#------------------------------------------------------------------------------ #$Date: 2019-12-17 23:28:44 +0200 (Tue, 17 Dec 2019) $ #$Revision: 245264 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/00/3500081.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500081 _publ_author_name 'Thierry Maris' _chemical_formula_sum 'C16 H36 N Br' _cell_angle_alpha 90.000 _cell_angle_beta 110.348 _cell_angle_gamma 90.000 _cell_length_a 13.9825 _cell_length_b 13.8659 _cell_length_c 20.0516 _exptl_crystal_F_000 1392.00 _reflns_d_resolution_high 0.8073 _cod_data_source_file c4nbr.fcf _cod_data_source_block c4nbr _shelx_title ' C4NBr in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 526.21 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 126.56 95.66 3.93 o 4 0 0 9064.38 9340.61 185.77 o 6 0 0 35136.47 36283.75 1250.68 o 8 0 0 19133.80 20608.77 451.13 o 10 0 0 9098.12 9137.47 145.98 o 12 0 0 6972.66 7488.74 151.57 o 14 0 0 855.33 961.83 21.25 o 16 0 0 190.05 161.65 4.93 o 1 1 0 27.74 -0.82 0.82 o 3 1 0 11528.62 11138.22 156.90 o 5 1 0 690.02 595.20 9.07 o 7 1 0 9415.57 10118.51 157.63 o 9 1 0 6649.59 6760.97 126.26 o 11 1 0 5029.92 5065.55 73.01 o 13 1 0 5505.55 5804.26 83.38 o 15 1 0 2669.35 2689.30 38.86 o 0 2 0 1579.31 1001.46 28.37 o 2 2 0 55625.96 38195.90 823.92 o 4 2 0 38793.68 32475.49 475.76 o 6 2 0 37201.81 37181.79 544.32 o 8 2 0 18055.95 19387.48 300.50 o 10 2 0 3388.08 3144.01 36.58 o 12 2 0 72.80 93.18 3.11 o 14 2 0 2587.83 2696.97 39.28 o 16 2 0 361.76 349.34 11.13 o 1 3 0 1975.85 1825.82 23.71 o 3 3 0 2320.42 2175.81 32.37 o 5 3 0 8517.10 8924.67 120.93 o 7 3 0 6696.59 6160.02 91.84 o 9 3 0 7042.84 7408.60 138.00 o 11 3 0 9768.28 10178.82 144.86 o 13 3 0 3323.90 3494.70 70.45 o 15 3 0 2135.95 2098.20 32.69 o 0 4 0 180035.38 111450.74 8327.37 o 2 4 0 58597.21 45070.69 796.84 o 4 4 0 9358.81 8921.44 116.37 o 6 4 0 10499.16 10559.10 149.50 o 8 4 0 25205.58 27734.03 429.24 o 10 4 0 3252.87 2984.82 39.34 o 12 4 0 8571.29 8898.19 136.00 o 14 4 0 546.65 570.35 9.92 o 1 5 0 140.33 112.28 2.53 o 3 5 0 2837.25 2695.79 33.43 o 5 5 0 233.31 184.45 4.76 o 7 5 0 9197.96 9415.43 159.21 o 9 5 0 4353.19 4061.35 59.09 o 11 5 0 745.99 760.31 15.81 o 13 5 0 8950.40 9297.91 169.84 o 15 5 0 1727.07 1621.83 33.53 o 0 6 0 45768.55 43463.46 2006.21 o 2 6 0 26473.34 27563.15 393.48 o 4 6 0 18907.64 19944.49 239.80 o 6 6 0 48265.56 54258.29 859.24 o 8 6 0 8734.36 8286.56 133.50 o 10 6 0 3142.70 2847.77 52.83 o 12 6 0 529.41 583.64 15.84 o 14 6 0 2129.69 2142.05 50.11 o 1 7 0 222.78 256.72 4.95 o 3 7 0 36.18 19.77 1.59 o 5 7 0 6620.95 6464.22 104.41 o 7 7 0 6183.06 5963.14 109.26 o 9 7 0 3738.09 3543.04 89.68 o 11 7 0 5847.78 5845.07 155.80 o 13 7 0 2502.22 2575.54 61.29 o 0 8 0 28312.44 33799.25 870.72 o 2 8 0 19393.28 21552.86 328.53 o 4 8 0 16272.31 16883.35 285.40 o 6 8 0 8186.48 7546.07 138.12 o 8 8 0 4476.95 4089.78 83.80 o 10 8 0 4292.26 4347.07 104.26 o 12 8 0 4654.34 4784.54 138.57 o 14 8 0 94.86 94.11 4.28 o 1 9 0 738.74 712.81 15.64 o 3 9 0 7.17 24.40 7.69 o 5 9 0 5495.34 5224.21 102.24 o 7 9 0 2004.27 1761.01 30.43 o 9 9 0 2454.38 2392.49 58.82 o 11 9 0 2838.62 2821.95 104.13 o 13 9 0 1956.94 1816.33 53.40 o 0 10 0 17531.99 18254.43 569.52 o 2 10 0 19419.55 21771.37 404.97 o 4 10 0 9040.00 9041.63 115.00 o 6 10 0 25065.58 26375.34 425.05 o 8 10 0 4653.11 4548.31 109.25 o 10 10 0 2406.10 2359.02 57.49 o 12 10 0 528.48 533.03 16.94 o 1 11 0 14.46 17.59 2.02 o 3 11 0 245.92 264.12 5.80 o 5 11 0 1834.97 1748.00 30.51 o 7 11 0 4968.80 4927.84 89.52 o 9 11 0 1760.09 1726.82 42.70 o 11 11 0 317.25 261.26 10.91 o 0 12 0 13159.74 14852.34 293.95 o 2 12 0 8950.72 9427.85 125.64 o 4 12 0 7814.75 7978.68 120.21 o 6 12 0 2850.72 2917.90 48.95 o 8 12 0 4642.82 4415.66 84.41 o 10 12 0 441.07 410.46 14.08 o 1 13 0 245.14 267.17 5.78 o 3 13 0 281.24 296.24 6.97 o 5 13 0 1016.27 953.55 17.88 o 7 13 0 1949.77 1951.53 36.27 o 9 13 0 734.46 722.28 23.24 o 0 14 0 3263.32 3496.51 71.29 o 2 14 0 11028.87 12075.11 179.37 o 4 14 0 4020.54 4340.71 70.81 o 6 14 0 6360.10 6589.33 116.44 o 8 14 0 2842.39 2657.33 95.13 o 1 15 0 19.84 26.98 1.57 o 3 15 0 146.58 154.17 4.05 o 5 15 0 1204.67 1246.75 23.29 o 7 15 0 613.72 527.93 20.61 o 0 16 0 17276.40 18750.02 367.06 o 2 16 0 708.11 718.85 13.93 o 4 16 0 2778.92 2614.76 46.72 o 1 17 0 13.76 13.61 1.32 o -15 1 1 0.39 3.37 0.74 o -13 1 1 1462.51 1607.12 24.40 o -11 1 1 67.46 50.01 2.07 o -9 1 1 140.40 115.44 3.41 o -7 1 1 226.99 301.96 8.23 o -5 1 1 269.88 220.53 3.98 o -3 1 1 6211.85 6207.56 81.31 o -1 1 1 2.36 -0.74 0.74 o 1 1 1 39.17 -0.63 0.63 o 3 1 1 36101.44 28415.19 451.18 o 5 1 1 5233.29 5641.02 79.83 o 7 1 1 20.30 25.09 1.44 o 9 1 1 81.02 108.46 4.10 o 11 1 1 491.31 492.35 8.70 o 13 1 1 883.20 891.80 14.20 o 15 1 1 122.98 119.75 2.70 o -16 2 1 0.44 0.76 0.58 o -14 2 1 114.52 108.22 2.85 o -12 2 1 295.62 255.69 5.26 o -10 2 1 170.53 141.17 2.92 o -8 2 1 250.36 209.90 4.70 o -6 2 1 33.28 8.05 1.23 o -4 2 1 1755.16 1735.63 23.31 o -2 2 1 0.00 -0.50 0.50 o 0 2 1 16.59 1.19 0.45 o 2 2 1 235.12 170.34 4.02 o 4 2 1 4577.02 4858.27 66.18 o 6 2 1 1227.95 1365.57 20.14 o 8 2 1 55.88 48.67 2.55 o 10 2 1 34.66 24.48 1.34 o 12 2 1 91.80 88.90 2.73 o 14 2 1 36.07 36.65 1.63 o -15 3 1 162.22 141.03 3.24 o -13 3 1 362.38 362.66 7.16 o -11 3 1 27.19 42.96 2.15 o -9 3 1 350.92 332.19 6.93 o -7 3 1 44.99 61.61 2.14 o -5 3 1 6.51 -0.77 0.77 o -3 3 1 3.22 -0.59 0.59 o -1 3 1 4939.64 4748.72 57.71 o 1 3 1 27908.85 23644.81 330.31 o 3 3 1 6.94 5.72 1.01 o 5 3 1 260.20 226.27 3.88 o 7 3 1 452.03 441.09 7.85 o 9 3 1 0.34 5.18 1.54 o 11 3 1 3.53 10.74 1.26 o 13 3 1 1.61 2.72 0.90 o 15 3 1 1.04 1.78 0.68 o -16 4 1 191.28 160.34 8.98 o -14 4 1 659.39 647.10 11.90 o -12 4 1 40.11 30.36 1.81 o -10 4 1 22.31 34.24 1.79 o -8 4 1 783.91 827.93 15.27 o -6 4 1 242.25 256.33 4.62 o -4 4 1 74.31 52.95 1.54 o -2 4 1 4643.91 4733.43 55.95 o 0 4 1 333.71 317.36 5.35 o 2 4 1 137.68 111.71 2.52 o 4 4 1 247.87 233.87 4.00 o 6 4 1 6943.72 7436.81 100.90 o 8 4 1 4.54 6.71 1.32 o 10 4 1 6.30 2.27 0.94 o 12 4 1 5.72 4.30 1.02 o 14 4 1 676.86 671.44 14.72 o -15 5 1 187.26 174.70 4.64 o -13 5 1 241.19 255.05 7.05 o -11 5 1 1296.94 1254.99 24.71 o -9 5 1 49.01 32.32 1.70 o -7 5 1 1021.92 924.56 17.06 o -5 5 1 199.45 185.33 4.08 o -3 5 1 0.06 -0.54 0.54 o -1 5 1 3.07 -0.84 0.84 o 1 5 1 1238.35 1218.39 15.37 o 3 5 1 5.93 6.62 0.71 o 5 5 1 66.78 56.30 1.87 o 7 5 1 348.40 302.66 6.27 o 9 5 1 1654.99 1477.27 21.45 o 11 5 1 441.94 465.45 10.33 o 13 5 1 12.91 12.48 1.35 o 15 5 1 173.55 158.64 4.93 o -14 6 1 24.97 27.00 1.65 o -12 6 1 22.65 24.56 2.03 o -10 6 1 15.92 11.72 1.58 o -8 6 1 7.25 7.96 1.76 o -6 6 1 243.70 218.51 4.88 o -4 6 1 924.15 876.47 13.75 o -2 6 1 338.33 271.59 5.41 o 0 6 1 3.78 -0.72 0.72 o 2 6 1 409.60 394.17 5.94 o 4 6 1 8404.55 9051.05 112.72 o 6 6 1 2.30 2.61 0.97 o 8 6 1 50.14 25.31 2.02 o 10 6 1 72.07 65.70 2.73 o 12 6 1 275.05 246.26 7.13 o 14 6 1 157.90 154.74 4.62 o -15 7 1 30.23 25.85 2.00 o -13 7 1 390.86 421.36 12.60 o -11 7 1 35.86 33.59 2.64 o -9 7 1 90.45 97.64 3.37 o -7 7 1 114.00 114.82 3.75 o -5 7 1 2600.91 2417.97 40.03 o -3 7 1 183.46 183.45 4.11 o -1 7 1 62.58 53.32 2.05 o 1 7 1 36.04 61.31 2.17 o 3 7 1 37.54 52.13 1.90 o 5 7 1 869.52 872.57 15.55 o 7 7 1 124.63 117.44 4.46 o 9 7 1 8.04 23.27 9.10 o 11 7 1 0.45 3.69 1.80 o 13 7 1 20.76 18.61 1.77 o -14 8 1 44.26 48.47 3.07 o -12 8 1 33.72 34.63 2.25 o -10 8 1 0.70 1.37 1.06 o -8 8 1 64.51 56.87 2.25 o -6 8 1 403.99 343.98 7.81 o -4 8 1 479.03 464.91 8.62 o -2 8 1 96.49 174.06 4.34 o 0 8 1 2.65 -0.92 1.17 o 2 8 1 80.35 108.02 3.89 o 4 8 1 621.73 743.58 14.46 o 6 8 1 779.05 709.15 12.87 o 8 8 1 22.65 23.78 2.60 o 10 8 1 15.74 18.49 2.73 o 12 8 1 49.38 34.80 3.54 o 14 8 1 0.83 5.76 1.92 o -13 9 1 596.59 558.72 17.87 o -11 9 1 321.18 306.08 12.52 o -9 9 1 7.31 8.22 1.61 o -7 9 1 32.93 30.92 1.87 o -5 9 1 1022.66 939.47 17.07 o -3 9 1 42.23 54.76 2.75 o -1 9 1 11.70 24.17 2.09 o 1 9 1 4.68 10.46 1.54 o 3 9 1 402.67 416.39 10.21 o 5 9 1 64.02 44.13 2.26 o 7 9 1 4.82 2.16 1.64 o 9 9 1 0.08 2.00 1.64 o 11 9 1 5.44 4.98 1.57 o 13 9 1 37.35 29.90 2.46 o -12 10 1 10.02 16.36 2.24 o -10 10 1 59.69 56.63 2.94 o -8 10 1 15.76 18.35 2.02 o -6 10 1 1045.53 865.37 14.99 o -4 10 1 440.21 402.72 6.52 o -2 10 1 54.16 34.93 2.65 o 0 10 1 1.84 3.95 1.40 o 2 10 1 1.17 3.01 1.03 o 4 10 1 4.97 25.08 1.70 o 6 10 1 285.86 285.49 6.73 o 8 10 1 120.75 135.98 8.96 o 10 10 1 14.92 18.67 3.04 o 12 10 1 10.83 4.48 2.56 o -11 11 1 63.79 56.35 2.91 o -9 11 1 516.83 475.03 11.60 o -7 11 1 1768.63 1689.46 32.42 o -5 11 1 246.09 237.06 6.59 o -3 11 1 97.39 104.87 2.94 o -1 11 1 47.34 50.94 1.91 o 1 11 1 290.39 244.37 4.19 o 3 11 1 1.14 3.18 1.19 o 5 11 1 0.74 1.89 1.22 o 7 11 1 356.64 345.44 10.75 o 9 11 1 48.63 51.59 4.28 o 11 11 1 9.94 8.17 1.81 o -10 12 1 33.29 25.61 2.71 o -8 12 1 41.31 47.55 2.46 o -6 12 1 221.18 231.30 6.93 o -4 12 1 31.88 32.81 2.36 o -2 12 1 918.59 925.99 16.08 o 0 12 1 0.15 1.88 1.20 o 2 12 1 46.89 49.98 2.38 o 4 12 1 27.72 41.79 2.37 o 6 12 1 39.74 30.38 2.07 o 8 12 1 50.32 60.31 4.28 o 10 12 1 65.14 85.47 4.53 o -9 13 1 847.91 800.58 24.32 o -7 13 1 413.06 403.08 8.89 o -5 13 1 36.55 26.11 2.23 o -3 13 1 2.73 2.96 1.14 o -1 13 1 181.48 205.72 4.89 o 1 13 1 501.44 539.94 9.12 o 3 13 1 50.22 46.41 2.47 o 5 13 1 7.96 10.86 1.38 o 7 13 1 293.12 290.71 6.80 o 9 13 1 434.31 438.21 14.99 o -8 14 1 52.39 42.25 2.15 o -6 14 1 1.46 1.05 1.00 o -4 14 1 0.10 1.48 0.98 o -2 14 1 682.00 747.85 14.05 o 0 14 1 8.12 7.42 1.18 o 2 14 1 149.59 166.80 3.76 o 4 14 1 1169.64 1128.37 18.46 o 6 14 1 178.12 153.37 3.82 o 8 14 1 21.49 23.46 2.26 o -7 15 1 53.18 55.78 2.24 o -5 15 1 467.02 462.05 9.65 o -3 15 1 102.22 100.69 3.18 o -1 15 1 32.06 37.93 1.98 o 1 15 1 1127.77 1126.75 18.23 o 3 15 1 999.57 1007.59 17.68 o 5 15 1 279.00 284.41 6.34 o 7 15 1 72.17 59.54 4.48 o -6 16 1 40.20 26.24 2.56 o -4 16 1 583.44 547.87 11.97 o -2 16 1 1464.92 1481.52 23.04 o 0 16 1 40.32 46.05 1.84 o 2 16 1 367.81 352.52 7.46 o 4 16 1 95.23 78.83 2.39 o -1 17 1 103.64 95.92 3.33 o 1 17 1 178.59 167.35 5.89 o -16 0 2 1757.94 1726.17 50.87 o -14 0 2 2800.85 3023.37 62.41 o -12 0 2 13419.87 14780.66 296.64 o -10 0 2 12201.32 12674.40 280.21 o -8 0 2 13265.62 13437.11 506.86 o -6 0 2 44478.93 41481.62 1463.40 o -2 0 2 160.38 94.43 2.94 o 0 0 2 96837.97 59161.49 2395.33 o 2 0 2 17575.59 16916.16 374.78 o 4 0 2 38776.96 33437.58 1274.69 o 6 0 2 19708.18 22156.56 439.99 o 8 0 2 3607.03 3290.78 88.54 o 10 0 2 405.69 411.47 8.65 o 12 0 2 458.11 462.97 11.71 o 14 0 2 44.83 49.62 3.05 o -15 1 2 3326.72 3507.30 50.62 o -13 1 2 2328.19 2455.16 36.35 o -11 1 2 2678.16 2639.65 30.90 o -9 1 2 4839.58 4690.94 74.17 o -7 1 2 2777.12 3196.97 51.56 o -5 1 2 101.47 71.87 2.42 o -3 1 2 1909.51 1763.09 26.54 o -1 1 2 5.27 -1.13 1.13 o 1 1 2 1662.58 1776.60 24.38 o 3 1 2 24094.89 23691.94 514.68 o 5 1 2 8956.55 8850.65 124.75 o 7 1 2 8640.20 8494.54 146.58 o 9 1 2 11555.67 12204.96 225.88 o 11 1 2 7383.75 8041.23 114.91 o 13 1 2 5154.22 5552.47 79.60 o 15 1 2 2412.50 2238.33 38.14 o -16 2 2 796.94 739.80 13.09 o -14 2 2 2575.41 2607.32 41.08 o -12 2 2 2899.85 3234.65 47.31 o -10 2 2 13821.77 14362.37 176.88 o -8 2 2 19742.08 21422.97 331.29 o -6 2 2 26400.96 26883.18 379.41 o -4 2 2 64616.44 46919.82 697.13 o -2 2 2 55018.61 36092.80 710.92 o 0 2 2 1077.17 1235.52 16.18 o 4 2 2 12816.98 12795.88 172.92 o 6 2 2 4066.18 3960.01 56.59 o 8 2 2 5115.68 5224.42 98.01 o 10 2 2 15616.15 16405.89 183.94 o 12 2 2 482.22 518.86 9.02 o 14 2 2 135.73 140.32 3.14 o -15 3 2 1875.24 1884.44 31.73 o -13 3 2 694.26 801.31 13.88 o -11 3 2 8841.24 9013.93 137.88 o -9 3 2 246.60 212.52 5.41 o -7 3 2 14.45 4.43 2.11 o -5 3 2 41.32 20.38 1.41 o -3 3 2 170.02 110.50 2.43 o -1 3 2 7464.37 7402.16 102.53 o 1 3 2 20282.71 19332.80 310.42 o 3 3 2 4711.88 4960.53 64.92 o 5 3 2 53634.49 53853.93 1269.14 o 7 3 2 6572.15 6430.40 111.90 o 9 3 2 11241.42 11153.66 143.34 o 11 3 2 8232.18 8522.32 121.50 o 13 3 2 3735.12 3884.41 64.06 o 15 3 2 3130.82 2915.41 52.79 o -16 4 2 1880.96 1726.18 40.30 o -14 4 2 1341.99 1322.29 23.22 o -12 4 2 14812.20 16168.88 245.56 o -10 4 2 5155.67 5025.03 62.17 o -8 4 2 18156.90 19449.43 325.34 o -6 4 2 32795.80 35074.48 553.86 o -4 4 2 53616.54 43823.64 776.78 o -2 4 2 54584.67 44432.28 907.77 o 0 4 2 14322.90 14233.05 197.41 o 2 4 2 20069.46 20219.48 294.24 o 4 4 2 75202.23 67019.75 1725.84 o 6 4 2 2430.70 1881.87 27.58 o 8 4 2 8198.19 8056.87 150.23 o 10 4 2 1536.38 1511.16 25.54 o 12 4 2 4.58 8.77 1.12 o 14 4 2 83.34 96.09 3.02 o -15 5 2 1688.18 1644.09 30.67 o -13 5 2 3228.47 3217.39 59.64 o -11 5 2 1418.33 1397.29 27.27 o -9 5 2 5391.59 5137.02 83.70 o -7 5 2 5856.91 5860.73 100.01 o -5 5 2 480.18 472.51 8.30 o -3 5 2 306.41 303.54 6.21 o -1 5 2 593.62 530.07 8.05 o 1 5 2 592.03 468.25 6.47 o 3 5 2 26574.79 28901.01 395.96 o 5 5 2 31.89 41.03 1.66 o 7 5 2 6347.04 6151.53 115.32 o 9 5 2 13892.03 13472.61 187.99 o 11 5 2 3787.70 4090.13 74.99 o 13 5 2 4024.28 4162.42 80.30 o -14 6 2 1152.95 1198.14 23.02 o -12 6 2 2028.22 2142.16 40.72 o -10 6 2 24706.40 26459.09 541.93 o -8 6 2 4686.39 4298.97 79.02 o -6 6 2 28017.27 31810.66 504.55 o -4 6 2 35746.81 37924.02 547.02 o -2 6 2 26850.21 28264.72 440.28 o 0 6 2 37748.40 38452.72 840.41 o 2 6 2 39462.08 40001.97 691.25 o 4 6 2 7368.67 6915.49 101.48 o 6 6 2 5265.39 5210.30 86.59 o 8 6 2 5649.62 5435.04 104.45 o 10 6 2 2482.84 2219.34 50.89 o 12 6 2 815.50 816.43 18.43 o 14 6 2 297.92 250.49 6.15 o -13 7 2 2897.52 2984.29 61.91 o -11 7 2 4157.30 4081.20 74.72 o -9 7 2 694.00 602.96 10.14 o -7 7 2 944.16 820.39 16.01 o -5 7 2 329.14 343.18 7.52 o -3 7 2 1.70 2.16 1.40 o -1 7 2 1989.66 2295.21 36.17 o 1 7 2 5682.32 6151.92 94.45 o 3 7 2 10434.87 10117.44 130.75 o 5 7 2 9401.42 9258.70 157.27 o 7 7 2 14422.49 14483.43 254.60 o 9 7 2 4397.46 4368.18 105.19 o 11 7 2 6598.71 6502.43 190.77 o 13 7 2 1609.75 1632.04 48.78 o -14 8 2 2580.30 2198.91 88.69 o -12 8 2 3387.27 3307.98 68.59 o -10 8 2 4547.22 4584.97 70.40 o -8 8 2 15978.59 15972.50 206.19 o -6 8 2 4942.63 4576.42 84.58 o -4 8 2 42421.82 50692.67 841.36 o -2 8 2 19571.51 21993.60 351.38 o 0 8 2 14061.56 15042.81 241.32 o 2 8 2 21520.46 23946.97 446.05 o 4 8 2 21328.99 22886.93 425.41 o 6 8 2 5697.28 5295.19 98.23 o 8 8 2 5131.27 4963.24 118.79 o 10 8 2 1350.66 1429.63 40.86 o 12 8 2 625.13 651.55 21.06 o -13 9 2 659.28 679.61 21.53 o -11 9 2 1417.90 1342.04 28.86 o -9 9 2 3548.27 3301.84 55.38 o -7 9 2 295.15 270.62 5.35 o -5 9 2 1501.01 1407.97 25.44 o -3 9 2 11.81 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