#------------------------------------------------------------------------------ #$Date: 2019-12-17 23:28:55 +0200 (Tue, 17 Dec 2019) $ #$Revision: 245265 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/00/3500082.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500082 _publ_author_name 'Thierry Maris' _chemical_formula_sum 'C20 H44 N Br' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.5034 _cell_length_b 22.9748 _cell_length_c 9.2342 _exptl_crystal_F_000 824.00 _reflns_d_resolution_high 0.8282 _cod_data_source_file c5nbr.fcf _cod_data_source_block c5nbr _shelx_title ' JW1758 in Ccca #68' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.96 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y+1/2, z' 'x, -y+1/2, -z+1/2' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z' 'x+1/2, -y+1, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z' '-x, y-1/2, z-1/2' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z' '-x+1/2, y, z-1/2' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 758.92 783.24 25.06 o 4 0 0 3435.15 3411.36 119.36 o 6 0 0 2914.95 2962.52 92.28 o 8 0 0 2138.39 2162.20 64.23 o 10 0 0 1282.62 1410.61 50.94 o 12 0 0 3342.78 3310.85 98.47 o 2 2 0 22926.89 24146.67 494.32 o 4 2 0 13598.90 14591.46 299.61 o 6 2 0 5493.84 5190.68 126.63 o 8 2 0 2184.83 2040.64 37.13 o 10 2 0 673.23 733.98 18.98 o 12 2 0 1253.96 1299.56 28.38 o 0 4 0 1591.50 1754.06 52.81 o 4 4 0 3290.71 3205.61 69.33 o 6 4 0 2943.53 2736.89 75.02 o 8 4 0 1903.98 1817.76 33.06 o 10 4 0 3064.37 3284.68 72.85 o 12 4 0 143.42 104.66 6.23 o 0 6 0 21309.30 21163.36 628.97 o 2 6 0 23170.47 25293.88 597.96 o 4 6 0 5782.38 6234.19 133.46 o 6 6 0 3878.11 3779.73 76.16 o 8 6 0 1513.63 1331.22 26.50 o 10 6 0 2833.26 2871.21 92.09 o 12 6 0 218.14 209.19 9.92 o 0 8 0 2065.65 2096.85 70.65 o 2 8 0 5291.09 5584.12 130.87 o 4 8 0 19091.41 21590.81 514.37 o 6 8 0 2590.73 2235.33 45.67 o 8 8 0 5325.19 4866.44 231.25 o 10 8 0 118.64 107.25 6.61 o 12 8 0 246.42 229.32 10.97 o 0 10 0 16830.56 17834.74 635.11 o 2 10 0 4266.03 4268.13 106.37 o 4 10 0 5576.12 5921.15 142.27 o 6 10 0 1935.73 1942.66 41.97 o 8 10 0 4916.66 5038.70 136.38 o 10 10 0 554.12 613.97 19.26 o 0 12 0 4629.14 4482.48 190.87 o 2 12 0 2658.38 2429.12 61.09 o 4 12 0 3400.22 3151.56 67.18 o 6 12 0 17851.54 17680.15 380.86 o 8 12 0 137.64 111.49 6.97 o 10 12 0 324.27 317.62 11.98 o 0 14 0 1900.39 1497.86 50.34 o 2 14 0 4357.77 4389.51 102.09 o 4 14 0 1545.76 1512.62 33.44 o 6 14 0 8303.32 7852.04 213.09 o 8 14 0 1164.85 1211.73 31.92 o 10 14 0 345.81 332.98 12.19 o 0 16 0 1987.85 1834.24 61.31 o 2 16 0 2322.30 2169.31 51.62 o 4 16 0 6017.28 5740.62 142.82 o 6 16 0 437.96 371.53 29.09 o 8 16 0 2365.13 2484.06 111.19 o 10 16 0 308.92 383.64 25.77 o 0 18 0 1698.70 1621.68 96.51 o 2 18 0 645.48 575.84 16.12 o 4 18 0 5962.61 5914.48 592.28 o 6 18 0 1055.64 1239.29 65.37 o 8 18 0 1015.37 1076.58 50.64 o 0 20 0 1170.92 1221.46 90.35 o 2 20 0 3147.38 3391.11 134.05 o 4 20 0 433.99 449.90 32.11 o 6 20 0 303.66 328.00 25.18 o 8 20 0 717.78 798.31 37.93 o 0 22 0 256.00 204.03 23.06 o 2 22 0 2408.49 2699.80 107.49 o 4 22 0 375.81 417.58 29.06 o 6 22 0 695.72 686.06 32.25 o 0 24 0 3178.08 3803.56 257.21 o 2 24 0 256.86 265.62 32.29 o 4 24 0 153.55 118.85 11.49 o 6 24 0 571.57 592.28 45.31 o 0 26 0 2579.03 2993.14 201.86 o 2 26 0 231.37 256.93 27.13 o 4 26 0 187.65 211.63 21.71 o 1 1 1 369.64 435.72 8.61 o 3 1 1 14157.96 14672.48 217.04 o 5 1 1 6682.63 6954.29 113.15 o 7 1 1 3288.86 3081.78 44.47 o 9 1 1 1660.91 1710.44 28.53 o 11 1 1 267.27 295.28 7.39 o 2 2 1 1191.74 1195.50 19.30 o 4 2 1 3.33 8.90 1.02 o 6 2 1 84.36 104.55 2.70 o 8 2 1 0.16 1.25 3.02 o 10 2 1 12.28 5.02 2.78 o 12 2 1 107.31 82.27 3.06 o 1 3 1 363.15 272.15 5.44 o 3 3 1 21565.37 22759.29 353.83 o 5 3 1 5710.03 5610.88 91.33 o 7 3 1 3860.21 3550.37 48.74 o 9 3 1 1618.04 1679.48 27.44 o 11 3 1 3.22 12.05 2.41 o 2 4 1 14246.71 15108.85 262.41 o 4 4 1 1242.26 1401.74 21.28 o 6 4 1 44.37 49.85 2.09 o 8 4 1 205.81 199.43 5.39 o 10 4 1 81.61 62.00 3.35 o 12 4 1 41.85 26.91 2.75 o 1 5 1 23210.22 23910.35 387.04 o 3 5 1 34.03 28.09 2.01 o 5 5 1 7355.69 7998.71 123.80 o 7 5 1 2725.15 2629.21 34.21 o 9 5 1 621.61 623.42 11.57 o 11 5 1 504.90 484.96 9.96 o 2 6 1 764.62 879.16 14.27 o 4 6 1 261.77 338.32 6.10 o 6 6 1 38.86 54.21 2.12 o 8 6 1 86.80 70.50 4.09 o 10 6 1 162.96 174.75 6.91 o 12 6 1 3.85 0.64 2.58 o 1 7 1 12499.66 12736.74 198.95 o 3 7 1 218.35 132.64 3.28 o 5 7 1 8185.51 8671.42 137.38 o 7 7 1 3356.84 3074.66 42.94 o 9 7 1 15.82 10.23 3.25 o 11 7 1 704.51 707.03 14.28 o 2 8 1 1763.79 2029.11 35.39 o 4 8 1 1189.71 1447.29 25.24 o 6 8 1 144.03 169.67 3.89 o 8 8 1 274.92 241.24 6.38 o 10 8 1 5.21 1.27 2.91 o 12 8 1 6.60 0.98 2.69 o 1 9 1 5629.51 5695.93 93.86 o 3 9 1 10798.09 12628.95 224.49 o 5 9 1 657.02 480.81 11.59 o 7 9 1 1159.50 1102.78 18.19 o 9 9 1 861.55 911.47 21.61 o 11 9 1 319.05 337.56 8.04 o 2 10 1 915.17 1040.20 17.91 o 4 10 1 0.97 3.94 2.29 o 6 10 1 139.24 151.49 4.07 o 8 10 1 229.44 207.09 7.67 o 10 10 1 17.30 7.10 3.02 o 1 11 1 5972.10 6146.82 104.18 o 3 11 1 5679.38 5940.39 98.47 o 5 11 1 1114.78 975.75 17.09 o 7 11 1 27.65 28.78 2.58 o 9 11 1 1314.28 1344.00 26.70 o 11 11 1 452.46 456.26 9.53 o 2 12 1 71.48 78.14 3.89 o 4 12 1 85.87 96.07 3.11 o 6 12 1 22.81 29.51 3.35 o 8 12 1 19.37 7.53 3.55 o 10 12 1 0.19 -2.54 2.54 o 1 13 1 4878.19 4734.84 82.57 o 3 13 1 3488.61 3488.47 56.34 o 5 13 1 992.66 977.25 15.73 o 7 13 1 100.53 86.46 4.68 o 9 13 1 709.79 669.79 13.51 o 11 13 1 201.93 182.32 15.19 o 2 14 1 79.16 88.83 4.01 o 4 14 1 278.32 279.64 6.56 o 6 14 1 364.65 352.02 8.48 o 8 14 1 37.32 27.89 4.22 o 10 14 1 0.04 0.42 2.73 o 1 15 1 3683.09 3515.35 56.06 o 3 15 1 3608.59 3641.34 62.55 o 5 15 1 20.51 17.73 2.66 o 7 15 1 263.10 248.88 11.52 o 9 15 1 770.90 792.55 18.71 o 2 16 1 148.49 151.44 4.39 o 4 16 1 271.09 240.90 6.53 o 6 16 1 45.98 31.21 7.78 o 8 16 1 218.13 216.21 25.20 o 10 16 1 12.00 8.68 3.30 o 1 17 1 2544.68 2514.36 44.44 o 3 17 1 622.18 510.93 11.84 o 5 17 1 965.63 1086.76 41.78 o 7 17 1 441.18 468.78 23.24 o 9 17 1 2.13 8.04 3.82 o 2 18 1 5.77 0.88 2.41 o 4 18 1 179.81 184.02 17.66 o 6 18 1 9.48 12.29 4.67 o 8 18 1 12.25 7.39 4.21 o 1 19 1 2199.22 2139.16 63.02 o 3 19 1 11.95 3.59 7.63 o 5 19 1 1036.91 1111.12 35.90 o 7 19 1 591.73 676.57 29.43 o 9 19 1 3.72 4.34 4.61 o 2 20 1 105.25 70.52 6.98 o 4 20 1 0.01 -1.36 6.99 o 6 20 1 0.74 -4.59 4.59 o 8 20 1 2.97 1.63 3.33 o 1 21 1 560.81 594.92 23.42 o 3 21 1 719.30 819.34 33.09 o 5 21 1 232.37 243.48 12.99 o 7 21 1 175.84 156.92 11.41 o 2 22 1 162.38 137.59 8.84 o 4 22 1 113.26 79.04 8.23 o 6 22 1 8.17 5.09 3.87 o 1 23 1 38.41 34.98 6.91 o 3 23 1 699.37 763.60 30.28 o 5 23 1 513.22 545.75 19.10 o 2 24 1 16.25 5.93 8.15 o 4 24 1 0.19 -3.98 3.98 o 6 24 1 36.41 40.65 7.00 o 1 25 1 62.48 51.08 6.13 o 3 25 1 283.74 297.25 13.69 o 5 25 1 175.27 173.99 13.02 o 2 26 1 37.51 25.11 4.04 o 4 26 1 1.59 1.86 3.79 o 1 27 1 1.25 1.33 2.94 o 2 0 2 4518.56 4565.54 129.08 o 4 0 2 6595.33 6725.67 176.12 o 6 0 2 12978.39 12584.00 341.32 o 8 0 2 968.71 853.29 18.78 o 10 0 2 694.94 757.80 17.30 o 12 0 2 1289.31 1242.23 28.74 o 1 1 2 23702.86 24815.68 530.89 o 3 1 2 146.64 132.84 3.58 o 5 1 2 283.02 312.63 6.58 o 7 1 2 178.88 193.57 4.59 o 9 1 2 26.89 20.50 3.01 o 11 1 2 40.18 39.25 2.99 o 2 2 2 21895.29 23176.80 433.76 o 4 2 2 4433.83 4303.26 76.96 o 6 2 2 4519.53 4325.19 74.65 o 8 2 2 2645.23 2554.48 37.21 o 10 2 2 1343.50 1375.61 21.67 o 12 2 2 854.43 857.22 17.34 o 1 3 2 6409.69 6703.03 132.49 o 3 3 2 1335.31 1472.47 26.06 o 5 3 2 736.47 863.36 18.17 o 7 3 2 32.52 32.61 2.21 o 9 3 2 33.39 27.06 3.48 o 11 3 2 367.48 383.37 8.18 o 0 4 2 6107.81 6064.64 182.55 o 2 4 2 20004.58 20234.87 348.58 o 4 4 2 18431.42 20407.24 394.30 o 6 4 2 2147.28 1951.00 30.48 o 8 4 2 2862.50 2726.13 40.82 o 10 4 2 1312.29 1383.29 23.12 o 12 4 2 319.13 306.86 8.04 o 1 5 2 1033.22 1038.04 19.52 o 3 5 2 7092.84 8131.59 145.21 o 5 5 2 78.67 86.71 2.70 o 7 5 2 54.20 55.92 2.87 o 9 5 2 178.79 181.52 6.48 o 11 5 2 1.30 1.48 2.60 o 0 6 2 9204.79 9206.51 214.37 o 2 6 2 10565.25 10962.51 187.68 o 4 6 2 13287.78 14722.79 274.44 o 6 6 2 3610.87 3546.03 54.66 o 8 6 2 2159.27 1994.47 42.25 o 10 6 2 1545.04 1595.86 27.24 o 12 6 2 166.21 170.02 5.99 o 1 7 2 141.97 125.05 3.21 o 3 7 2 10114.88 11490.58 197.67 o 5 7 2 281.41 304.00 6.00 o 7 7 2 56.22 52.86 2.61 o 9 7 2 1432.58 1522.79 33.64 o 11 7 2 44.56 35.40 2.95 o 0 8 2 6646.54 6469.23 171.74 o 2 8 2 23067.68 25602.03 439.38 o 4 8 2 5098.94 5377.61 96.36 o 6 8 2 1816.08 1694.21 26.06 o 8 8 2 3105.30 2971.12 72.14 o 10 8 2 1398.46 1438.43 26.73 o 1 9 2 34.68 52.56 2.35 o 3 9 2 1.69 2.11 1.27 o 5 9 2 447.70 496.95 8.19 o 7 9 2 4.51 -0.64 2.12 o 9 9 2 12.28 15.74 3.81 o 11 9 2 100.19 78.06 3.37 o 0 10 2 3363.50 3327.56 88.99 o 2 10 2 7884.69 8262.61 140.93 o 4 10 2 8122.81 8211.29 151.29 o 6 10 2 5064.89 4901.60 68.53 o 8 10 2 1732.46 1696.76 33.85 o 10 10 2 321.40 333.52 8.45 o 1 11 2 1374.30 1463.38 28.24 o 3 11 2 40.81 43.14 2.89 o 5 11 2 1548.31 1628.88 25.60 o 7 11 2 2241.04 2144.94 43.19 o 9 11 2 34.70 22.97 3.91 o 11 11 2 31.64 19.67 2.78 o 0 12 2 18415.91 19074.32 502.66 o 2 12 2 1896.33 1732.27 32.16 o 4 12 2 2059.58 2038.96 30.73 o 6 12 2 6789.35 6756.93 106.81 o 8 12 2 811.45 816.92 18.05 o 10 12 2 412.70 409.10 9.84 o 1 13 2 184.02 174.60 4.61 o 3 13 2 107.21 96.98 3.86 o 5 13 2 27.48 26.10 2.45 o 7 13 2 155.97 142.93 11.53 o 9 13 2 27.84 21.10 3.77 o 0 14 2 4857.17 4486.08 103.83 o 2 14 2 3300.46 3212.51 60.67 o 4 14 2 3330.56 3280.43 52.67 o 6 14 2 3112.51 2829.72 53.90 o 8 14 2 1016.73 1045.95 29.38 o 10 14 2 190.48 196.86 6.81 o 1 15 2 261.69 277.76 6.88 o 3 15 2 136.71 127.90 4.81 o 5 15 2 1144.51 1053.13 17.85 o 7 15 2 512.20 533.83 17.68 o 9 15 2 8.61 7.09 3.00 o 0 16 2 817.46 776.68 24.85 o 2 16 2 2918.92 2863.12 47.63 o 4 16 2 3894.03 3665.43 64.77 o 6 16 2 1148.07 1154.66 26.39 o 8 16 2 1115.84 1127.28 31.45 o 10 16 2 343.07 376.06 17.65 o 1 17 2 137.08 131.23 5.11 o 3 17 2 2.03 3.11 2.47 o 5 17 2 41.84 39.06 5.51 o 7 17 2 17.93 19.55 6.59 o 9 17 2 31.81 22.35 3.57 o 0 18 2 1924.63 1828.14 92.60 o 2 18 2 2319.13 2263.57 64.93 o 4 18 2 1589.19 1642.65 59.74 o 6 18 2 536.94 583.14 18.89 o 8 18 2 517.72 550.27 20.30 o 1 19 2 31.45 19.76 3.06 o 3 19 2 1700.44 1877.49 77.41 o 5 19 2 23.55 9.64 6.53 o 7 19 2 29.76 29.97 8.02 o 0 20 2 551.93 531.85 35.08 o 2 20 2 1707.73 1844.23 53.41 o 4 20 2 1610.82 1759.97 54.35 o 6 20 2 473.62 504.70 18.60 o 8 20 2 521.17 545.25 22.64 o 1 21 2 2.26 -2.69 5.84 o 3 21 2 131.86 111.41 9.47 o 5 21 2 11.25 2.06 5.03 o 7 21 2 18.49 14.81 7.18 o 0 22 2 1173.86 1388.08 71.27 o 2 22 2 1072.72 1056.20 31.20 o 4 22 2 555.96 593.97 21.42 o 6 22 2 261.53 242.53 11.03 o 1 23 2 620.21 667.64 23.43 o 3 23 2 0.19 -4.71 4.71 o 5 23 2 38.81 25.49 3.90 o 0 24 2 1828.89 2079.29 78.29 o 2 24 2 358.63 364.61 15.46 o 4 24 2 208.40 217.10 9.27 o 1 25 2 18.50 16.84 3.38 o 3 25 2 3.84 -2.12 3.61 o 0 26 2 720.77 705.82 24.21 o 2 26 2 320.43 353.32 13.98 o 1 27 2 164.75 161.97 15.19 o 1 1 3 6266.65 6479.94 167.80 o 3 1 3 11652.71 12793.83 267.64 o 5 1 3 3328.10 3183.89 67.42 o 7 1 3 995.07 895.30 13.88 o 9 1 3 1670.30 1742.23 29.77 o 11 1 3 154.43 164.38 6.58 o 2 2 3 71.42 102.72 3.29 o 4 2 3 1215.79 1405.48 28.87 o 6 2 3 51.89 52.56 2.30 o 8 2 3 86.28 82.11 3.17 o 10 2 3 5.40 5.87 2.47 o 12 2 3 64.91 49.43 3.69 o 1 3 3 17397.06 18196.37 403.36 o 3 3 3 8152.15 8722.03 174.63 o 5 3 3 201.50 147.28 3.79 o 7 3 3 1608.77 1560.10 22.89 o 9 3 3 1388.88 1520.93 27.32 o 11 3 3 647.02 666.18 12.99 o 2 4 3 4383.34 4718.61 96.30 o 4 4 3 246.03 263.01 7.26 o 6 4 3 142.56 142.48 3.97 o 8 4 3 2.55 3.64 2.28 o 10 4 3 462.06 479.37 10.73 o 12 4 3 3.98 3.20 3.45 o 1 5 3 4908.59 4939.48 102.88 o 3 5 3 1243.97 1041.69 21.05 o 5 5 3 7853.67 7412.02 144.26 o 7 5 3 3414.80 3294.09 52.80 o 9 5 3 7.59 12.20 3.84 o 11 5 3 415.23 422.94 9.12 o 2 6 3 2814.44 3361.76 68.54 o 4 6 3 724.23 729.88 15.66 o 6 6 3 69.21 62.43 2.64 o 8 6 3 77.18 57.33 3.97 o 10 6 3 292.42 303.73 8.54 o 1 7 3 16655.06 17564.27 335.44 o 3 7 3 20.57 59.94 2.54 o 5 7 3 2584.43 2372.81 36.84 o 7 7 3 1940.66 1863.37 29.75 o 9 7 3 502.65 567.94 14.30 o 11 7 3 531.80 526.02 10.42 o 2 8 3 57.46 62.81 2.52 o 4 8 3 4700.68 4858.51 97.34 o 6 8 3 43.69 38.92 2.42 o 8 8 3 540.80 523.70 14.73 o 10 8 3 0.30 2.40 2.65 o 1 9 3 2056.57 1924.87 37.19 o 3 9 3 3664.36 3434.37 63.74 o 5 9 3 3283.03 2912.47 42.76 o 7 9 3 1014.57 953.09 15.52 o 9 9 3 747.19 864.00 19.31 o 11 9 3 63.98 55.79 3.02 o 2 10 3 522.38 561.17 12.01 o 4 10 3 0.72 9.16 2.03 o 6 10 3 108.25 81.77 3.18 o 8 10 3 257.26 226.00 9.09 o 10 10 3 35.63 30.39 2.90 o 1 11 3 550.75 475.87 10.05 o 3 11 3 5537.55 4978.18 82.57 o 5 11 3 2224.84 2090.55 32.77 o 7 11 3 1066.00 1020.64 23.07 o 9 11 3 763.51 769.33 18.64 o 11 11 3 45.64 46.57 3.27 o 2 12 3 287.75 257.00 6.56 o 4 12 3 14.48 18.26 2.27 o 6 12 3 6.55 7.94 2.50 o 8 12 3 17.59 16.74 3.94 o 10 12 3 11.05 5.13 2.80 o 1 13 3 2737.59 2443.67 41.98 o 3 13 3 3120.94 2876.08 47.81 o 5 13 3 186.64 146.49 4.49 o 7 13 3 815.23 926.19 26.96 o 9 13 3 894.55 929.14 28.55 o 2 14 3 150.81 150.11 4.39 o 4 14 3 32.23 19.78 2.59 o 6 14 3 36.66 38.69 6.93 o 8 14 3 24.04 14.28 4.27 o 10 14 3 8.43 9.03 2.32 o 1 15 3 571.58 473.58 11.02 o 3 15 3 2613.51 2456.35 41.44 o 5 15 3 2013.28 1859.49 43.77 o 7 15 3 915.34 991.27 25.85 o 9 15 3 180.82 211.24 8.13 o 2 16 3 50.72 37.26 3.41 o 4 16 3 530.05 498.44 10.45 o 6 16 3 2.18 3.36 3.29 o 8 16 3 125.29 101.43 5.65 o 1 17 3 2293.85 2127.10 49.55 o 3 17 3 170.98 159.11 5.44 o 5 17 3 1023.46 1164.17 30.82 o 7 17 3 571.45 548.03 19.23 o 9 17 3 230.76 248.83 13.74 o 2 18 3 71.83 61.95 4.98 o 4 18 3 267.18 235.12 16.75 o 6 18 3 0.08 -1.61 3.84 o 8 18 3 102.34 95.89 6.27 o 1 19 3 1360.43 1470.80 39.25 o 3 19 3 173.47 172.23 10.14 o 5 19 3 969.93 1088.02 33.78 o 7 19 3 416.10 429.10 20.17 o 2 20 3 716.61 731.52 19.70 o 4 20 3 1.31 6.96 5.58 o 6 20 3 2.26 1.83 3.76 o 8 20 3 6.45 4.34 4.34 o 1 21 3 356.13 396.37 13.04 o 3 21 3 551.78 688.67 24.45 o 5 21 3 341.54 391.57 13.80 o 7 21 3 344.63 349.04 21.97 o 2 22 3 111.21 83.06 4.86 o 4 22 3 90.85 82.91 5.75 o 6 22 3 2.65 0.95 4.12 o 1 23 3 489.99 557.83 15.15 o 3 23 3 468.73 524.25 16.79 o 5 23 3 7.36 6.81 3.21 o 2 24 3 23.83 17.98 4.09 o 4 24 3 45.09 41.13 3.95 o 1 25 3 59.43 65.94 4.46 o 3 25 3 397.70 429.79 16.03 o 2 26 3 10.15 11.25 3.40 o 0 0 4 4392.17 4129.40 200.51 o 2 0 4 8822.05 10461.54 367.79 o 4 0 4 3218.24 3115.74 82.93 o 6 0 4 17937.77 17589.37 355.30 o 8 0 4 1092.32 1112.99 29.85 o 10 0 4 767.37 752.23 17.72 o 1 1 4 48.71 75.82 3.27 o 3 1 4 843.26 1021.89 23.79 o 5 1 4 458.33 435.23 7.02 o 7 1 4 1182.55 1205.01 18.94 o 9 1 4 19.83 21.35 3.29 o 11 1 4 73.37 57.36 3.14 o 0 2 4 8187.62 8668.56 266.80 o 2 2 4 7857.87 8403.61 195.26 o 4 2 4 6569.34 6666.60 111.21 o 6 2 4 7914.87 7734.78 104.89 o 8 2 4 2179.81 2370.97 41.46 o 10 2 4 803.44 832.10 15.77 o 1 3 4 309.16 429.24 12.59 o 3 3 4 1863.61 2208.59 49.41 o 5 3 4 341.47 379.83 6.67 o 7 3 4 0.03 5.81 2.20 o 9 3 4 99.73 95.53 4.79 o 11 3 4 29.20 16.82 2.42 o 0 4 4 7343.00 7781.47 265.38 o 2 4 4 2446.82 2284.48 54.00 o 4 4 4 18120.68 17577.42 305.35 o 6 4 4 2113.91 2182.97 34.11 o 8 4 4 4251.59 4425.13 86.47 o 10 4 4 350.54 342.22 9.87 o 1 5 4 55.93 60.84 2.74 o 3 5 4 952.96 1013.33 23.65 o 5 5 4 211.42 213.10 5.65 o 7 5 4 335.77 347.14 7.41 o 9 5 4 10.49 13.79 3.36 o 11 5 4 41.05 24.89 2.43 o 0 6 4 5115.52 4840.21 138.31 o 2 6 4 9478.21 10033.76 207.27 o 4 6 4 11656.67 11299.44 148.37 o 6 6 4 1285.93 1261.17 18.64 o 8 6 4 3083.58 3106.78 65.21 o 10 6 4 790.59 797.81 17.71 o 1 7 4 835.34 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