#------------------------------------------------------------------------------ #$Date: 2023-04-05 18:59:14 +0300 (Wed, 05 Apr 2023) $ #$Revision: 282417 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/20/2312052.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312052 _cell_angle_alpha 90.000 _cell_angle_beta 97.235 _cell_angle_gamma 90.000 _cell_length_a 23.1874 _cell_length_b 30.2708 _cell_length_c 7.2839 _exptl_crystal_F_000 2328.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file zv20194sup3.hkl _cod_data_source_block 4 _shelx_title ' shelxt_a.res in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 245.61 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 79.87 145.15 7.96 o 10 0 0 383.03 514.84 8.99 o 12 0 0 2378.51 2206.02 34.11 o 14 0 0 21881.15 22057.27 440.40 o 16 0 0 16926.71 16944.89 199.97 o 18 0 0 36674.29 37407.12 1040.45 o 20 0 0 12822.37 12845.64 172.67 o 22 0 0 7207.71 6953.21 101.86 o 24 0 0 41.73 22.86 10.37 o 26 0 0 1366.62 1420.47 35.52 o 28 0 0 316.88 313.32 20.92 o 30 0 0 5.00 4.16 12.38 o 5 1 0 5086.99 5957.61 64.63 o 11 1 0 11167.53 7678.75 53.83 o 13 1 0 14792.40 18165.33 182.39 o 15 1 0 191.32 32.92 3.98 o 17 1 0 183.53 59.57 5.21 o 19 1 0 45.35 10.67 5.55 o 21 1 0 107.33 29.30 7.38 o 23 1 0 300.80 497.66 15.23 o 25 1 0 1534.12 1403.19 24.39 o 27 1 0 1094.20 1135.34 22.80 o 29 1 0 672.87 714.35 19.71 o 10 2 0 20354.09 24478.72 686.65 o 12 2 0 5064.88 5968.57 42.18 o 14 2 0 423.89 627.55 9.05 o 16 2 0 1672.79 1971.56 24.05 o 18 2 0 1722.05 1737.59 22.26 o 20 2 0 317.48 290.08 11.33 o 22 2 0 132.74 306.69 16.83 o 24 2 0 77.89 103.33 9.56 o 26 2 0 166.91 249.47 12.36 o 28 2 0 201.86 147.59 11.16 o 30 2 0 57.53 77.32 10.31 o 5 3 0 455.27 84.20 2.68 o 9 3 0 12547.00 11634.69 105.52 o 11 3 0 34.87 165.80 5.62 o 13 3 0 2386.41 1879.95 17.23 o 15 3 0 10.80 21.25 3.63 o 17 3 0 5.40 5.69 4.21 o 19 3 0 555.18 546.39 12.25 o 21 3 0 2669.12 2579.36 33.22 o 23 3 0 127.73 200.27 10.59 o 25 3 0 240.43 271.43 12.66 o 27 3 0 197.21 256.29 12.68 o 29 3 0 11.25 8.75 8.38 o 6 4 0 12001.94 13151.65 260.50 o 8 4 0 12.66 233.14 4.93 o 10 4 0 7488.48 5714.46 38.77 o 12 4 0 5297.72 5925.72 41.89 o 14 4 0 17210.35 15208.07 126.84 o 16 4 0 23171.27 24235.78 394.87 o 18 4 0 10395.34 10705.92 89.20 o 20 4 0 1365.88 1302.94 20.87 o 22 4 0 47.01 46.85 6.78 o 24 4 0 1116.10 1012.88 20.09 o 26 4 0 225.66 292.48 13.21 o 28 4 0 5.95 6.37 8.48 o 30 4 0 50.62 138.32 11.29 o 7 5 0 2815.44 1005.10 8.59 o 9 5 0 16895.19 19602.34 388.12 o 11 5 0 9359.36 6977.92 46.81 o 13 5 0 1532.73 1305.44 12.98 o 15 5 0 9160.82 8567.66 68.91 o 17 5 0 2211.17 2583.14 26.62 o 19 5 0 384.97 291.37 8.63 o 21 5 0 162.10 230.29 9.63 o 23 5 0 2232.50 2142.26 28.18 o 25 5 0 2439.88 2478.53 34.53 o 27 5 0 2540.01 2455.63 35.31 o 29 5 0 711.76 723.28 20.33 o 6 6 0 19.26 53.88 2.16 o 8 6 0 19.76 66.68 2.56 o 10 6 0 5371.27 5334.00 37.57 o 12 6 0 1748.93 2307.16 20.37 o 14 6 0 1245.23 1237.92 14.03 o 16 6 0 160.90 120.91 5.52 o 18 6 0 104.94 174.81 6.93 o 20 6 0 1024.72 1146.16 17.56 o 22 6 0 1458.09 1684.77 23.67 o 24 6 0 188.31 117.70 8.75 o 26 6 0 643.03 941.77 20.35 o 28 6 0 454.30 345.38 14.21 o 30 6 0 195.36 165.25 11.71 o 1 7 0 2834.73 1430.61 8.79 o 5 7 0 8338.22 5679.89 38.19 o 9 7 0 25987.89 24252.44 478.69 o 13 7 0 28.57 167.71 5.12 o 15 7 0 4167.50 4665.00 40.29 o 17 7 0 880.13 1096.68 14.93 o 19 7 0 4897.39 4424.71 41.75 o 21 7 0 4190.35 4487.94 49.83 o 23 7 0 33.89 39.56 6.48 o 25 7 0 72.30 30.41 6.80 o 27 7 0 23.79 19.00 7.75 o 29 7 0 67.73 75.62 9.68 o 6 8 0 3159.19 4474.31 30.17 o 8 8 0 3289.06 2753.35 19.72 o 10 8 0 531.95 376.76 5.67 o 12 8 0 6555.93 6601.49 49.12 o 14 8 0 8286.12 7938.72 64.34 o 16 8 0 22008.33 22259.95 200.75 o 18 8 0 22117.72 22584.01 195.21 o 20 8 0 9029.94 8986.54 81.16 o 22 8 0 4644.20 4903.90 48.89 o 24 8 0 77.89 138.77 8.60 o 26 8 0 36.84 70.41 7.57 o 28 8 0 924.07 968.42 21.38 o 30 8 0 0.23 -4.25 10.20 o 1 9 0 3591.66 1668.19 9.80 o 3 9 0 20.36 257.35 3.63 o 5 9 0 39.85 46.32 2.27 o 13 9 0 9817.12 8198.35 65.85 o 15 9 0 6193.34 6924.02 57.48 o 17 9 0 681.45 590.10 10.66 o 19 9 0 1271.20 1395.58 20.22 o 21 9 0 245.37 387.18 10.88 o 23 9 0 1274.12 1078.83 19.17 o 25 9 0 3143.66 3243.00 41.37 o 27 9 0 2180.88 2349.01 36.28 o 29 9 0 4463.75 4707.25 66.25 o 2 10 0 10893.98 12311.34 131.29 o 4 10 0 554.10 841.67 7.02 o 6 10 0 6209.15 7174.29 54.50 o 8 10 0 2277.64 1813.59 14.15 o 10 10 0 6727.78 7643.64 55.34 o 12 10 0 450.18 438.70 7.66 o 14 10 0 349.46 344.10 8.80 o 16 10 0 102.96 125.57 5.66 o 18 10 0 87.00 67.22 5.68 o 20 10 0 2523.61 2403.31 35.38 o 22 10 0 1431.68 1604.15 21.93 o 24 10 0 697.55 686.77 23.35 o 26 10 0 373.21 442.96 12.87 o 28 10 0 74.67 40.40 10.51 o 1 11 0 2309.65 1864.78 11.09 o 3 11 0 16747.71 19796.61 391.76 o 5 11 0 1545.92 974.13 8.75 o 7 11 0 56.36 45.20 2.90 o 9 11 0 1383.27 856.71 9.56 o 11 11 0 1514.95 1271.23 13.26 o 13 11 0 1444.87 1525.01 16.71 o 15 11 0 1398.67 1410.85 16.53 o 17 11 0 8790.18 8478.34 69.43 o 19 11 0 6070.33 5725.89 54.87 o 21 11 0 113.70 177.66 7.96 o 23 11 0 301.74 149.24 9.21 o 25 11 0 516.52 676.00 16.10 o 27 11 0 3.78 -5.05 9.13 o 29 11 0 33.25 31.36 10.76 o 0 12 0 2153.08 712.83 8.14 o 4 12 0 20914.27 19975.25 281.42 o 6 12 0 1686.91 1746.99 16.13 o 8 12 0 8217.37 9401.94 63.51 o 10 12 0 170.10 184.17 6.88 o 12 12 0 171.86 243.84 6.11 o 14 12 0 4598.27 4432.96 37.69 o 16 12 0 3115.71 3241.11 32.07 o 18 12 0 319.37 366.76 10.27 o 20 12 0 3651.23 3625.69 38.45 o 22 12 0 8651.54 8539.45 81.40 o 24 12 0 3904.03 3823.96 47.70 o 26 12 0 1121.53 953.40 23.15 o 28 12 0 1.18 12.91 9.52 o 1 13 0 2024.45 2229.76 13.48 o 3 13 0 2002.06 2203.63 14.64 o 5 13 0 32640.04 32306.38 636.86 o 7 13 0 20074.74 23174.41 585.93 o 9 13 0 4772.25 3124.05 27.28 o 11 13 0 17682.62 19018.70 163.29 o 13 13 0 15096.34 14151.06 106.56 o 15 13 0 18774.01 18926.60 141.00 o 17 13 0 15189.54 15008.65 122.27 o 19 13 0 3809.98 3739.56 40.57 o 21 13 0 22.57 24.63 7.15 o 23 13 0 1533.85 1495.27 25.64 o 25 13 0 2331.66 2340.38 36.18 o 27 13 0 1903.12 1913.76 34.57 o 29 13 0 743.67 783.43 30.92 o 0 14 0 3110.30 3902.84 29.26 o 2 14 0 2924.93 2407.66 14.44 o 4 14 0 5116.81 6185.13 37.93 o 6 14 0 1563.16 1445.88 12.04 o 8 14 0 56.01 12.93 2.96 o 10 14 0 9582.91 10678.38 87.24 o 12 14 0 1127.34 968.99 13.64 o 14 14 0 1748.04 1673.33 18.87 o 16 14 0 554.93 623.96 11.57 o 18 14 0 1995.41 1647.90 23.95 o 20 14 0 3479.57 3747.40 40.02 o 22 14 0 2554.77 2152.76 34.52 o 24 14 0 4872.68 5499.64 62.26 o 26 14 0 516.96 335.23 14.94 o 28 14 0 298.23 434.66 18.19 o 1 15 0 9.64 14.01 1.60 o 3 15 0 3363.79 3742.97 22.33 o 5 15 0 8253.10 8652.48 58.60 o 7 15 0 4748.09 5320.76 35.33 o 9 15 0 2863.04 3236.11 27.64 o 11 15 0 689.26 617.95 10.10 o 13 15 0 170.06 154.92 6.78 o 15 15 0 14.44 128.37 6.70 o 17 15 0 466.43 461.60 12.26 o 19 15 0 152.90 208.79 8.28 o 21 15 0 190.97 293.77 13.78 o 23 15 0 141.80 63.22 8.79 o 25 15 0 58.05 137.91 11.17 o 27 15 0 17.38 15.29 8.82 o 0 16 0 778.52 1817.38 15.35 o 2 16 0 450.49 477.60 4.72 o 4 16 0 5483.45 4668.12 31.14 o 6 16 0 6683.73 6754.88 44.01 o 8 16 0 2161.65 1834.68 16.73 o 10 16 0 353.89 348.96 7.49 o 12 16 0 22.70 27.94 4.27 o 14 16 0 53.78 52.82 5.24 o 16 16 0 1166.01 1200.02 16.50 o 18 16 0 1588.46 1830.04 22.68 o 20 16 0 3156.11 3006.90 36.31 o 22 16 0 3022.98 3241.06 44.10 o 24 16 0 3727.78 3723.62 46.69 o 26 16 0 710.37 658.60 19.46 o 28 16 0 31.32 51.67 9.90 o 1 17 0 449.68 230.13 3.65 o 3 17 0 1369.12 1778.46 12.31 o 5 17 0 3166.68 2946.76 21.98 o 7 17 0 10676.91 11515.65 75.44 o 9 17 0 8100.30 8148.66 58.21 o 11 17 0 5831.52 5481.35 44.24 o 13 17 0 3586.39 3583.02 32.78 o 15 17 0 1606.15 1614.26 20.45 o 17 17 0 8689.42 8692.11 78.93 o 19 17 0 3228.80 3286.93 35.76 o 21 17 0 7.15 7.29 6.85 o 23 17 0 1160.97 1216.39 23.21 o 25 17 0 1153.45 1142.03 23.50 o 27 17 0 2394.25 2423.84 37.04 o 0 18 0 2505.04 2063.70 17.99 o 2 18 0 337.46 195.36 4.98 o 4 18 0 311.32 144.45 5.13 o 6 18 0 2072.15 2633.65 21.26 o 8 18 0 3085.24 2716.39 22.37 o 10 18 0 454.66 566.43 8.83 o 12 18 0 1504.78 1314.16 16.59 o 14 18 0 438.96 402.10 10.75 o 16 18 0 95.06 109.19 7.37 o 18 18 0 170.32 177.11 8.78 o 20 18 0 2493.63 2616.03 34.53 o 22 18 0 3664.75 3456.57 53.97 o 24 18 0 1952.93 2021.73 31.22 o 26 18 0 1590.90 1461.44 28.87 o 1 19 0 3290.20 3245.60 20.00 o 3 19 0 929.14 991.41 8.97 o 5 19 0 2920.83 3732.73 27.68 o 7 19 0 2680.76 2732.16 22.81 o 9 19 0 600.20 433.03 8.27 o 11 19 0 64.34 58.18 4.55 o 13 19 0 4589.84 4652.03 39.53 o 15 19 0 5981.03 5874.71 53.41 o 17 19 0 3464.08 3612.82 40.07 o 19 19 0 1639.08 1526.32 22.35 o 21 19 0 14.38 26.27 8.10 o 23 19 0 0.54 13.62 7.36 o 25 19 0 267.11 255.27 16.35 o 27 19 0 2.35 15.54 9.38 o 0 20 0 401.62 402.24 8.97 o 2 20 0 108.58 119.87 3.44 o 4 20 0 3053.36 2798.70 21.30 o 6 20 0 10077.93 10352.17 72.22 o 8 20 0 4328.59 4512.56 36.11 o 10 20 0 930.95 792.38 10.42 o 12 20 0 367.32 300.79 7.82 o 14 20 0 979.46 1122.49 16.31 o 16 20 0 634.50 483.60 13.45 o 18 20 0 114.69 118.70 7.42 o 20 20 0 3116.67 3065.78 37.82 o 22 20 0 3384.26 3415.84 47.73 o 24 20 0 1943.45 2043.63 34.90 o 26 20 0 1040.92 1020.22 27.96 o 1 21 0 1550.77 1776.20 12.92 o 3 21 0 4188.07 4452.67 30.00 o 5 21 0 2720.47 2356.97 19.73 o 7 21 0 8314.49 7822.62 56.34 o 9 21 0 5268.44 5604.67 41.59 o 11 21 0 8132.33 7882.99 56.33 o 13 21 0 26564.17 26891.54 181.58 o 15 21 0 8502.17 8383.71 71.29 o 17 21 0 157.62 151.07 7.36 o 19 21 0 3.02 26.70 6.72 o 21 21 0 5.04 91.88 10.03 o 23 21 0 523.30 691.51 22.22 o 25 21 0 2090.70 2132.76 37.91 o 0 22 0 3765.85 2963.42 27.35 o 2 22 0 8690.11 9551.33 56.77 o 4 22 0 5903.17 5064.58 35.44 o 6 22 0 3610.51 3754.69 28.59 o 8 22 0 1071.17 883.97 11.08 o 10 22 0 381.69 379.02 8.61 o 12 22 0 754.19 686.87 14.54 o 14 22 0 476.88 567.23 12.64 o 16 22 0 7697.28 7505.29 63.01 o 18 22 0 13010.64 13293.52 112.59 o 20 22 0 5032.17 4706.83 51.11 o 22 22 0 1034.42 1219.59 31.97 o 24 22 0 493.37 516.28 19.30 o 1 23 0 181.07 191.05 5.33 o 3 23 0 1484.90 1724.15 14.87 o 5 23 0 13754.55 13302.28 89.77 o 7 23 0 14197.06 14897.93 97.57 o 9 23 0 1233.20 1112.49 14.17 o 11 23 0 828.97 961.58 12.12 o 13 23 0 121.02 105.46 6.29 o 15 23 0 461.06 371.04 10.02 o 17 23 0 261.94 248.64 9.28 o 19 23 0 875.07 792.25 18.45 o 21 23 0 15.59 37.90 8.08 o 23 23 0 73.63 227.42 16.84 o 25 23 0 80.58 149.08 13.16 o 0 24 0 151.07 227.40 6.67 o 2 24 0 298.05 325.18 6.05 o 4 24 0 915.28 1027.16 12.41 o 6 24 0 106.71 157.37 6.01 o 8 24 0 433.52 489.13 8.39 o 10 24 0 235.46 165.57 6.68 o 12 24 0 84.04 60.15 4.59 o 14 24 0 91.65 103.93 5.81 o 16 24 0 622.74 710.51 13.37 o 18 24 0 967.42 852.95 14.51 o 20 24 0 1840.77 2091.75 27.04 o 22 24 0 2104.85 1924.33 34.77 o 24 24 0 230.99 281.07 15.97 o 1 25 0 24.27 44.78 3.41 o 3 25 0 401.87 366.47 9.12 o 5 25 0 246.69 191.77 6.38 o 7 25 0 816.40 727.96 11.00 o 9 25 0 1888.20 1891.11 22.15 o 11 25 0 5528.11 5456.07 44.40 o 13 25 0 3422.95 3759.17 31.26 o 15 25 0 3674.96 3410.93 30.23 o 17 25 0 1960.87 2020.55 22.61 o 19 25 0 186.53 148.20 8.62 o 21 25 0 1.45 14.79 7.07 o 23 25 0 5.85 13.71 9.98 o 0 26 0 18351.67 18362.87 161.10 o 2 26 0 15659.95 16337.40 101.60 o 4 26 0 1749.44 1890.79 18.70 o 6 26 0 864.24 914.54 12.27 o 8 26 0 399.94 469.31 9.59 o 10 26 0 826.70 866.85 13.39 o 12 26 0 1151.95 1162.93 18.07 o 14 26 0 2248.35 2372.68 23.28 o 16 26 0 2082.21 2081.77 23.24 o 18 26 0 3805.05 3715.65 38.34 o 20 26 0 1355.58 1335.17 22.23 o 22 26 0 378.43 328.54 14.34 o 1 27 0 1549.72 1522.71 15.28 o 3 27 0 1956.23 2187.02 19.40 o 5 27 0 318.48 310.29 7.81 o 7 27 0 378.40 517.29 10.05 o 9 27 0 743.33 797.26 14.05 o 11 27 0 1304.16 1195.38 15.68 o 13 27 0 1419.21 1566.83 21.44 o 15 27 0 2.54 14.46 4.41 o 17 27 0 382.18 347.32 9.46 o 19 27 0 559.01 621.43 17.64 o 21 27 0 657.50 674.10 16.83 o 0 28 0 524.26 514.59 12.53 o 2 28 0 215.37 193.38 6.51 o 4 28 0 3312.64 3181.99 28.93 o 6 28 0 821.87 568.29 10.30 o 8 28 0 930.34 989.16 13.55 o 10 28 0 5.88 3.12 4.65 o 12 28 0 315.84 318.39 9.54 o 14 28 0 44.67 34.50 6.47 o 16 28 0 75.11 105.28 7.19 o 18 28 0 364.33 268.20 12.81 o 20 28 0 134.78 177.48 10.03 o 22 28 0 576.19 551.86 17.91 o 1 29 0 1757.65 1732.62 18.14 o 3 29 0 3578.20 3420.50 35.82 o 5 29 0 4158.46 4069.84 36.68 o 7 29 0 5608.65 5628.59 50.62 o 9 29 0 3948.55 3848.78 34.75 o 11 29 0 1556.20 1519.60 19.07 o 13 29 0 1563.21 1718.65 23.52 o 15 29 0 1288.06 1149.09 20.06 o 17 29 0 184.39 206.25 12.44 o 19 29 0 10.26 27.76 8.44 o 21 29 0 118.43 159.85 11.87 o 0 30 0 40668.46 43198.92 495.39 o 2 30 0 22043.63 21900.65 150.11 o 4 30 0 11589.90 11196.74 86.26 o 6 30 0 2975.25 2709.54 25.43 o 8 30 0 4.59 4.54 4.29 o 10 30 0 224.59 268.88 8.81 o 12 30 0 672.80 735.41 12.88 o 14 30 0 4138.59 4199.05 43.19 o 16 30 0 2959.95 3092.04 35.67 o 18 30 0 2064.71 1954.27 31.94 o 20 30 0 1032.22 1212.50 25.11 o 1 31 0 0.83 2.12 4.48 o 3 31 0 292.42 315.54 9.63 o 5 31 0 3209.58 3240.35 37.03 o 7 31 0 3130.97 3064.09 33.16 o 9 31 0 3808.34 3786.94 35.68 o 11 31 0 547.14 522.58 12.59 o 13 31 0 177.46 233.25 9.82 o 15 31 0 106.64 118.64 8.74 o 17 31 0 42.59 39.43 9.02 o 19 31 0 115.23 138.51 11.52 o 0 32 0 14053.17 14194.27 209.32 o 2 32 0 2708.99 2609.93 30.48 o 4 32 0 138.53 86.89 7.46 o 6 32 0 48.38 22.60 6.59 o 8 32 0 27.30 24.92 6.13 o 10 32 0 1016.12 932.18 14.77 o 12 32 0 1636.98 1450.87 20.54 o 14 32 0 371.78 338.56 12.11 o 16 32 0 135.51 117.36 9.66 o 18 32 0 883.37 811.53 20.62 o 1 33 0 342.27 476.46 12.72 o 3 33 0 1209.44 1112.89 17.83 o 5 33 0 2531.09 2344.73 29.13 o 7 33 0 5448.07 5596.90 56.22 o 9 33 0 3770.08 3714.57 38.27 o 11 33 0 1325.28 1234.99 17.91 o 13 33 0 260.82 278.97 11.53 o 15 33 0 264.50 259.77 12.02 o 17 33 0 35.33 37.66 9.84 o 0 34 0 2538.50 2674.55 42.56 o 2 34 0 5061.03 5068.32 54.84 o 4 34 0 3963.52 3977.31 41.56 o 6 34 0 1233.12 1384.84 20.57 o 8 34 0 2.75 9.31 6.85 o 10 34 0 2061.32 1996.62 28.07 o 12 34 0 3819.34 3923.51 43.07 o 14 34 0 2571.00 2615.73 33.28 o 16 34 0 1667.96 1720.23 27.87 o 1 35 0 225.93 208.79 10.30 o 3 35 0 2520.76 2524.23 34.02 o 5 35 0 4863.47 5239.06 55.29 o 7 35 0 1825.31 1637.76 25.59 o 9 35 0 2333.29 2793.86 36.46 o 11 35 0 1258.56 1165.53 22.53 o 13 35 0 868.74 770.69 17.71 o 15 35 0 675.15 797.98 19.51 o 0 36 0 79.66 152.61 12.39 o 2 36 0 30.13 0.51 6.75 o 4 36 0 188.08 207.37 10.88 o 6 36 0 275.49 293.69 13.24 o 8 36 0 98.47 131.88 10.37 o 10 36 0 5.17 18.47 8.78 o 12 36 0 15.13 23.08 9.74 o 1 37 0 30.91 46.04 8.13 o 3 37 0 879.03 788.50 20.37 o 5 37 0 2297.53 2372.38 32.87 o 7 37 0 2405.50 2055.32 32.11 o 9 37 0 2704.07 2857.37 56.36 o 11 37 0 3124.63 2961.48 44.62 o 0 38 0 2345.28 2220.14 52.21 o 2 38 0 2920.75 3085.01 47.37 o 4 38 0 1741.65 1716.84 31.97 o 6 38 0 398.28 337.86 16.33 o 8 38 0 18.22 24.87 9.11 o 10 38 0 264.31 336.69 15.75 o 1 39 0 0.74 21.51 9.92 o 3 39 0 42.35 26.07 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1961.18 2100.39 19.64 o 5 19 2 409.00 544.81 10.19 o 7 19 2 511.04 434.40 10.27 o 9 19 2 272.75 270.38 7.87 o 11 19 2 247.26 223.15 10.72 o 13 19 2 1048.30 643.55 15.11 o 15 19 2 1811.95 1811.90 22.39 o 17 19 2 470.67 373.71 10.86 o 19 19 2 151.96 138.43 8.83 o 21 19 2 81.46 114.07 9.43 o 23 19 2 249.41 275.64 13.21 o 25 19 2 645.87 730.43 23.39 o -26 20 2 39.99 63.32 10.60 o -24 20 2 719.49 606.94 18.69 o -22 20 2 1219.57 1209.79 23.01 o -20 20 2 1472.89 1326.47 25.10 o -18 20 2 209.44 225.53 11.57 o -16 20 2 820.56 768.97 15.47 o -14 20 2 950.92 982.99 15.30 o -12 20 2 1144.17 1116.22 13.95 o -10 20 2 7814.58 7706.30 63.09 o -8 20 2 16537.21 16983.60 122.90 o -6 20 2 9434.90 9838.34 76.14 o -4 20 2 10487.47 10422.89 83.16 o -2 20 2 15380.81 15963.95 112.36 o 0 20 2 12861.38 12829.71 85.95 o 2 20 2 8558.91 8438.32 62.22 o 4 20 2 351.75 289.47 9.05 o 6 20 2 7749.71 8532.53 65.57 o 8 20 2 12442.06 11880.38 89.42 o 10 20 2 25142.37 26243.80 219.26 o 12 20 2 12476.77 12852.61 113.90 o 14 20 2 3701.19 3513.65 44.00 o 16 20 2 2995.49 2762.30 33.98 o 18 20 2 787.51 780.41 19.28 o 20 20 2 117.94 156.99 10.92 o 22 20 2 149.82 106.23 12.80 o 24 20 2 217.51 318.67 14.81 o -25 21 2 48.63 66.33 11.20 o -23 21 2 331.92 259.10 15.54 o -21 21 2 360.21 465.43 17.51 o -19 21 2 4015.66 3573.41 42.88 o -17 21 2 9276.35 9995.73 91.12 o -15 21 2 7658.89 7192.74 54.88 o -13 21 2 5133.78 5601.88 45.20 o -11 21 2 11587.80 11595.49 87.55 o -9 21 2 8057.34 8732.79 69.40 o -7 21 2 3427.80 3058.63 28.10 o -5 21 2 299.43 191.21 5.97 o -3 21 2 4176.02 4722.27 40.38 o -1 21 2 10449.20 10227.22 70.35 o 1 21 2 44212.54 45271.85 2146.75 o 3 21 2 60322.35 59864.81 1676.21 o 5 21 2 20333.04 21496.53 159.72 o 7 21 2 8750.45 8815.13 73.74 o 9 21 2 6477.26 6337.51 57.67 o 11 21 2 5257.76 5163.52 50.24 o 13 21 2 1236.98 1372.73 23.15 o 15 21 2 4403.01 4198.40 49.96 o 17 21 2 5959.02 5880.11 68.88 o 19 21 2 4363.23 4491.18 51.75 o 21 21 2 3421.09 3550.41 48.79 o 23 21 2 2202.71 2176.30 36.06 o -24 22 2 1222.02 1243.81 26.90 o -22 22 2 2493.44 2348.23 35.69 o -20 22 2 1374.14 1367.12 24.60 o -18 22 2 383.33 378.77 13.26 o -16 22 2 2202.95 2063.35 21.76 o -14 22 2 1014.97 1066.74 14.22 o -12 22 2 2631.49 2631.55 27.43 o -10 22 2 11634.80 11828.24 89.09 o -8 22 2 11465.46 11727.10 87.51 o -6 22 2 7393.23 7040.00 59.20 o -4 22 2 6465.58 7095.36 59.27 o -2 22 2 2737.27 2302.39 23.71 o 0 22 2 225.53 350.72 7.45 o 2 22 2 1908.52 2398.71 22.22 o 4 22 2 634.94 454.97 9.83 o 6 22 2 1799.10 2034.84 22.73 o 8 22 2 9269.62 9390.06 81.57 o 10 22 2 6036.19 6131.51 55.08 o 12 22 2 5647.36 5466.60 53.68 o 14 22 2 8189.22 7877.05 73.16 o 16 22 2 2834.28 2686.20 33.34 o 18 22 2 1531.86 1477.02 26.43 o 20 22 2 409.90 447.16 17.92 o 22 22 2 6.84 6.44 10.62 o 24 22 2 32.21 8.44 10.76 o -25 23 2 49.65 80.42 12.52 o -23 23 2 212.32 161.47 12.07 o -21 23 2 342.81 450.36 16.21 o -19 23 2 2662.19 2191.63 29.38 o -17 23 2 2038.81 2211.89 25.44 o -15 23 2 1449.60 1313.38 16.26 o -13 23 2 0.19 6.45 4.49 o -11 23 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5481.29 5157.50 48.96 o 8 24 2 10312.86 11245.27 96.38 o 10 24 2 7667.31 7595.06 72.18 o 12 24 2 2084.52 2331.80 29.83 o 14 24 2 2613.38 2667.16 35.71 o 16 24 2 1205.78 1074.37 20.10 o 18 24 2 2018.52 2109.45 31.24 o 20 24 2 189.48 103.10 12.10 o 22 24 2 562.89 541.50 22.18 o -23 25 2 497.42 454.76 16.20 o -21 25 2 1523.00 1617.04 25.03 o -19 25 2 2566.27 2629.32 31.64 o -17 25 2 5900.59 5925.83 50.42 o -15 25 2 6889.64 7071.68 54.53 o -13 25 2 3167.98 3247.73 31.53 o -11 25 2 37.66 17.27 5.01 o -9 25 2 67.92 55.75 5.84 o -7 25 2 93.80 119.96 7.31 o -5 25 2 122.64 135.24 6.13 o -3 25 2 2450.06 2238.67 25.40 o -1 25 2 13503.81 13883.68 96.80 o 1 25 2 7393.88 7996.04 60.85 o 3 25 2 806.38 794.46 12.10 o 5 25 2 3305.65 3947.32 42.90 o 7 25 2 11152.62 10756.22 92.52 o 9 25 2 3126.82 3516.07 39.02 o 11 25 2 1140.03 864.75 15.32 o 13 25 2 3.47 4.76 6.03 o 15 25 2 1100.90 1230.17 21.46 o 17 25 2 204.89 171.81 12.62 o 19 25 2 208.40 245.51 13.14 o 21 25 2 271.92 209.22 15.42 o -22 26 2 825.35 915.19 21.61 o -20 26 2 22.87 26.23 7.86 o -18 26 2 499.96 484.82 11.99 o -16 26 2 993.03 873.78 14.14 o -14 26 2 575.20 631.39 16.68 o -12 26 2 502.07 521.27 11.85 o -10 26 2 274.57 338.50 10.31 o -8 26 2 1308.47 1519.41 20.13 o -6 26 2 1793.15 1545.64 18.84 o -4 26 2 2576.59 2871.92 32.57 o -2 26 2 36.71 81.43 5.94 o 0 26 2 3177.73 2873.15 29.61 o 2 26 2 989.66 1005.33 15.03 o 4 26 2 644.23 633.85 12.17 o 6 26 2 85.83 91.44 8.93 o 8 26 2 1908.64 1936.95 25.96 o 10 26 2 3194.68 3076.48 37.37 o 12 26 2 4279.89 4263.31 44.47 o 14 26 2 3501.20 3330.96 38.07 o 16 26 2 680.56 713.02 22.80 o 18 26 2 97.51 101.29 10.52 o 20 26 2 30.73 35.68 10.44 o -21 27 2 385.66 376.83 14.23 o -19 27 2 1736.25 1795.73 30.70 o -17 27 2 2095.91 2085.82 22.90 o -15 27 2 1789.88 1784.59 22.87 o -13 27 2 7.92 -4.17 5.01 o -11 27 2 233.80 288.18 10.97 o -9 27 2 1703.69 1739.72 23.91 o -7 27 2 1517.16 1505.08 19.03 o -5 27 2 775.79 727.24 12.85 o -3 27 2 657.32 641.03 12.39 o -1 27 2 1796.60 1591.82 19.45 o 1 27 2 6468.96 6022.19 53.25 o 3 27 2 4866.95 4961.20 46.96 o 5 27 2 618.66 426.74 14.29 o 7 27 2 374.68 571.74 14.13 o 9 27 2 306.59 460.54 12.82 o 11 27 2 111.79 77.66 8.48 o 13 27 2 437.85 466.93 13.47 o 15 27 2 471.39 438.64 14.22 o 17 27 2 471.23 460.22 16.82 o 19 27 2 194.89 162.43 13.99 o 21 27 2 3.67 20.93 11.98 o -20 28 2 3.46 1.02 7.29 o -18 28 2 337.45 321.88 11.22 o -16 28 2 270.07 324.14 11.80 o -14 28 2 471.97 407.64 11.67 o -12 28 2 188.77 176.78 8.76 o -10 28 2 682.57 689.13 14.95 o -8 28 2 5679.99 5628.35 51.78 o -6 28 2 5801.25 5506.01 62.21 o -4 28 2 2624.08 2711.52 29.30 o -2 28 2 857.64 835.76 14.30 o 0 28 2 1247.32 1211.31 18.79 o 2 28 2 296.11 354.05 10.20 o 4 28 2 15.69 30.57 6.03 o 6 28 2 942.20 805.24 15.87 o 8 28 2 953.24 931.53 17.49 o 10 28 2 2364.57 2316.86 28.89 o 12 28 2 3306.21 3014.76 35.00 o 14 28 2 1155.61 1074.58 22.26 o 16 28 2 21.97 12.57 7.82 o 18 28 2 88.22 79.39 11.21 o 20 28 2 211.08 167.15 15.09 o -21 29 2 293.00 298.30 13.71 o -19 29 2 2972.49 3139.87 39.91 o -17 29 2 3384.24 3281.91 36.58 o -15 29 2 2705.40 2861.15 34.25 o -13 29 2 3729.84 3505.12 35.83 o -11 29 2 5475.85 5090.60 46.88 o -9 29 2 781.57 822.26 14.73 o -7 29 2 70.73 65.19 6.59 o -5 29 2 357.67 452.70 11.75 o -3 29 2 897.52 725.47 13.32 o -1 29 2 2727.27 3006.70 34.04 o 1 29 2 3781.12 3217.35 34.67 o 3 29 2 5821.26 5881.44 53.20 o 5 29 2 5951.22 5997.80 57.04 o 7 29 2 1501.03 1300.69 20.44 o 9 29 2 437.64 537.10 14.22 o 11 29 2 9.93 12.57 6.37 o 13 29 2 51.10 43.20 8.30 o 15 29 2 14.02 -1.77 8.62 o 17 29 2 1447.51 1650.60 30.16 o 19 29 2 1909.70 1908.77 36.01 o -20 30 2 433.58 450.44 19.51 o -18 30 2 0.81 -2.26 7.38 o -16 30 2 796.37 811.04 17.84 o -14 30 2 1333.27 1284.37 22.36 o -12 30 2 4456.70 4384.50 43.79 o -10 30 2 5741.96 5486.51 58.59 o -8 30 2 10808.10 11134.00 101.92 o -6 30 2 2221.72 1907.09 25.35 o -4 30 2 2049.50 2279.09 26.82 o -2 30 2 509.66 545.57 12.21 o 0 30 2 355.47 262.53 9.57 o 2 30 2 766.82 728.95 16.06 o 4 30 2 543.11 625.41 14.48 o 6 30 2 191.28 181.50 9.37 o 8 30 2 147.82 188.62 10.15 o 10 30 2 1720.54 1718.55 24.62 o 12 30 2 1183.87 1249.77 21.02 o 14 30 2 1654.72 1617.65 28.84 o 16 30 2 1044.81 974.46 23.69 o 18 30 2 1411.74 1458.48 31.40 o -19 31 2 1133.85 1152.82 22.49 o -17 31 2 1402.05 1383.92 24.23 o -15 31 2 265.19 328.28 14.38 o -13 31 2 8.73 32.53 7.40 o -11 31 2 574.12 428.56 13.69 o -9 31 2 1285.57 1328.71 21.10 o -7 31 2 2496.62 2300.88 31.26 o -5 31 2 1186.81 1141.40 17.99 o -3 31 2 1736.14 1945.56 24.46 o -1 31 2 509.80 399.93 22.25 o 1 31 2 915.53 1005.78 17.30 o 3 31 2 38.36 69.43 6.44 o 5 31 2 75.08 48.64 6.80 o 7 31 2 51.35 102.77 10.38 o 9 31 2 4.49 29.51 6.86 o 11 31 2 19.40 4.20 6.48 o 13 31 2 281.08 326.84 15.06 o 15 31 2 241.38 236.45 14.22 o 17 31 2 349.55 365.01 18.58 o -18 32 2 34.54 21.95 8.23 o -16 32 2 265.63 276.89 12.33 o -14 32 2 5.26 -4.77 6.72 o -12 32 2 57.43 69.52 8.43 o -10 32 2 100.98 114.80 7.96 o -8 32 2 139.12 181.67 8.63 o -6 32 2 115.55 135.83 8.48 o -4 32 2 1652.11 1538.38 20.83 o -2 32 2 430.94 445.36 12.38 o 0 32 2 238.20 221.91 11.33 o 2 32 2 0.23 0.90 5.94 o 4 32 2 257.26 279.15 14.33 o 6 32 2 3.10 4.72 6.33 o 8 32 2 49.11 30.04 6.95 o 10 32 2 167.41 196.45 10.47 o 12 32 2 362.17 314.23 12.97 o 14 32 2 1011.84 869.01 22.81 o 16 32 2 379.08 379.04 18.80 o -17 33 2 1992.29 1906.88 29.38 o -15 33 2 1159.92 1253.84 23.48 o -13 33 2 424.35 360.40 13.60 o -11 33 2 1029.92 1109.90 20.01 o -9 33 2 52.77 42.91 6.72 o -7 33 2 3.22 16.70 6.68 o -5 33 2 711.18 583.20 20.02 o -3 33 2 1796.14 1844.30 22.60 o -1 33 2 1818.11 1900.23 28.24 o 1 33 2 220.42 212.88 10.98 o 3 33 2 178.32 285.27 12.56 o 5 33 2 972.67 919.14 17.86 o 7 33 2 1010.37 1026.01 19.60 o 9 33 2 776.81 645.42 16.73 o 11 33 2 614.39 625.12 18.16 o 13 33 2 202.31 199.75 11.42 o 15 33 2 4.35 -7.37 9.81 o -16 34 2 443.58 444.78 17.49 o -14 34 2 1409.30 1311.30 23.79 o -12 34 2 2166.99 2305.46 31.95 o -10 34 2 2921.37 2797.67 35.51 o -8 34 2 2525.91 2907.02 34.33 o -6 34 2 2124.79 1990.62 26.65 o -4 34 2 503.45 532.56 13.99 o -2 34 2 82.33 132.03 8.84 o 0 34 2 464.85 591.99 16.86 o 2 34 2 1163.86 883.39 21.45 o 4 34 2 64.13 118.40 9.53 o 6 34 2 46.09 36.96 7.48 o 8 34 2 199.50 228.75 11.06 o 10 34 2 233.86 284.06 13.10 o 12 34 2 973.01 962.98 20.98 o 14 34 2 1184.38 1127.00 28.81 o -13 35 2 408.87 581.50 17.34 o -11 35 2 503.94 518.75 16.17 o -9 35 2 191.71 234.11 12.79 o -7 35 2 304.79 307.75 13.33 o -5 35 2 106.35 131.80 9.11 o -3 35 2 761.84 797.46 18.43 o -1 35 2 2204.99 2137.08 32.13 o 1 35 2 4726.52 5161.21 59.12 o 3 35 2 2643.88 2520.15 33.40 o 5 35 2 178.25 224.49 12.22 o 7 35 2 5.89 -6.54 6.54 o 9 35 2 28.38 61.38 8.66 o 11 35 2 436.42 467.26 17.40 o 13 35 2 1092.00 1123.09 24.33 o -12 36 2 0.24 3.96 7.80 o -10 36 2 255.40 296.52 13.49 o -8 36 2 390.88 344.62 13.47 o -6 36 2 531.48 639.34 16.84 o -4 36 2 203.65 232.07 11.37 o -2 36 2 200.41 162.34 11.17 o 0 36 2 2500.62 2670.53 48.32 o 2 36 2 2366.58 2059.54 29.64 o 4 36 2 12.68 0.87 6.79 o 6 36 2 499.62 513.14 17.18 o 8 36 2 149.83 226.17 11.94 o 10 36 2 15.45 22.18 8.24 o -11 37 2 147.09 145.80 10.47 o -9 37 2 498.68 596.77 17.70 o -7 37 2 461.64 451.32 14.94 o -5 37 2 288.95 297.65 12.69 o -3 37 2 18.62 31.55 8.39 o -1 37 2 565.86 570.81 18.48 o 1 37 2 584.67 564.98 21.10 o 3 37 2 568.02 507.51 17.03 o 5 37 2 396.91 383.39 16.78 o 7 37 2 1188.30 1206.62 25.25 o 9 37 2 343.36 362.41 14.55 o -8 38 2 716.02 628.80 17.43 o -6 38 2 1505.93 1741.38 28.33 o -4 38 2 255.08 225.48 12.49 o -2 38 2 361.36 464.78 17.87 o 0 38 2 1056.81 893.06 21.57 o 2 38 2 397.63 398.90 18.85 o 4 38 2 124.36 179.57 14.87 o 6 38 2 503.56 505.76 18.25 o -5 39 2 900.42 911.46 24.58 o -3 39 2 1028.60 1071.19 24.04 o -1 39 2 69.98 59.37 9.10 o 1 39 2 20.81 28.34 10.35 o 3 39 2 30.18 34.89 9.45 o -29 1 3 757.69 773.43 34.76 o -27 1 3 201.11 187.11 14.61 o -25 1 3 1031.36 911.56 22.04 o -23 1 3 2741.96 2726.33 34.57 o -21 1 3 8244.86 7607.02 76.86 o -19 1 3 6196.56 6107.29 67.32 o -17 1 3 5227.67 5326.71 55.18 o -15 1 3 9237.97 8773.52 95.98 o -13 1 3 4812.17 4601.59 54.24 o -11 1 3 23.03 52.19 5.22 o -9 1 3 464.32 409.76 10.83 o -5 1 3 21686.64 19773.82 250.57 o -3 1 3 18085.68 19355.87 389.41 o 1 1 3 6875.54 6737.58 48.84 o 3 1 3 657.14 602.96 7.44 o 5 1 3 91.09 59.72 3.38 o 7 1 3 300.29 301.14 5.36 o 9 1 3 2725.22 2336.85 20.36 o 11 1 3 6484.79 7039.62 51.10 o 13 1 3 1945.92 1718.13 17.84 o 15 1 3 3721.81 3728.41 36.40 o 17 1 3 1939.37 1770.69 21.04 o 19 1 3 2585.63 2832.95 31.26 o 21 1 3 191.47 315.78 12.27 o 23 1 3 85.99 55.80 8.54 o 25 1 3 131.24 203.28 12.61 o 27 1 3 50.36 33.28 9.40 o -30 2 3 1493.34 1407.32 31.09 o -28 2 3 1045.62 1095.43 28.57 o -26 2 3 364.69 394.09 15.65 o -24 2 3 1866.77 1492.04 30.13 o -22 2 3 6497.84 6498.10 67.86 o -20 2 3 712.23 507.38 16.60 o -18 2 3 613.50 424.28 13.28 o -16 2 3 2646.86 2940.16 36.11 o -14 2 3 19281.39 17966.70 184.60 o -12 2 3 37032.20 36817.46 1033.27 o -2 2 3 1807.56 2428.49 21.43 o 0 2 3 16132.09 16803.00 339.63 o 2 2 3 13868.56 13915.14 178.33 o 4 2 3 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