Crystallography Open Database

Information card for entry 2311984

2311983 << 2311984 >> 2311985

Preview

Coordinates	2311984.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	3,4-Dimethylpyridine‒3,4-dimethylpyridinium diiodidoaurate(I)
Formula	C14 H19 Au I2 N2
Calculated formula	C14 H19 Au I2 N2
Title of publication	3,4-Lutidinium salts with the diiodidoaurate(I) anion: structure of [(3,4-lut)<sub>2</sub>H]<sup>+</sup>·[AuI<sub>2</sub>]<sup>-</sup> and of two polymorphs of [(3,4-lut)<sub>2</sub>H<sup>+</sup>]<sub>2</sub>·[AuI<sub>2</sub>]<sup>-</sup>·I<sup/>.
Authors of publication	Döring, Cindy; Sui, Zhihong; Jones, Peter G.
Journal of publication	Acta crystallographica. Section C, Structural chemistry
Year of publication	2018
Journal volume	74
Journal issue	Pt 3
Pages of publication	289 - 294
a	15.527 ± 0.0005 Å
b	7.46802 ± 0.00001 Å
c	17.0254 ± 0.0005 Å
α	90°
β	116.528 ± 0.004°
γ	90°
Cell volume	1766.35 ± 0.1 Å³
Cell temperature	105 ± 2 K
Ambient diffraction temperature	105 ± 2 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.027
Residual factor for significantly intense reflections	0.0207
Weighted residual factors for significantly intense reflections	0.0396
Weighted residual factors for all reflections included in the refinement	0.0411
Goodness-of-fit parameter for all reflections included in the refinement	1.098
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
246229 (current)	2019-12-27	cif/ Adding structures of 2311984, 2311985, 2311986, 2311987 via cif-deposit CGI script.	2311984.cif