#------------------------------------------------------------------------------ #$Date: 2016-04-06 22:09:09 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181921 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/01/2310159.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2310159 _cell_angle_alpha 90.000 _cell_angle_beta 90.020 _cell_angle_gamma 90.000 _cell_length_a 13.3857 _cell_length_b 20.1057 _cell_length_c 19.8813 _exptl_crystal_F_000 2960.00 _reflns_d_resolution_high 0.7412 _cod_data_source_file bp5072sin12h3_twin_f_dmesup8.hkl _cod_data_source_block sin12h3_twin_f_dme #BEGIN Tags that were not found in dictionaries: _shelx_title ' F_DME_SIN12h3_twin in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 871.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 86173.16 60677.88 960.73 o 4 0 0 12212.88 16521.73 652.94 o 6 0 0 30969.82 29322.76 904.14 o 8 0 0 221397.00 228156.92 4252.48 o 10 0 0 593.95 1110.29 432.84 o 12 0 0 5241.10 4475.47 958.00 o 14 0 0 62420.21 81352.86 2912.01 o 16 0 0 444.14 399.60 1206.40 o 2 1 0 60948.97 51777.33 675.91 o 3 1 0 25581.65 38280.21 483.57 o 4 1 0 120254.07 126762.20 1229.55 o 5 1 0 11763.96 8592.92 309.28 o 6 1 0 12828.65 11754.59 416.96 o 7 1 0 356.63 607.68 177.05 o 8 1 0 27240.16 31318.09 629.16 o 9 1 0 18400.32 20300.56 553.24 o 10 1 0 27685.21 29796.20 863.00 o 11 1 0 10203.25 9697.50 617.60 o 12 1 0 13826.29 13324.15 720.26 o 13 1 0 2890.21 3494.53 510.78 o 14 1 0 448.11 835.89 466.41 o 15 1 0 1588.97 2232.07 647.10 o 16 1 0 86.75 -137.97 618.76 o 17 1 0 52.33 -220.73 898.80 o 1 2 0 2443.29 2413.95 87.43 o 2 2 0 52743.25 30251.25 578.41 o 3 2 0 26622.83 27958.66 448.24 o 4 2 0 15248.16 9863.82 259.83 o 5 2 0 12153.96 13222.54 341.78 o 6 2 0 1189.37 2457.12 200.08 o 7 2 0 14213.27 15273.49 435.17 o 8 2 0 234.81 311.22 190.92 o 9 2 0 11263.43 12679.40 511.41 o 10 2 0 5724.67 5801.28 432.98 o 11 2 0 608.10 964.32 324.94 o 12 2 0 2488.74 3218.42 479.00 o 13 2 0 1009.82 918.61 385.73 o 14 2 0 3607.36 3541.35 613.37 o 15 2 0 426.01 715.56 641.87 o 16 2 0 2.60 72.84 654.50 o 17 2 0 1324.60 909.56 1476.60 o 1 3 0 90371.95 57459.44 824.39 o 2 3 0 29.45 261.54 79.84 o 3 3 0 413452.66 468111.94 6010.76 o 4 3 0 2930.31 2825.26 168.16 o 5 3 0 61743.36 57286.14 633.97 o 6 3 0 4990.76 5707.19 267.59 o 7 3 0 32577.99 35342.07 616.33 o 8 3 0 1159.28 1100.86 207.29 o 9 3 0 10109.82 11143.66 555.48 o 10 3 0 1047.49 906.86 271.70 o 11 3 0 15772.38 18678.95 693.66 o 12 3 0 374.04 507.57 342.21 o 13 3 0 777.38 755.48 388.43 o 14 3 0 2375.80 3047.39 586.88 o 15 3 0 29.46 -305.14 566.61 o 16 3 0 72.35 -46.98 749.92 o 17 3 0 5345.85 4452.90 1347.21 o 0 4 0 70063.40 46183.04 578.92 o 1 4 0 4604.02 3673.29 144.61 o 2 4 0 54.73 1165.97 111.82 o 3 4 0 12517.65 14204.54 741.46 o 4 4 0 1561.82 3255.02 218.35 o 5 4 0 1075.27 2124.42 210.08 o 6 4 0 1700.69 2723.30 203.02 o 7 4 0 10055.79 11164.00 374.95 o 8 4 0 17.80 187.65 190.06 o 9 4 0 1764.24 2596.35 324.09 o 10 4 0 830.01 677.59 291.31 o 11 4 0 10327.22 9929.87 577.72 o 12 4 0 5252.63 5031.09 536.62 o 13 4 0 17.70 393.56 360.23 o 14 4 0 2223.49 2634.57 641.88 o 15 4 0 0.42 147.08 715.57 o 16 4 0 129.07 367.38 811.84 o 17 4 0 480.64 1051.88 1012.95 o 1 5 0 758812.00 850373.00 6829.78 o 2 5 0 597.64 750.26 105.64 o 3 5 0 172560.42 162304.00 993.36 o 4 5 0 2600.56 2706.23 255.60 o 5 5 0 1061.27 246.32 138.60 o 6 5 0 1453.10 1489.65 223.03 o 7 5 0 2799.60 2930.36 300.40 o 8 5 0 1043.29 974.26 241.16 o 9 5 0 152316.06 160988.06 1721.72 o 10 5 0 411.96 374.91 247.16 o 11 5 0 53482.53 58933.34 1288.54 o 12 5 0 657.41 960.37 341.47 o 13 5 0 20589.39 26636.23 1080.38 o 14 5 0 0.19 -27.62 521.01 o 15 5 0 5775.93 6193.00 1743.00 o 16 5 0 29.65 407.33 677.53 o 17 5 0 2379.10 2496.52 1598.38 o 0 6 0 123649.05 104772.98 1111.79 o 1 6 0 23134.56 22780.27 358.45 o 2 6 0 427.69 -60.49 76.44 o 3 6 0 38950.21 39592.48 637.93 o 4 6 0 351.51 802.93 128.24 o 5 6 0 20333.98 18349.64 520.56 o 6 6 0 413.30 681.29 228.54 o 7 6 0 15425.09 16370.71 586.59 o 8 6 0 1936.95 2511.16 304.15 o 9 6 0 7516.26 7991.27 486.98 o 10 6 0 5694.53 6359.51 478.44 o 11 6 0 17118.99 19310.35 789.50 o 12 6 0 4084.74 4022.64 558.94 o 13 6 0 281.10 331.51 459.80 o 14 6 0 5314.12 5583.08 939.29 o 15 6 0 975.16 834.42 692.95 o 16 6 0 140.37 270.34 843.12 o 17 6 0 433.57 175.06 1175.95 o 1 7 0 8785.74 4887.36 208.61 o 2 7 0 11373.54 10817.45 288.19 o 3 7 0 64151.95 54950.19 639.26 o 4 7 0 27268.08 27747.28 482.12 o 5 7 0 983.44 1354.56 163.53 o 6 7 0 9759.44 10383.80 440.33 o 7 7 0 3599.43 4504.17 374.95 o 8 7 0 29760.42 31861.49 925.56 o 9 7 0 1824.70 2129.59 350.13 o 10 7 0 0.58 67.69 260.60 o 11 7 0 20425.72 23189.25 869.30 o 12 7 0 623.05 426.12 330.72 o 13 7 0 9351.27 9394.39 787.67 o 14 7 0 107.87 510.31 589.72 o 15 7 0 145.75 83.65 774.01 o 16 7 0 1256.12 1084.47 1233.04 o 17 7 0 7717.83 9122.21 2287.21 o 0 8 0 138651.47 127003.22 1324.30 o 1 8 0 4845.82 5157.21 223.42 o 2 8 0 8474.53 5672.43 241.53 o 3 8 0 805.79 843.47 140.35 o 4 8 0 221404.13 242938.16 2245.44 o 5 8 0 10967.79 11188.37 371.66 o 6 8 0 188483.22 195265.64 2329.17 o 7 8 0 5910.04 6913.27 418.67 o 8 8 0 139869.52 144213.61 1626.78 o 9 8 0 505.52 786.01 286.77 o 10 8 0 15676.84 17576.21 993.61 o 11 8 0 17.34 183.63 311.68 o 12 8 0 38637.64 49542.46 2303.64 o 13 8 0 443.06 247.69 458.54 o 14 8 0 8927.86 9817.28 1472.63 o 15 8 0 186.78 -102.49 742.50 o 16 8 0 18613.15 29117.23 3192.96 o 1 9 0 2061.14 2064.88 171.74 o 2 9 0 3200.82 3898.90 223.85 o 3 9 0 2632.67 2180.10 193.87 o 4 9 0 4518.73 4955.30 281.50 o 5 9 0 3575.75 3274.99 250.13 o 6 9 0 8877.38 8917.43 435.51 o 7 9 0 592.30 528.30 221.35 o 8 9 0 11283.46 13004.90 564.91 o 9 9 0 1663.86 1988.00 336.97 o 10 9 0 3072.79 2068.34 406.00 o 11 9 0 299.39 227.21 319.84 o 12 9 0 281.14 222.48 394.63 o 13 9 0 3.01 -179.68 408.01 o 14 9 0 15.65 559.88 645.62 o 15 9 0 734.57 440.32 830.12 o 16 9 0 59.46 578.46 1278.71 o 0 10 0 426273.72 461322.63 3277.69 o 1 10 0 675.90 909.72 152.36 o 2 10 0 1633.41 2456.78 245.46 o 3 10 0 2696.53 2842.45 232.59 o 4 10 0 7654.64 8593.19 352.50 o 5 10 0 38.95 -16.68 131.39 o 6 10 0 4451.88 4842.60 362.33 o 7 10 0 6.79 71.01 193.46 o 8 10 0 42362.71 41670.21 1041.72 o 9 10 0 570.38 640.31 299.32 o 10 10 0 6530.05 5381.71 535.45 o 11 10 0 3314.66 3832.52 573.64 o 12 10 0 184.85 563.33 436.18 o 13 10 0 20.39 175.19 506.91 o 14 10 0 712.51 1093.13 602.77 o 15 10 0 1.20 -48.97 782.19 o 16 10 0 272.05 947.61 1309.15 o 1 11 0 8401.17 9188.29 345.17 o 2 11 0 28539.77 28829.98 542.60 o 3 11 0 10568.90 10356.78 360.72 o 4 11 0 8568.83 8760.71 418.75 o 5 11 0 932.72 770.53 241.03 o 6 11 0 32535.46 31767.38 867.77 o 7 11 0 3426.68 4173.38 425.19 o 8 11 0 4503.17 4592.41 467.46 o 9 11 0 1934.29 2480.94 414.07 o 10 11 0 6679.26 6103.87 646.85 o 11 11 0 5026.40 4908.02 752.63 o 12 11 0 3340.70 3002.86 589.46 o 13 11 0 668.72 846.10 556.33 o 14 11 0 144.25 -85.84 529.78 o 15 11 0 137.47 -199.42 805.37 o 0 12 0 25.81 -8.89 176.89 o 1 12 0 7636.32 8083.14 338.90 o 2 12 0 64783.39 65265.48 993.38 o 3 12 0 18880.57 19364.18 580.58 o 4 12 0 36917.77 36997.80 789.21 o 5 12 0 22172.24 23164.20 746.11 o 6 12 0 10796.94 11850.21 605.81 o 7 12 0 36338.83 35548.82 986.03 o 8 12 0 13397.14 12819.29 846.15 o 9 12 0 3896.58 4457.26 502.99 o 10 12 0 6314.58 5949.36 654.07 o 11 12 0 37.46 437.05 411.15 o 12 12 0 12948.08 12348.99 1102.93 o 13 12 0 265.22 253.24 527.56 o 14 12 0 208.22 274.37 548.12 o 15 12 0 441.03 730.48 894.25 o 1 13 0 9465.00 9644.82 436.08 o 2 13 0 5048.77 5042.11 357.73 o 3 13 0 493668.81 481908.13 4636.86 o 4 13 0 12599.20 12325.62 513.74 o 5 13 0 62387.89 58312.38 1185.55 o 6 13 0 11440.88 10176.68 605.85 o 7 13 0 13988.31 11585.89 654.90 o 8 13 0 7712.48 7379.89 593.66 o 9 13 0 12812.00 13278.56 866.86 o 10 13 0 2308.76 1864.29 505.22 o 11 13 0 63868.45 73355.44 2434.61 o 12 13 0 133.06 126.00 426.18 o 13 13 0 933.25 1046.73 619.16 o 14 13 0 137.51 -10.87 578.22 o 15 13 0 350.63 296.84 1233.04 o 0 14 0 7427.36 7759.42 704.41 o 1 14 0 0.00 224.70 195.13 o 2 14 0 372.58 339.13 190.51 o 3 14 0 18152.61 18360.44 614.80 o 4 14 0 1153.75 1034.28 271.05 o 5 14 0 46471.44 45043.11 1088.11 o 6 14 0 18930.87 16747.33 725.21 o 7 14 0 29784.59 29647.11 964.93 o 8 14 0 8707.85 8605.88 639.69 o 9 14 0 17104.15 19751.99 990.13 o 10 14 0 25.95 275.09 417.16 o 11 14 0 347.77 578.93 447.59 o 12 14 0 3.76 -12.82 438.40 o 13 14 0 56.03 279.27 576.30 o 14 14 0 1397.70 1298.23 705.42 o 15 14 0 130.05 -270.20 1244.46 o 1 15 0 8461.37 8960.35 556.11 o 2 15 0 2995.40 3109.36 381.48 o 3 15 0 3591.26 3514.41 393.09 o 4 15 0 1925.67 2013.35 327.34 o 5 15 0 22242.67 20198.56 784.40 o 6 15 0 3.89 77.68 263.48 o 7 15 0 3363.51 2893.42 451.09 o 8 15 0 39.00 -149.99 333.88 o 9 15 0 5747.60 4926.53 648.62 o 10 15 0 1072.15 1475.26 507.64 o 11 15 0 773.70 657.98 468.93 o 12 15 0 1497.49 1150.64 531.98 o 13 15 0 4645.55 4061.69 853.97 o 14 15 0 118.04 84.45 723.86 o 0 16 0 191500.44 183356.25 3722.29 o 1 16 0 0.11 745.28 267.73 o 2 16 0 72717.90 69303.65 1358.95 o 3 16 0 159.60 98.39 219.20 o 4 16 0 6366.08 4982.19 545.35 o 5 16 0 946.85 884.94 351.71 o 6 16 0 22993.66 24795.07 914.59 o 7 16 0 1.10 -15.59 337.38 o 8 16 0 13857.13 14557.57 945.16 o 9 16 0 1717.10 1948.54 527.36 o 10 16 0 654.18 569.00 439.78 o 11 16 0 1.24 88.59 429.88 o 12 16 0 1760.20 1881.59 590.79 o 13 16 0 40.23 31.63 592.90 o 14 16 0 7702.85 7406.30 1270.27 o 1 17 0 213.66 -66.87 223.31 o 2 17 0 1636.81 1373.96 339.35 o 3 17 0 3393.59 3878.41 515.64 o 4 17 0 1749.69 1884.04 435.21 o 5 17 0 90.20 -116.91 287.55 o 6 17 0 4488.16 4161.02 578.77 o 7 17 0 12.99 120.21 413.53 o 8 17 0 668.72 764.21 485.95 o 9 17 0 573.47 485.09 443.38 o 10 17 0 506.33 25.47 427.92 o 11 17 0 832.22 606.24 490.75 o 12 17 0 1075.18 603.87 606.27 o 13 17 0 1546.83 1133.56 833.36 o 0 18 0 37445.20 34319.24 1493.77 o 1 18 0 386.66 616.80 306.87 o 2 18 0 35746.12 36750.22 1088.73 o 3 18 0 2238.96 2394.66 478.13 o 4 18 0 14482.87 16416.50 907.33 o 5 18 0 1229.05 1058.65 395.28 o 6 18 0 17571.34 19861.73 1158.39 o 7 18 0 1922.76 1753.28 569.76 o 8 18 0 13411.70 14355.89 1136.10 o 9 18 0 1918.92 1741.66 630.32 o 10 18 0 3115.86 3402.15 733.11 o 11 18 0 1.80 -133.91 517.59 o 12 18 0 15619.58 15843.14 1606.13 o 13 18 0 0.05 -235.95 1522.27 o 1 19 0 43.02 21.06 265.02 o 2 19 0 612.44 687.67 374.69 o 3 19 0 22.66 -173.07 284.68 o 4 19 0 19093.43 19892.01 995.53 o 5 19 0 24.10 201.20 431.43 o 6 19 0 10145.14 9715.56 1166.26 o 7 19 0 1762.00 1267.87 569.26 o 8 19 0 6856.24 5969.43 863.27 o 9 19 0 1009.40 843.27 567.71 o 10 19 0 4850.96 5020.01 847.47 o 11 19 0 17.54 -147.50 557.39 o 12 19 0 457.45 1107.45 1617.41 o 0 20 0 40228.90 42946.92 1775.40 o 1 20 0 730.87 828.20 355.74 o 2 20 0 467.97 1056.82 429.76 o 3 20 0 6.15 29.50 333.61 o 4 20 0 1392.79 2064.58 594.04 o 5 20 0 1530.03 1711.68 594.85 o 6 20 0 12616.95 11111.01 1040.62 o 7 20 0 210.24 118.93 464.77 o 8 20 0 5108.00 5548.77 852.01 o 9 20 0 180.11 205.31 541.54 o 10 20 0 6221.62 5544.82 901.82 o 11 20 0 2067.46 3091.80 1164.54 o 1 21 0 22347.28 24927.61 1134.34 o 2 21 0 265.15 561.91 391.54 o 3 21 0 36926.51 34651.25 1329.29 o 4 21 0 965.62 1521.95 564.73 o 5 21 0 23324.18 23994.44 1342.41 o 6 21 0 1366.95 1050.69 569.69 o 7 21 0 1917.04 1555.81 637.08 o 8 21 0 2289.05 2534.77 723.83 o 9 21 0 32718.79 33381.55 2432.22 o 10 21 0 752.51 524.35 906.22 o 0 22 0 560.07 455.35 518.80 o 1 22 0 735.96 582.60 424.05 o 2 22 0 2171.49 1864.33 535.49 o 3 22 0 427.15 -4.62 444.67 o 4 22 0 343.40 644.79 505.00 o 5 22 0 262.20 -157.48 466.15 o 6 22 0 377.17 414.06 529.73 o 7 22 0 147.10 428.20 567.20 o 8 22 0 331.03 52.28 549.90 o 9 22 0 79.52 947.46 922.95 o 10 22 0 3.26 871.50 1206.40 o 1 23 0 11.83 -6.73 403.96 o 2 23 0 605.56 547.77 531.09 o 3 23 0 6921.33 7446.53 954.31 o 4 23 0 291.01 157.54 514.94 o 5 23 0 368.85 1304.16 608.13 o 6 23 0 14.51 32.16 517.43 o 7 23 0 749.31 322.52 601.10 o 8 23 0 2470.99 2728.67 1468.99 o 9 23 0 0.04 247.37 1122.67 o 0 24 0 192.77 -76.45 656.18 o 1 24 0 705.51 -126.71 471.55 o 2 24 0 60.53 -136.43 492.24 o 3 24 0 6809.52 8778.45 1038.11 o 4 24 0 4523.47 4957.19 897.17 o 5 24 0 4103.09 3872.20 870.25 o 6 24 0 5248.15 5084.84 940.32 o 7 24 0 2329.95 1762.03 1427.13 o 1 25 0 20484.21 22810.56 1735.54 o 2 25 0 62.83 -238.06 501.68 o 3 25 0 34.24 511.26 580.20 o 4 25 0 889.19 66.64 617.26 o 5 25 0 8250.51 6814.75 1169.76 o 1 26 0 783.13 943.81 1320.57 o 2 26 0 4331.31 4058.51 1182.70 o 3 26 0 1238.45 1131.62 1097.94 o -15 0 1 1244.96 1716.36 1282.51 o -13 0 1 3750.01 4096.00 718.14 o -11 0 1 3616.12 3119.75 567.93 o -9 0 1 31771.08 33418.14 975.51 o -7 0 1 4519.62 3632.38 353.24 o -5 0 1 21250.98 19013.10 602.72 o -3 0 1 48478.68 51730.81 906.42 o 3 0 1 46604.27 50782.31 806.38 o 5 0 1 18019.43 17768.70 1156.93 o 7 0 1 3948.11 3380.27 359.27 o 9 0 1 29655.04 32430.46 1084.59 o 11 0 1 3134.96 2583.13 526.42 o 13 0 1 3205.96 2893.29 635.55 o 15 0 1 1079.06 1033.50 795.03 o 17 0 1 485.64 616.52 1347.21 o -17 1 1 190.58 102.75 1324.38 o -16 1 1 344.66 726.09 865.58 o -15 1 1 2079.18 2352.26 772.33 o -14 1 1 121.84 366.07 390.31 o -13 1 1 1242.50 1557.47 430.00 o -12 1 1 669.87 487.49 330.06 o -11 1 1 3390.35 3997.97 460.79 o -10 1 1 3523.50 3986.80 377.98 o -9 1 1 3693.32 3462.18 314.46 o -8 1 1 35.95 145.67 187.95 o -7 1 1 458.45 387.82 167.16 o -6 1 1 110.25 116.56 114.17 o -5 1 1 3809.87 3200.73 190.45 o -4 1 1 8038.33 7478.51 249.18 o -3 1 1 6552.72 8571.25 331.46 o -2 1 1 2388.46 3612.44 141.09 o -1 1 1 27353.79 22646.97 271.84 o 0 1 1 21.08 8.01 19.82 o 1 1 1 27527.84 22535.12 517.27 o 2 1 1 2316.71 3545.77 125.90 o 3 1 1 6633.86 8529.51 218.91 o 4 1 1 7694.68 7625.60 239.40 o 5 1 1 3266.20 2698.59 182.86 o 6 1 1 124.17 117.36 121.39 o 7 1 1 491.66 585.86 176.42 o 8 1 1 32.65 85.11 176.73 o 9 1 1 3165.02 2802.92 267.67 o 10 1 1 3474.44 4120.07 381.03 o 11 1 1 3717.75 3746.02 434.10 o 12 1 1 573.73 517.90 329.42 o 13 1 1 1077.69 1231.02 394.26 o 14 1 1 139.56 306.67 469.93 o 15 1 1 1775.11 1538.74 589.88 o 16 1 1 340.01 267.68 642.05 o 17 1 1 185.80 -435.97 911.49 o -17 2 1 746.48 -338.71 1343.40 o -16 2 1 45.62 -544.21 1080.81 o -15 2 1 77.01 112.93 493.52 o -14 2 1 462.53 202.82 433.84 o -13 2 1 12.85 182.24 348.40 o -12 2 1 1556.24 1225.38 385.82 o -11 2 1 1329.72 1522.99 359.67 o -10 2 1 25.68 186.65 223.67 o -9 2 1 1387.35 1679.63 273.39 o -8 2 1 424.40 355.22 172.42 o -7 2 1 2951.00 3182.74 299.12 o -6 2 1 1062.09 1117.17 180.88 o -5 2 1 2047.98 1734.44 178.97 o -4 2 1 1936.30 2094.96 177.82 o -3 2 1 2729.01 2643.04 169.71 o -2 2 1 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