Crystallography Open Database

Information card for entry 2312403

Preview

Coordinates	2312403.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Dichloridobis{(<i>S</i>)-(+)-1-(4-bromophenyl)-<i>N</i>-[(4-methoxyphenyl)methylidene]ethylamine-κ<i>N</i>}palladium(II)
Formula	C32 H32 Br2 Cl2 N2 O2 Pd
Calculated formula	C32 H32 Br2 Cl2 N2 O2 Pd
Title of publication	(<i>S</i>)-(+)-1-(4-Bromo-phen-yl)-<i>N</i>-[(4-methoxyphen-yl)methyl-idene]ethyl-amine and bis-{(<i>S</i>)-(+)-1-(4-bromo-phen-yl)-<i>N</i>-[(4-methoxyphen-yl)methyl-idene]ethyl-amine-κ<i>N</i>}di-chlorido-palladium(II).
Authors of publication	Anzaldo, Bertin; Moreno Morales, Gloria E.; Villamizar C, Claudia P; Mendoza, Ángel; Hernández Téllez, Guadalupe
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2024
Journal volume	80
Journal issue	Pt 2
Pages of publication	213 - 217
a	9.0493 ± 0.0004 Å
b	25.1365 ± 0.0008 Å
c	14.1725 ± 0.0007 Å
α	90°
β	90.185 ± 0.004°
γ	90°
Cell volume	3223.8 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0753
Residual factor for significantly intense reflections	0.0466
Weighted residual factors for significantly intense reflections	0.0937
Weighted residual factors for all reflections included in the refinement	0.1074
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
290314 (current)	2024-03-05	cif/ Adding structures of 2312402, 2312403 via cif-deposit CGI script.	2312403.cif