Crystallography Open Database

Information card for entry 2311449

Preview

Coordinates	2311449.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	μ~2~-Chlorido-dichlorido(μ~2~-2-{[2-(dimethylamino)ethyl]iminomethyl}phenolato)(<i>N</i>,<i>N</i>-dimethylethylenediamine)dicopper(II) 0.11-hydrate
Formula	C15 H27.22 Cl3 Cu2 N4 O1.11
Calculated formula	C15 H27 Cl3 Cu2 N4 O1.108
Title of publication	<i>N</i>,<i>N</i>',<i>N</i>'' <i>versus N</i>,<i>N</i>',<i>O</i> imine-containing coordination motifs: ligand-directed synthesis of mononuclear and binuclear Cu<sup>II</sup> compounds.
Authors of publication	Ferraz de Paiva, Raphael Enoque; Nakahata, Douglas Hideki; de Carvalho, Marcos Alberto; Rodrigues Goulart Bergamini, Fernando; Corbi, Pedro Paulo
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2017
Journal volume	73
Journal issue	Pt 10
Pages of publication	1563 - 1567
a	11.0838 ± 0.0004 Å
b	18.0949 ± 0.0007 Å
c	10.661 ± 0.0004 Å
α	90°
β	101.474 ± 0.002°
γ	90°
Cell volume	2095.44 ± 0.14 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0256
Residual factor for significantly intense reflections	0.022
Weighted residual factors for significantly intense reflections	0.0545
Weighted residual factors for all reflections included in the refinement	0.0562
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
245893 (current)	2019-12-25	cif/ Adding structures of 2311449, 2311450 via cif-deposit CGI script.	2311449.cif