#------------------------------------------------------------------------------ #$Date: 2023-04-11 18:56:26 +0300 (Tue, 11 Apr 2023) $ #$Revision: 282569 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/00/03/3000355.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3000355 _diffrn_ambient_pressure 100 _diffrn_ambient_temperature 90 _diffrn_radiation_polarisn_ratio 0.9900 _diffrn_radiation_probe x-ray _diffrn_radiation_wavelength 0.39360 _pd_meas_2theta_range_inc 0.00960 _pd_meas_2theta_range_max 27.49040 _pd_meas_2theta_range_min 3.50000 _pd_proc_2theta_range_inc 0.00960 _pd_proc_2theta_range_max 27.49410 _pd_proc_2theta_range_min 3.50370 _pd_proc_ls_background_function ; Background function: "chebyschev-1" function with 8 terms: 178508.629, 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107575.278 0.000007683249 131154.669 125168.013 107564.369 0.000007624586 132833.956 124458.136 107553.415 0.000007528196 135171.861 124775.435 107542.415 0.000007397989 137467.603 126635.154 107531.368 0.000007274441 142750.983 131010.837 107520.274 0.000007005206 150577.003 139316.632 107509.131 0.00000664112 161458.983 153150.028 107497.938 0.000006193523 183975.755 173687.91 107486.695 0.000005435499 209551.912 200780.52 107475.401 0.000004772087 248144.547 232131.734 107464.056 0.000004029909 278867.639 262818.772 107452.657 0.000003585931 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 1 1 0 2006.3354 1877.1972 -0.0 3.22887 100.00 1 0 1 999.5376 994.8089 -0.0 2.44163 56.84 2 0 0 371.3650 343.3843 -0.0 2.28315 9.26 1 1 1 352.6820 373.3452 180.0 2.15315 15.61 2 1 0 94.9214 105.2494 0.0 2.04211 3.79 2 1 1 1402.9309 1256.6086 -0.0 1.66765 74.70 2 2 0 1928.2257 1746.7259 -0.0 1.61443 24.09 0 0 2 1939.6941 1732.0186 -0.0 1.44469 9.67 3 1 0 746.8136 667.1681 -0.0 1.44399 14.95 2 2 1 29.4774 13.2644 180.0 1.40935 0.56 3 0 1 1301.1330 1282.4962 -0.0 1.34667 22.65 1 1 2 705.8991 746.4547 -0.0 1.31871 11.75 3 1 1 35.1989 49.4461 0.0 1.29167 1.13 3 2 0 21.3356 14.6508 180.0 1.26647 0.33 2 0 2 208.1377 252.7524 -0.0 1.22081 2.98 2 1 2 25.4040 25.2234 0.0 1.17939 0.68 3 2 1 303.7221 296.8308 -0.0 1.15993 7.86 4 0 0 891.7389 715.7213 -0.0 1.14158 5.60 4 1 0 110.8408 59.4855 180.0 1.10749 1.31 2 2 2 766.5712 751.2074 -0.0 1.07658 8.55 3 3 0 701.3047 684.8889 -0.0 1.07629 3.92 4 1 1 367.7527 377.0521 -0.0 1.03413 7.59 3 1 2 337.1049 338.4037 -0.0 1.02130 6.77 4 2 0 297.7121 297.7047 -0.0 1.02106 3.00 3 3 1 19.9476 11.2032 180.0 1.00859 0.20 4 2 1 10.8694 12.3464 -0.0 0.96271 0.19 3 2 2 13.5142 6.3135 180.0 0.95234 0.24 1 0 3 226.4257 259.5891 -0.0 0.94239 1.94 1 1 3 39.9699 39.0268 180.0 0.92294 0.33 4 3 0 2.6258 15.9067 0.0 0.91326 0.02 4 0 2 388.6489 383.4698 -0.0 0.89569 3.02 5 1 0 350.5621 347.3740 -0.0 0.89553 2.72 4 1 2 46.9666 30.2858 180.0 0.87894 0.70 2 1 3 309.5655 311.9633 -0.0 0.87110 4.54 4 3 1 322.0476 329.7586 -0.0 0.87080 4.73 5 0 1 97.9954 100.3417 -0.0 0.87080 0.72 3 3 2 427.8308 378.7014 -0.0 0.86310 3.09 5 1 1 1.2059 0.7753 180.0 0.85538 0.02 5 2 0 0.6003 0.2374 0.0 0.84794 0.00 4 2 2 155.6355 171.4427 -0.0 0.83382 2.10