#------------------------------------------------------------------------------ #$Date: 2025-04-05 05:04:06 +0300 (Sat, 05 Apr 2025) $ #$Revision: 298755 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/28/2312805.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312805 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.7890 _cell_length_b 12.7890 _cell_length_c 6.8269 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.5988 _cod_data_source_file vp3040ch24_pk1508_1_rtsup4.hkl _cod_data_source_block ch24_pk1508_1_rt _shelx_title ' ch24_PK1508 in I4(1)/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 122.34 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 50.41 59.74 0.54 o 2 2 0 14968.25 13246.23 43.78 o -2 4 0 1404.27 1264.10 10.58 o 0 4 0 2422.99 2551.82 26.13 o 2 4 0 14134.71 12863.03 54.37 o 4 4 0 3505.84 3751.58 29.77 o -4 6 0 273.16 236.29 1.43 o -2 6 0 1194.14 1444.99 10.37 o 0 6 0 10957.97 11254.25 51.60 o 2 6 0 644.94 663.23 4.12 o 4 6 0 36.89 32.37 0.73 o 6 6 0 481.00 406.52 2.81 o -6 8 0 82.09 84.99 0.87 o -4 8 0 722.72 724.78 5.34 o -2 8 0 1960.49 2121.31 10.82 o 0 8 0 1183.20 1390.96 7.32 o 2 8 0 1789.74 1866.78 15.96 o 4 8 0 5526.70 6063.71 36.85 o 6 8 0 184.05 168.20 2.30 o 8 8 0 268.31 270.52 3.06 o -8 10 0 416.81 386.27 2.72 o -6 10 0 123.86 116.13 1.11 o -4 10 0 2417.98 2368.29 11.05 o -2 10 0 44.01 36.22 1.19 o 0 10 0 361.66 369.98 2.35 o 2 10 0 1787.99 1824.56 9.61 o 4 10 0 1140.82 1070.02 13.37 o 6 10 0 375.99 398.82 4.60 o 8 10 0 3.78 4.00 0.33 o 10 10 0 1037.35 1048.39 7.90 o -10 12 0 0.24 0.19 0.21 o -8 12 0 243.84 251.99 3.16 o -6 12 0 128.45 124.22 1.81 o -4 12 0 316.98 311.21 7.05 o -2 12 0 135.40 112.72 2.32 o 0 12 0 81.75 75.97 2.40 o 2 12 0 424.60 347.57 2.83 o 4 12 0 88.93 122.14 1.78 o 6 12 0 45.71 47.74 1.54 o 8 12 0 0.56 0.46 0.24 o 10 12 0 8.56 8.50 0.70 o 12 12 0 50.71 52.92 1.67 o -12 14 0 57.24 65.11 2.94 o -10 14 0 74.11 87.53 2.17 o -8 14 0 46.78 48.30 1.69 o -6 14 0 8.91 7.27 0.41 o -4 14 0 182.28 169.48 3.38 o -2 14 0 26.65 28.22 1.13 o 0 14 0 0.69 0.69 0.20 o 2 14 0 380.16 403.31 4.61 o 4 14 0 13.89 23.54 0.71 o 6 14 0 142.55 123.33 2.92 o 8 14 0 0.01 -0.10 0.29 o 10 14 0 16.70 16.54 0.82 o 12 14 0 91.93 95.00 4.16 o 14 14 0 113.21 109.86 4.12 o -10 16 0 3.08 1.64 0.55 o -8 16 0 7.15 6.24 0.96 o -6 16 0 56.16 58.45 1.81 o -4 16 0 5.63 7.06 0.70 o -2 16 0 235.01 251.18 4.83 o 0 16 0 0.04 1.67 0.34 o 2 16 0 87.50 91.95 1.79 o 4 16 0 8.22 7.87 0.58 o 6 16 0 0.44 0.32 0.33 o 8 16 0 18.84 20.02 0.92 o 10 16 0 32.67 34.70 2.07 o 12 16 0 7.45 7.84 0.86 o -8 18 0 6.92 8.01 1.11 o -6 18 0 223.72 228.39 17.95 o -4 18 0 69.89 66.82 2.00 o -2 18 0 2.37 2.88 0.43 o 0 18 0 246.38 267.53 16.83 o 2 18 0 1.36 0.60 0.91 o 4 18 0 77.11 74.15 2.35 o 6 18 0 8.13 5.81 0.76 o 8 18 0 62.30 63.00 4.22 o 10 18 0 9.15 8.13 0.88 o -6 20 0 60.07 52.04 4.60 o -4 20 0 19.76 16.85 1.65 o -2 20 0 27.55 31.22 1.78 o 0 20 0 36.82 35.48 1.71 o 2 20 0 9.93 8.39 0.90 o 4 20 0 8.88 9.81 0.98 o 0 1 1 3262.07 3011.70 12.54 o -1 2 1 5915.84 5650.02 40.59 o 1 2 1 1569.98 1604.78 11.04 o -2 3 1 4342.76 4387.83 15.94 o 0 3 1 6963.88 6685.28 22.21 o 2 3 1 500.52 549.93 3.07 o -3 4 1 2916.77 3195.49 13.98 o -1 4 1 2794.28 2926.92 13.96 o 1 4 1 33.65 68.28 1.03 o 3 4 1 515.97 535.37 3.20 o -4 5 1 2.07 0.97 0.27 o -2 5 1 567.92 619.32 1.92 o 0 5 1 1561.74 1570.52 5.93 o 2 5 1 844.41 896.10 6.03 o 4 5 1 748.02 730.41 3.09 o -5 6 1 167.75 230.73 1.11 o -3 6 1 279.28 304.09 1.83 o -1 6 1 244.42 225.37 1.42 o 1 6 1 774.85 781.62 4.98 o 3 6 1 1.05 1.28 0.27 o 5 6 1 1088.54 1231.06 5.46 o -6 7 1 980.94 986.43 3.73 o -4 7 1 182.52 178.42 1.38 o -2 7 1 1784.36 1811.33 7.05 o 0 7 1 3916.51 4441.70 43.38 o 2 7 1 470.17 412.94 2.06 o 4 7 1 3.72 0.52 0.12 o 6 7 1 345.08 333.60 2.46 o -7 8 1 19.26 23.09 0.36 o -5 8 1 33.18 31.96 0.38 o -3 8 1 300.93 333.16 2.62 o -1 8 1 76.26 82.01 1.48 o 1 8 1 2071.16 2341.19 9.06 o 3 8 1 7.21 5.06 0.21 o 5 8 1 19.28 23.00 0.33 o 7 8 1 2020.36 1987.83 7.46 o -8 9 1 477.65 500.19 3.66 o -6 9 1 265.66 283.20 1.40 o -4 9 1 39.46 42.99 0.53 o -2 9 1 407.30 441.87 2.56 o 0 9 1 61.92 47.26 0.53 o 2 9 1 285.04 252.02 1.75 o 4 9 1 162.86 205.48 2.47 o 6 9 1 0.69 0.02 0.13 o 8 9 1 494.23 466.44 4.08 o -9 10 1 11.88 10.94 0.46 o -7 10 1 471.54 480.87 3.37 o -5 10 1 52.25 52.83 0.55 o -3 10 1 1931.93 1887.87 13.84 o -1 10 1 8.04 6.11 0.32 o 1 10 1 23.63 31.86 0.47 o 3 10 1 1560.22 1561.28 9.62 o 5 10 1 1.10 2.65 0.27 o 7 10 1 18.54 18.99 0.36 o 9 10 1 486.97 487.46 5.58 o -10 11 1 40.66 41.34 0.66 o -8 11 1 121.68 115.84 1.27 o -6 11 1 198.53 172.20 1.23 o -4 11 1 291.52 268.80 2.94 o -2 11 1 29.79 32.19 0.47 o 0 11 1 421.07 415.94 3.98 o 2 11 1 1339.40 1405.09 8.94 o 4 11 1 94.59 80.21 1.33 o 6 11 1 62.18 58.00 0.68 o 8 11 1 300.19 277.09 3.72 o 10 11 1 78.87 82.52 1.12 o -11 12 1 13.97 16.56 0.57 o -9 12 1 1.68 1.57 0.17 o -7 12 1 119.93 124.41 1.55 o -5 12 1 71.07 78.27 0.93 o -3 12 1 191.21 179.15 1.95 o -1 12 1 1184.85 1128.17 14.31 o 1 12 1 54.27 60.76 1.02 o 3 12 1 10.56 12.01 0.32 o 5 12 1 34.05 30.47 0.46 o 7 12 1 49.12 59.80 0.83 o 9 12 1 122.04 128.26 1.32 o 11 12 1 3.88 2.91 0.34 o -12 13 1 0.40 0.07 0.26 o -10 13 1 0.02 -0.12 0.22 o -8 13 1 80.02 78.14 1.00 o -6 13 1 255.25 260.32 2.52 o -4 13 1 48.16 42.91 0.68 o -2 13 1 120.09 118.07 1.83 o 0 13 1 364.37 353.44 2.92 o 2 13 1 64.80 51.01 0.68 o 4 13 1 17.05 15.72 0.39 o 6 13 1 36.33 29.82 0.62 o 8 13 1 21.16 21.06 0.55 o 10 13 1 32.78 31.06 0.84 o 12 13 1 1.24 0.29 0.22 o -13 14 1 32.90 31.23 1.50 o -11 14 1 40.37 39.19 1.23 o -9 14 1 4.41 2.79 0.28 o -7 14 1 12.82 15.06 0.48 o -5 14 1 63.81 65.35 0.90 o -3 14 1 31.02 29.07 0.64 o -1 14 1 54.26 45.47 0.67 o 1 14 1 43.57 41.56 0.64 o 3 14 1 12.32 17.08 0.42 o 5 14 1 2.80 2.33 0.22 o 7 14 1 116.30 119.16 1.33 o 9 14 1 129.70 135.13 1.79 o 11 14 1 69.23 67.48 1.29 o 13 14 1 3.13 3.74 0.41 o -14 15 1 0.66 0.41 0.30 o -12 15 1 13.94 13.56 0.99 o -10 15 1 4.63 4.95 0.41 o -8 15 1 10.33 11.77 0.57 o -6 15 1 14.28 10.60 0.43 o -4 15 1 0.01 0.06 0.16 o -2 15 1 66.35 61.62 1.15 o 0 15 1 0.76 0.41 0.19 o 2 15 1 82.98 87.82 1.24 o 4 15 1 115.75 123.34 1.50 o 6 15 1 38.33 35.69 0.73 o 8 15 1 1.41 1.55 0.26 o 10 15 1 38.43 37.39 0.88 o 12 15 1 0.27 0.21 0.20 o 14 15 1 3.72 4.06 0.44 o -13 16 1 0.05 0.69 0.54 o -11 16 1 29.02 27.31 1.89 o -9 16 1 46.05 45.18 1.32 o -7 16 1 3.31 3.26 0.55 o -5 16 1 26.95 27.70 0.90 o -3 16 1 10.33 9.85 0.45 o -1 16 1 130.00 139.33 1.58 o 1 16 1 5.84 6.17 0.37 o 3 16 1 11.39 11.55 0.49 o 5 16 1 80.13 88.18 1.49 o 7 16 1 13.42 14.78 0.65 o 9 16 1 44.03 46.79 1.19 o 11 16 1 60.21 60.26 1.66 o 13 16 1 10.90 9.57 0.74 o -10 17 1 3.74 4.15 0.81 o -8 17 1 7.88 7.44 0.74 o -6 17 1 18.57 20.79 0.72 o -4 17 1 198.14 200.73 3.39 o -2 17 1 18.01 15.55 0.56 o 0 17 1 80.78 83.03 1.65 o 2 17 1 107.12 112.21 1.52 o 4 17 1 91.12 85.44 1.51 o 6 17 1 17.25 17.41 0.71 o 8 17 1 10.68 10.40 0.57 o 10 17 1 0.14 0.13 0.24 o 12 17 1 13.61 13.37 1.02 o -9 18 1 5.76 5.14 0.63 o -7 18 1 3.06 3.02 0.45 o -5 18 1 16.33 15.85 0.68 o -3 18 1 144.63 148.92 3.43 o -1 18 1 47.42 48.11 1.13 o 1 18 1 179.72 188.12 3.77 o 3 18 1 28.82 29.44 1.05 o 5 18 1 0.67 0.17 0.33 o 7 18 1 25.09 24.18 0.99 o 9 18 1 15.25 17.59 0.86 o 11 18 1 2.18 1.91 0.48 o -8 19 1 4.33 3.15 0.45 o -6 19 1 50.65 51.78 1.60 o -4 19 1 14.86 13.08 0.63 o -2 19 1 35.70 33.38 1.52 o 0 19 1 0.11 0.27 0.33 o 2 19 1 13.48 14.79 0.84 o 4 19 1 27.77 32.46 1.15 o 6 19 1 12.40 14.06 0.93 o 8 19 1 40.76 37.14 1.73 o -7 20 1 49.14 43.99 1.81 o -5 20 1 1.82 1.60 0.33 o -3 20 1 23.01 21.08 0.97 o -1 20 1 76.78 80.73 2.81 o 1 20 1 7.19 7.77 0.60 o 3 20 1 37.58 38.08 1.27 o 5 20 1 3.20 2.30 0.76 o -2 21 1 31.52 29.37 2.19 o 0 21 1 0.49 0.09 0.47 o 1 1 2 2208.54 2097.77 8.75 o 0 2 2 9379.21 8896.14 53.27 o 2 2 2 6505.07 6409.69 25.23 o -1 3 2 243.08 193.38 1.28 o 1 3 2 1240.67 1145.97 5.10 o 3 3 2 2972.82 2987.64 13.22 o -2 4 2 505.18 511.54 3.63 o 0 4 2 743.02 768.38 3.57 o 2 4 2 7217.14 7466.89 44.76 o 4 4 2 30.76 29.65 0.32 o -3 5 2 1006.17 1208.87 10.71 o -1 5 2 475.51 551.38 2.10 o 1 5 2 55.00 47.70 0.69 o 3 5 2 87.22 88.23 0.91 o 5 5 2 0.77 1.99 0.24 o -4 6 2 1308.23 1344.35 8.67 o -2 6 2 198.34 201.59 1.89 o 0 6 2 5.41 5.73 0.24 o 2 6 2 7329.64 7502.85 50.28 o 4 6 2 152.96 153.88 1.69 o 6 6 2 527.37 535.10 3.34 o -5 7 2 563.58 513.68 4.45 o -3 7 2 0.24 0.88 0.30 o -1 7 2 2393.90 2461.65 10.66 o 1 7 2 66.03 141.32 1.13 o 3 7 2 0.04 2.57 0.23 o 5 7 2 0.95 2.08 0.16 o 7 7 2 452.48 425.52 2.99 o -6 8 2 1424.43 1441.60 11.57 o -4 8 2 1021.44 961.94 8.47 o -2 8 2 325.84 340.19 2.25 o 0 8 2 1468.26 1445.52 19.14 o 2 8 2 584.43 557.62 2.73 o 4 8 2 3.78 0.74 0.11 o 6 8 2 130.09 136.96 1.14 o 8 8 2 10.52 10.20 0.27 o -7 9 2 248.59 250.58 1.92 o -5 9 2 91.28 97.59 0.87 o -3 9 2 677.54 684.55 4.66 o -1 9 2 178.56 153.08 2.37 o 1 9 2 98.69 103.55 1.10 o 3 9 2 11.78 9.07 0.32 o 5 9 2 20.99 20.73 0.44 o 7 9 2 488.39 497.72 3.43 o 9 9 2 15.81 18.96 0.43 o -8 10 2 202.02 199.75 1.79 o -6 10 2 156.34 151.99 1.19 o -4 10 2 141.22 156.72 1.62 o -2 10 2 1028.34 966.18 7.61 o 0 10 2 561.05 601.37 4.70 o 2 10 2 217.09 195.76 1.73 o 4 10 2 622.81 589.36 4.35 o 6 10 2 1.26 2.51 0.21 o 8 10 2 189.40 168.21 1.51 o 10 10 2 83.60 88.59 0.98 o -9 11 2 180.47 180.36 1.58 o -7 11 2 0.78 1.13 0.18 o -5 11 2 0.07 0.45 0.11 o -3 11 2 357.23 308.38 3.10 o -1 11 2 145.57 133.94 1.32 o 1 11 2 428.05 435.10 3.67 o 3 11 2 176.14 167.16 1.92 o 5 11 2 316.63 300.69 2.80 o 7 11 2 1.49 0.79 0.17 o 9 11 2 577.85 582.66 4.96 o 11 11 2 18.22 20.42 0.55 o -10 12 2 12.42 13.28 0.43 o -8 12 2 499.68 515.42 5.62 o -6 12 2 83.81 84.23 1.01 o -4 12 2 1.90 0.52 0.13 o -2 12 2 20.43 28.32 0.54 o 0 12 2 3.69 7.29 0.31 o 2 12 2 108.62 105.83 1.22 o 4 12 2 169.16 146.90 1.51 o 6 12 2 141.37 142.29 1.75 o 8 12 2 6.04 6.12 0.32 o 10 12 2 27.25 24.19 0.58 o 12 12 2 62.79 64.31 1.12 o -11 13 2 65.31 64.02 1.23 o -9 13 2 41.58 41.32 0.84 o -7 13 2 3.75 4.52 0.27 o -5 13 2 32.17 31.25 0.58 o -3 13 2 27.93 28.21 0.72 o -1 13 2 354.51 320.52 4.57 o 1 13 2 4.28 7.51 0.28 o 3 13 2 104.77 93.77 1.13 o 5 13 2 5.48 5.44 0.30 o 7 13 2 242.92 244.41 2.39 o 9 13 2 27.86 27.33 0.72 o 11 13 2 87.27 89.14 1.63 o 13 13 2 0.57 0.22 0.33 o -12 14 2 68.82 72.52 1.82 o -10 14 2 1.78 1.78 0.27 o -8 14 2 46.17 46.30 0.90 o -6 14 2 12.71 12.60 0.47 o -4 14 2 0.10 0.02 0.18 o -2 14 2 25.93 28.47 0.62 o 0 14 2 5.26 4.99 0.26 o 2 14 2 9.16 10.45 0.45 o 4 14 2 0.41 0.41 0.24 o 6 14 2 106.83 118.80 1.51 o 8 14 2 4.21 5.29 0.36 o 10 14 2 21.91 22.48 0.76 o 12 14 2 106.01 107.86 1.70 o 14 14 2 0.09 -0.14 0.30 o -13 15 2 22.05 20.94 1.30 o -11 15 2 6.38 6.23 0.56 o -9 15 2 98.45 98.82 1.76 o -7 15 2 1.20 1.70 0.26 o -5 15 2 18.11 19.72 0.55 o -3 15 2 8.60 6.03 0.33 o -1 15 2 199.45 198.62 2.52 o 1 15 2 28.86 28.90 0.73 o 3 15 2 9.76 10.16 0.53 o 5 15 2 0.08 -0.11 0.23 o 7 15 2 37.57 38.65 0.89 o 9 15 2 69.01 73.26 1.39 o 11 15 2 22.99 20.79 0.76 o 13 15 2 6.53 5.65 0.60 o -12 16 2 1.55 1.12 0.57 o -10 16 2 1.75 2.73 0.49 o -8 16 2 58.90 56.66 1.32 o -6 16 2 17.62 18.14 0.59 o -4 16 2 22.90 21.97 0.66 o -2 16 2 110.88 115.11 1.74 o 0 16 2 21.44 27.44 0.74 o 2 16 2 1.60 1.09 0.26 o 4 16 2 80.51 84.78 1.33 o 6 16 2 7.67 7.36 0.43 o 8 16 2 21.66 21.69 0.79 o 10 16 2 3.85 3.13 0.36 o 12 16 2 30.02 26.72 1.24 o -9 17 2 2.85 3.79 0.82 o -7 17 2 60.94 62.62 1.66 o -5 17 2 24.89 25.01 0.90 o -3 17 2 94.84 91.66 1.43 o -1 17 2 7.68 7.09 0.50 o 1 17 2 76.10 73.59 1.26 o 3 17 2 0.04 -0.20 0.24 o 5 17 2 2.68 2.90 0.32 o 7 17 2 26.29 26.96 0.96 o 9 17 2 11.07 11.42 0.61 o 11 17 2 25.17 25.05 1.13 o -10 18 2 0.34 0.14 0.47 o -8 18 2 58.77 61.97 1.71 o -6 18 2 6.38 5.37 0.56 o -4 18 2 30.85 27.21 0.87 o -2 18 2 0.50 -0.10 0.29 o 0 18 2 0.09 0.29 0.28 o 2 18 2 8.70 7.60 0.46 o 4 18 2 59.44 62.73 1.36 o 6 18 2 4.93 4.70 0.43 o 8 18 2 12.25 13.30 0.67 o 10 18 2 19.32 19.88 1.24 o -9 19 2 45.28 40.54 2.50 o -7 19 2 4.85 4.94 0.55 o -5 19 2 6.65 5.24 0.58 o -3 19 2 0.02 0.04 0.25 o -1 19 2 21.15 21.48 0.81 o 1 19 2 32.14 34.50 1.09 o 3 19 2 0.82 0.71 0.33 o 5 19 2 19.69 20.34 0.93 o 7 19 2 4.36 3.83 0.47 o -6 20 2 24.64 22.91 1.34 o -4 20 2 13.96 14.47 1.44 o -2 20 2 8.73 8.51 0.55 o 0 20 2 8.22 8.13 0.62 o 2 20 2 0.10 0.48 0.32 o 4 20 2 3.39 4.28 1.02 o 0 1 3 4635.75 4621.99 15.67 o -1 2 3 761.60 734.06 2.71 o 1 2 3 3462.83 3650.43 18.99 o -2 3 3 377.56 420.96 1.86 o 0 3 3 50.77 56.14 0.57 o 2 3 3 2537.78 2474.59 8.18 o -3 4 3 2.14 5.93 0.14 o -1 4 3 361.07 356.12 2.86 o 1 4 3 1472.44 1366.25 7.05 o 3 4 3 1.00 4.44 0.22 o -4 5 3 1020.21 1067.37 8.76 o -2 5 3 7.46 3.52 0.16 o 0 5 3 3986.97 4151.25 21.93 o 2 5 3 356.93 328.99 5.02 o 4 5 3 452.73 449.06 3.20 o -5 6 3 1028.36 957.97 6.27 o -3 6 3 1.04 2.55 0.20 o -1 6 3 228.84 257.02 1.88 o 1 6 3 20.54 27.82 1.03 o 3 6 3 0.62 1.70 0.23 o 5 6 3 152.10 158.44 1.86 o -6 7 3 61.23 61.98 1.31 o -4 7 3 45.72 50.48 1.14 o -2 7 3 69.82 67.49 0.82 o 0 7 3 9.05 7.63 0.27 o 2 7 3 74.15 76.39 1.06 o 4 7 3 0.40 0.14 0.22 o 6 7 3 74.35 76.58 0.77 o -7 8 3 9.20 3.29 0.19 o -5 8 3 162.66 166.11 1.84 o -3 8 3 40.39 46.96 0.83 o -1 8 3 1876.84 1865.57 7.57 o 1 8 3 332.70 310.75 3.74 o 3 8 3 1320.37 1340.40 8.98 o 5 8 3 226.68 203.14 2.06 o 7 8 3 2.01 0.75 0.12 o -8 9 3 420.01 387.80 3.49 o -6 9 3 5.45 5.52 0.24 o -4 9 3 356.22 339.02 2.29 o -2 9 3 190.58 192.37 1.54 o 0 9 3 127.71 112.37 2.91 o 2 9 3 920.26 927.74 7.74 o 4 9 3 0.41 2.05 0.24 o 6 9 3 341.82 350.97 2.46 o 8 9 3 0.01 -0.20 0.20 o -9 10 3 35.77 33.12 0.61 o -7 10 3 42.30 44.22 0.64 o -5 10 3 406.78 393.89 2.20 o -3 10 3 66.95 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