#------------------------------------------------------------------------------ #$Date: 2016-04-06 22:09:09 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181921 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/01/2310158.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2310158 _cell_angle_alpha 90.000 _cell_angle_beta 90.057 _cell_angle_gamma 90.000 _cell_length_a 13.3825 _cell_length_b 20.1207 _cell_length_c 19.8810 _exptl_crystal_F_000 2968.00 _reflns_d_resolution_high 0.7413 _cod_data_source_file bp5072str3h6_2_twin_f_co2sup3.hkl _cod_data_source_block str3h6_2_twin_f_co2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' F_CO2_STR3h6_twin in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 918.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 50412.79 56583.16 1015.54 o 4 0 0 20531.04 19105.28 567.85 o 6 0 0 35614.86 28930.56 594.75 o 8 0 0 231833.64 232261.80 8183.95 o 10 0 0 1429.02 1291.43 394.86 o 12 0 0 4738.85 5228.10 923.98 o 14 0 0 71767.95 70812.51 11291.67 o 16 0 0 545.64 -359.37 654.26 o 1 1 0 135717.78 110209.39 11136.07 o 2 1 0 72153.08 64831.48 1376.89 o 3 1 0 41165.72 37411.91 1441.77 o 4 1 0 121323.06 124483.45 2346.81 o 5 1 0 8424.04 7584.45 226.25 o 6 1 0 13404.69 12577.69 300.32 o 7 1 0 617.25 880.21 198.66 o 8 1 0 24934.55 27453.00 1027.65 o 9 1 0 21348.45 21617.59 468.93 o 10 1 0 28357.11 28371.49 618.08 o 11 1 0 11197.13 10545.21 582.64 o 12 1 0 15190.14 14070.55 865.01 o 13 1 0 3934.95 4068.43 446.76 o 14 1 0 1241.43 2240.09 440.75 o 15 1 0 1954.90 2310.07 563.69 o 16 1 0 89.68 -225.81 537.34 o 17 1 0 20.87 -353.93 441.61 o 0 2 0 175240.11 168158.88 1161.27 o 1 2 0 3838.75 3091.88 74.34 o 2 2 0 30022.35 27825.93 1521.03 o 3 2 0 29880.09 30376.95 715.71 o 4 2 0 10518.39 9435.81 275.43 o 5 2 0 11095.04 11820.51 231.99 o 6 2 0 2180.50 3005.60 245.92 o 7 2 0 15609.64 15632.48 365.41 o 8 2 0 347.27 780.62 214.56 o 9 2 0 11050.38 11367.28 387.59 o 10 2 0 6929.47 7547.40 404.58 o 11 2 0 1116.89 1274.24 339.14 o 12 2 0 3198.86 3689.34 421.89 o 13 2 0 994.55 919.13 337.07 o 14 2 0 3459.71 4290.31 576.05 o 15 2 0 605.19 703.23 511.09 o 16 2 0 0.02 -80.45 393.64 o 17 2 0 2062.28 2961.93 834.44 o 1 3 0 63121.47 61500.36 431.31 o 2 3 0 504.90 880.57 85.36 o 3 3 0 477306.13 484077.16 9478.52 o 4 3 0 2422.74 2470.79 195.77 o 5 3 0 55825.94 50868.25 1678.24 o 6 3 0 5305.92 5501.54 168.77 o 7 3 0 33019.89 33518.88 678.59 o 8 3 0 1134.00 1179.47 221.38 o 9 3 0 10669.57 11204.49 416.92 o 10 3 0 1546.84 1722.33 301.35 o 11 3 0 16054.76 18247.40 678.27 o 12 3 0 166.76 61.05 301.64 o 13 3 0 556.54 703.11 343.22 o 14 3 0 2751.11 2325.93 395.22 o 15 3 0 43.35 106.75 359.57 o 16 3 0 56.68 73.97 425.50 o 17 3 0 6247.99 8465.80 1761.02 o 0 4 0 48232.54 45770.28 788.77 o 1 4 0 4299.97 3866.32 104.52 o 2 4 0 1330.67 1636.01 110.85 o 3 4 0 8889.63 9782.73 190.61 o 4 4 0 3437.62 3906.05 149.03 o 5 4 0 754.78 1476.70 150.96 o 6 4 0 2064.60 3436.84 161.29 o 7 4 0 10844.22 11055.47 531.76 o 8 4 0 13.61 -38.60 129.37 o 9 4 0 828.78 1112.07 246.56 o 10 4 0 1158.14 1442.40 283.42 o 11 4 0 13818.40 13107.20 472.63 o 12 4 0 5507.28 4895.02 410.05 o 13 4 0 186.09 378.86 332.88 o 14 4 0 3298.48 3502.91 417.76 o 15 4 0 21.83 -317.82 411.40 o 16 4 0 190.02 123.13 410.55 o 17 4 0 204.06 411.36 439.25 o 1 5 0 843243.25 857287.19 9658.79 o 2 5 0 1083.17 1143.93 98.66 o 3 5 0 159987.80 163510.19 1552.49 o 4 5 0 2062.86 2408.53 127.90 o 5 5 0 1477.20 515.20 108.13 o 6 5 0 1184.92 1391.49 133.96 o 7 5 0 2446.68 2229.16 193.01 o 8 5 0 859.69 881.14 158.10 o 9 5 0 166467.36 161037.77 2969.70 o 10 5 0 537.47 473.93 263.92 o 11 5 0 54038.27 55070.91 1868.12 o 12 5 0 810.60 915.39 324.61 o 13 5 0 23926.09 25861.10 1365.15 o 14 5 0 4.97 -274.60 315.29 o 15 5 0 7015.57 8188.22 1602.09 o 16 5 0 21.88 336.95 425.88 o 17 5 0 3147.65 2026.31 643.85 o 0 6 0 104783.64 103193.91 1873.86 o 1 6 0 24211.15 23892.43 270.83 o 2 6 0 3.38 47.26 65.73 o 3 6 0 41480.41 40640.83 453.89 o 4 6 0 1141.97 1792.76 124.64 o 5 6 0 20155.56 18240.66 318.63 o 6 6 0 885.37 1654.24 182.45 o 7 6 0 16875.89 16559.69 366.26 o 8 6 0 2982.26 3476.99 259.98 o 9 6 0 5967.89 6833.09 350.09 o 10 6 0 6225.77 7492.85 396.62 o 11 6 0 19904.29 20829.09 722.87 o 12 6 0 4606.35 4212.22 396.61 o 13 6 0 100.68 -40.26 321.78 o 14 6 0 6683.40 7445.59 1233.68 o 15 6 0 1277.86 1857.86 456.92 o 16 6 0 24.25 267.95 431.08 o 17 6 0 544.76 1198.21 836.84 o 1 7 0 6093.17 4589.19 135.63 o 2 7 0 12473.04 11488.68 189.96 o 3 7 0 60300.85 51766.36 456.30 o 4 7 0 31396.61 31624.85 389.62 o 5 7 0 1553.77 2389.03 181.67 o 6 7 0 8681.67 8520.60 237.34 o 7 7 0 5029.28 6066.50 222.88 o 8 7 0 33263.07 33667.13 469.05 o 9 7 0 1882.78 2011.23 284.13 o 10 7 0 12.43 -231.13 257.73 o 11 7 0 24533.55 25176.05 1047.04 o 12 7 0 508.11 834.15 340.10 o 13 7 0 11067.34 9576.50 842.22 o 14 7 0 267.14 247.50 369.86 o 15 7 0 237.72 180.75 367.61 o 16 7 0 2258.76 2314.22 532.19 o 0 8 0 132069.34 122311.84 2768.24 o 1 8 0 5159.53 4766.78 146.36 o 2 8 0 10950.60 6457.90 156.92 o 3 8 0 1395.79 1243.38 131.12 o 4 8 0 234867.05 257799.28 2267.48 o 5 8 0 9604.77 9009.25 237.78 o 6 8 0 203085.88 199183.05 2974.09 o 7 8 0 6802.92 7201.25 245.54 o 8 8 0 142740.38 144706.77 2154.19 o 9 8 0 510.37 716.35 251.40 o 10 8 0 16098.14 16658.98 828.65 o 11 8 0 31.57 -60.54 297.22 o 12 8 0 46017.39 46069.12 1839.27 o 13 8 0 487.90 -76.99 365.55 o 14 8 0 10055.48 9909.63 1374.79 o 15 8 0 271.84 341.95 402.82 o 16 8 0 21833.08 21193.85 3921.76 o 1 9 0 1350.92 1565.37 123.16 o 2 9 0 2734.99 3520.54 140.32 o 3 9 0 2012.66 1969.44 156.75 o 4 9 0 6414.99 6561.76 204.76 o 5 9 0 3799.34 4435.42 197.70 o 6 9 0 7878.60 7805.09 242.78 o 7 9 0 490.39 837.15 160.25 o 8 9 0 15557.14 16040.09 411.11 o 9 9 0 1746.14 2382.97 327.13 o 10 9 0 3738.65 2486.18 362.24 o 11 9 0 224.45 234.76 353.15 o 12 9 0 693.64 744.17 391.03 o 13 9 0 59.90 457.82 417.10 o 14 9 0 34.17 104.43 392.28 o 15 9 0 819.70 605.17 432.63 o 16 9 0 413.54 488.19 529.38 o 0 10 0 450368.16 475210.25 10113.79 o 1 10 0 1144.47 1486.31 132.36 o 2 10 0 1990.11 3024.14 171.99 o 3 10 0 2463.48 2607.95 145.01 o 4 10 0 7202.66 7511.28 213.48 o 5 10 0 31.97 17.51 128.28 o 6 10 0 5184.11 5623.90 253.64 o 7 10 0 7.04 -56.29 154.45 o 8 10 0 45811.48 43260.95 623.60 o 9 10 0 477.65 532.50 329.39 o 10 10 0 6887.84 6863.43 518.21 o 11 10 0 4241.83 4668.36 497.07 o 12 10 0 70.59 89.23 366.54 o 13 10 0 7.75 -184.03 387.14 o 14 10 0 910.05 1173.24 452.88 o 15 10 0 14.83 -25.62 431.36 o 16 10 0 405.23 163.56 775.98 o 1 11 0 8074.68 8311.35 212.92 o 2 11 0 30634.72 31360.08 341.09 o 3 11 0 10553.02 9361.38 216.02 o 4 11 0 9975.77 9060.67 270.04 o 5 11 0 999.05 1123.06 167.66 o 6 11 0 31892.82 31865.25 469.24 o 7 11 0 5147.20 5493.45 294.34 o 8 11 0 5435.03 5614.12 512.34 o 9 11 0 2188.09 2521.61 398.63 o 10 11 0 6687.80 6730.22 584.17 o 11 11 0 5246.54 6869.83 607.78 o 12 11 0 3610.90 3631.82 511.09 o 13 11 0 686.33 968.95 435.39 o 14 11 0 123.31 334.45 419.23 o 15 11 0 42.07 -387.34 406.07 o 0 12 0 12.46 -55.95 142.99 o 1 12 0 7773.44 7788.39 214.28 o 2 12 0 66791.68 61761.42 720.53 o 3 12 0 22989.76 21618.02 424.78 o 4 12 0 38765.64 35011.16 470.00 o 5 12 0 23789.44 22547.40 405.09 o 6 12 0 12900.08 13227.57 391.83 o 7 12 0 38147.88 35327.82 590.61 o 8 12 0 14322.28 11983.53 463.22 o 9 12 0 5135.13 6431.35 770.57 o 10 12 0 8046.53 7177.74 544.52 o 11 12 0 38.29 314.56 386.58 o 12 12 0 15882.98 15141.11 821.36 o 13 12 0 418.81 572.09 417.48 o 14 12 0 352.48 -169.49 427.00 o 15 12 0 559.06 694.57 465.24 o 1 13 0 9529.77 9212.27 240.16 o 2 13 0 7195.33 6581.23 256.48 o 3 13 0 525959.94 501383.09 6537.30 o 4 13 0 11140.46 10378.85 306.53 o 5 13 0 68680.41 61620.95 905.00 o 6 13 0 13519.66 11933.72 399.52 o 7 13 0 13203.35 11109.32 402.59 o 8 13 0 8974.96 8840.32 445.26 o 9 13 0 13993.80 13858.05 638.53 o 10 13 0 2020.78 1916.47 419.84 o 11 13 0 75938.08 73430.05 1532.36 o 12 13 0 145.49 424.27 403.97 o 13 13 0 1153.42 703.21 433.08 o 14 13 0 86.18 84.36 414.10 o 15 13 0 474.94 1106.91 897.70 o 0 14 0 7190.49 7888.61 336.01 o 1 14 0 0.26 149.08 138.99 o 2 14 0 372.62 397.77 155.79 o 3 14 0 22570.37 21848.43 465.96 o 4 14 0 1226.17 1542.59 228.36 o 5 14 0 49764.21 45900.41 667.38 o 6 14 0 19934.15 18422.76 517.31 o 7 14 0 35713.80 32706.07 718.16 o 8 14 0 10129.34 9250.16 443.84 o 9 14 0 19848.87 19376.42 684.26 o 10 14 0 42.58 50.68 364.41 o 11 14 0 223.64 186.40 395.36 o 12 14 0 6.68 401.64 413.38 o 13 14 0 13.99 -227.87 369.69 o 14 14 0 1867.74 1827.41 764.16 o 1 15 0 9129.54 8531.87 330.82 o 2 15 0 3310.12 3340.88 258.01 o 3 15 0 3577.59 4018.61 387.05 o 4 15 0 2251.88 2747.32 267.89 o 5 15 0 22811.82 19729.86 489.69 o 6 15 0 12.11 7.00 220.08 o 7 15 0 3513.65 3797.19 316.97 o 8 15 0 71.87 -101.50 262.70 o 9 15 0 7214.99 7412.90 560.68 o 10 15 0 1561.88 2035.77 450.35 o 11 15 0 923.70 1382.08 430.00 o 12 15 0 1847.63 1917.85 486.18 o 13 15 0 5170.58 4748.90 847.66 o 14 15 0 161.84 206.77 686.04 o 0 16 0 213886.16 189498.42 3789.61 o 1 16 0 201.88 605.56 220.29 o 2 16 0 78028.91 68445.01 1093.49 o 3 16 0 82.56 33.88 190.57 o 4 16 0 6637.65 5878.81 344.71 o 5 16 0 1383.79 1364.80 255.37 o 6 16 0 27066.59 26205.29 766.36 o 7 16 0 23.45 224.31 235.15 o 8 16 0 15409.54 16466.16 569.92 o 9 16 0 1921.89 1839.74 428.77 o 10 16 0 568.55 1049.18 415.35 o 11 16 0 1.45 -52.10 380.75 o 12 16 0 1898.51 2065.16 500.45 o 13 16 0 12.18 142.10 605.59 o 1 17 0 218.10 240.13 217.47 o 2 17 0 2060.63 2287.41 292.76 o 3 17 0 4179.89 4691.88 349.87 o 4 17 0 2457.50 2784.34 312.54 o 5 17 0 60.09 97.61 226.49 o 6 17 0 4237.88 4956.05 352.03 o 7 17 0 56.54 272.99 244.11 o 8 17 0 1154.21 1593.62 325.11 o 9 17 0 500.01 816.31 441.42 o 10 17 0 810.04 1135.16 420.16 o 11 17 0 920.29 1345.31 454.24 o 12 17 0 1854.60 1772.21 507.22 o 13 17 0 2403.99 2742.24 1837.25 o 0 18 0 41413.12 35825.11 1156.12 o 1 18 0 816.83 548.45 251.72 o 2 18 0 41280.72 37050.28 1042.62 o 3 18 0 2497.65 2566.08 304.86 o 4 18 0 15219.02 14874.20 520.45 o 5 18 0 1158.28 1230.36 288.27 o 6 18 0 20901.02 21464.84 561.61 o 7 18 0 3333.82 3828.25 550.03 o 8 18 0 15359.17 16419.17 986.14 o 9 18 0 2001.31 1984.49 438.74 o 10 18 0 4340.09 4538.25 804.89 o 11 18 0 3.78 303.09 451.51 o 12 18 0 18486.41 16000.06 1082.15 o 1 19 0 8.61 34.48 225.19 o 2 19 0 792.06 1519.98 299.53 o 3 19 0 102.19 -107.30 244.89 o 4 19 0 24379.36 21570.88 644.05 o 5 19 0 20.51 41.39 311.85 o 6 19 0 12115.59 11565.66 590.53 o 7 19 0 2164.54 2164.64 327.84 o 8 19 0 8949.96 9287.34 807.77 o 9 19 0 1246.15 1689.84 459.27 o 10 19 0 5991.30 7462.40 1065.68 o 11 19 0 99.89 -173.78 412.87 o 12 19 0 723.02 676.46 1090.08 o 0 20 0 47941.36 44157.46 1346.19 o 1 20 0 639.72 684.82 287.22 o 2 20 0 728.85 1331.27 315.86 o 3 20 0 1.98 300.00 265.40 o 4 20 0 1517.77 1359.52 317.08 o 5 20 0 1837.73 2143.65 347.05 o 6 20 0 13550.25 12142.22 865.83 o 7 20 0 268.55 291.04 270.86 o 8 20 0 6211.20 6195.71 513.84 o 9 20 0 178.43 -222.87 414.38 o 10 20 0 8750.62 7873.31 1098.99 o 11 20 0 3006.71 4218.62 1439.04 o 1 21 0 27848.71 25587.81 772.53 o 2 21 0 148.27 404.82 272.75 o 3 21 0 43113.46 38231.20 1407.18 o 4 21 0 1864.56 1640.74 344.31 o 5 21 0 27268.19 22883.06 746.51 o 6 21 0 2002.18 2267.49 430.56 o 7 21 0 1997.87 2319.11 413.66 o 8 21 0 2158.58 1415.31 441.34 o 9 21 0 40612.38 37101.79 1208.14 o 10 21 0 1207.21 -132.93 654.42 o 0 22 0 395.37 1201.99 438.40 o 1 22 0 902.31 1317.40 315.05 o 2 22 0 2494.00 2169.08 360.25 o 3 22 0 489.93 475.30 282.82 o 4 22 0 352.81 430.91 276.31 o 5 22 0 235.49 468.61 286.77 o 6 22 0 495.48 666.59 307.30 o 7 22 0 334.87 926.92 320.08 o 8 22 0 433.16 607.38 935.74 o 9 22 0 4.57 -448.85 665.67 o 10 22 0 0.08 -833.04 1156.36 o 1 23 0 7.25 211.20 259.86 o 2 23 0 954.82 1183.98 319.89 o 3 23 0 8314.68 7925.53 537.53 o 4 23 0 200.57 313.56 281.25 o 5 23 0 752.50 1252.46 339.10 o 6 23 0 2.87 669.86 307.75 o 7 23 0 1225.50 1337.52 350.06 o 8 23 0 3359.50 3668.74 909.12 o 0 24 0 434.12 143.92 393.98 o 1 24 0 670.44 915.45 320.81 o 2 24 0 100.14 78.87 320.64 o 3 24 0 7579.46 8631.67 574.68 o 4 24 0 5868.83 5227.44 567.15 o 5 24 0 6128.96 5519.68 502.46 o 6 24 0 6330.01 7169.64 694.53 o 7 24 0 2700.04 2810.90 569.72 o 8 24 0 6854.89 7417.47 1080.29 o 1 25 0 26129.03 24216.11 999.25 o 2 25 0 22.34 127.19 288.39 o 3 25 0 60.65 182.50 304.59 o 4 25 0 778.72 1378.49 392.01 o 5 25 0 9438.85 9340.76 841.76 o 6 25 0 339.82 1274.28 646.65 o -17 0 1 579.78 455.14 501.31 o -15 0 1 1449.13 1621.84 812.63 o -13 0 1 3952.96 3585.44 714.20 o -11 0 1 3775.03 3001.75 1335.14 o -9 0 1 32875.00 33022.85 1965.76 o -7 0 1 5175.70 5406.06 647.52 o -5 0 1 25994.10 23475.07 884.39 o -3 0 1 47904.81 51335.09 1449.45 o -1 0 1 135887.19 89632.14 34956.75 o 1 0 1 135316.95 88476.88 35703.33 o 3 0 1 46031.69 50369.63 779.85 o 7 0 1 4515.07 3972.83 549.09 o 9 0 1 30775.99 31447.39 810.76 o 11 0 1 3284.99 2043.53 438.95 o 13 0 1 3422.71 2266.25 522.50 o 15 0 1 1316.25 272.61 1428.34 o 17 0 1 553.95 526.28 1271.66 o -17 1 1 268.95 464.29 373.56 o -16 1 1 496.37 906.43 409.02 o -15 1 1 3090.66 3176.53 626.63 o -14 1 1 119.62 545.19 363.76 o -13 1 1 1325.64 1621.37 423.65 o -12 1 1 731.08 621.55 350.20 o -11 1 1 3753.76 4517.54 468.01 o -10 1 1 4361.88 5042.51 465.45 o -9 1 1 4576.50 4845.92 308.91 o -8 1 1 33.51 167.88 208.30 o -7 1 1 352.61 328.48 191.16 o -6 1 1 221.52 238.54 104.60 o -5 1 1 4159.75 4123.51 142.33 o -4 1 1 7149.43 7566.90 163.72 o -3 1 1 4197.47 4628.56 130.59 o -2 1 1 3716.35 3609.11 91.03 o -1 1 1 34343.38 30745.83 437.42 o 0 1 1 20.70 17.32 16.18 o 1 1 1 34449.85 29671.84 933.78 o 2 1 1 3610.99 3634.72 85.52 o 3 1 1 4273.24 4617.47 236.18 o 4 1 1 6819.84 7190.29 144.34 o 5 1 1 3687.44 3460.45 254.45 o 6 1 1 247.29 446.29 150.24 o 7 1 1 377.37 265.70 177.90 o 8 1 1 30.19 -86.37 189.03 o 9 1 1 4009.16 2953.25 268.96 o 10 1 1 4315.30 4614.68 339.84 o 11 1 1 4015.34 4229.01 362.43 o 12 1 1 633.23 705.79 317.35 o 13 1 1 1180.60 1007.31 427.27 o 14 1 1 132.46 165.54 372.61 o 15 1 1 2666.61 1456.10 764.81 o 16 1 1 495.64 -101.19 759.47 o 17 1 1 252.39 206.80 643.75 o -17 2 1 985.45 1888.77 791.02 o -16 2 1 37.90 561.25 526.27 o -15 2 1 136.49 597.67 352.57 o -14 2 1 835.00 693.65 366.02 o -13 2 1 14.11 116.04 332.58 o -12 2 1 1883.97 1966.18 351.74 o -11 2 1 1520.32 1601.37 315.77 o -10 2 1 102.10 191.21 259.37 o -9 2 1 1291.84 1574.75 279.11 o -8 2 1 440.42 463.77 228.73 o -7 2 1 3210.29 3122.34 272.29 o -6 2 1 1295.69 1121.12 223.28 o -5 2 1 2474.81 2211.32 188.87 o -4 2 1 1618.35 1714.03 106.41 o -3 2 1 1997.02 2261.54 110.34 o -2 2 1 2988.35 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