data_2310160 _cell_angle_alpha 90.000 _cell_angle_beta 90.023 _cell_angle_gamma 90.000 _cell_length_a 13.3810 _cell_length_b 20.1068 _cell_length_c 19.8750 _exptl_crystal_F_000 2984.00 _reflns_d_resolution_high 0.7337 _[local]_cod_data_source_file bp5072sin24h3_twin_f_dmesup9.hkl _[local]_cod_data_source_block sin24h3_twin_f_dme _shelx_title ' F_DME_SIN24h3_twin in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 891.04 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 71171.08 61363.73 657.38 o 4 0 0 15998.26 16136.61 1017.47 o 6 0 0 34643.08 27740.43 681.31 o 8 0 0 225163.20 233340.08 2341.94 o 10 0 0 595.79 506.07 370.96 o 12 0 0 6186.96 6548.17 1322.25 o 16 0 0 456.82 1005.69 952.14 o 1 1 0 180709.95 70018.67 12401.92 o 2 1 0 59882.04 52578.50 602.71 o 3 1 0 32177.56 38816.38 1056.26 o 4 1 0 121051.25 128264.66 1356.81 o 5 1 0 9415.48 8416.14 293.29 o 6 1 0 12716.24 12205.95 344.63 o 7 1 0 557.82 355.39 200.65 o 8 1 0 27796.67 31600.80 1417.22 o 9 1 0 19408.53 20084.51 533.57 o 10 1 0 28448.37 30077.03 749.49 o 11 1 0 10294.47 11182.65 676.39 o 12 1 0 14335.17 13943.55 801.85 o 13 1 0 3230.25 4179.81 724.25 o 14 1 0 456.88 1406.66 733.10 o 15 1 0 1509.25 2626.35 731.78 o 16 1 0 113.12 626.41 648.80 o 17 1 0 111.66 255.89 700.59 o 0 2 0 242416.88 129571.42 36452.86 o 1 2 0 2584.24 2429.30 135.22 o 2 2 0 41529.54 27567.10 1233.13 o 3 2 0 27219.73 27771.13 329.00 o 4 2 0 12204.35 10039.87 253.36 o 5 2 0 12079.29 13183.77 313.86 o 6 2 0 1686.62 2230.69 200.46 o 7 2 0 14382.69 15556.99 457.78 o 8 2 0 395.29 583.93 209.92 o 9 2 0 11678.63 13136.24 450.89 o 10 2 0 6215.14 6612.52 471.24 o 11 2 0 595.64 560.37 363.04 o 12 2 0 2432.13 3204.32 569.40 o 13 2 0 975.31 1213.44 564.44 o 14 2 0 4014.67 3331.93 790.98 o 15 2 0 767.82 573.51 739.40 o 16 2 0 0.04 304.81 641.33 o 17 2 0 1377.21 2438.21 979.59 o 1 3 0 77178.53 55867.57 1629.67 o 2 3 0 18.26 126.75 96.66 o 3 3 0 439371.66 475957.44 11404.85 o 4 3 0 2890.07 2894.28 228.47 o 5 3 0 57743.30 55897.45 603.45 o 6 3 0 5328.96 5886.17 263.43 o 7 3 0 34242.03 34838.92 923.03 o 8 3 0 1076.17 1267.19 230.28 o 9 3 0 11175.36 12048.45 559.60 o 10 3 0 1205.40 1115.03 354.75 o 11 3 0 16910.92 21539.60 1134.61 o 12 3 0 468.93 738.95 506.00 o 13 3 0 757.53 840.45 553.16 o 14 3 0 2815.66 3203.23 724.22 o 15 3 0 19.02 536.50 711.32 o 16 3 0 27.23 364.33 656.19 o 17 3 0 6101.38 8119.60 1445.37 o 0 4 0 56074.33 44797.49 1516.42 o 1 4 0 4441.29 3596.82 154.27 o 2 4 0 242.37 1514.39 193.03 o 3 4 0 12861.96 15692.17 1323.01 o 4 4 0 2572.50 3954.02 235.12 o 5 4 0 997.36 2390.79 224.00 o 6 4 0 1936.28 2760.81 266.90 o 7 4 0 10211.22 11319.61 464.89 o 8 4 0 12.90 -183.66 223.73 o 9 4 0 2049.26 3206.49 452.65 o 10 4 0 940.86 908.23 335.97 o 11 4 0 10727.25 9703.97 815.46 o 12 4 0 5332.80 6033.37 600.20 o 13 4 0 14.61 -68.85 507.38 o 14 4 0 2255.54 2423.21 655.21 o 15 4 0 0.01 -412.15 591.76 o 16 4 0 182.71 345.34 779.75 o 17 4 0 572.79 1257.21 1752.84 o 1 5 0 793953.63 851916.81 12061.20 o 2 5 0 622.74 770.26 125.26 o 3 5 0 163789.05 159676.00 1400.86 o 4 5 0 2511.77 3127.85 271.97 o 5 5 0 1739.35 738.21 181.70 o 6 5 0 1492.83 1918.08 255.13 o 7 5 0 2653.66 2486.81 315.58 o 8 5 0 904.24 951.68 270.63 o 9 5 0 155148.20 160598.05 1846.63 o 10 5 0 450.96 669.33 369.45 o 11 5 0 56599.03 59278.90 1771.78 o 12 5 0 836.93 1052.32 450.30 o 13 5 0 20367.28 28857.13 1409.85 o 14 5 0 0.49 -528.80 528.80 o 15 5 0 6272.94 7803.35 1082.79 o 16 5 0 20.07 -149.76 759.37 o 17 5 0 2547.31 3961.82 1804.97 o 0 6 0 116812.61 104837.55 1862.97 o 1 6 0 22615.45 22695.14 351.20 o 2 6 0 172.86 65.24 107.18 o 3 6 0 38380.22 39278.32 472.90 o 4 6 0 519.75 915.71 177.44 o 5 6 0 20400.02 19266.78 510.73 o 6 6 0 826.57 1249.56 267.06 o 7 6 0 15621.14 16911.86 535.31 o 8 6 0 2010.58 2023.69 317.74 o 9 6 0 7844.15 9132.83 636.77 o 10 6 0 5878.72 6701.98 494.15 o 11 6 0 17881.24 19349.09 803.79 o 12 6 0 3994.56 3586.87 549.47 o 13 6 0 390.22 817.83 476.29 o 14 6 0 5236.22 5770.88 761.95 o 15 6 0 933.81 790.88 603.93 o 16 6 0 169.52 381.19 929.03 o 17 6 0 522.05 449.61 1479.17 o 1 7 0 6840.31 5236.63 215.43 o 2 7 0 11630.03 10699.25 287.74 o 3 7 0 59312.68 54627.39 588.94 o 4 7 0 27808.41 27842.17 622.06 o 5 7 0 989.60 963.02 219.67 o 6 7 0 10036.64 10085.39 440.55 o 7 7 0 3880.57 4111.45 376.44 o 8 7 0 30745.50 31243.55 935.17 o 9 7 0 1767.61 2192.01 366.01 o 10 7 0 0.55 -333.81 333.81 o 11 7 0 20508.07 24916.93 892.07 o 12 7 0 591.77 492.69 446.07 o 13 7 0 10154.70 9675.16 758.05 o 14 7 0 225.44 114.97 641.37 o 15 7 0 112.82 -589.30 624.26 o 16 7 0 1136.71 964.84 886.17 o 17 7 0 8471.21 6920.15 2150.33 o 0 8 0 133324.53 128602.04 2932.37 o 1 8 0 4895.46 5329.73 229.96 o 2 8 0 9636.78 5778.67 293.39 o 3 8 0 735.98 626.92 146.30 o 4 8 0 230168.45 244887.44 4465.19 o 5 8 0 11635.51 11693.10 579.33 o 6 8 0 187857.09 197451.66 3478.68 o 7 8 0 5865.48 5875.04 398.19 o 8 8 0 145201.52 150783.88 3843.22 o 9 8 0 468.41 321.86 314.25 o 10 8 0 15526.32 16677.32 748.01 o 11 8 0 12.84 -159.14 392.35 o 12 8 0 41250.66 48565.41 1555.63 o 13 8 0 400.86 -45.06 503.36 o 14 8 0 9623.54 9197.01 1017.76 o 15 8 0 217.97 -557.46 772.83 o 1 9 0 1404.45 1918.53 179.93 o 2 9 0 3356.76 3942.93 227.78 o 3 9 0 2153.52 2516.76 212.14 o 4 9 0 4545.39 4996.35 291.60 o 5 9 0 3643.54 3711.21 323.19 o 6 9 0 9066.84 9873.15 456.93 o 7 9 0 390.01 244.97 253.84 o 8 9 0 11506.96 12098.49 542.28 o 9 9 0 1559.93 1592.33 406.51 o 10 9 0 3299.52 2252.74 466.76 o 11 9 0 402.49 -8.96 455.74 o 12 9 0 220.65 -350.71 465.42 o 13 9 0 7.94 -286.45 547.50 o 14 9 0 18.76 -74.28 525.80 o 15 9 0 824.12 341.16 677.74 o 16 9 0 36.44 374.30 1075.43 o 0 10 0 440521.91 462462.00 8206.08 o 1 10 0 657.49 812.22 163.70 o 2 10 0 1989.47 2926.41 225.85 o 3 10 0 2781.21 2946.33 249.46 o 4 10 0 7319.05 8664.12 352.31 o 5 10 0 17.76 -129.58 197.75 o 6 10 0 4573.33 4587.50 365.46 o 7 10 0 26.60 -44.02 238.35 o 8 10 0 45069.59 44749.69 1334.18 o 9 10 0 554.88 456.28 409.94 o 10 10 0 6788.09 6471.93 656.44 o 11 10 0 3918.18 4425.50 708.85 o 12 10 0 236.43 288.39 511.70 o 13 10 0 25.21 -75.31 497.60 o 14 10 0 814.49 453.36 543.26 o 15 10 0 0.61 535.88 710.25 o 16 10 0 329.58 -309.09 1049.20 o 1 11 0 8296.32 9769.40 363.01 o 2 11 0 29135.37 29629.02 542.70 o 3 11 0 10504.18 10374.63 367.49 o 4 11 0 8524.61 9138.50 366.79 o 5 11 0 916.93 876.38 276.15 o 6 11 0 33223.93 32091.47 827.18 o 7 11 0 4091.03 4784.77 451.27 o 8 11 0 4859.94 5061.79 493.14 o 9 11 0 2133.46 2565.04 509.10 o 10 11 0 6848.82 6130.43 671.96 o 11 11 0 5526.52 6306.53 796.81 o 12 11 0 3517.74 3923.22 664.33 o 13 11 0 642.59 239.55 534.89 o 14 11 0 92.48 118.87 547.11 o 15 11 0 101.41 -553.37 553.37 o 16 11 0 196.06 478.78 1195.60 o 0 12 0 23.96 141.34 223.47 o 1 12 0 7677.76 8404.88 347.59 o 2 12 0 64854.12 64873.93 792.51 o 3 12 0 19670.54 20132.89 568.09 o 4 12 0 38906.88 36863.36 907.98 o 5 12 0 23392.04 23982.82 732.06 o 6 12 0 11288.36 11272.49 592.98 o 7 12 0 37811.29 35786.16 936.52 o 8 12 0 13930.88 12329.71 860.02 o 9 12 0 4178.65 4448.45 604.19 o 10 12 0 6723.14 5990.18 686.01 o 11 12 0 13.34 629.10 513.63 o 12 12 0 13875.13 12028.90 926.72 o 13 12 0 323.08 284.43 528.87 o 14 12 0 283.22 22.83 565.19 o 15 12 0 438.95 644.19 606.59 o 1 13 0 9716.32 10953.73 461.85 o 2 13 0 5252.02 5610.52 376.40 o 3 13 0 506545.03 495479.91 8533.26 o 4 13 0 12964.55 13299.77 583.47 o 5 13 0 62379.36 59635.72 1130.51 o 6 13 0 12022.94 11728.70 625.29 o 7 13 0 14738.32 13060.84 913.69 o 8 13 0 7634.69 6944.82 872.65 o 9 13 0 13669.67 13559.78 1278.44 o 10 13 0 2280.59 2413.40 568.93 o 11 13 0 68816.53 75850.48 2381.20 o 12 13 0 151.78 254.71 519.26 o 13 13 0 1011.58 1024.53 568.29 o 14 13 0 153.94 23.08 565.89 o 15 13 0 493.68 452.34 794.55 o 0 14 0 7804.74 7611.69 702.77 o 1 14 0 1.06 137.91 237.05 o 2 14 0 261.96 488.81 229.13 o 3 14 0 18424.19 18195.90 598.04 o 4 14 0 1119.62 1378.19 334.90 o 5 14 0 49626.04 47483.41 1058.59 o 6 14 0 18996.77 18569.96 748.33 o 7 14 0 30860.94 29176.33 1045.78 o 8 14 0 9493.23 10698.25 803.41 o 9 14 0 17998.13 19204.34 975.53 o 10 14 0 36.83 -171.05 448.51 o 11 14 0 440.05 837.08 528.67 o 12 14 0 17.63 113.96 521.77 o 13 14 0 47.27 371.26 566.32 o 14 14 0 1446.80 887.31 635.37 o 15 14 0 123.92 -117.29 1094.71 o 1 15 0 8518.26 9025.17 548.71 o 2 15 0 3100.65 3267.36 394.86 o 3 15 0 3680.94 4049.50 424.00 o 4 15 0 1836.92 1946.17 375.91 o 5 15 0 23350.11 21215.72 782.49 o 6 15 0 9.79 -115.11 305.18 o 7 15 0 3874.62 4242.70 593.68 o 8 15 0 67.07 -238.08 431.91 o 9 15 0 6032.55 6434.57 724.28 o 10 15 0 1291.66 1495.96 552.92 o 11 15 0 857.94 513.38 546.24 o 12 15 0 1848.37 1749.65 618.45 o 13 15 0 5161.57 4082.40 751.89 o 14 15 0 169.73 -195.56 578.48 o 0 16 0 200531.58 189975.00 2895.54 o 1 16 0 0.92 178.89 276.30 o 2 16 0 76281.81 69117.15 1268.64 o 3 16 0 177.53 153.27 339.09 o 4 16 0 6394.13 5685.86 584.68 o 5 16 0 1100.61 923.07 364.14 o 6 16 0 24183.17 25210.49 1012.67 o 7 16 0 9.98 -351.22 399.59 o 8 16 0 14683.49 16191.89 978.49 o 9 16 0 1921.74 1729.83 592.62 o 10 16 0 705.77 838.92 532.42 o 11 16 0 0.31 -97.00 507.44 o 12 16 0 1886.75 1335.08 624.41 o 13 16 0 40.12 607.02 611.53 o 14 16 0 8616.08 5799.37 1870.13 o 1 17 0 249.69 -5.87 289.39 o 2 17 0 1785.01 1599.67 447.71 o 3 17 0 3478.18 4750.99 606.58 o 4 17 0 1891.47 2279.37 484.09 o 5 17 0 94.74 -43.77 353.27 o 6 17 0 5154.10 5301.99 744.67 o 7 17 0 16.17 -191.22 493.70 o 8 17 0 679.92 277.24 477.38 o 9 17 0 519.82 -119.17 474.79 o 10 17 0 567.09 352.98 531.59 o 11 17 0 831.89 379.37 521.65 o 12 17 0 1261.82 1352.26 651.93 o 13 17 0 2000.27 897.48 685.24 o 0 18 0 39090.36 34528.29 1635.89 o 1 18 0 448.66 481.14 335.62 o 2 18 0 37347.95 37239.48 1234.13 o 3 18 0 2277.31 3233.97 535.65 o 4 18 0 15203.03 17143.37 905.61 o 5 18 0 1454.35 1219.75 539.39 o 6 18 0 17799.53 20272.58 1158.56 o 7 18 0 1919.15 2162.12 660.67 o 8 18 0 14357.41 14490.98 1114.29 o 9 18 0 1849.87 1486.32 655.75 o 10 18 0 3557.01 3693.25 788.38 o 11 18 0 0.66 110.58 548.28 o 12 18 0 16632.87 14108.50 1112.00 o 13 18 0 5.81 -868.44 927.97 o 1 19 0 12.11 473.23 353.03 o 2 19 0 587.26 1292.78 441.14 o 3 19 0 49.86 180.59 386.06 o 4 19 0 20981.66 19106.64 960.13 o 5 19 0 7.46 211.42 502.25 o 6 19 0 11161.85 10238.65 963.15 o 7 19 0 1840.91 1418.25 635.11 o 8 19 0 7125.72 7508.57 1003.17 o 9 19 0 1080.92 1278.56 661.73 o 10 19 0 5535.24 5031.95 880.47 o 11 19 0 5.09 431.58 663.00 o 12 19 0 465.99 488.71 1368.39 o 0 20 0 41682.23 42227.79 1654.47 o 1 20 0 843.61 751.13 442.07 o 2 20 0 486.60 1062.29 458.76 o 3 20 0 10.42 -360.15 360.15 o 4 20 0 1507.51 1492.36 589.30 o 5 20 0 1528.42 1973.28 647.92 o 6 20 0 13069.90 13053.85 1062.35 o 7 20 0 265.79 392.66 565.94 o 8 20 0 4993.20 4403.71 830.05 o 9 20 0 264.29 -330.54 567.09 o 10 20 0 7256.87 6215.89 973.87 o 11 20 0 2407.42 1599.77 1089.09 o 12 20 0 23.67 -123.81 1479.17 o 1 21 0 24442.78 25870.62 1101.39 o 2 21 0 241.76 604.94 440.39 o 3 21 0 39187.91 39848.88 1343.02 o 4 21 0 993.38 1350.48 597.79 o 5 21 0 24506.27 25432.65 1320.14 o 6 21 0 1418.39 1184.74 597.63 o 7 21 0 1962.97 1697.00 679.27 o 8 21 0 2554.51 1767.34 672.76 o 9 21 0 35036.13 32211.39 1608.91 o 10 21 0 776.66 407.06 969.56 o 11 21 0 19873.12 12576.16 2404.46 o 0 22 0 657.64 365.46 752.58 o 1 22 0 907.33 873.47 481.55 o 2 22 0 2361.39 2060.82 541.17 o 3 22 0 538.41 717.79 529.76 o 4 22 0 445.61 -40.71 504.51 o 5 22 0 317.99 342.70 563.95 o 6 22 0 389.98 107.73 538.57 o 7 22 0 109.41 514.99 614.43 o 8 22 0 398.14 -184.16 599.31 o 9 22 0 100.41 338.84 1309.75 o 10 22 0 3.46 860.13 1446.58 o 1 23 0 20.44 -183.60 487.40 o 2 23 0 695.14 962.87 486.35 o 3 23 0 7804.86 7815.59 930.53 o 4 23 0 352.52 69.06 516.76 o 5 23 0 420.77 1194.01 626.03 o 6 23 0 3.15 -49.33 557.50 o 7 23 0 989.90 813.74 664.06 o 8 23 0 2408.95 1029.55 1466.13 o 0 24 0 247.69 861.17 1091.45 o 1 24 0 863.70 1090.74 578.83 o 2 24 0 121.32 333.71 534.79 o 3 24 0 7554.96 7627.90 1064.67 o 4 24 0 5264.16 4249.15 822.11 o 5 24 0 4846.12 4698.19 872.31 o 6 24 0 5802.41 4753.90 892.80 o 7 24 0 2683.08 2599.94 1616.00 o 1 25 0 22737.83 21164.44 1781.61 o 2 25 0 67.27 180.64 703.21 o 3 25 0 84.26 315.28 563.41 o 4 25 0 956.57 1451.02 774.35 o 5 25 0 8791.10 6705.92 1749.59 o 0 26 0 76187.12 77203.31 4502.66 o 1 26 0 829.33 3010.46 1472.65 o 2 26 0 4560.98 5695.11 1922.26 o 3 26 0 1330.51 4320.21 1798.46 o 4 26 0 31.92 221.55 970.91 o -17 0 1 731.44 2560.85 1596.46 o -15 0 1 1298.16 716.78 1257.62 o -13 0 1 3706.25 3189.15 743.46 o -11 0 1 3650.85 3300.40 661.56 o -9 0 1 32514.96 33629.80 941.06 o -7 0 1 4319.33 4248.13 417.57 o -5 0 1 20716.48 19483.28 1114.26 o -3 0 1 47670.52 51513.00 647.22 o -1 0 1 121681.28 73182.99 16759.53 o 1 0 1 121934.23 59458.57 23755.61 o 3 0 1 46603.04 49695.05 1785.12 o 5 0 1 19461.70 19165.46 613.67 o 7 0 1 4103.18 3314.42 378.23 o 9 0 1 31637.78 33683.02 934.75 o 11 0 1 3459.86 1972.73 720.82 o 13 0 1 3501.71 3984.29 1000.64 o 15 0 1 1230.84 2036.85 1016.76 o 17 0 1 696.11 894.11 1021.53 o -17 1 1 216.42 871.07 1038.82 o -16 1 1 335.89 753.45 760.85 o -15 1 1 2321.98 2602.08 806.58 o -14 1 1 111.41 178.52 685.46 o -13 1 1 1133.45 2064.49 516.78 o -12 1 1 603.58 745.77 446.97 o -11 1 1 3503.48 3756.46 491.89 o -10 1 1 3992.77 4677.26 418.84 o -9 1 1 3504.25 2784.94 281.02 o -8 1 1 24.48 5.74 201.29 o -7 1 1 366.40 480.13 216.22 o -6 1 1 51.29 230.68 147.58 o -5 1 1 3353.81 2763.28 196.41 o -4 1 1 7691.21 7441.85 238.26 o -3 1 1 6424.13 8149.87 514.07 o -2 1 1 2465.25 3557.67 129.58 o -1 1 1 26781.10 21478.59 1001.64 o 0 1 1 45.06 25.30 22.79 o 1 1 1 26816.62 21987.65 719.46 o 2 1 1 2370.86 3354.38 165.46 o 3 1 1 6459.59 7250.50 469.85 o 4 1 1 7642.00 7498.20 240.57 o 5 1 1 3163.73 2898.65 197.48 o 6 1 1 52.90 147.28 147.39 o 7 1 1 376.74 244.87 202.77 o 8 1 1 25.96 -83.83 191.83 o 9 1 1 3312.03 3300.45 306.96 o 10 1 1 3971.58 4572.74 439.54 o 11 1 1 3655.34 3626.58 531.21 o 12 1 1 568.32 1074.55 555.44 o 13 1 1 1074.03 1657.44 709.64 o 14 1 1 116.39 492.08 602.88 o 15 1 1 2185.56 2736.32 738.24 o 16 1 1 330.71 1063.37 693.28 o 17 1 1 207.49 129.81 720.79 o 18 1 1 353.86 1355.36 1720.26 o -17 2 1 866.93 1569.99 1100.12 o -16 2 1 43.36 -73.94 722.54 o -15 2 1 128.98 343.41 616.07 o -14 2 1 633.85 574.58 543.76 o -13 2 1 19.15 -484.86 484.86 o -12 2 1 1613.04 1468.15 468.19 o -11 2 1 1197.47 968.29 351.80 o -10 2 1 26.58 46.15 278.34 o -9 2 1 1389.06 1519.39 302.89 o -8 2 1 371.44 677.18 230.05 o -7 2 1 2977.20 3059.23 315.40 o -6 2 1 1133.89 1246.04 175.25 o -5 2 1 1682.84 1813.09 173.24 o -4 2 1 1978.33 1955.89 158.63 o -3 2 1 2819.51 2629.75 152.35 o -2 2 1 2805.48 3036.42 128.77 o -1 2 1 529.90 217.22 60.36 o 0 2 1 3021.34 3104.51 103.60 o 1 2 1 531.13 249.57 61.52 o 2 2 1 2781.66 2988.90 147.13 o 3 2 1 2807.45 2645.49 180.59 o 4 2 1 1976.12 1913.58 151.71 o 5 2 1 1593.95 1234.06 157.59 o 6 2 1 1193.24 1105.35 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