#------------------------------------------------------------------------------ #$Date: 2025-06-26 05:25:19 +0300 (Thu, 26 Jun 2025) $ #$Revision: 300208 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/28/2312871.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312871 _cell_angle_alpha 89.773 _cell_angle_beta 84.559 _cell_angle_gamma 86.205 _cell_length_a 11.5267 _cell_length_b 12.4802 _cell_length_c 16.7877 _exptl_crystal_F_000 1076.00 _reflns_d_resolution_high 0.7357 _cod_data_source_file dg3074Rubqsup3.hkl _cod_data_source_block Rubq _shelx_title ' AK_Ru_bq in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.14 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1386.57 1349.49 20.18 o 3 0 0 5417.78 5574.30 72.62 o 4 0 0 2796.10 2841.08 58.22 o 5 0 0 661.18 611.90 35.88 o 6 0 0 150.42 164.03 22.78 o 7 0 0 8162.67 8218.08 256.54 o 8 0 0 1517.30 1597.00 79.03 o 9 0 0 254.02 238.25 32.55 o 10 0 0 305.12 285.13 36.46 o 11 0 0 206.82 175.72 30.59 o 12 0 0 11.12 24.72 18.87 o 13 0 0 41.90 63.11 29.28 o 14 0 0 56.74 15.61 24.72 o -14 1 0 255.74 283.11 45.56 o -13 1 0 45.72 62.46 25.37 o -12 1 0 62.20 54.65 21.47 o -11 1 0 175.70 227.12 36.44 o -10 1 0 1595.58 1530.11 86.17 o -9 1 0 1177.57 1319.06 75.02 o -8 1 0 31.81 24.07 16.92 o -7 1 0 4299.59 4684.64 162.72 o -6 1 0 4705.78 4532.03 152.68 o -5 1 0 591.56 654.07 37.82 o -4 1 0 5191.52 5387.15 139.27 o -3 1 0 11.83 10.34 3.03 o -2 1 0 3640.35 3597.25 61.26 o 2 1 0 6273.10 6248.92 78.65 o 3 1 0 2180.21 2173.75 35.79 o 4 1 0 4.88 6.72 4.41 o 5 1 0 954.77 874.15 30.58 o 6 1 0 6567.74 6592.47 145.32 o 7 1 0 32.04 17.93 10.55 o 8 1 0 1515.63 1449.88 51.24 o 9 1 0 862.40 874.18 58.02 o 10 1 0 10.31 13.01 19.52 o 11 1 0 15.86 14.31 19.52 o 12 1 0 0.44 -16.91 22.12 o 13 1 0 547.97 571.73 59.26 o 14 1 0 817.25 637.09 66.45 o -14 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286.89 218.69 38.40 o 4 14 0 130.09 100.86 27.98 o 5 14 0 291.18 259.05 39.70 o 6 14 0 381.62 395.13 48.82 o 7 14 0 11.74 3.90 17.57 o 8 14 0 22.98 23.42 18.87 o 9 14 0 96.00 93.04 30.58 o -3 15 0 430.43 341.78 50.13 o -2 15 0 131.82 203.67 42.30 o -1 15 0 278.90 233.00 43.61 o 0 15 0 92.87 46.20 23.42 o 1 15 0 0.54 3.90 16.26 o 2 15 0 2.55 -1.95 19.52 o 3 15 0 108.75 96.95 31.23 o 4 15 0 445.63 441.39 53.38 o 5 15 0 19.51 -14.96 24.07 o 6 15 0 53.75 54.00 24.07 o 7 15 0 7.57 21.47 15.61 o -6 -15 1 3.82 5.20 19.52 o -5 -15 1 188.38 124.29 32.54 o -4 -15 1 254.60 263.58 41.00 o -3 -15 1 116.61 75.48 29.28 o -2 -15 1 485.65 436.87 54.69 o -1 -15 1 260.49 186.79 37.10 o 0 -15 1 78.46 31.88 24.72 o 1 -15 1 137.00 121.68 35.14 o 2 -15 1 3.62 -6.51 22.12 o 3 -15 1 382.63 257.13 42.96 o -8 -14 1 30.02 10.41 22.12 o -7 -14 1 67.41 83.28 25.37 o -6 -14 1 204.24 197.18 35.79 o -5 -14 1 38.59 53.35 24.72 o -4 -14 1 1425.69 1377.95 92.60 o -3 -14 1 450.31 471.37 53.39 o -2 -14 1 18.66 27.32 23.42 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