data_2310157 _cell_angle_alpha 90.000 _cell_angle_beta 90.040 _cell_angle_gamma 90.000 _cell_length_a 13.3883 _cell_length_b 20.1320 _cell_length_c 19.9016 _exptl_crystal_F_000 2968.00 _reflns_d_resolution_high 0.7407 _[local]_cod_data_source_file bp5072sin3h4_twin_f_co2sup5.hkl _[local]_cod_data_source_block sin3h4_twin_f_co2 _shelx_title ' F_CO2_SIN3h4_twin in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 898.53 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 64585.29 63646.36 2991.10 o 4 0 0 15713.69 13800.73 1711.53 o 6 0 0 34298.62 25256.31 1847.51 o 8 0 0 236063.27 231056.13 7531.05 o 10 0 0 1600.42 1720.80 535.02 o 12 0 0 3841.92 3694.18 726.40 o 14 0 0 67459.63 68428.59 16498.00 o 16 0 0 592.23 856.04 1385.45 o 1 1 0 161982.56 155102.69 3234.29 o 2 1 0 74447.76 66333.37 1534.63 o 3 1 0 33202.15 31352.70 1298.91 o 4 1 0 120265.84 115000.56 4492.77 o 5 1 0 10158.72 7975.78 462.24 o 6 1 0 13409.72 11355.60 404.16 o 7 1 0 616.12 788.22 201.03 o 8 1 0 21934.33 21946.99 1151.48 o 9 1 0 20771.42 20890.60 998.83 o 10 1 0 26552.91 26097.07 922.08 o 11 1 0 10514.62 10047.11 1000.51 o 12 1 0 15328.38 15184.79 821.79 o 13 1 0 3577.55 3861.05 533.63 o 14 1 0 1904.57 1691.41 682.12 o 15 1 0 1929.45 785.42 1155.50 o 16 1 0 71.84 -458.58 658.37 o 17 1 0 8.30 -956.99 1135.69 o 0 2 0 198526.17 191268.05 2125.01 o 1 2 0 3882.37 3430.70 90.00 o 2 2 0 39423.86 37072.55 754.35 o 3 2 0 30830.38 30324.07 1171.56 o 4 2 0 12382.04 10737.81 566.72 o 5 2 0 11133.95 11067.06 457.95 o 6 2 0 1807.90 2764.45 191.69 o 7 2 0 15811.37 16395.89 602.93 o 8 2 0 419.13 501.82 195.81 o 9 2 0 10232.29 10673.81 447.19 o 10 2 0 6855.90 7172.51 438.43 o 11 2 0 946.39 480.96 414.25 o 12 2 0 3346.77 3624.49 506.63 o 13 2 0 780.46 642.49 687.95 o 14 2 0 3252.30 2288.61 616.20 o 15 2 0 608.18 -487.90 613.89 o 16 2 0 0.34 -862.15 862.15 o 17 2 0 1825.83 836.34 777.06 o 1 3 0 77346.13 74740.60 389.39 o 2 3 0 844.76 1026.54 102.38 o 3 3 0 450721.94 461469.47 4150.06 o 4 3 0 2325.44 2089.16 199.32 o 5 3 0 58923.64 54492.94 2165.51 o 6 3 0 5232.27 5967.27 463.81 o 7 3 0 30826.85 29333.16 2170.51 o 8 3 0 1147.77 1154.39 268.97 o 9 3 0 10497.44 10743.71 455.92 o 10 3 0 1345.89 1322.81 342.44 o 11 3 0 15391.99 17744.10 794.78 o 12 3 0 106.85 202.48 414.43 o 13 3 0 647.86 -171.87 505.01 o 14 3 0 2358.82 2354.11 612.21 o 15 3 0 53.06 -77.40 642.62 o 16 3 0 7.73 -405.85 937.61 o 17 3 0 5740.63 5461.39 1316.20 o 0 4 0 58414.54 55438.61 822.76 o 1 4 0 4857.22 4487.20 177.25 o 2 4 0 305.53 420.55 110.33 o 3 4 0 7221.44 7476.59 238.40 o 4 4 0 2418.01 2909.97 203.36 o 5 4 0 508.99 1315.79 187.41 o 6 4 0 1580.38 2460.63 239.18 o 7 4 0 11215.14 11881.06 418.27 o 8 4 0 9.70 44.97 237.11 o 9 4 0 391.57 569.10 287.54 o 10 4 0 1110.80 949.39 334.66 o 11 4 0 15462.24 14355.99 579.69 o 12 4 0 5410.90 4907.93 669.76 o 13 4 0 290.84 807.29 514.56 o 14 4 0 2951.75 3239.18 643.35 o 15 4 0 81.80 -601.54 601.54 o 16 4 0 147.76 -720.49 748.96 o 17 4 0 85.82 -913.94 1467.14 o 1 5 0 807358.63 844073.44 7872.76 o 2 5 0 1283.07 1238.31 127.21 o 3 5 0 170692.11 175488.02 1400.48 o 4 5 0 1813.83 2122.77 189.99 o 5 5 0 1198.23 286.08 169.23 o 6 5 0 1016.50 1173.85 234.05 o 7 5 0 2533.14 2519.64 287.91 o 8 5 0 857.08 926.64 268.88 o 9 5 0 163510.45 158793.69 2933.18 o 10 5 0 565.50 208.37 332.76 o 11 5 0 49925.63 49211.17 2123.44 o 12 5 0 721.21 831.73 508.11 o 13 5 0 22542.21 28274.62 1204.13 o 14 5 0 21.07 40.48 531.36 o 15 5 0 6786.86 8292.71 913.25 o 16 5 0 31.62 -608.45 608.45 o 17 5 0 3443.23 3137.71 1173.39 o 0 6 0 117216.80 116803.19 1949.74 o 1 6 0 25498.38 24703.54 439.49 o 2 6 0 114.84 96.06 105.69 o 3 6 0 40740.80 41182.46 561.74 o 4 6 0 656.36 1262.94 178.31 o 5 6 0 19558.85 17778.00 405.06 o 6 6 0 675.22 1310.78 252.68 o 7 6 0 15953.98 15032.90 659.77 o 8 6 0 3108.41 3144.84 329.05 o 9 6 0 4777.85 5246.78 398.74 o 10 6 0 5795.67 5970.42 741.77 o 11 6 0 19508.70 19305.80 870.35 o 12 6 0 4096.04 4220.27 517.06 o 13 6 0 26.91 -480.35 480.35 o 14 6 0 6403.79 7299.33 784.83 o 15 6 0 1293.11 1292.36 622.22 o 16 6 0 42.26 84.02 669.63 o 17 6 0 628.40 -489.02 981.68 o 1 7 0 7667.71 6207.15 230.05 o 2 7 0 13024.52 11913.87 236.80 o 3 7 0 61177.39 53401.43 701.19 o 4 7 0 33227.73 33297.99 414.77 o 5 7 0 1474.76 1809.41 227.38 o 6 7 0 7606.88 7538.17 363.90 o 7 7 0 5165.76 6292.68 361.58 o 8 7 0 35402.96 32825.87 1414.82 o 9 7 0 1920.64 2181.46 354.46 o 10 7 0 78.65 35.79 334.45 o 11 7 0 24272.71 25705.37 814.34 o 12 7 0 395.18 211.36 427.37 o 13 7 0 10088.97 11401.97 1194.44 o 14 7 0 255.53 553.00 565.63 o 15 7 0 209.37 -276.79 561.12 o 16 7 0 2169.25 2388.34 783.57 o 17 7 0 8794.70 9881.15 2431.08 o 0 8 0 135365.11 131845.59 3349.22 o 1 8 0 5678.05 5794.49 236.97 o 2 8 0 9180.36 5731.15 253.55 o 3 8 0 1662.03 1743.23 158.85 o 4 8 0 228236.89 245108.28 2605.91 o 5 8 0 8565.86 8566.43 287.00 o 6 8 0 200380.59 204924.27 1883.29 o 7 8 0 7488.33 7897.08 390.94 o 8 8 0 135908.52 135127.77 2647.03 o 9 8 0 374.98 1055.42 322.35 o 10 8 0 14648.48 15537.12 610.02 o 11 8 0 60.68 48.93 397.13 o 12 8 0 44470.69 47672.11 1810.07 o 13 8 0 476.54 -94.49 524.45 o 14 8 0 9777.74 10069.72 891.95 o 15 8 0 358.27 61.49 689.70 o 16 8 0 20315.01 23832.28 1752.08 o 17 8 0 90.81 -1738.35 1790.63 o 1 9 0 1547.48 1843.82 179.99 o 2 9 0 2755.15 3363.88 228.33 o 3 9 0 2552.76 2682.62 190.33 o 4 9 0 7116.73 8040.43 299.18 o 5 9 0 3611.12 3925.28 238.93 o 6 9 0 6552.46 7241.20 362.45 o 7 9 0 274.56 89.82 249.72 o 8 9 0 17715.66 17910.23 545.52 o 9 9 0 1607.27 2125.27 359.21 o 10 9 0 3909.52 2888.03 408.94 o 11 9 0 236.92 146.63 404.93 o 12 9 0 947.14 471.25 451.73 o 13 9 0 31.64 61.52 513.28 o 14 9 0 142.67 -434.13 626.55 o 15 9 0 721.06 470.44 715.35 o 16 9 0 539.05 1050.39 1008.22 o 0 10 0 442965.84 466610.91 3964.65 o 1 10 0 1303.20 1619.52 191.23 o 2 10 0 1420.64 2441.32 232.12 o 3 10 0 2436.34 2712.20 197.68 o 4 10 0 7689.30 8272.22 298.61 o 5 10 0 59.05 -85.17 163.36 o 6 10 0 4876.77 5425.05 342.34 o 7 10 0 0.27 -246.35 246.35 o 8 10 0 43871.41 39879.52 748.67 o 9 10 0 391.85 828.52 390.52 o 10 10 0 6168.71 5708.28 599.75 o 11 10 0 4278.81 4643.09 598.02 o 12 10 0 82.30 -51.17 505.92 o 13 10 0 7.29 -219.56 545.16 o 14 10 0 921.24 1305.98 666.27 o 15 10 0 79.41 -637.03 680.95 o 16 10 0 444.99 -76.31 1128.66 o 1 11 0 8820.12 9493.54 326.37 o 2 11 0 33281.47 33037.82 548.69 o 3 11 0 10034.88 9435.61 366.31 o 4 11 0 9300.71 9475.31 373.90 o 5 11 0 762.04 805.59 278.34 o 6 11 0 30916.33 30994.41 711.66 o 7 11 0 5272.73 6315.16 454.83 o 8 11 0 5050.15 5273.00 514.87 o 9 11 0 2156.27 1881.02 428.48 o 10 11 0 5520.34 4994.72 585.37 o 11 11 0 5032.26 5021.24 642.58 o 12 11 0 3358.35 3222.09 726.68 o 13 11 0 511.50 -238.20 542.62 o 14 11 0 147.41 637.78 666.47 o 15 11 0 43.18 -35.72 699.28 o 16 11 0 263.35 636.97 1852.72 o 0 12 0 42.73 -191.03 295.62 o 1 12 0 8584.12 8810.59 329.14 o 2 12 0 66060.48 63726.71 1239.88 o 3 12 0 24116.71 24456.71 521.59 o 4 12 0 37723.38 35488.93 621.52 o 5 12 0 23186.99 21765.45 606.97 o 6 12 0 13593.73 13796.76 545.79 o 7 12 0 37081.49 35182.37 804.83 o 8 12 0 13267.94 12095.38 599.56 o 9 12 0 5731.90 6928.20 594.26 o 10 12 0 7548.15 6978.14 865.77 o 11 12 0 214.59 341.52 495.82 o 12 12 0 15191.98 15437.58 883.23 o 13 12 0 420.19 -152.82 547.81 o 14 12 0 219.47 -625.39 625.39 o 15 12 0 458.76 217.65 704.27 o 16 12 0 3524.03 4594.21 1829.84 o 1 13 0 9664.39 9444.20 452.19 o 2 13 0 8431.43 8577.29 447.93 o 3 13 0 516708.03 508038.91 6304.09 o 4 13 0 9982.55 10458.89 434.21 o 5 13 0 68890.23 65394.56 1281.08 o 6 13 0 14279.30 12725.48 554.22 o 7 13 0 11924.01 10458.02 575.61 o 8 13 0 8561.23 9190.45 575.32 o 9 13 0 13125.29 14437.97 1173.24 o 10 13 0 1504.09 1943.97 510.82 o 11 13 0 72600.69 81227.20 1978.94 o 12 13 0 169.27 -154.15 499.60 o 13 13 0 1009.14 527.62 712.81 o 14 13 0 44.26 -221.78 568.63 o 15 13 0 441.25 380.72 1077.10 o 0 14 0 7213.96 8286.31 816.04 o 1 14 0 2.15 -9.46 247.66 o 2 14 0 369.14 640.86 281.11 o 3 14 0 23331.26 23255.26 648.62 o 4 14 0 1326.72 1685.62 385.74 o 5 14 0 48852.30 46639.77 876.26 o 6 14 0 18803.25 17545.36 635.42 o 7 14 0 35199.62 33494.84 835.20 o 8 14 0 10443.72 10554.46 599.42 o 9 14 0 19709.02 21640.22 963.99 o 10 14 0 46.44 10.69 459.81 o 11 14 0 102.52 540.76 492.18 o 12 14 0 0.13 49.60 505.92 o 13 14 0 6.46 40.80 569.01 o 14 14 0 1629.40 1547.75 666.16 o 15 14 0 92.15 -338.09 865.27 o 1 15 0 9321.55 8989.64 501.69 o 2 15 0 3812.72 3739.41 388.87 o 3 15 0 3841.83 3990.17 401.85 o 4 15 0 2637.95 2968.70 452.24 o 5 15 0 22176.31 20184.17 779.72 o 6 15 0 62.30 50.60 387.56 o 7 15 0 3006.68 2986.95 515.88 o 8 15 0 89.85 224.85 355.29 o 9 15 0 7337.26 7716.69 650.65 o 10 15 0 1393.34 975.02 516.91 o 11 15 0 1057.55 1159.05 541.14 o 12 15 0 2100.94 1687.98 578.71 o 13 15 0 4692.03 3504.85 693.68 o 14 15 0 149.41 22.04 609.36 o 0 16 0 209559.47 195990.30 2484.38 o 1 16 0 576.80 710.94 352.96 o 2 16 0 77799.34 67974.09 1081.65 o 3 16 0 55.95 -109.74 312.06 o 4 16 0 6753.77 6356.82 566.68 o 5 16 0 1633.03 827.38 438.70 o 6 16 0 25746.86 26397.41 891.67 o 7 16 0 19.20 -78.80 430.76 o 8 16 0 14876.25 15713.79 936.91 o 9 16 0 2081.08 1752.04 635.55 o 10 16 0 593.19 148.65 611.24 o 11 16 0 33.07 806.02 617.67 o 12 16 0 1742.14 1587.89 694.95 o 13 16 0 0.01 -658.49 658.49 o 14 16 0 8605.83 10900.02 2254.63 o 1 17 0 245.99 324.82 358.04 o 2 17 0 2556.56 2850.21 415.06 o 3 17 0 4012.37 4358.42 518.22 o 4 17 0 2522.63 2621.85 490.52 o 5 17 0 31.66 44.95 395.23 o 6 17 0 3899.03 3561.15 593.34 o 7 17 0 16.03 -94.67 431.41 o 8 17 0 1465.62 597.92 548.51 o 9 17 0 591.81 606.70 771.59 o 10 17 0 844.70 872.35 607.59 o 11 17 0 792.25 904.32 662.08 o 12 17 0 2048.77 2169.07 733.50 o 13 17 0 1898.88 2049.81 812.17 o 0 18 0 39871.12 33645.60 1231.84 o 1 18 0 1148.72 879.15 361.11 o 2 18 0 40672.32 38162.78 907.99 o 3 18 0 2099.34 2240.74 478.78 o 4 18 0 15207.65 15053.24 769.62 o 5 18 0 1008.83 790.11 439.33 o 6 18 0 21233.02 22329.90 902.39 o 7 18 0 3374.62 3558.59 695.13 o 8 18 0 14371.44 15804.88 1180.82 o 9 18 0 1363.02 1438.18 628.79 o 10 18 0 4329.15 4635.45 777.69 o 11 18 0 0.01 159.43 643.03 o 12 18 0 17054.94 17866.24 2370.81 o 13 18 0 5.11 365.97 1999.76 o 1 19 0 4.68 42.92 331.42 o 2 19 0 628.92 1347.05 512.32 o 3 19 0 40.10 -220.15 407.09 o 4 19 0 24817.73 23482.39 908.60 o 5 19 0 14.98 193.93 426.78 o 6 19 0 11944.29 11839.71 789.25 o 7 19 0 1902.98 978.44 582.50 o 8 19 0 8515.35 8375.95 1371.51 o 9 19 0 1217.20 1436.46 650.24 o 10 19 0 5723.86 6659.85 853.63 o 11 19 0 119.18 890.89 692.10 o 12 19 0 737.91 -274.48 1757.96 o 0 20 0 46672.32 45842.74 1484.97 o 1 20 0 567.85 525.15 374.30 o 2 20 0 829.30 1293.57 455.05 o 3 20 0 1.74 207.31 439.92 o 4 20 0 1428.62 1672.54 505.55 o 5 20 0 2225.85 2165.69 530.54 o 6 20 0 13119.38 13322.95 837.44 o 7 20 0 273.78 142.94 543.37 o 8 20 0 6428.53 6130.57 801.02 o 9 20 0 183.27 307.79 601.57 o 10 20 0 8917.33 7216.57 897.32 o 11 20 0 3293.94 2803.58 2058.57 o 12 20 0 50.18 169.91 1829.84 o 1 21 0 26827.71 25923.81 861.09 o 2 21 0 31.27 264.31 425.10 o 3 21 0 40334.82 38354.04 1281.43 o 4 21 0 2214.00 3195.17 570.85 o 5 21 0 25832.25 23515.85 965.37 o 6 21 0 1910.56 1746.29 626.83 o 7 21 0 2140.73 1500.51 612.23 o 8 21 0 1935.43 1892.63 667.63 o 9 21 0 39005.92 38048.75 2860.69 o 10 21 0 1592.90 4287.06 1895.19 o 11 21 0 19507.31 23435.06 2757.83 o 0 22 0 560.52 970.58 583.67 o 1 22 0 782.16 1282.61 468.46 o 2 22 0 2899.82 2806.77 539.54 o 3 22 0 632.25 896.18 458.83 o 4 22 0 447.74 238.21 533.52 o 5 22 0 197.64 302.02 469.00 o 6 22 0 335.74 149.57 558.95 o 7 22 0 325.96 1037.37 612.41 o 8 22 0 408.93 -86.67 601.22 o 9 22 0 1.33 1914.80 1901.73 o 10 22 0 4.19 359.43 1718.75 o 1 23 0 20.35 -361.58 404.24 o 2 23 0 820.40 496.90 565.97 o 3 23 0 8241.97 8086.76 717.24 o 4 23 0 196.53 135.56 450.12 o 5 23 0 803.42 1388.34 616.80 o 6 23 0 1.81 208.01 571.25 o 7 23 0 1021.52 803.60 649.33 o 8 23 0 3323.77 4260.92 1849.45 o 0 24 0 264.26 420.82 734.20 o 1 24 0 892.18 630.10 464.10 o 2 24 0 307.97 279.61 453.24 o 3 24 0 7336.22 8011.18 744.79 o 4 24 0 5785.22 4690.78 669.06 o 5 24 0 6896.06 6458.47 856.93 o 6 24 0 6189.86 6530.11 876.21 o 7 24 0 2150.34 3437.49 1921.34 o 1 25 0 25439.86 24759.29 1054.93 o 2 25 0 33.71 79.27 471.43 o 3 25 0 72.83 335.73 481.19 o 4 25 0 891.66 994.67 588.57 o 5 25 0 8671.86 10469.32 2319.98 o 0 26 0 84790.53 81068.59 3914.56 o 1 26 0 301.36 759.56 771.04 o 2 26 0 4458.62 4868.86 999.11 o 3 26 0 1995.05 2541.09 884.93 o -17 0 1 501.92 352.90 1169.79 o -15 0 1 1110.57 544.09 931.91 o -13 0 1 4304.09 4785.51 832.71 o -11 0 1 3500.20 3912.63 679.48 o -9 0 1 30976.63 31664.80 1354.90 o -7 0 1 4723.39 5259.72 398.18 o -5 0 1 26209.48 23905.46 543.28 o -3 0 1 45386.82 46374.54 1860.12 o -1 0 1 142296.63 122512.07 2891.12 o 1 0 1 142666.20 98254.29 36069.26 o 3 0 1 43581.50 45718.38 2235.05 o 7 0 1 4277.41 3552.79 734.81 o 9 0 1 29560.39 29671.99 2506.52 o 11 0 1 3125.38 2139.82 632.21 o 13 0 1 3853.05 2902.03 914.99 o 15 0 1 1017.45 627.37 935.26 o 17 0 1 472.11 -512.05 2424.54 o -17 1 1 227.51 451.28 849.33 o -16 1 1 286.55 -819.70 819.70 o -15 1 1 2661.29 2017.05 1023.45 o -14 1 1 91.25 34.47 529.15 o -13 1 1 1122.33 1689.03 503.16 o -12 1 1 746.20 797.69 439.80 o -11 1 1 3944.98 3418.63 472.40 o -10 1 1 3885.15 4302.56 443.14 o -9 1 1 4901.08 4225.44 350.52 o -8 1 1 41.84 58.53 202.22 o -7 1 1 432.30 163.04 187.21 o -6 1 1 81.26 127.97 152.47 o -5 1 1 3444.78 3501.83 269.95 o -4 1 1 7684.30 7319.78 365.92 o -3 1 1 3656.56 4197.97 183.95 o -2 1 1 3245.49 3164.83 124.43 o -1 1 1 36346.37 30735.00 808.62 o 0 1 1 30.79 10.17 16.64 o 1 1 1 36490.64 29403.47 1668.69 o 2 1 1 3057.96 3323.68 123.81 o 3 1 1 3713.45 4058.56 212.69 o 4 1 1 7575.47 7020.85 481.57 o 5 1 1 3130.97 2829.69 299.80 o 6 1 1 90.81 59.49 154.45 o 7 1 1 454.51 543.18 192.33 o 8 1 1 38.59 98.54 196.00 o 9 1 1 4436.97 3356.25 620.01 o 10 1 1 3840.98 3903.98 434.13 o 11 1 1 4155.61 4445.67 473.31 o 12 1 1 666.06 1035.06 458.15 o 13 1 1 1027.43 1129.28 540.07 o 14 1 1 98.00 13.90 609.19 o 15 1 1 2372.78 1506.17 696.47 o 16 1 1 281.13 -90.94 665.82 o 17 1 1 216.00 -608.31 708.80 o -17 2 1 883.62 1036.87 898.57 o -16 2 1 30.39 -869.73 869.73 o -15 2 1 154.64 -490.33 600.88 o -14 2 1 795.66 322.86 562.03 o -13 2 1 12.17 -444.06 454.70 o -12 2 1 1526.09 1953.26 479.97 o -11 2 1 1532.35 1201.73 429.89 o -10 2 1 124.81 -114.52 294.89 o -9 2 1 1031.31 1307.54 307.93 o -8 2 1 481.42 335.97 202.50 o -7 2 1 3060.16 3101.44 233.24 o -6 2 1 1121.21 764.82 173.79 o -5 2 1 2550.10 2885.40 175.17 o -4 2 1 1484.01 1425.98 132.52 o -3 2 1 2044.55 2387.79 182.71 o -2 2 1 2964.53 3090.98 197.06 o -1 2 1 5.28 24.82 53.75 o 0 2 1 4474.67 4059.50 100.40 o 1 2 1 5.91 91.35 52.12 o 2 2 1 2920.42 2907.11 116.71 o 3 2 1 2033.23 2177.07 138.90 o 4 2 1 1488.14 1683.23 163.33 o 5 2 1 2280.44 2151.98 350.15 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