data_2310156 _cell_angle_alpha 90.000 _cell_angle_beta 90.049 _cell_angle_gamma 90.000 _cell_length_a 13.3834 _cell_length_b 20.1182 _cell_length_c 19.8867 _exptl_crystal_F_000 2968.00 _reflns_d_resolution_high 0.7401 _[local]_cod_data_source_file bp5072sin05h_twin_f_co2sup4.hkl _[local]_cod_data_source_block sin05h_twin_f_co2 _shelx_title ' F_CO2_SIN05h_twin in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 884.22 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 79249.62 49960.04 7069.53 o 4 0 0 13734.28 16276.03 690.40 o 6 0 0 33284.42 27440.87 490.46 o 8 0 0 228672.77 231338.44 5542.91 o 10 0 0 1578.31 1721.95 341.72 o 12 0 0 4173.73 4100.89 1045.27 o 14 0 0 68300.29 82057.80 2003.63 o 16 0 0 575.72 -406.98 749.06 o 1 1 0 190935.02 97109.23 25791.15 o 2 1 0 74406.47 63776.52 1317.13 o 3 1 0 28132.56 34532.68 1672.41 o 4 1 0 119805.35 117034.66 3776.20 o 5 1 0 10681.36 7314.25 209.81 o 6 1 0 13830.48 11780.42 307.99 o 7 1 0 692.76 925.37 141.25 o 8 1 0 22234.40 24236.28 507.00 o 9 1 0 20999.61 21615.74 561.31 o 10 1 0 26160.45 26798.64 726.15 o 11 1 0 10022.57 10110.65 397.21 o 12 1 0 14910.25 14878.59 539.47 o 13 1 0 3697.88 5180.11 599.40 o 14 1 0 2104.89 3197.43 593.15 o 15 1 0 1980.33 2327.27 594.03 o 16 1 0 70.01 -400.01 563.26 o 17 1 0 8.06 -551.05 551.05 o 0 2 0 229905.66 166264.25 2718.43 o 1 2 0 3979.41 3253.44 75.25 o 2 2 0 49234.07 31550.88 1090.00 o 3 2 0 30703.11 28433.83 1463.45 o 4 2 0 14265.48 9531.08 485.47 o 5 2 0 10861.69 11235.96 326.51 o 6 2 0 1934.16 2896.48 153.58 o 7 2 0 15237.28 16244.23 375.00 o 8 2 0 368.12 518.95 149.80 o 9 2 0 10771.83 10765.41 316.72 o 10 2 0 6791.33 6988.10 422.82 o 11 2 0 978.94 1464.34 272.45 o 12 2 0 3134.23 4337.36 507.21 o 13 2 0 900.08 790.70 474.13 o 14 2 0 3250.41 4416.76 625.52 o 15 2 0 521.58 332.76 526.31 o 16 2 0 2.00 -518.78 518.78 o 17 2 0 2200.17 1245.44 648.08 o 1 3 0 90405.40 64463.28 734.59 o 2 3 0 789.23 1139.04 88.70 o 3 3 0 434322.25 447123.47 18443.39 o 4 3 0 2364.56 2577.11 138.39 o 5 3 0 59268.57 52083.30 766.19 o 6 3 0 5411.67 5891.56 227.24 o 7 3 0 30354.82 30504.93 1627.58 o 8 3 0 1103.50 1375.54 184.78 o 9 3 0 10469.71 10827.95 344.39 o 10 3 0 1550.10 1751.19 221.87 o 11 3 0 15393.67 18171.36 581.98 o 12 3 0 105.91 163.14 311.34 o 13 3 0 610.48 431.92 338.26 o 14 3 0 2530.29 3722.96 603.76 o 15 3 0 33.96 -305.51 483.16 o 16 3 0 58.44 -551.27 551.27 o 17 3 0 5733.73 7179.75 1172.44 o 0 4 0 68796.28 48237.23 1004.98 o 1 4 0 4551.48 4088.22 114.74 o 3 4 0 7852.10 7996.61 309.13 o 4 4 0 2240.96 3489.14 209.97 o 5 4 0 553.77 1381.75 134.75 o 6 4 0 1758.52 3092.72 181.53 o 7 4 0 10329.78 10936.45 541.65 o 8 4 0 26.35 -37.76 143.79 o 9 4 0 379.94 728.47 200.18 o 10 4 0 1152.77 1423.14 264.99 o 11 4 0 15235.19 16699.05 1199.14 o 12 4 0 4893.91 4849.25 451.46 o 13 4 0 320.93 421.78 347.57 o 14 4 0 3052.63 3155.59 595.97 o 15 4 0 101.84 -410.74 503.32 o 16 4 0 235.79 -511.77 511.77 o 17 4 0 82.56 -527.00 700.88 o 1 5 0 781843.44 836574.44 11668.37 o 2 5 0 1209.60 1199.91 94.71 o 3 5 0 174564.08 161181.63 2336.18 o 4 5 0 1780.54 2079.03 138.06 o 5 5 0 1124.51 266.85 108.08 o 6 5 0 1094.00 1261.78 189.37 o 7 5 0 2544.84 2707.10 208.70 o 8 5 0 804.59 911.97 179.98 o 9 5 0 158961.94 158788.94 2213.77 o 10 5 0 549.43 214.11 230.48 o 11 5 0 49437.41 52020.63 938.48 o 12 5 0 656.88 1021.20 360.69 o 13 5 0 22555.82 27644.03 754.99 o 14 5 0 11.47 -347.51 347.51 o 15 5 0 6898.16 9226.66 770.00 o 16 5 0 20.35 -513.53 513.53 o 17 5 0 3133.09 2637.85 804.49 o 0 6 0 119885.57 103154.06 1884.10 o 1 6 0 24684.09 23618.91 385.50 o 2 6 0 207.69 -33.95 71.23 o 3 6 0 41196.13 40524.57 728.46 o 4 6 0 644.84 1550.54 133.61 o 5 6 0 19885.92 17115.12 424.43 o 6 6 0 784.83 1280.23 172.72 o 7 6 0 16768.23 15964.96 336.10 o 8 6 0 3055.31 3575.46 234.32 o 9 6 0 4905.04 6357.58 351.43 o 10 6 0 6130.27 7386.58 403.80 o 11 6 0 19056.80 19884.62 547.21 o 12 6 0 4089.48 4060.57 423.98 o 13 6 0 11.96 223.02 397.85 o 14 6 0 6375.56 6974.34 740.84 o 15 6 0 1455.68 1946.34 558.16 o 16 6 0 18.67 -109.01 531.08 o 17 6 0 550.34 -220.69 1053.59 o 1 7 0 8335.53 5069.38 148.99 o 2 7 0 13158.89 11851.14 238.97 o 3 7 0 61724.33 50498.19 888.38 o 4 7 0 32760.69 31576.66 375.24 o 5 7 0 1650.30 2472.76 179.00 o 6 7 0 7597.31 7156.74 252.46 o 7 7 0 5372.67 6162.41 256.38 o 8 7 0 34545.55 33289.65 566.86 o 9 7 0 1730.73 2061.40 279.78 o 10 7 0 26.23 -234.66 234.66 o 11 7 0 23569.20 25374.95 663.77 o 12 7 0 381.25 92.15 290.39 o 13 7 0 10299.71 10502.51 625.90 o 14 7 0 293.59 335.45 379.11 o 15 7 0 233.14 -248.65 368.20 o 16 7 0 2317.94 2612.05 649.90 o 17 7 0 8909.59 11611.44 1316.80 o 0 8 0 133408.67 118295.88 2245.01 o 1 8 0 5185.25 4798.97 156.82 o 2 8 0 9195.37 5468.29 164.89 o 3 8 0 1665.22 1598.25 123.91 o 4 8 0 225213.33 242527.53 6215.98 o 5 8 0 8728.57 8062.11 259.57 o 6 8 0 199810.69 192626.81 3820.31 o 7 8 0 7478.57 7336.46 363.09 o 8 8 0 134603.50 135198.86 1352.21 o 9 8 0 325.16 433.85 249.39 o 10 8 0 15166.92 15810.92 636.12 o 11 8 0 48.73 -214.38 282.49 o 12 8 0 43266.85 48730.90 843.77 o 13 8 0 511.12 154.57 366.49 o 14 8 0 9358.05 10095.39 697.34 o 15 8 0 302.96 -9.87 379.33 o 16 8 0 19472.67 25105.11 985.83 o 1 9 0 1571.08 1543.31 124.43 o 2 9 0 2669.81 3386.11 157.23 o 3 9 0 2291.21 2125.58 144.26 o 4 9 0 6903.08 7045.84 245.56 o 5 9 0 3735.53 3996.14 221.73 o 6 9 0 6489.50 6686.14 256.05 o 7 9 0 411.98 181.48 155.94 o 8 9 0 16943.62 16974.57 621.94 o 9 9 0 1746.75 2111.19 302.22 o 10 9 0 3774.17 3485.70 390.89 o 11 9 0 167.95 64.24 296.48 o 12 9 0 834.27 660.90 337.29 o 13 9 0 42.24 -322.23 322.23 o 14 9 0 137.12 110.23 382.72 o 15 9 0 578.62 331.02 459.46 o 16 9 0 453.69 -74.44 699.84 o 0 10 0 432610.56 447119.03 9632.75 o 1 10 0 1185.58 1326.45 133.77 o 2 10 0 1541.95 2804.35 161.90 o 3 10 0 2543.11 2883.33 173.50 o 4 10 0 7337.38 7675.26 228.22 o 5 10 0 78.20 -16.48 132.82 o 6 10 0 4842.31 5157.29 342.86 o 7 10 0 0.59 -147.43 184.12 o 8 10 0 42629.36 41403.60 823.53 o 9 10 0 323.64 501.63 255.98 o 10 10 0 6590.87 7146.32 450.61 o 11 10 0 3886.50 4532.14 421.29 o 12 10 0 58.08 -288.68 288.68 o 13 10 0 11.25 -109.40 331.57 o 14 10 0 888.28 1222.36 458.22 o 15 10 0 28.84 -371.62 812.95 o 16 10 0 371.02 386.59 556.22 o 1 11 0 8301.31 8110.73 228.25 o 2 11 0 31389.62 30786.50 375.45 o 3 11 0 9693.71 8890.26 238.90 o 4 11 0 9567.32 9428.15 248.07 o 5 11 0 866.48 945.98 167.34 o 6 11 0 30629.81 30209.51 608.62 o 7 11 0 5247.78 5582.18 357.25 o 8 11 0 5235.69 6537.82 519.92 o 9 11 0 2188.26 2401.17 330.51 o 10 11 0 5474.97 6441.02 500.46 o 11 11 0 5089.73 5643.49 509.83 o 12 11 0 3149.91 3817.31 492.82 o 13 11 0 600.56 120.87 395.96 o 14 11 0 204.09 12.83 453.92 o 15 11 0 22.22 -76.05 483.49 o 16 11 0 290.62 290.27 737.30 o 0 12 0 43.00 39.00 161.25 o 1 12 0 7799.90 7306.50 225.05 o 2 12 0 64414.42 59410.89 1054.39 o 3 12 0 24634.75 23394.70 393.98 o 4 12 0 36588.82 34055.48 705.17 o 5 12 0 21914.31 20851.21 483.19 o 6 12 0 12987.72 13548.43 403.41 o 7 12 0 36498.36 34114.19 982.82 o 8 12 0 12367.25 11374.40 566.91 o 9 12 0 5315.00 6075.16 523.40 o 10 12 0 7344.24 7904.48 596.80 o 11 12 0 157.63 140.70 372.49 o 12 12 0 14989.81 15683.78 653.75 o 13 12 0 362.75 239.29 491.69 o 14 12 0 252.30 -441.16 442.35 o 15 12 0 477.79 280.51 585.96 o 16 12 0 3485.55 2722.68 987.34 o 1 13 0 8597.58 8670.99 244.81 o 2 13 0 7666.20 6994.29 262.52 o 3 13 0 500646.81 490193.97 8090.11 o 4 13 0 9801.26 9757.18 304.98 o 5 13 0 66448.48 61989.07 1535.56 o 6 13 0 13957.68 11880.78 628.46 o 7 13 0 11398.46 10520.17 490.97 o 8 13 0 8096.63 8156.50 495.23 o 9 13 0 12598.43 13481.10 566.44 o 10 13 0 1635.20 1995.04 475.83 o 11 13 0 71009.75 74265.71 1337.74 o 12 13 0 135.40 45.33 414.62 o 13 13 0 938.19 212.92 415.85 o 14 13 0 51.33 -347.37 452.40 o 15 13 0 413.84 -246.22 1310.05 o 0 14 0 7052.20 7235.61 345.49 o 1 14 0 0.00 -135.34 135.34 o 2 14 0 362.46 444.26 153.82 o 3 14 0 22286.53 22363.34 432.78 o 4 14 0 1164.35 1403.97 232.34 o 5 14 0 47182.15 43945.17 1164.06 o 6 14 0 18787.70 17295.83 551.47 o 7 14 0 33567.77 31856.40 980.87 o 8 14 0 9927.60 10124.89 514.99 o 9 14 0 18633.27 20606.09 670.04 o 10 14 0 53.70 341.49 362.90 o 11 14 0 120.40 768.24 384.38 o 12 14 0 0.18 -57.88 348.01 o 13 14 0 4.39 49.22 411.50 o 14 14 0 1445.14 1016.21 487.26 o 15 14 0 104.96 -598.39 1423.31 o 1 15 0 9302.56 8265.43 339.06 o 2 15 0 3614.24 3823.84 288.08 o 3 15 0 3740.57 4243.04 291.58 o 4 15 0 2478.73 2631.74 272.13 o 5 15 0 21175.42 18942.59 563.41 o 6 15 0 21.76 -31.99 257.55 o 7 15 0 3158.04 3011.64 383.83 o 8 15 0 88.56 277.42 316.35 o 9 15 0 7370.80 7637.94 812.96 o 10 15 0 1323.05 1913.89 409.13 o 11 15 0 934.74 1097.32 410.81 o 12 15 0 1761.60 1861.82 437.40 o 13 15 0 4524.40 4416.39 564.92 o 14 15 0 175.51 -26.17 474.79 o 0 16 0 201225.14 186881.70 4594.92 o 1 16 0 423.30 756.86 212.22 o 2 16 0 73045.48 65589.36 1230.04 o 3 16 0 33.12 -46.11 210.60 o 4 16 0 6656.87 5934.64 479.35 o 5 16 0 1293.37 1080.57 393.60 o 6 16 0 24760.52 23718.51 803.46 o 7 16 0 16.62 -218.83 283.41 o 8 16 0 14457.87 14249.54 646.19 o 9 16 0 1867.51 1779.83 417.49 o 10 16 0 453.47 355.90 378.78 o 11 16 0 25.21 -208.39 370.15 o 12 16 0 1747.01 1066.91 443.45 o 13 16 0 3.37 -399.97 425.03 o 14 16 0 8925.32 10482.60 1388.78 o 1 17 0 224.06 69.82 199.15 o 2 17 0 2304.87 2562.35 289.85 o 3 17 0 3716.50 4250.28 363.47 o 4 17 0 2377.14 2659.15 406.44 o 5 17 0 42.95 -50.37 310.23 o 6 17 0 3639.56 3815.26 475.90 o 7 17 0 7.81 -139.73 321.15 o 8 17 0 1188.63 1433.63 423.53 o 9 17 0 406.18 547.13 371.30 o 10 17 0 693.14 492.83 372.57 o 11 17 0 900.88 351.84 409.01 o 12 17 0 2015.66 2430.14 502.41 o 13 17 0 1973.36 987.04 508.28 o 0 18 0 37712.31 33906.71 927.76 o 1 18 0 1149.45 991.14 246.84 o 2 18 0 38214.14 37594.24 904.13 o 3 18 0 1874.35 2478.15 338.75 o 4 18 0 13595.81 14308.30 629.14 o 5 18 0 1118.99 793.38 365.14 o 6 18 0 19670.23 19601.22 747.43 o 7 18 0 3070.36 3555.12 595.04 o 8 18 0 13295.03 12949.45 678.51 o 9 18 0 1444.55 1050.23 436.83 o 10 18 0 4282.23 4736.23 821.13 o 11 18 0 0.08 365.94 428.71 o 12 18 0 16233.23 18076.70 880.99 o 13 18 0 0.09 -1179.68 1243.80 o 1 19 0 9.49 351.89 236.34 o 2 19 0 679.44 1172.01 288.62 o 3 19 0 55.04 -83.40 299.31 o 4 19 0 22755.81 22135.46 763.91 o 5 19 0 14.40 -152.20 324.60 o 6 19 0 11031.50 9794.64 630.65 o 7 19 0 1795.60 1376.61 438.58 o 8 19 0 7938.69 8071.56 808.18 o 9 19 0 1199.98 567.30 404.48 o 10 19 0 5190.54 6601.69 659.24 o 11 19 0 100.11 -275.66 427.96 o 12 19 0 714.14 1136.94 1419.04 o 0 20 0 44238.16 43023.25 1541.15 o 1 20 0 680.36 993.42 396.95 o 2 20 0 710.26 1655.70 375.55 o 3 20 0 0.38 -54.11 322.17 o 4 20 0 1298.67 1514.65 402.71 o 5 20 0 1813.04 2069.69 444.22 o 6 20 0 12046.13 11125.19 646.94 o 7 20 0 165.03 131.34 366.30 o 8 20 0 6188.60 6065.73 615.53 o 9 20 0 130.53 -37.41 402.60 o 10 20 0 8093.23 8261.20 770.91 o 11 20 0 2910.63 4351.15 1547.27 o 1 21 0 24782.71 24428.83 969.22 o 2 21 0 78.19 503.23 335.80 o 3 21 0 37704.43 36412.70 1009.48 o 4 21 0 1929.29 1761.45 427.71 o 5 21 0 24515.78 21484.66 807.92 o 6 21 0 1695.77 1496.00 435.37 o 7 21 0 1717.33 1977.18 463.51 o 8 21 0 1799.98 1662.17 485.17 o 9 21 0 36478.54 33934.36 2385.67 o 10 21 0 1346.17 897.59 1320.73 o 0 22 0 487.23 1098.09 413.70 o 1 22 0 750.31 435.36 354.09 o 2 22 0 2480.78 2545.44 445.74 o 3 22 0 543.24 535.47 356.93 o 4 22 0 404.98 95.29 351.87 o 5 22 0 172.04 -208.04 333.63 o 6 22 0 407.90 544.65 396.04 o 7 22 0 334.38 380.32 402.35 o 8 22 0 296.83 445.68 427.09 o 9 22 0 2.08 662.50 1269.44 o 1 23 0 26.35 -91.42 298.52 o 2 23 0 853.40 1213.34 400.80 o 3 23 0 7137.48 7837.41 630.92 o 4 23 0 157.99 261.44 364.04 o 5 23 0 608.55 1156.32 437.40 o 6 23 0 2.14 -57.71 376.57 o 7 23 0 948.48 870.08 457.06 o 8 23 0 2961.97 1816.54 1316.46 o 0 24 0 267.76 1295.09 931.78 o 1 24 0 560.76 720.37 382.70 o 2 24 0 180.27 -15.46 346.63 o 3 24 0 6480.95 7392.77 651.04 o 4 24 0 5234.97 5299.83 830.39 o 5 24 0 6052.91 6051.29 642.52 o 6 24 0 5858.31 6378.64 836.38 o 7 24 0 2058.23 2248.24 1346.38 o 1 25 0 23148.35 23233.00 1002.54 o 2 25 0 30.36 -24.67 354.21 o 3 25 0 81.41 -81.71 369.77 o 4 25 0 720.64 425.88 422.14 o 5 25 0 7825.78 8609.92 1002.79 o 2 26 0 3828.92 4005.32 766.12 o 3 26 0 1797.26 1122.80 876.21 o -17 0 1 535.55 142.23 1953.32 o -15 0 1 1007.23 276.72 738.18 o -13 0 1 4629.92 4866.27 825.14 o -11 0 1 3640.67 3489.52 1017.10 o -9 0 1 31855.30 33218.67 1740.52 o -7 0 1 5064.37 4666.16 353.10 o -5 0 1 27992.01 25887.07 681.71 o -3 0 1 45620.88 46961.78 1803.10 o -1 0 1 142408.11 47685.08 21609.83 o 1 0 1 143182.11 79727.93 25106.93 o 3 0 1 42031.41 39570.48 5191.53 o 5 0 1 21702.04 15431.59 4648.21 o 7 0 1 4110.71 4354.02 374.27 o 9 0 1 28579.47 30317.10 588.06 o 11 0 1 2843.88 1510.15 350.42 o 13 0 1 3638.16 3710.19 815.69 o 15 0 1 851.59 1313.64 1179.68 o 17 0 1 486.28 726.65 868.93 o -17 1 1 264.52 -557.68 557.68 o -16 1 1 315.19 -206.16 529.82 o -15 1 1 2825.08 2966.43 608.40 o -14 1 1 74.60 -218.59 483.10 o -13 1 1 972.77 1406.19 492.77 o -12 1 1 681.50 395.45 265.70 o -11 1 1 3613.15 3447.06 313.82 o -10 1 1 4109.84 4595.44 322.72 o -9 1 1 5333.27 5899.99 304.03 o -8 1 1 52.73 -15.44 188.43 o -7 1 1 384.38 396.89 139.25 o -6 1 1 50.99 -101.77 115.64 o -5 1 1 3639.28 3144.14 208.99 o -4 1 1 7795.14 7158.97 252.12 o -3 1 1 3686.06 3810.36 140.38 o -2 1 1 3222.12 3360.30 89.20 o -1 1 1 36237.86 25933.49 2062.02 o 0 1 1 22.95 0.01 16.72 o 1 1 1 36585.91 30835.87 475.08 o 2 1 1 2843.24 2842.58 130.81 o 3 1 1 3808.77 4038.30 211.31 o 4 1 1 7481.60 6794.96 343.70 o 5 1 1 2967.77 3009.42 163.05 o 6 1 1 65.24 114.83 99.49 o 7 1 1 436.57 210.78 131.38 o 8 1 1 54.81 -127.08 127.08 o 9 1 1 4269.50 4221.61 434.03 o 10 1 1 4010.48 4205.15 338.75 o 11 1 1 4044.41 4371.97 478.45 o 12 1 1 530.66 507.47 319.83 o 13 1 1 788.86 762.42 503.41 o 14 1 1 83.60 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