#------------------------------------------------------------------------------ #$Date: 2019-12-17 23:28:31 +0200 (Tue, 17 Dec 2019) $ #$Revision: 245263 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/00/3500080.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500080 _publ_author_name 'Thierry Maris' _chemical_formula_sum 'C12 H28 N Br' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.2048 _cell_length_b 8.2048 _cell_length_c 10.7389 _exptl_crystal_F_000 284.00 _reflns_d_resolution_high 0.8084 _cod_data_source_file c3nbr.fcf _cod_data_source_block c3nbr _shelx_title ' C3NBr in I-4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 97.61 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' 'y, -x, -z' '-y, x, -z' '-x, -y, z' 'x+1/2, y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' '-x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 326.48 364.00 6.11 o 0 2 0 351.95 396.49 6.35 o 2 2 0 7678.28 7345.35 128.56 o -1 3 0 1745.89 1789.92 27.71 o 1 3 0 4035.09 4202.82 60.34 o 3 3 0 1370.79 1412.76 27.35 o -2 4 0 1314.70 1227.14 24.01 o 0 4 0 1935.62 1995.68 29.49 o 2 4 0 1715.74 1744.14 33.69 o 4 4 0 1236.77 1225.62 26.11 o -3 5 0 945.98 920.49 19.99 o -1 5 0 1938.98 2015.70 35.53 o 1 5 0 1146.31 1173.08 20.87 o 3 5 0 374.65 366.58 9.50 o 5 5 0 123.64 121.99 4.33 o -4 6 0 1341.70 1342.44 29.44 o -2 6 0 733.12 708.58 12.65 o 0 6 0 569.73 544.18 13.99 o 2 6 0 1395.66 1294.09 22.15 o 4 6 0 1761.94 1852.00 40.83 o 6 6 0 279.46 289.44 7.99 o -5 7 0 547.76 573.86 13.66 o -3 7 0 89.26 88.39 4.12 o -1 7 0 801.08 756.12 17.45 o 1 7 0 269.06 246.44 7.06 o 3 7 0 489.53 491.88 16.53 o 5 7 0 50.39 52.70 2.86 o 7 7 0 151.90 138.04 4.31 o -6 8 0 103.66 103.02 4.35 o -4 8 0 193.28 188.44 6.82 o -2 8 0 530.54 549.31 22.71 o 0 8 0 986.68 949.51 22.64 o 2 8 0 258.92 274.86 10.10 o 4 8 0 247.32 268.64 8.42 o 6 8 0 247.22 234.92 7.55 o -3 9 0 354.84 357.12 11.73 o -1 9 0 1.22 1.96 1.15 o 1 9 0 351.25 361.88 13.75 o 3 9 0 102.31 111.93 4.68 o 1 0 1 3901.31 3831.00 78.31 o 3 0 1 2930.75 3177.33 54.01 o 5 0 1 1514.32 1443.79 27.40 o 7 0 1 575.77 560.02 12.78 o 9 0 1 295.54 317.01 10.85 o -8 1 1 222.99 227.31 7.73 o -6 1 1 1062.96 985.46 21.69 o -4 1 1 2112.26 2177.36 38.28 o -2 1 1 6120.90 5722.03 118.62 o 0 1 1 4298.33 3862.91 66.26 o 2 1 1 5146.40 5183.72 83.65 o 4 1 1 1224.58 1246.67 22.75 o 6 1 1 832.86 786.26 17.30 o 8 1 1 390.60 409.27 10.38 o -9 2 1 340.77 364.80 11.38 o -7 2 1 1009.82 1005.75 22.91 o -5 2 1 1369.51 1409.97 28.92 o -3 2 1 791.49 828.77 18.26 o -1 2 1 5204.73 5219.05 80.79 o 1 2 1 5728.47 5639.22 86.78 o 3 2 1 3440.86 3738.95 64.67 o 5 2 1 879.62 864.84 18.52 o 7 2 1 611.63 605.92 17.63 o 9 2 1 247.30 239.09 7.04 o -8 3 1 363.25 376.44 11.33 o -6 3 1 460.14 430.70 7.60 o -4 3 1 2109.59 2208.88 44.61 o -2 3 1 3363.62 3611.60 62.47 o 0 3 1 2901.38 3174.68 42.56 o 2 3 1 990.90 1031.65 16.53 o 4 3 1 1602.56 1671.68 31.21 o 6 3 1 981.85 915.41 14.30 o 8 3 1 402.61 398.43 10.18 o -9 4 1 117.04 118.48 4.58 o -7 4 1 348.18 359.67 8.44 o -5 4 1 1566.92 1554.63 25.73 o -3 4 1 1648.98 1711.56 35.06 o -1 4 1 1237.85 1233.11 20.01 o 1 4 1 2172.74 2256.95 33.57 o 3 4 1 2016.87 2123.16 47.97 o 5 4 1 738.46 722.35 12.67 o 7 4 1 208.63 205.57 5.58 o 9 4 1 142.57 138.55 5.26 o -8 5 1 263.01 268.55 7.14 o -6 5 1 611.10 612.88 14.22 o -4 5 1 812.86 778.77 11.22 o -2 5 1 847.95 831.47 15.63 o 0 5 1 1532.91 1505.06 27.99 o 2 5 1 1288.31 1343.14 31.02 o 4 5 1 1747.01 1719.00 24.73 o 6 5 1 354.65 379.38 8.79 o 8 5 1 296.86 285.51 10.24 o -7 6 1 275.42 288.57 7.58 o -5 6 1 362.56 366.74 9.22 o -3 6 1 952.30 880.73 15.45 o -1 6 1 834.85 817.63 18.22 o 1 6 1 1069.31 1010.64 26.06 o 3 6 1 382.25 353.01 7.92 o 5 6 1 593.16 611.24 13.84 o 7 6 1 209.35 205.54 5.45 o -6 7 1 221.90 225.86 5.88 o -4 7 1 208.17 210.01 6.93 o -2 7 1 634.91 614.96 18.09 o 0 7 1 557.16 567.70 17.29 o 2 7 1 1101.07 1044.15 26.89 o 4 7 1 320.82 327.44 9.91 o 6 7 1 308.17 299.47 7.02 o -5 8 1 291.78 280.90 7.69 o -3 8 1 388.12 408.64 12.47 o -1 8 1 369.94 381.19 15.44 o 1 8 1 199.30 198.15 7.16 o 3 8 1 365.21 375.32 10.27 o 5 8 1 247.28 245.56 7.08 o -4 9 1 136.43 138.78 12.03 o -2 9 1 286.67 275.80 18.69 o 0 9 1 320.42 347.57 14.52 o 2 9 1 322.79 335.36 11.04 o 4 9 1 123.26 119.22 6.67 o 0 0 2 345.69 292.93 7.19 o 2 0 2 5535.27 5814.31 113.34 o 4 0 2 1442.13 1482.17 26.38 o 6 0 2 1044.08 1007.29 22.37 o 8 0 2 230.38 228.16 7.77 o -9 1 2 159.15 170.63 5.93 o -7 1 2 1233.13 1191.74 28.13 o -5 1 2 867.87 846.06 17.03 o -3 1 2 3562.86 3866.35 69.20 o -1 1 2 9025.57 7956.75 183.44 o 1 1 2 9527.43 7937.67 155.15 o 3 1 2 2223.51 2295.67 41.08 o 5 1 2 1498.22 1514.64 39.60 o 7 1 2 389.42 377.43 10.93 o 9 1 2 676.64 683.32 18.65 o -8 2 2 263.15 277.19 9.19 o -6 2 2 412.72 398.45 7.24 o -4 2 2 1692.83 1687.12 33.09 o -2 2 2 1283.47 1286.45 18.53 o 0 2 2 5652.47 5649.86 82.37 o 2 2 2 1034.96 1085.97 23.28 o 4 2 2 1844.48 1915.27 37.99 o 6 2 2 672.29 641.69 11.21 o 8 2 2 264.62 276.82 7.57 o -9 3 2 266.14 282.46 8.08 o -7 3 2 478.96 494.14 11.49 o -5 3 2 1841.23 1833.52 34.85 o -3 3 2 2001.34 2072.86 40.47 o -1 3 2 2184.60 2271.03 34.35 o 1 3 2 3682.93 3949.11 62.91 o 3 3 2 2049.70 2141.58 40.69 o 5 3 2 958.56 947.87 22.23 o 7 3 2 925.29 887.55 21.21 o 9 3 2 130.83 130.15 4.70 o -8 4 2 264.32 280.30 7.91 o -6 4 2 226.08 220.14 6.17 o -4 4 2 486.12 448.25 9.44 o -2 4 2 1926.28 1961.36 32.25 o 0 4 2 1282.31 1287.11 19.25 o 2 4 2 1714.31 1730.03 31.18 o 4 4 2 467.98 441.02 11.47 o 6 4 2 431.25 442.81 9.59 o 8 4 2 252.27 252.33 6.95 o -7 5 2 450.08 485.51 11.23 o -5 5 2 1112.66 1147.97 23.70 o -3 5 2 934.31 923.69 17.79 o -1 5 2 1499.54 1488.96 28.32 o 1 5 2 875.12 840.27 17.06 o 3 5 2 1882.72 1898.34 42.38 o 5 5 2 1050.24 1076.94 23.21 o 7 5 2 212.62 209.35 5.47 o -8 6 2 135.44 132.97 5.12 o -6 6 2 292.14 291.74 8.15 o -4 6 2 375.30 373.69 10.46 o -2 6 2 649.06 591.95 11.13 o 0 6 2 1083.83 1006.52 21.05 o 2 6 2 429.79 411.51 8.40 o 4 6 2 219.60 223.95 6.67 o 6 6 2 289.10 295.19 7.00 o 8 6 2 102.82 102.90 7.71 o -7 7 2 200.61 184.19 5.29 o -5 7 2 215.34 214.46 7.19 o -3 7 2 971.88 957.04 22.63 o -1 7 2 411.01 408.31 18.13 o 1 7 2 1163.55 1115.23 46.21 o 3 7 2 460.35 454.70 12.76 o 5 7 2 475.43 492.19 11.68 o 7 7 2 215.74 192.18 6.32 o -6 8 2 94.69 79.28 5.01 o -4 8 2 262.59 272.68 8.36 o -2 8 2 227.22 255.42 13.55 o 0 8 2 261.42 260.60 12.67 o 2 8 2 272.87 275.79 8.56 o 4 8 2 284.03 277.36 7.39 o 6 8 2 104.01 99.64 5.73 o -3 9 2 134.63 135.59 7.06 o -1 9 2 657.23 716.16 34.25 o 1 9 2 169.85 166.98 7.02 o 3 9 2 253.28 261.14 9.97 o 1 0 3 4948.67 5102.69 77.20 o 3 0 3 2126.14 2261.49 38.71 o 5 0 3 1078.87 1052.16 21.94 o 7 0 3 456.40 455.36 12.96 o 9 0 3 168.92 187.97 6.92 o -8 1 3 792.57 863.34 23.09 o -6 1 3 655.62 615.39 10.80 o -4 1 3 1425.59 1425.10 30.48 o -2 1 3 939.89 903.03 13.50 o 0 1 3 4787.22 4943.93 93.73 o 2 1 3 1918.42 1963.28 32.19 o 4 1 3 2078.99 2136.40 39.73 o 6 1 3 908.21 863.21 14.78 o 8 1 3 370.06 362.32 10.49 o -9 2 3 96.81 98.97 3.97 o -7 2 3 188.08 207.18 6.81 o -5 2 3 829.36 792.89 18.73 o -3 2 3 6468.67 7156.69 120.19 o -1 2 3 1902.25 1934.29 30.74 o 1 2 3 873.20 856.12 13.90 o 3 2 3 1723.74 1785.74 30.15 o 5 2 3 1312.35 1310.20 30.59 o 7 2 3 567.22 574.66 17.20 o 9 2 3 231.40 228.17 7.50 o -8 3 3 219.14 231.02 7.01 o -6 3 3 1446.85 1449.27 27.53 o -4 3 3 285.56 272.22 6.59 o -2 3 3 1514.10 1533.37 25.96 o 0 3 3 2205.42 2295.50 36.85 o 2 3 3 6246.49 6971.64 126.21 o 4 3 3 1134.00 1111.49 23.60 o 6 3 3 350.10 335.10 7.84 o 8 3 3 143.17 161.42 5.83 o -9 4 3 218.69 212.89 7.86 o -7 4 3 405.82 415.38 9.45 o -5 4 3 761.24 782.35 15.66 o -3 4 3 1075.02 1060.95 22.16 o -1 4 3 2205.37 2223.57 37.86 o 1 4 3 1495.81 1492.38 26.79 o 3 4 3 286.34 273.70 6.99 o 5 4 3 1070.46 1015.19 21.07 o 7 4 3 668.90 674.03 14.42 o 9 4 3 168.93 142.40 10.89 o -8 5 3 104.17 104.55 3.16 o -6 5 3 173.39 181.66 5.25 o -4 5 3 1044.44 972.19 21.04 o -2 5 3 1329.47 1289.84 28.10 o 0 5 3 1013.60 992.37 23.51 o 2 5 3 832.75 781.38 16.32 o 4 5 3 704.23 721.67 14.95 o 6 5 3 432.22 434.57 10.30 o 8 5 3 91.75 85.52 3.20 o -7 6 3 275.86 275.42 6.72 o -5 6 3 409.05 408.46 10.62 o -3 6 3 424.96 388.35 10.27 o -1 6 3 871.04 831.42 19.67 o 1 6 3 693.39 645.02 15.50 o 3 6 3 1462.81 1386.63 29.89 o 5 6 3 192.54 191.17 5.69 o 7 6 3 209.30 204.29 5.22 o -6 7 3 217.04 214.09 5.71 o -4 7 3 646.23 625.49 14.95 o -2 7 3 549.63 554.59 25.16 o 0 7 3 449.53 434.38 20.86 o 2 7 3 166.98 163.86 7.36 o 4 7 3 412.63 417.40 10.37 o 6 7 3 253.91 240.97 5.92 o -5 8 3 109.93 105.31 3.57 o -3 8 3 132.24 137.56 8.29 o -1 8 3 399.61 405.52 17.69 o 1 8 3 806.52 861.83 28.50 o 3 8 3 217.66 214.99 9.39 o 5 8 3 111.36 109.70 3.49 o -4 9 3 169.58 142.19 10.53 o -2 9 3 226.78 252.81 10.90 o 0 9 3 153.00 165.30 9.07 o 2 9 3 96.72 98.95 7.38 o 4 9 3 201.49 202.52 12.91 o 0 0 4 1195.52 1221.93 29.75 o 2 0 4 1642.91 1665.19 27.24 o 4 0 4 3325.58 3496.46 66.51 o 6 0 4 1053.00 1016.28 19.30 o 8 0 4 248.17 270.68 8.27 o -9 1 4 220.72 233.27 7.07 o -7 1 4 196.76 197.02 6.67 o -5 1 4 1502.32 1457.55 32.62 o -3 1 4 211.46 188.41 3.66 o -1 1 4 3073.15 3327.46 55.97 o 1 1 4 2950.96 3274.34 53.02 o 3 1 4 1906.74 1925.63 37.53 o 5 1 4 58.62 57.99 2.39 o 7 1 4 601.24 645.35 15.60 o 9 1 4 137.56 141.09 5.21 o -8 2 4 577.12 624.81 16.57 o -6 2 4 814.13 802.52 16.42 o -4 2 4 862.99 858.38 20.88 o -2 2 4 4465.76 4899.65 81.91 o 0 2 4 1652.67 1696.16 28.69 o 2 2 4 4626.33 5174.17 90.17 o 4 2 4 1013.51 1048.70 22.06 o 6 2 4 1077.81 1033.84 20.53 o 8 2 4 394.50 396.32 10.91 o -9 3 4 79.19 84.29 3.12 o -7 3 4 345.98 362.32 9.07 o -5 3 4 489.39 444.75 7.60 o -3 3 4 1074.56 1050.36 19.47 o -1 3 4 1917.40 1975.62 37.22 o 1 3 4 175.54 153.31 4.12 o 3 3 4 983.83 979.74 20.38 o 5 3 4 794.14 758.80 11.92 o 7 3 4 299.57 303.42 7.45 o 9 3 4 126.54 128.90 5.19 o -8 4 4 174.93 178.98 5.02 o -6 4 4 245.09 246.71 6.53 o -4 4 4 1567.04 1547.81 23.02 o -2 4 4 1004.92 1010.78 18.70 o 0 4 4 3343.31 3483.40 72.12 o 2 4 4 916.02 938.98 19.48 o 4 4 4 1575.16 1551.68 22.71 o 6 4 4 348.26 344.20 8.38 o 8 4 4 247.20 243.60 6.82 o -7 5 4 371.32 377.47 8.72 o -5 5 4 459.90 489.01 11.75 o -3 5 4 770.98 746.93 12.37 o -1 5 4 71.08 62.42 2.56 o 1 5 4 1477.93 1397.55 33.01 o 3 5 4 485.75 448.81 8.87 o 5 5 4 473.67 500.08 11.65 o 7 5 4 157.53 166.36 4.64 o -6 6 4 256.31 264.01 7.21 o -4 6 4 390.86 373.21 11.38 o -2 6 4 1087.19 1055.52 24.68 o 0 6 4 1050.01 996.87 20.43 o 2 6 4 775.46 741.01 18.60 o 4 6 4 252.72 256.84 7.10 o 6 6 4 262.52 274.23 6.75 o -5 7 4 152.93 156.67 5.77 o -3 7 4 263.03 254.75 9.12 o -1 7 4 592.85 684.97 28.30 o 1 7 4 243.91 248.63 12.45 o 3 7 4 362.85 361.49 10.60 o 5 7 4 351.74 346.28 10.27 o -4 8 4 249.25 237.75 7.16 o -2 8 4 425.13 434.29 26.19 o 0 8 4 211.92 228.36 12.46 o 2 8 4 564.44 559.66 17.69 o 4 8 4 173.41 174.72 7.52 o -3 9 4 126.82 131.41 6.21 o -1 9 4 141.19 148.64 7.54 o 1 9 4 227.21 213.01 10.56 o 3 9 4 81.80 81.71 4.77 o 1 0 5 2254.50 2270.49 44.05 o 3 0 5 1138.15 1153.20 24.22 o 5 0 5 854.77 810.85 14.20 o 7 0 5 670.03 706.66 18.53 o 9 0 5 198.04 197.95 6.05 o -8 1 5 158.72 180.17 6.04 o -6 1 5 548.16 550.86 13.65 o -4 1 5 1042.88 1041.81 23.16 o -2 1 5 2782.20 3018.53 57.89 o 0 1 5 2251.34 2306.83 38.97 o 2 1 5 754.90 730.55 13.03 o 4 1 5 2171.89 2100.77 40.24 o 6 1 5 502.42 508.58 13.00 o 8 1 5 287.83 288.04 8.60 o -9 2 5 107.82 111.81 3.87 o -7 2 5 495.12 501.20 12.36 o -5 2 5 753.12 738.01 11.82 o -3 2 5 1312.73 1246.45 25.68 o -1 2 5 756.57 715.25 14.40 o 1 2 5 2850.24 3125.27 55.26 o 3 2 5 1381.41 1434.92 29.34 o 5 2 5 1111.54 1040.00 15.74 o 7 2 5 103.59 114.42 3.99 o 9 2 5 196.44 193.17 6.83 o -8 3 5 186.60 192.19 5.84 o -6 3 5 378.51 399.62 9.33 o -4 3 5 1445.68 1379.90 22.25 o -2 3 5 1546.56 1556.22 30.87 o 0 3 5 1133.82 1156.94 20.28 o 2 3 5 1393.94 1392.10 26.27 o 4 3 5 555.35 559.25 10.33 o 6 3 5 847.99 868.21 16.88 o 8 3 5 281.28 272.58 7.54 o -7 4 5 268.78 269.10 5.95 o -5 4 5 437.92 406.45 9.95 o -3 4 5 585.83 579.28 10.31 o -1 4 5 2004.14 2003.47 47.56 o 1 4 5 959.88 965.58 21.66 o 3 4 5 1488.76 1439.06 22.27 o 5 4 5 233.95 248.77 6.83 o 7 4 5 333.08 331.84 8.57 o -6 5 5 400.80 432.06 10.94 o -4 5 5 224.76 234.66 7.92 o -2 5 5 1147.92 1032.57 17.16 o 0 5 5 964.24 914.70 16.54 o 2 5 5 758.48 747.68 14.05 o 4 5 5 424.88 397.97 10.98 o 6 5 5 408.88 423.92 10.64 o -7 6 5 73.54 65.37 2.67 o -5 6 5 431.91 444.92 12.67 o -3 6 5 778.90 775.12 20.00 o -1 6 5 506.72 503.18 13.98 o 1 6 5 500.58 493.91 14.34 o 3 6 5 391.25 420.14 11.94 o 5 6 5 404.19 437.50 13.74 o 7 6 5 116.75 110.22 4.66 o -6 7 5 114.78 115.22 4.22 o -4 7 5 358.00 339.49 8.23 o -2 7 5 117.86 126.66 5.35 o 0 7 5 683.12 716.49 40.11 o 2 7 5 499.88 478.45 15.38 o 4 7 5 258.47 263.49 8.03 o 6 7 5 88.33 80.03 3.09 o -3 8 5 296.73 274.56 14.56 o -1 8 5 275.47 293.96 13.52 o 1 8 5 152.47 179.83 9.85 o 3 8 5 184.52 190.54 7.76 o -2 9 5 181.95 179.14 8.29 o 0 9 5 199.96 199.26 9.38 o 2 9 5 114.90 121.34 9.22 o 0 0 6 1382.11 1526.51 37.48 o 2 0 6 2086.76 2059.78 42.09 o 4 0 6 247.15 239.59 9.39 o 6 0 6 301.49 305.62 8.58 o 8 0 6 269.50 264.27 11.08 o -9 1 6 112.80 113.33 5.80 o -7 1 6 604.53 626.29 15.28 o -5 1 6 825.60 800.56 18.20 o -3 1 6 2041.39 2159.87 47.33 o -1 1 6 1049.91 1012.22 19.94 o 1 1 6 1025.00 1021.06 20.32 o 3 1 6 1692.99 1740.09 39.79 o 5 1 6 1989.85 1966.98 47.42 o 7 1 6 301.32 327.64 9.53 o 9 1 6 110.89 113.44 8.43 o -8 2 6 96.58 98.43 3.62 o -6 2 6 410.33 407.31 9.29 o -4 2 6 882.59 840.36 13.07 o -2 2 6 442.08 435.57 10.02 o 0 2 6 2042.11 2032.42 37.14 o 2 2 6 443.00 444.43 11.34 o 4 2 6 708.43 660.34 10.93 o 6 2 6 159.00 159.31 5.21 o 8 2 6 233.52 233.90 7.55 o -7 3 6 206.47 207.65 5.16 o -5 3 6 429.40 408.32 9.70 o -3 3 6 1038.79 1000.60 15.84 o -1 3 6 1739.61 1733.68 35.73 o 1 3 6 1987.63 2113.44 48.33 o 3 3 6 1097.80 1065.51 17.29 o 5 3 6 603.27 584.67 12.80 o 7 3 6 412.11 410.51 9.96 o -8 4 6 133.75 132.71 8.57 o -6 4 6 454.74 493.93 11.18 o -4 4 6 542.08 559.57 14.88 o -2 4 6 648.94 597.42 10.45 o 0 4 6 338.91 314.48 7.54 o 2 4 6 845.89 804.87 13.93 o 4 4 6 535.31 542.62 13.25 o 6 4 6 297.52 310.70 7.71 o 8 4 6 90.68 91.88 4.46 o -7 5 6 126.45 116.71 3.65 o -5 5 6 256.42 265.33 8.08 o -3 5 6 648.49 642.31 15.62 o -1 5 6 1962.81 1946.98 43.11 o 1 5 6 842.53 816.05 21.35 o 3 5 6 399.91 390.00 10.06 o 5 5 6 281.37 298.52 8.80 o 7 5 6 209.66 200.37 5.52 o -6 6 6 213.73 216.86 6.58 o -4 6 6 294.52 314.53 9.74 o -2 6 6 187.61 185.06 5.24 o 0 6 6 251.64 256.54 8.78 o 2 6 6 434.75 433.86 12.32 o 4 6 6 457.64 485.32 13.55 o 6 6 6 206.43 208.43 6.34 o -5 7 6 207.12 197.45 6.05 o -3 7 6 406.37 393.34 10.39 o -1 7 6 292.88 307.89 8.70 o 1 7 6 620.81 625.09 18.78 o 3 7 6 201.67 208.57 7.61 o 5 7 6 130.48 123.97 4.09 o -4 8 6 88.42 80.91 6.98 o -2 8 6 228.14 228.27 11.79 o 0 8 6 284.78 300.38 12.89 o 2 8 6 90.55 96.35 4.71 o 4 8 6 123.79 129.24 8.00 o -1 9 6 122.20 116.57 7.20 o 1 0 7 980.80 994.65 21.41 o 3 0 7 754.06 732.42 15.66 o 5 0 7 1116.20 1106.68 27.13 o 7 0 7 201.64 207.87 6.21 o -8 1 7 113.52 113.64 4.00 o -6 1 7 271.22 270.24 8.15 o -4 1 7 1141.79 1112.81 20.66 o -2 1 7 993.49 962.84 24.82 o 0 1 7 995.03 989.14 19.83 o 2 1 7 1432.85 1449.52 31.08 o 4 1 7 484.73 471.04 11.03 o 6 1 7 512.05 519.74 14.68 o 8 1 7 138.14 140.45 4.56 o -7 2 7 423.98 449.11 13.10 o -5 2 7 470.57 471.99 10.51 o -3 2 7 276.86 254.75 5.08 o -1 2 7 1425.58 1431.75 30.04 o 1 2 7 1039.37 998.59 21.83 o 3 2 7 1473.22 1435.59 22.39 o 5 2 7 214.07 216.68 6.34 o 7 2 7 419.41 427.20 10.94 o -8 3 7 88.91 83.56 5.01 o -6 3 7 257.09 241.69 6.71 o -4 3 7 522.16 504.83 11.65 o -2 3 7 1457.91 1373.05 21.01 o 0 3 7 716.07 681.18 14.70 o 2 3 7 239.54 228.04 4.92 o 4 3 7 632.51 651.94 14.69 o 6 3 7 452.52 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