o 13 4 0 732.65 634.77 373.71 o 14 4 0 4339.32 4645.53 509.78 o 15 4 0 157.59 471.08 451.37 o 16 4 0 224.35 -327.60 661.58 o 17 4 0 22.83 268.39 1011.34 o 1 5 0 813913.25 820896.38 21992.36 o 2 5 0 1369.53 1376.82 128.74 o 3 5 0 173479.25 173096.03 2280.42 o 4 5 0 1758.71 2193.81 139.02 o 5 5 0 1392.62 140.50 117.78 o 6 5 0 1082.43 1152.38 157.67 o 7 5 0 2754.71 2895.14 192.92 o 8 5 0 768.25 618.13 209.32 o 9 5 0 173844.14 173501.23 1965.92 o 10 5 0 801.32 454.11 297.17 o 11 5 0 53971.41 55393.63 804.70 o 12 5 0 841.70 697.82 491.90 o 13 5 0 27093.63 29258.44 882.04 o 14 5 0 21.14 138.24 450.28 o 15 5 0 8543.58 9385.50 788.28 o 16 5 0 24.30 1213.69 471.96 o 17 5 0 4367.45 5461.68 1563.53 o 0 6 0 116736.83 115845.28 952.98 o 1 6 0 25429.82 25527.47 488.62 o 2 6 0 70.45 80.97 112.19 o 3 6 0 42168.86 40693.01 753.52 o 4 6 0 947.12 1432.66 139.34 o 5 6 0 20049.63 18461.48 273.18 o 6 6 0 924.60 1303.33 159.24 o 7 6 0 17648.53 17740.13 315.44 o 8 6 0 3921.80 4338.85 299.74 o 9 6 0 4463.46 5143.64 564.27 o 10 6 0 6884.47 7832.62 483.37 o 11 6 0 21714.99 22475.58 640.18 o 12 6 0 4822.19 4760.12 495.49 o 13 6 0 6.47 875.61 568.22 o 14 6 0 8293.92 9551.45 730.66 o 15 6 0 1943.38 3660.70 524.96 o 16 6 0 0.09 1165.49 474.42 o 17 6 0 805.03 921.21 1159.78 o 1 7 0 7313.93 6294.89 204.70 o 2 7 0 13321.18 12088.13 363.18 o 3 7 0 61137.46 50722.98 1178.66 o 4 7 0 35984.55 33353.89 605.42 o 5 7 0 1811.90 2334.97 174.90 o 6 7 0 6862.42 7093.21 229.04 o 7 7 0 6258.02 6813.96 233.91 o 8 7 0 39502.02 38655.52 656.24 o 9 7 0 2089.61 2525.08 327.18 o 10 7 0 118.64 177.05 305.61 o 11 7 0 27926.88 27924.72 637.25 o 12 7 0 424.12 344.82 349.98 o 13 7 0 11844.36 12679.34 648.94 o 14 7 0 439.12 851.27 492.41 o 15 7 0 307.35 996.27 439.89 o 16 7 0 3575.76 4818.49 587.65 o 0 8 0 132378.84 129551.11 922.14 o 1 8 0 5626.09 5833.66 282.76 o 2 8 0 10286.42 5534.42 203.77 o 3 8 0 2011.70 2160.80 171.09 o 4 8 0 231579.69 236444.06 5139.68 o 5 8 0 8956.96 8091.49 251.81 o 6 8 0 210569.72 206431.30 2920.56 o 7 8 0 8159.21 7770.56 309.07 o 8 8 0 141208.58 142915.13 1652.11 o 9 8 0 331.29 207.06 284.90 o 10 8 0 16898.09 17490.73 533.33 o 11 8 0 159.18 182.84 333.26 o 12 8 0 51640.07 54089.28 1681.57 o 13 8 0 651.09 838.07 441.46 o 14 8 0 11260.07 10659.10 736.31 o 15 8 0 464.53 1610.07 545.33 o 16 8 0 24655.48 26746.15 1088.06 o 1 9 0 1396.95 2073.87 173.62 o 2 9 0 2638.33 3878.08 203.16 o 3 9 0 2313.06 2283.28 189.64 o 4 9 0 7845.30 7817.96 263.30 o 5 9 0 3655.52 4069.48 233.02 o 6 9 0 6214.00 6613.68 260.88 o 7 9 0 280.90 472.48 243.67 o 8 9 0 20512.74 21314.30 515.10 o 9 9 0 1912.11 2184.47 345.67 o 10 9 0 4528.95 4134.72 412.24 o 11 9 0 100.19 588.74 345.06 o 12 9 0 1081.62 640.76 403.57 o 13 9 0 83.48 5.41 490.39 o 14 9 0 278.74 806.79 442.19 o 15 9 0 634.34 1645.48 686.25 o 16 9 0 1023.15 2720.72 712.25 o 0 10 0 448654.09 476004.09 5894.42 o 1 10 0 1364.70 1862.03 185.43 o 2 10 0 1293.52 2840.23 200.91 o 3 10 0 2546.45 2750.50 210.02 o 4 10 0 7242.06 7793.95 270.41 o 5 10 0 57.01 -164.17 166.26 o 6 10 0 5137.60 6019.78 289.04 o 7 10 0 13.63 -92.77 247.73 o 8 10 0 45624.86 43556.77 685.75 o 9 10 0 379.14 449.87 315.21 o 10 10 0 6890.28 7892.04 482.31 o 11 10 0 5399.37 6145.11 517.88 o 12 10 0 41.51 102.68 394.13 o 13 10 0 0.09 -750.16 750.16 o 14 10 0 1256.90 1910.74 598.73 o 15 10 0 55.94 501.48 837.18 o 16 10 0 532.04 2695.60 977.70 o 1 11 0 8818.32 9566.06 294.35 o 2 11 0 33534.71 33243.04 424.67 o 3 11 0 9440.56 9342.09 292.36 o 4 11 0 9800.95 9909.88 298.25 o 5 11 0 944.47 933.41 218.32 o 6 11 0 32542.89 32010.59 572.36 o 7 11 0 6255.48 7095.67 401.62 o 8 11 0 5989.14 7008.17 448.75 o 9 11 0 2079.72 2957.73 381.53 o 10 11 0 5972.53 6534.45 498.22 o 11 11 0 5456.00 7063.49 532.72 o 12 11 0 3633.81 3763.41 591.64 o 13 11 0 603.23 419.11 624.60 o 14 11 0 275.38 -288.88 565.05 o 15 11 0 4.90 -357.88 566.25 o 0 12 0 34.52 76.43 233.36 o 1 12 0 8563.85 8677.18 294.61 o 2 12 0 65735.75 62160.81 686.31 o 3 12 0 26179.58 24998.63 401.50 o 4 12 0 39312.04 35424.24 739.12 o 5 12 0 23036.68 22058.92 443.37 o 6 12 0 15059.26 15052.80 465.15 o 7 12 0 40242.48 38003.26 660.94 o 8 12 0 13733.17 12195.61 486.26 o 9 12 0 6564.66 7793.84 474.54 o 10 12 0 8604.89 8760.81 547.94 o 11 12 0 366.72 108.29 459.43 o 12 12 0 18244.91 16625.54 781.68 o 13 12 0 570.80 -176.73 493.11 o 14 12 0 370.78 63.97 593.61 o 15 12 0 661.36 489.44 601.09 o 1 13 0 9114.53 9422.48 333.82 o 2 13 0 9167.45 9001.40 308.57 o 3 13 0 528009.19 504186.06 5126.55 o 4 13 0 10151.78 9783.93 362.13 o 5 13 0 72631.04 67184.23 955.73 o 6 13 0 15678.59 14139.64 479.34 o 7 13 0 11408.37 10381.80 462.86 o 8 13 0 9126.87 9719.98 484.25 o 9 13 0 13567.15 14047.15 911.27 o 10 13 0 1599.42 2293.17 510.09 o 11 13 0 85405.45 81758.73 1396.56 o 12 13 0 198.28 -462.78 462.78 o 13 13 0 1228.58 1520.08 629.04 o 14 13 0 64.69 -430.79 883.66 o 0 14 0 7378.74 7586.66 509.06 o 1 14 0 0.73 -43.04 188.89 o 2 14 0 332.61 550.94 207.78 o 3 14 0 25280.82 24666.58 488.50 o 4 14 0 1438.97 2148.12 277.48 o 5 14 0 50710.93 46521.55 903.14 o 6 14 0 19713.50 18345.40 534.54 o 7 14 0 38597.99 35502.54 684.93 o 8 14 0 11759.70 11537.91 652.69 o 9 14 0 21854.04 21149.40 795.71 o 10 14 0 88.74 -277.91 431.90 o 11 14 0 105.40 -85.84 541.62 o 12 14 0 17.39 -466.85 466.85 o 13 14 0 12.28 -535.39 535.39 o 14 14 0 1903.06 1091.85 606.43 o 1 15 0 9972.66 9437.19 345.09 o 2 15 0 4082.28 4055.14 289.63 o 3 15 0 4062.04 4817.65 337.96 o 4 15 0 2885.16 3701.29 325.15 o 5 15 0 21506.41 19688.31 544.91 o 6 15 0 31.18 -61.78 326.07 o 7 15 0 3308.21 3490.59 452.42 o 8 15 0 146.50 -151.14 408.88 o 9 15 0 9100.06 9898.77 700.67 o 10 15 0 1738.48 1190.49 502.87 o 11 15 0 1217.25 1084.63 534.49 o 12 15 0 2437.02 2206.95 846.14 o 13 15 0 5363.93 5929.99 932.55 o 14 15 0 284.52 -1892.07 1892.07 o 0 16 0 213481.64 196173.20 4375.82 o 1 16 0 844.13 1062.53 247.18 o 2 16 0 78010.28 69857.92 1006.87 o 3 16 0 19.57 -118.53 246.75 o 4 16 0 7221.99 7393.70 395.94 o 5 16 0 1691.83 1071.18 363.90 o 6 16 0 28121.34 27915.99 721.26 o 7 16 0 77.34 -332.13 408.97 o 8 16 0 15904.74 17008.07 749.06 o 9 16 0 2283.17 1649.11 598.18 o 10 16 0 584.72 84.67 464.76 o 11 16 0 41.13 -682.11 733.59 o 12 16 0 1810.86 2225.53 585.56 o 13 16 0 1.39 -727.30 727.30 o 14 16 0 11513.35 7730.55 2386.85 o 1 17 0 245.49 166.17 237.32 o 2 17 0 2822.71 3234.45 330.67 o 3 17 0 4468.80 5160.22 404.33 o 4 17 0 2523.28 3314.72 415.42 o 5 17 0 35.37 -280.53 317.18 o 6 17 0 3939.25 4150.65 547.94 o 7 17 0 13.77 -230.90 589.42 o 8 17 0 1767.38 1624.00 512.80 o 9 17 0 540.62 398.03 477.16 o 10 17 0 1087.90 1090.11 524.97 o 11 17 0 965.31 20.94 611.32 o 12 17 0 2849.23 2995.09 764.05 o 13 17 0 2507.78 -509.75 1071.10 o 0 18 0 40051.08 35481.07 1101.53 o 1 18 0 1306.38 1033.91 287.86 o 2 18 0 43108.98 39503.63 1059.44 o 3 18 0 2464.36 2961.82 373.22 o 4 18 0 15245.85 15579.76 624.63 o 5 18 0 1121.93 869.87 375.64 o 6 18 0 23778.21 24068.79 845.45 o 7 18 0 4003.53 4083.94 602.46 o 8 18 0 15427.67 15578.32 780.34 o 9 18 0 1501.42 900.47 518.82 o 10 18 0 6123.16 5114.64 659.32 o 11 18 0 7.69 -681.60 681.60 o 12 18 0 18926.15 17363.04 926.05 o 1 19 0 17.42 9.72 284.79 o 2 19 0 720.87 886.74 318.52 o 3 19 0 52.23 128.09 312.07 o 4 19 0 28269.29 25194.27 1077.42 o 5 19 0 12.36 -71.35 421.83 o 6 19 0 12684.54 11791.98 712.61 o 7 19 0 2048.89 1385.75 520.75 o 8 19 0 9645.14 9596.45 725.30 o 9 19 0 1444.96 1283.01 539.37 o 10 19 0 6365.34 7106.95 738.88 o 11 19 0 253.50 -99.25 1111.81 o 12 19 0 916.16 -1278.53 1278.53 o 0 20 0 52872.29 44826.88 1390.77 o 1 20 0 681.88 445.76 369.28 o 2 20 0 1012.82 1489.27 350.46 o 3 20 0 0.09 -153.88 339.27 o 4 20 0 1479.98 809.57 442.25 o 5 20 0 2470.53 3149.71 881.82 o 6 20 0 13018.02 13282.12 752.61 o 7 20 0 221.04 232.77 529.05 o 8 20 0 7548.95 7887.02 720.22 o 9 20 0 122.09 -436.69 949.55 o 10 20 0 10989.42 9956.10 811.21 o 11 20 0 4063.39 1175.61 1539.78 o 1 21 0 28918.79 26916.70 835.50 o 2 21 0 48.65 134.53 313.46 o 3 21 0 41971.72 40946.20 1423.35 o 4 21 0 2765.14 3196.44 803.90 o 5 21 0 28396.70 24775.01 1879.68 o 6 21 0 2196.79 2074.80 872.04 o 7 21 0 1897.34 2133.78 632.46 o 8 21 0 1890.48 1378.72 864.42 o 9 21 0 43373.38 38896.29 1390.62 o 10 21 0 2011.47 547.45 3186.43 o 0 22 0 496.43 674.71 561.52 o 1 22 0 901.42 1693.08 429.72 o 2 22 0 3061.68 2534.47 517.73 o 3 22 0 560.60 986.53 447.60 o 4 22 0 457.99 640.76 452.36 o 5 22 0 125.00 120.16 476.42 o 6 22 0 444.56 166.20 1023.82 o 7 22 0 440.32 400.51 682.74 o 8 22 0 371.25 -380.65 1016.40 o 9 22 0 0.71 -49.07 1939.56 o 1 23 0 24.85 -156.55 344.67 o 2 23 0 1015.32 859.13 586.47 o 3 23 0 8143.32 8492.66 989.69 o 4 23 0 223.66 1049.41 487.82 o 5 23 0 959.73 1570.07 679.82 o 6 23 0 0.52 -210.29 828.60 o 7 23 0 1098.81 569.41 815.29 o 8 23 0 3834.62 5054.74 1203.32 o 9 23 0 56.52 -1476.44 1476.44 o 0 24 0 260.70 77.48 542.32 o 1 24 0 834.39 928.09 574.45 o 2 24 0 227.60 70.58 529.25 o 3 24 0 7728.74 8950.97 1028.54 o 4 24 0 5957.94 4906.85 920.42 o 5 24 0 7988.71 9043.16 1083.76 o 6 24 0 6586.60 8312.85 1907.11 o 7 24 0 2075.35 1801.02 882.70 o 1 25 0 28302.90 24941.46 1306.56 o 2 25 0 33.21 70.68 605.53 o 3 25 0 103.68 -392.56 1062.80 o 4 25 0 900.99 520.79 677.67 o 5 25 0 8453.31 8823.04 1413.11 o 1 26 0 232.50 1017.28 1333.95 o 2 26 0 4551.77 5052.59 918.98 o 3 26 0 2527.01 2034.41 819.06 o -17 0 1 667.63 2177.06 1159.78 o -15 0 1 1165.51 769.98 701.91 o -13 0 1 4968.88 3529.54 983.06 o -11 0 1 3524.53 2183.35 456.61 o -9 0 1 32732.75 33939.11 634.67 o -7 0 1 5602.97 5457.50 319.58 o -5 0 1 25836.19 25929.79 450.88 o -3 0 1 46061.28 49482.82 421.00 o -1 0 1 140907.94 97882.03 27177.83 o 1 0 1 140723.02 56788.60 52112.94 o 3 0 1 45607.99 50801.89 427.49 o 7 0 1 5360.26 5179.14 306.25 o 9 0 1 32066.79 34049.39 1155.99 o 11 0 1 3371.04 2448.49 445.54 o 13 0 1 4755.20 2885.17 732.29 o 15 0 1 1130.61 1423.86 955.93 o 17 0 1 653.81 2327.48 1104.36 o -17 1 1 328.80 226.25 626.75 o -16 1 1 487.38 28.07 513.92 o -15 1 1 3568.79 2424.12 587.90 o -14 1 1 67.28 -434.88 434.88 o -13 1 1 1380.71 1798.60 398.97 o -12 1 1 863.43 738.19 309.48 o -11 1 1 4141.84 5306.38 377.70 o -10 1 1 4265.90 5052.50 319.38 o -9 1 1 5666.60 5764.23 403.30 o -8 1 1 61.37 28.54 163.65 o -7 1 1 389.24 435.03 159.11 o -6 1 1 305.32 -29.78 128.29 o -5 1 1 3549.75 3659.70 201.90 o -4 1 1 7561.19 7691.26 194.89 o -3 1 1 3574.51 4007.58 231.67 o -2 1 1 3354.16 3343.32 137.74 o -1 1 1 36483.34 32900.15 665.19 o 0 1 1 17.58 4.14 21.24 o 1 1 1 36550.14 30022.10 1930.15 o 2 1 1 3330.47 3283.60 89.38 o 3 1 1 3605.61 4118.26 141.72 o 4 1 1 7429.45 7833.88 171.14 o 5 1 1 3429.84 3797.26 156.27 o 6 1 1 312.60 359.53 122.41 o 7 1 1 399.31 297.13 153.78 o 8 1 1 59.29 -146.00 171.97 o 9 1 1 5447.79 4296.38 306.39 o 10 1 1 4222.93 4818.10 309.45 o 11 1 1 4222.18 5131.29 369.88 o 12 1 1 825.13 860.35 305.50 o 13 1 1 1337.58 1410.30 340.69 o 14 1 1 69.73 243.92 372.62 o 15 1 1 3412.56 2246.43 592.57 o 16 1 1 486.48 232.74 663.47 o 17 1 1 321.14 627.91 728.80 o -17 2 1 975.75 1298.17 1136.40 o -16 2 1 42.72 572.84 580.70 o -15 2 1 161.64 301.37 487.00 o -14 2 1 909.55 805.83 408.04 o -13 2 1 22.46 437.01 364.93 o -12 2 1 1762.35 1667.01 374.28 o -11 2 1 1797.16 1790.41 307.88 o -10 2 1 174.60 32.54 229.27 o -9 2 1 1190.73 1054.34 227.82 o -8 2 1 453.06 721.02 185.05 o -7 2 1 3261.31 3257.71 224.55 o -6 2 1 1379.97 1443.84 169.55 o -5 2 1 3157.55 2722.57 277.15 o -4 2 1 1731.83 2009.85 187.11 o -3 2 1 2184.55 2463.59 194.70 o -2 2 1 3098.02 3319.94 145.25 o -1 2 1 101.37 168.62 55.41 o 0 2 1 4848.82 4328.62 106.06 o 1 2 1 101.31 16.04 49.18 o 2 2 1 3076.50 3022.93 154.47 o 3 2 1 2134.04 2699.16 154.28 o 4 2 1 1733.81 1700.76 118.84 o 5 2 1 3017.11 2478.84 287.15 o 6 2 1 1435.23 1592.89 147.77 o 7 2 1 3145.55 3116.71 199.89 o 8 2 1 433.64 412.53 179.62 o 9 2 1 1143.88 1020.62 204.27 o 10 2 1 169.15 110.55 239.75 o 11 2 1 1765.03 1923.70 294.73 o 12 2 1 1691.79 1749.97 332.53 o 13 2 1 23.15 -185.47 340.76 o 14 2 1 920.20 1084.95 417.23 o 15 2 1 161.76 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